CN107290511A - The detection method that a kind of Cement treated material level is matched somebody with somebody - Google Patents

The detection method that a kind of Cement treated material level is matched somebody with somebody Download PDF

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Publication number
CN107290511A
CN107290511A CN201710473140.4A CN201710473140A CN107290511A CN 107290511 A CN107290511 A CN 107290511A CN 201710473140 A CN201710473140 A CN 201710473140A CN 107290511 A CN107290511 A CN 107290511A
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somebody
treated material
quality
compound
cement
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CN107290511B (en
Inventor
侯茜茜
孙政
何桂平
徐世颖
吴世珍
蒋小花
刘星光
李洁
马帅
陈剑
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Shenzhen Traffic Engineering Test Center Co.,Ltd.
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SHENZHEN HIGHWAY TRAFFIC ENGINEERING TEST CENTER
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/38Concrete; Lime; Mortar; Gypsum; Bricks; Ceramics; Glass
    • G01N33/383Concrete or cement
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N5/00Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid
    • G01N5/04Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid by removing a component, e.g. by evaporation, and weighing the remainder

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Physics & Mathematics (AREA)
  • Analytical Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Ceramic Engineering (AREA)
  • Food Science & Technology (AREA)
  • Medicinal Chemistry (AREA)
  • Preparation Of Clay, And Manufacture Of Mixtures Containing Clay Or Cement (AREA)

Abstract

The invention discloses the detection method that a kind of Cement treated material level is matched somebody with somebody, including:Take Cement treated material sample;Two parts of sample qualities are weighed, m ' is designated as respectively1、m’2, sample quality is placed on temperature to be dried at 105 DEG C ± 5 DEG C, and cool down, weigh drying sample, respectively m '3、m’4;Other two parts of sample qualities are weighed, m is designated as respectively1、m2, it is placed in water-bath, it is 55 DEG C ± 1 DEG C to control water temperature, is taken out after immersion 2h, is laid in a vessel disk and is dried in the case where temperature is 105 DEG C ± 5 DEG C, and cool down;Cement cleaning agent is added in sample after the cooling period to well mixed, compound is formed, stir-fries to mix surface without obvious Behavior of Hardened Cement Paste;The muddy water of mixture in clean container is filtered out by bushing screen;There is part fine powder mixture to fall within bushing screen;Compound on bushing screen is mixed with compound in clean container, is dried, weighed, quality m in the case where temperature is 105 DEG C ± 5 DEG C3;It is m to quality3Compound carry out bushing screen;Calculate screening result.

