CN104215549B - Density testing method of mineral aggregate in recycled asphalt pavement material - Google Patents

Density testing method of mineral aggregate in recycled asphalt pavement material Download PDF

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Publication number
CN104215549B
CN104215549B CN201410465437.2A CN201410465437A CN104215549B CN 104215549 B CN104215549 B CN 104215549B CN 201410465437 A CN201410465437 A CN 201410465437A CN 104215549 B CN104215549 B CN 104215549B
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aggregate
density
mineral
filler
asphalt pavement
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CN104215549A (en
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方杨
黄建跃
吴传海
李善强
张国民
王水声
王璐
许新权
李豁
伍宇
周勇
严超
傅广文
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HUALU TRAFFIC SCIENCE-TECHNOLOGY Co Ltd GUANGDONG
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HUALU TRAFFIC SCIENCE-TECHNOLOGY Co Ltd GUANGDONG
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Abstract

The invention discloses a density testing method of mineral aggregate in a recycled asphalt pavement material. The method comprises the following steps of extracting and drying the recycled asphalt pavement material by utilizing a trichloro ethylene solvent to obtain mineral aggregate; screening and grading the mineral aggregate; washing coarse aggregate and fine aggregate by utilizing an anionic surfactant aqueous solution until that all surface bubbles are discharged and no foam floats on the water surface, testing the mineral aggregate by adopting a mesh basket method after the mineral aggregate is dried to obtain the appearance relative density and the gross volume relative density; soaking filler in waterless coal oil, and testing so as to acquire the relative density of the filler; and respectively calculating the gross volume relative density and the appearance relative density of the mineral aggregate in the recycled asphalt pavement material according to a density synthesis formula 1 and a density synthesis formula 2. The method has advantages that the mineral aggregate is washed in two ways, so that the determination precision of the overall density of the mineral aggregate can be improved; the operation is carried out inn a fuming cupboard, so that the environmental pollution is small, and the body health of test personnel is not influenced; the operation is simple and easy, and data are real and reliable.

Description

A kind of density measurement method for reclaiming asphalt pavement material Mineral Material
Technical field
The present invention relates to field of road, and in particular to coarse aggregate, fine aggregate in a kind of recovery asphalt pavement material, The method of testing of the hybrid density of the mineral aggregates such as filler.
Background technology
Using after for many years, its overall performance is reduced bituminous paving, it is impossible to meet road with requiring.By old asphalt pavement milling, Excavate, it is broken after, the recovery asphalt pavement material (hereinafter referred to as RAP) for obtaining still has very high value, can be used for Various pavement recyclings.Applied of Asphalt Pavement Recycle Technique had both saved ample resources and fund, reduced the destruction to environment of cutting into a mountain for quarrying again, Realize economic circulation development, Green Development and sustainable development.RAP is made up of mineral aggregate and Colophonium, and mineral aggregate is by certain proportion Coarse aggregate, fine aggregate, filler composition, mineral aggregate surface is wrapped in Colophonium.The density of mineral aggregate is to calculate reclaimed asphalt mixture body One of important parameter of product index.
Due to the mixture that RAP is mineral aggregate and Colophonium, must separate before test.Existing separation method is combustion method and extracting Method, the drawbacks of two methods have certain.The easy quick efficiency high of combustion method, but the high temperature of combustion furnace can cause part ore deposit Material ablation is decomposed, and surface opening hole increases, and aggregate water absorption is raised, and affects density result accuracy.Extraction process is using organic Solvent, while dissolving mineral aggregate surface Colophonium, trichloro ethylene replaces Colophonium to continue contamination mineral aggregate.