Description

The detection method that a kind of Cement treated material level is matched somebody with somebody
Technical field
The present invention relates to the detection method that Cement treated material level is matched somebody with somebody, belong to pavement material detection field, can be applied to Base course, the construction graded of underlayment Cement treated material are examined and evaluation.
Background technology
It is existing with the high speed development of highway in China transport development, road construction theory is also with high, Heavy Traffic amount Development progressively tends at this stage the more this structure type of bituminous paving+semi-rigid type base of maturation.Although this pavement structure Form has the advantages that many main flows for becoming road construction, but easily occurs in practical engineering application due to semi-rigid Asphalt Pavement Cracking disease caused by base material microcrack, and then influence the durability of road.
Semi-rigid sub-base material generally refers to Cement treated material, wherein usually 5% cement for base material Stable graded broken stone, what it is for subbase course material is usually 4% cement stabilized grading crushed stones.The master of semi-rigid sub-base material cracking Factor is wanted to include dry shrinkage and cracking, temperature contracting cracking, the major influence factors of dry shrinkage and cracking are the consumption control of cement, stabilizing material Three aspects such as Gradation Control, the control of optimum moisture content;The influence factor of temperature contracting cracking is external environment condition, and this needs Carry out its water conservation of rigorous concentration, insulated curing when Cement treated material construction.
At this stage, for influenceing the cement consumption of dry shrinkage and cracking, optimum moisture content two indices all as Construction control Important detection parameter, also there is corresponding detection method, but the level of Cement treated material site operation is not with but corresponding Detection method, the cracking of this bituminous paving for the cracking of Cement treated material and caused by the later stage all will be a quality Hidden danger.The level of site operation effectively verified with corresponding detection method is lacked to it, see whether with design level match somebody with somebody between deposit In larger deviation.
In view of the above-mentioned problems, the present invention proposes the detection method that a kind of Cement treated material level is matched somebody with somebody, it is mainly used in constructing Cement treated material level in journey is with detection and checking.
The content of the invention
In order to solve the above technical problems, it is an object of the invention to provide the detection method that a kind of Cement treated material level is matched somebody with somebody, This method can detect the grading of aggregates of job site Cement treated material.
The purpose of the present invention is realized by following technical scheme:
The detection method that a kind of Cement treated material level is matched somebody with somebody, including:
Step A takes Cement treated material sample, and the specimen material includes four parts, and is bisected into two groups;
Step B weighs two parts of sample qualities, and m ' is designated as respectively1、m’2, sample quality is placed on oven temperature for 105 DEG C Dried at ± 5 DEG C to constant weight, and be cooled to room temperature, weigh drying sample, respectively m '3、m’4
Step C weighs other two parts of sample qualities, and m is designated as respectively1、m2, it is placed in water bath with thermostatic control, it is 55 to control water temperature DEG C ± 1 DEG C, take out after soak time at least 2h, it is to be dried at 105 DEG C ± 5 DEG C to be laid in a vessel disk in oven temperature It is dry, and it is cooled to room temperature;
Cement cleaning agent is added in the samples of step D after the cooling period to well mixed, compound is formed, stir-fries to compound Surface is without obvious Behavior of Hardened Cement Paste;
The compound that Behavior of Hardened Cement Paste is cleaned up is placed in clean container by step E, and added water stirring, and cleaning is filtered out by bushing screen The muddy water of mixture in container, until being clean water;It is described filter out during there is part fine powder mixture to fall within bushing screen;