Conventional coarse aggregate density test method according to《Highway engineering is gathered materials testing regulationss》In (JTG E42-2005) " T0304-2005 coarse aggregates density and the moisture content test (basket method) " is operated and is calculated, and the liquid medium which adopts is for water;Often Fine aggregate density test method according to《Highway engineering is gathered materials testing regulationss》In (JTG E42-2005), " T0330-2005 is thin Density of gathering materials and the moisture content test " is operated and is calculated, and the liquid medium which adopts is for water;Conventional packing density test method is pressed According to《Highway engineering is gathered materials testing regulationss》" T0352-2000 breeze density tests " operation and calculating in (JTG E42-2005), its The liquid medium for adopting is distilled water or kerosene.Above test method is gathered materials and filler suitable for free of contamination cleaning.But for By the RAP mineral aggregates that trichloro ethylene is infected with, directly can not use.
When water is medium, because water and trichloro ethylene are immiscible, a large amount of bubbles of mineral aggregate surface attachment, water cannot infiltrate mineral aggregate Surface.Mineral aggregate is less, and phenomenon is more obvious, and stirring and long-time immersion can not eliminate this phenomenon, and mineral aggregate density test is basic Cannot carry out;When kerosene is medium, because trichloro ethylene differs larger with kerosene proportion, the trichloro ethylene on filler surface is dissolved in kerosene Afterwards, kerosene density and cubical expansivity change, and cause indirectly packing volume deviation larger.
Based on above reason, it is necessary to secondary eluting is carried out to trichloro ethylene, eliminate its interference to density test, but at present There is no targetedly method.
At the same time, because particle diameter is different, density measurement method is also different, RAP ore deposits for coarse aggregate, fine aggregate, filler The necessary screened stepping of three class materials in material, difference test density, then enter line density composite calulation, obtain mineral aggregate density.But It is《Highway engineering is gathered materials testing regulationss》(JTG E42-2005) only provides the respective density computational methods of three class materials, does not give Go out the density computational methods of the mineral aggregate being made up of three class materials.
The content of the invention
For the problems referred to above, the present invention is intended to provide one kind can eliminate the interference of mineral aggregate surface attachments and accurately can survey Surely reclaim coarse aggregate, fine aggregate, the method for testing of the hybrid density of filler in bituminous paving mineral aggregate.
To realize the technical purpose, the solution of the present invention is:A kind of density measurement for reclaiming asphalt pavement material Mineral Material Method, the method for testing step are as follows:
(1) the pre- thermal softening of asphalt pavement material will be reclaimed, fritter will manually be separated into, and then Colophonium will be reclaimed in fume hood Ground surface material is stripped with trichloroethylene solvent, and mineral aggregate is obtained after the completion of extracting, and mineral aggregate is put into 100~110 DEG C of baking oven Middle drying and processing;
(2) mineral aggregate is cooled to after room temperature, carries out screening stepping:
When the mineral aggregate nominal maximum particle diameter in RAP be more than 2.36mm when, mineral aggregate should be divided into more than 2.36mm coarse aggregate, 0.15~2.36mm fine aggregates, 0~0.15mm filler third gear;
When the mineral aggregate nominal maximum particle diameter in RAP be less than 2.36mm when, mineral aggregate should be divided into 0.15~2.36mm fine aggregates, 0 Two grades of~0.15mm fillers;
(3) the aqueous solution of anionic surfactant of configuration quality percentage ratio 0.2%~0.3%, coarse aggregate is immersed in molten In liquid, it is sufficiently stirred for, eluriates for several times repeatedly, and constantly slowly injects new water, until coarse aggregate blibbing is all discharged, and water Face non-foam floating, then coarse aggregate is put in 100~110 DEG C of baking oven carries out drying and processing;
Clean coarse aggregate is obtained, then according to《Highway engineering is gathered materials testing regulationss》In JTG E42 " coarse aggregate density and The moisture content test (basket method) " is operated, and apparent relative density (dimensionless), the bulk specific gravity for obtaining coarse aggregate is (immeasurable Guiding principle);
(4) the aqueous solution of anionic surfactant of mass percent 0.3%~0.5% is prepared, fine aggregate is immersed in molten In liquid, fully stir, eluriate repeatedly, and constantly slowly inject new water, until fine aggregate blibbing is all discharged, the water surface is still After foam floating, fine aggregate is poured into tray, be cooled to room temperature after drying in being put into 100~110 DEG C of baking oven;
Clean fine aggregate is obtained, then according to《Highway engineering is gathered materials testing regulationss》" fine aggregate density in (JTG E42) And the moisture content test (basket method) " operation, obtain apparent relative density (dimensionless), the bulk specific gravity (nothing of fine aggregate Dimension);
(5) in fume hood, filler is immersed in anhydrous kerosene, is fully stirred, the bubble effusion allowed inside filler is quiet A period of time is put after filler precipitation, kerosene is carefully poured out;New kerosene is added again, repeats aforesaid operations at least 1 time;
Pour filler into tray, treat that kerosene evaporates into face and does, be often cooled to after drying in being put into 110~120 DEG C of baking oven Temperature, obtains clean filler, according to《Highway engineering is gathered materials testing regulationss》" breeze density test " operation in JTG E42, liquid Medium selects anhydrous kerosene, test to obtain the relative density (dimensionless) of filler;
(6) the apparent relative density (dimensionless) of RAP Mineral Materials is calculated according to density composite formula 1;
In formula:P1、P2、P3- coarse aggregate, fine aggregate, filler account for the percentage ratio of mineral aggregate gross mass, itself and be 100;
D1、D2The apparent relative density of-coarse aggregate, fine aggregate;D3The relative density of-filler.
(7) the bulk specific gravity (dimensionless) of RAP Mineral Materials is calculated according to density composite formula 2;
In formula:P1、P2、P3- coarse aggregate, fine aggregate, filler account for the percentage ratio of mineral aggregate gross mass, itself and be 100;
R1、R2The bulk specific gravity of-coarse aggregate, fine aggregate;R3The relative density of-filler.
Preferably, the step (4), fine aggregate is placed in 0.15mm square hole screens and is eluriated in batches.
Preferably, the anion surfactant is dodecylbenzene sodium sulfonate, fatty alcohol-ether sodium sulfate or alkene Base sodium sulfonate.
Preferably, the step (1), it is 110~130 DEG C to reclaim asphalt pavement material preheating softening temperature.
Preferably, the step (5), the drying temperature of filler is 110~120 DEG C.
The advantages of the present invention are:
1. the density measurement method of the recovery asphalt pavement material Mineral Material of the present invention, is taken out with trichloroethylene solvent Carry, it can be ensured that the Colophonium in coarse aggregate, fine aggregate, filler surface and space is removed clean;Carry out in fume hood simultaneously Operation, environmental pollution are little, do not affect testing crew healthy;
2. the density measurement method of the recovery asphalt pavement material Mineral Material of the present invention, coarse aggregate and fine aggregate using it is cloudy from Sub- surfactant washing, can clean trichloro ethylene, improve certainty of measurement, while eluriated and water filling, can be further Trichloro ethylene in clean deep layer space;
3. the density measurement method of the recovery asphalt pavement material Mineral Material of the present invention, filler is using at anhydrous kerosene mode There is hydration reaction with water in reason, the cement that may contain in preventing filler, affect result of the test;
4. two types material is treated, cleaning treatment is carried out respectively using two ways, it is ensured that the precision of measurement, from And improve the measurement accuracy of mineral aggregate global density;
5. the present invention recovery asphalt pavement material Mineral Material density measurement method, simple and easy to do, data are true and reliable, Low cost, low stain can provide accurate parameter for reclaimed asphalt mixture volume index, be that one kind has higher innovation Density measurement method.
Specific embodiment
The present invention is described in further details with reference to specific embodiment.