Step F mixes the compound on bushing screen with compound in clean container, is placed in baking oven, is 105 in temperature Dried at DEG C ± 5 DEG C to constant weight, weigh dry pack, quality m3
Step G is m to quality by bushing screen3Compound carry out bushing screen;
Step H calculates screening result.
Compared with prior art, one or more embodiments of the invention can have the following advantages that:
Inorganic binder Site Detection blank is filled up, this has notable meaning for inorganic binder Site quality control Justice.Abundant completion hydrated reaction of cement has been failed in the very first time in view of the Cement treated material of site operation, and it is commercially available Cement cleaning agent be weaker than hydrolysis product of cement-CSH gels to the solvability of unhydrated particle, therefore in order to more accurate complete Into test, the Cement treated material for fetching is soaked by 55 DEG C of ± 1 DEG C of waters bath with thermostatic control, cement fast hydration is realized, then adopt Hydrolysis product of cement is thoroughly dissolved with cement cleaning agent, then will gather materials by WATER-WASHING METHOD separates with solvent, finally by combination Bushing screen completes level with detection.
Embodiment
To make the object, technical solutions and advantages of the present invention clearer, below in conjunction with embodiment the present invention is made into The description of one step in detail.
In order to verify feasibility and accuracy of the Cement treated material level with detection method in the present invention, using known level After the synthetic aggravation matched somebody with somebody is mixed and stirred with cement, water, tested by detection method, specific implementation process is as follows:
(1) Cement treated material that field sampling is returned is used into quartering, wherein two parts be used for mixture gradation detection, Two parts are used for moisture content detection, and every part of quality is no less than 2kg.
(2) two parts of sample qualities are weighed, m ' is designated as respectively1、m’2(being accurate to 0.1g), is put into baking oven together with enamel tray (105 DEG C ± 5 DEG C of temperature of control) drying is cooled to room temperature to constant weight, weighs correspondence drying sample quality, respectively m '3、m ’4
(3) two parts of sample qualities are weighed, m is designated as respectively1、m2(being accurate to 0.1g), is then placed in two aluminium by sample respectively In pot, then aluminum pot inserted in thermostat water bath together with sample.
(4) thermostat water bath is opened, 55 DEG C ± 1 DEG C of water temperature is controlled, sample soak time must not be less than 2h.
(5) aluminum pot is taken out, sample is poured into enamel tray, tiling is scattered.
(6) (105 DEG C ± 5 DEG C of temperature of control) drying and then by the enamel tray for filling sample is put into baking oven, and is cooled to Room temperature.
(7) side addition cement cleaning agent, while being stir-fried back and forth with perching knife, until mix surface is without obvious Behavior of Hardened Cement Paste.Will place The compound managed is put in a clean container, is added sufficient amount of clean water submerged compound, is sufficiently stirred for splash bar, is made thin Powder is suspended in water.
(8) use 2.36mm and 0.075mm to constitute bushing screen (0.075mm is bottom sieve), carefully fine powder will be mixed with container Suspension is poured out, and is flowed into by bushing screen in another clean container, is tried not to pour out coarse aggregate.(7)-(8) step is repeated, directly Untill the water poured out is clean, it can be rinsed if necessary using sluggish flow.
(9) compound in the compound and container on bushing screen is all recycled in an enamel tray, carefully secreted The ponding of enamel panel surface, is then placed in baking oven (105 DEG C ± 5 DEG C of temperature of control) drying by enamel tray together with compound To constant weight, dry pack quality m3 is weighed.
(10) from the bottom to top, according to 0.075mm, 0.15mm, 0.3mm, 0.6mm, 1.18mm, 2.36mm, 4.75mm, 9.5mm, 13.2mm, 16.0mm, 19.0mm, 26.5mm, 31.5mm, 37.5mm, 53.0mm order composition bushing screen, enter to compound Weight is recorded into table 1 respectively on row screening, the sieve of each sieve aperture.
(11) parallel test repeat step 6~10 is carried out.