Specific embodiment of the present invention is a kind of density measurement method for reclaiming asphalt pavement material Mineral Material, described Method of testing step is as follows:
(1) the pre- thermal softening of asphalt pavement material will be reclaimed, fritter will manually be separated into, and then Colophonium will be reclaimed in fume hood Ground surface material is stripped with trichloroethylene solvent, and mineral aggregate is obtained after the completion of extracting.Mineral aggregate is put into into 100~110 DEG C of baking oven Middle drying and processing;
(2) mineral aggregate is cooled to after room temperature, carries out screening stepping:
When the mineral aggregate nominal maximum particle diameter in RAP be more than 2.36mm when, mineral aggregate should be divided into more than 2.36mm coarse aggregate, 0.15~2.36mm fine aggregates, 0~0.15mm filler third gear;
When the mineral aggregate nominal maximum particle diameter in RAP be less than 2.36mm when, mineral aggregate should be divided into 0.15~2.36mm fine aggregates, 0 Two grades of~0.15mm fillers;
(3) the aqueous solution of anionic surfactant of configuration quality percentage ratio 0.2%~0.3%, coarse aggregate is immersed in molten In liquid, it is sufficiently stirred for, eluriates for several times repeatedly, and constantly slowly injects new water, until coarse aggregate blibbing is all discharged, and water Face non-foam floating, till surface of aggregate infiltrates good, light, is then put into coarse aggregate in 100~110 DEG C of baking oven Carry out drying and processing;
Clean coarse aggregate is obtained, then according to《Highway engineering is gathered materials testing regulationss》" coarse aggregate density in (JTG E42) And the moisture content test (basket method) " operation, obtain apparent relative density (dimensionless), the bulk specific gravity (nothing of coarse aggregate Dimension);
(4) the aqueous solution of anionic surfactant of mass percent 0.3%~0.5% is prepared, fine aggregate is immersed in molten In liquid, fully stir, eluriate repeatedly, and constantly slowly inject new water, until fine aggregate blibbing is all discharged, the water surface is still After foam floating, fine aggregate is poured into tray, be cooled to room temperature after drying in being put into 100~110 DEG C of baking oven;
Clean fine aggregate is obtained, then according to《Highway engineering is gathered materials testing regulationss》" fine aggregate density in (JTG E42) And the moisture content test (basket method) " operation, obtain apparent relative density (dimensionless), the bulk specific gravity (nothing of fine aggregate Dimension);
According to《Highway engineering is gathered materials testing regulationss》" breeze density test " operation in (JTG E42), in fume hood In, filler is immersed in anhydrous kerosene, is fully stirred, the bubble effusion allowed inside filler, standing a period of time treats that filler sinks Behind shallow lake, kerosene is carefully poured out;New kerosene is added again, repeats aforesaid operations at least 1 time;
Pour filler into tray, treat that kerosene evaporates into face and does, be often cooled to after drying in being put into 110~120 DEG C of baking oven Temperature, liquid medium select anhydrous kerosene, test to obtain the relative density (dimensionless) of filler;
(6) the apparent relative density (dimensionless) of RAP Mineral Materials is calculated according to density composite formula 1;
In formula:P1、P2、P3- coarse aggregate, fine aggregate, filler account for the percentage ratio of mineral aggregate gross mass, itself and be 100;
D1、D2The apparent relative density of-coarse aggregate, fine aggregate;D3The relative density of-filler.
(7) the bulk specific gravity (dimensionless) of RAP Mineral Materials is calculated according to density composite formula 2;
In formula:P1、P2、P3- coarse aggregate, fine aggregate, filler account for the percentage ratio of mineral aggregate gross mass, itself and be 100;
R1、R2The bulk specific gravity of-coarse aggregate, fine aggregate;R3The relative density of-filler.
In order to preferably clean the trichloro ethylene on mineral aggregate surface, the anion surfactant is DBSA Sodium, fatty alcohol-ether sodium sulfate or sodium olefin sulfonate.
To prevent from gathering materials lost, institute's step 4 can immerse 0.15mm square hole screens in solution, and fine aggregate is placed in square hole in batches Eluriate in sieve.
Concrete test data is as follows:
Embodiment 1:
A kind of coarse aggregate, adopts《Highway engineering is gathered materials testing regulationss》The method of (JTG E42) obtains actual density.Will be thick Gathering materials, it is attached to be wrapped up in heated bitumen, measures density again using the inventive method, is shown in Table 1.
1 coarse aggregate density of table is contrasted
As can be seen from the above table, the mineral aggregate that asphalt pavement material is reclaimed in attached simulation is wrapped up in using coarse aggregate heated bitumen, then Carry out the laggard line parameter of the first to three step process to determine, the apparent relative density and bulk specific gravity two of drawn coarse aggregate Item result is of slight difference with the data of former coarse aggregate, equal coincidence loss standard.
As fine aggregate and coarse aggregate property and processing mode are similar, can derive, the method for testing is also complied with carefully The apparent relative density for gathering materials and the measure of bulk specific gravity are required.
Embodiment 2:
A kind of filler, adopts《Highway engineering is gathered materials testing regulationss》The method of (JTG E42) obtains actual density.By filler Wrapped up in heated bitumen attached, density is measured again using the inventive method, 2 are shown in Table.
2 packing density of table is contrasted
As can be seen from the above table, the mineral aggregate that asphalt pavement material is reclaimed in attached simulation, Ran Houjin are wrapped up in using filler heated bitumen Row first and second, the laggard line parameter measure of five steps process, the result of the apparent relative density of drawn filler and the data phase of filler Little, the coincidence loss standard of difference.
Embodiment 3:
A kind of RAP, the nominal maximum particle diameter of its Mineral Material is 9.5mm, measures density using the inventive method, is shown in Table 3.
Each shelves density of material in 3 mineral aggregate of table
Mineral aggregate in the RAP
Mineral aggregate in the RAP
As can be seen from the above table, the coarse aggregate containing more than 2.36mm in 3 mineral aggregate of table, it should using the thick of more than 2.36mm Gather materials, 0.15~2.36mm fine aggregates, 0~0.15mm third gear are sieved, then respectively each material is cleaned respectively and surveyed It is fixed.The apparent relative density and hair relative density of the RAP for being determined can be used for calculating reclaimed asphalt mixture volume index.
Embodiment 4:
A kind of RAP, the nominal maximum particle diameter of its Mineral Material is 2.36mm, measures density using the inventive method, is shown in Table 4.
Each shelves density of material in 4 mineral aggregate of table
Mineral aggregate in the RAP
Mineral aggregate in the RAP
As can be seen from the above table, do not contain the coarse aggregate of more than 2.36mm in 3 mineral aggregate of table, it should using 0.15~2.36mm Fine aggregate, two grades of 0~0.15mm fillers are sieved, and then respectively each material are cleaned respectively and are determined.The RAP for being determined Apparent relative density and hair relative density can be used for calculate reclaimed asphalt mixture volume index.
The above, only presently preferred embodiments of the present invention, not to limit the present invention, every skill according to the present invention Any trickle amendment, equivalent and improvement that art is substantially made to above example, should be included in technical solution of the present invention Protection domain within.