(12) screening result is calculated according to the following equation, and result is inserted in table 1;
Screening calculating includes:Calculating, 0.075mm lower parts of screen sub-prime amount and the 0.075mm of Cement treated material moisture content are logical Calculating, the calculating of accumulated retained percentage and each number sieve that the calculating for crossing rate, the calculating for sieving consume, each number screening meter are tailed over lead to Cross the calculating of rate.
The calculating formula of the Cement treated material moisture content is as follows:
w1=(m '1-m’3)/m’3* 100% (1)
w2=(m '2-m’4)/m’4* 100% (2)
W=(w1+w2)/2 (3)
W in formula1、w2Respectively two groups parallel test compound moisture content;m’1、m’2The first prothyl of respectively two groups compounds Amount;m’3、m’4The dry mass of respectively two groups compounds;W is the moisture content of Cement treated material;
Above-mentioned 0.075mm lower parts of screen sub-prime amount and the calculation formula of 0.075mm percent of pass are:
m0.075=m1/(1+w)-m3 (4)
P0.075=m0.075/m3 (5)
In formula:m0.075To wash the obtained quality less than 0.075mm parts in compound;P0.075To be small in compound In 0.075mm content;m1For initial mixing material quality;m3To sieve upper gross mass after washing.
The calculation formula of above-mentioned screening consume is:
m5=m3-(Σmi+m0.075) (6)
If the proportion of goods damageds are more than 0.3%, it should test again, m in formula5Cause that the quality of part is lost for screening;m3After washing Gross mass on sieve;miQuality more than the classifying screen sieved for each;m0.075It is less than 0.075mm parts for what washing in compound was obtained Quality.
Above-mentioned each number screening counts the calculation formula tailed over and is:
P’i=mi/(m3-m5) * 100% (7)
In formula:P’iFor each number sieve grader retained percentage;m5Cause that the quality of part is lost for screening;m3To be sieved after washing Upper gross mass;mi--- point meter on each sieve tails over quality;I is followed successively by 0.15mm, 0.3mm, 0.6mm ... to 57mm.
The accumulated retained percentage is the grader retained percentage sum of each number sieve more than this number is sieved, and is accurate to 0.1%;
The percent of pass Pi of each number sieve subtracts each number sieve accumulated retained percentage equal to 100, is accurate to 0.1%.
Table 1
Above-mentioned steps are after the synthetic aggravation matched somebody with somebody using known level is mixed and stirred with cement, water, to pass through detection side of the invention Method is tested, and is chosen 10-30mm, 10-20mm, 5-10mm and 0-5mm fourth gear and is gathered materials, and passing ratio, which is mixed to match somebody with somebody, to be obtained synthesizing level With rubble, each sieve aperture percent of pass is then obtained using dry sieve method and sees attached list 2:
Table 2
Screen size (mm) Standard percent of pass/% Survey percent of pass/% Difference/%
53 100 100 0.0
37.5 100 100 0.0
31.5 96.5 98.6 2.1
26.5 93.2 93.5 0.3
19 85 87.9 2.9
16 79.5 79.5 0.0
13.2 60.4 62.1 1.7
9.5 39.6 38.6 -1.0
4.75 21.4 20.5 -0.9
2.36 14 13.4 -0.6
1.18 9.6 10 0.4
0.6 6.5 6.7 0.2
0.3 5.2 5.6 0.4
0.15 4.4 4.8 0.4
0.075 4.2 4.4 0.2
According to 5% cement consumption, 5.2% optimal water consumption, formate gradation composition and the cement of respective quality, water are mixed and stirred together Uniformly.
The detection method provided according to the present embodiment, detects that testing result sees attached list 3 to the Cement treated material:
Table 3
The screening result for contrasting subordinate list 2 and subordinate list 3 is understood:Survey percent of pass more to coincide with standard percent of pass, wherein partially Difference is 2.9% to the maximum, and this meets repeatability error requirement for engineering detecting, shows the method tool that the present embodiment is provided There are accuracy and science.
Although disclosed herein embodiment as above, described content is only to facilitate understanding the present invention and adopting Embodiment, is not limited to the present invention.Any those skilled in the art to which this invention pertains, are not departing from this On the premise of the disclosed spirit and scope of invention, any modification and change can be made in the implementing form and in details, But the scope of patent protection of the present invention, still should be subject to the scope of the claims as defined in the appended claims.