Claims (5)

1. a kind of density measurement method for reclaiming asphalt pavement material Mineral Material, the method for testing step is as follows:
(1) the pre- thermal softening of asphalt pavement material will be reclaimed, fritter will manually be separated into, and then bituminous paving will be reclaimed in fume hood Material is stripped with trichloroethylene solvent, and mineral aggregate is obtained after the completion of extracting, mineral aggregate is put in 100~110 DEG C of baking oven and is dried Dry-cure;
(2) mineral aggregate is cooled to after room temperature, carries out screening stepping:
When mineral aggregate nominal maximum particle diameter is more than 2.36mm, mineral aggregate should be divided into the coarse aggregate of more than 2.36mm, 0.15~2.36mm Fine aggregate, 0~0.15mm filler third gear;
When mineral aggregate nominal maximum particle diameter is less than 2.36mm, mineral aggregate should be divided into 0.15~2.36mm fine aggregates, 0~0.15mm fillers Two grades;
(3) the aqueous solution of anionic surfactant of mass percent 0.2%~0.3% is prepared, coarse aggregate is immersed in into solution In, it is sufficiently stirred for, eluriates for several times repeatedly, and constantly slowly injects new water, until coarse aggregate blibbing is all discharged, and the water surface Non-foam is floated, and then coarse aggregate is put in 100~110 DEG C of baking oven carries out drying and processing;
Clean coarse aggregate is obtained, then according to《Highway engineering is gathered materials testing regulationss》" coarse aggregate density and water suction in JTG E42 Rate tests (basket method) " operation, obtain apparent relative density (dimensionless), the bulk specific gravity (dimensionless) of coarse aggregate;
(4) the aqueous solution of anionic surfactant of mass percent 0.3%~0.5% is prepared, fine aggregate is immersed in into solution In, fully stir, eluriate repeatedly, and constantly slowly inject new water, until fine aggregate blibbing is all discharged, water surface non-foam After floating, fine aggregate is poured into tray, be cooled to room temperature after drying in being put into 100~110 DEG C of baking oven;
Clean fine aggregate is obtained, then according to《Highway engineering is gathered materials testing regulationss》" fine aggregate density and water suction in JTG E42 Rate tests (basket method) " operation, obtain apparent relative density (dimensionless), the bulk specific gravity (dimensionless) of fine aggregate;
(5) in fume hood, filler is immersed in anhydrous kerosene, is fully stirred, the bubble effusion allowed inside filler stands one The section time, after filler precipitation, carefully pours out kerosene;New kerosene is added again, repeats aforesaid operations at least 1 time;
Pour filler into tray, treat that kerosene evaporates into face and does, room temperature is cooled to after drying in being put into 110~120 DEG C of baking oven, is obtained To clean filler, according to《Highway engineering is gathered materials testing regulationss》" breeze density test " operation in JTG E42, liquid medium choosing Anhydrous kerosene is selected, test obtains the relative density (dimensionless) of filler;
(6) the apparent relative density (dimensionless) for reclaiming asphalt pavement material Mineral Material is calculated according to density composite formula 1;
In formula:P1、P2、P3- coarse aggregate, fine aggregate, filler account for the percentage ratio of mineral aggregate gross mass, itself and be 100;
D1、D2The apparent relative density of-coarse aggregate, fine aggregate;D3The relative density of-filler;
(7) the bulk specific gravity (dimensionless) for reclaiming asphalt pavement material Mineral Material is calculated according to density composite formula 2;
In formula:P1、P2、P3- coarse aggregate, fine aggregate, filler account for the percentage ratio of mineral aggregate gross mass, itself and be 100;
R1、R2The bulk specific gravity of-coarse aggregate, fine aggregate;R3The relative density of-filler.
2. it is according to claim 1 reclaim asphalt pavement material Mineral Material density measurement method, it is characterised in that:It is described Step (4), fine aggregate is placed in batches in 0.15mm square hole screens and is eluriated.
3. it is according to claim 1 and 2 reclaim asphalt pavement material Mineral Material density measurement method, it is characterised in that: The anion surfactant is dodecylbenzene sodium sulfonate, fatty alcohol-ether sodium sulfate or sodium olefin sulfonate.
4. it is according to claim 1 and 2 reclaim asphalt pavement material Mineral Material density measurement method, it is characterised in that: The step (1), it is 110~130 DEG C to reclaim asphalt pavement material preheating softening temperature.
5. it is according to claim 1 and 2 reclaim asphalt pavement material Mineral Material density measurement method, it is characterised in that: The step (5), the drying temperature of filler is 110~120 DEG C.
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CN111693016A (en) * 2020-05-26 2020-09-22 安庆市凯瑞建材有限公司 Device for quickly and accurately measuring density of homogeneous fireproof insulation board
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