Claims (8)

1. the detection method that a kind of Cement treated material level is matched somebody with somebody, it is characterised in that the described method comprises the following steps:
Step A takes Cement treated material sample, and the specimen material includes four parts, and is bisected into two groups;
Step B weighs two parts of sample qualities, and m ' is designated as respectively1、m’2, sample quality is placed on oven temperature for 105 DEG C ± 5 DEG C It is lower to be dried to constant weight, and room temperature is cooled to, weigh drying sample, respectively m '3、m’4
Step C weighs other two parts of sample qualities, and m is designated as respectively1、m2, it is placed in water bath with thermostatic control, it is 55 DEG C ± 1 to control water temperature DEG C, taken out after soak time at least 2h, be laid in a vessel disk and dried in the case where oven temperature is 105 DEG C ± 5 DEG C, and it is cold But to room temperature;
Cement cleaning agent is added in the samples of step D after the cooling period to well mixed, compound is formed, stir-fries to mix surface Without obvious Behavior of Hardened Cement Paste;
The compound that Behavior of Hardened Cement Paste is cleaned up is placed in clean container by step E, and added water stirring, and clean container is filtered out by bushing screen The muddy water of middle mixture, until being clean water;It is described filter out during there is part fine powder mixture to fall within bushing screen;
Step F mixes the compound on bushing screen with compound in clean container, is placed in baking oven, is 105 DEG C ± 5 in temperature Dried at DEG C to constant weight, weigh dry pack, quality m3
Step G is m to quality by bushing screen3Compound carry out bushing screen;
Step H calculates screening result.
2. the detection method that Cement treated material level as claimed in claim 1 is matched somebody with somebody, it is characterised in that
In four parts of quality, every part is at least 2kg;
Bushing screen is constituted using 2.36mm and 0.075mm in the step E, and wherein 0.075mm is bottom sieve;
In the step G using 0.075mm, 0.15mm, 0.3mm, 0.6mm, 1.18mm, 2.36mm, 4.75mm, 9.5mm, 13.2mm, 16.0mm, 19.0mm, 26.5mm, 31.5mm, 37.5mm, 53.0mm order composition bushing screen.
3. the detection method that Cement treated material level as claimed in claim 1 is matched somebody with somebody, it is characterised in that sieved in the step H Calculating includes:The calculating of Cement treated material moisture content, the calculating of 0.075mm lower parts of screen sub-prime amount and 0.075mm percent of pass, sieve Calculating, the calculating of accumulated retained percentage and the calculating of each number sieve percent of pass for dividing the calculating of consume, each number screening meter to tail over.
4. the detection method that Cement treated material level as claimed in claim 3 is matched somebody with somebody, it is characterised in that the Cement treated material The calculating formula of moisture content is as follows:
w1=(m '1-m’3)/m’3* 100% (1)
w2=(m '2-m’4)/m’4* 100% (2)
W=(w1+w2)/2 (3)
W in formula1、w2Respectively two groups parallel test compound moisture content;m’1、m’2Respectively two groups compound initial masses;m ’3、m’4The dry mass of respectively two groups compounds;W is the moisture content of Cement treated material.
5. the detection method that Cement treated material level as claimed in claim 3 is matched somebody with somebody, it is characterised in that under the 0.075mm sieves The calculation formula of part mass and 0.075mm percent of pass is:
m0.075=m1/(1+w)-m3 (4)
P0.075=m0.075/m3 (5)
In formula:m0.075To wash the obtained quality less than 0.075mm parts in compound;P0.075To be less than in compound 0.075mm content;m1For initial mixing material quality;m3To sieve upper gross mass after washing.
6. the detection method that Cement treated material level as claimed in claim 3 is matched somebody with somebody, it is characterised in that the meter of the screening consume Calculating formula is:
m5=m3-(Σmi+m0.075) (6)
If the proportion of goods damageds are more than 0.3%, it should test again, m in formula5Cause that the quality of part is lost for screening;m3To be sieved after washing Gross mass;miQuality more than the classifying screen sieved for each;m0.075To wash the obtained matter less than 0.075mm parts in compound Amount.
7. the detection method that Cement treated material level as claimed in claim 3 is matched somebody with somebody, it is characterised in that each number screening meter sieve Remaining calculation formula is:
P’i=mi/(m3-m5) * 100% (7)
In formula:P’iFor each number sieve grader retained percentage;m5Cause that the quality of part is lost for screening;m3It is upper total to be sieved after washing Quality;mi--- point meter on each sieve tails over quality;I is followed successively by 0.15mm, 0.3mm, 0.6mm ... to 57mm.
8. the detection method that Cement treated material level as claimed in claim 3 is matched somebody with somebody, it is characterised in that described to add up to tail over percentage Rate is the grader retained percentage sum of each number sieve more than this number is sieved, and is accurate to 0.1%;
The percent of pass Pi of each number sieve subtracts each number sieve accumulated retained percentage equal to 100, is accurate to 0.1%.
CN201710473140.4A 2017-06-21 2017-06-21 Detection method for grading of cement stabilizing material Active CN107290511B (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108593481A (en) * 2018-04-11 2018-09-28 镇江市建科工程质量检测中心有限公司 A kind of detection method of cement stabilized macadam grading
CN111537385A (en) * 2020-04-26 2020-08-14 山东莱钢永锋钢铁有限公司 Cement fineness inspection method
CN114804688A (en) * 2022-06-27 2022-07-29 山西工程科技职业大学 Method for determining gradation and mixing ratio of regenerated mixed fine aggregate

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108593481A (en) * 2018-04-11 2018-09-28 镇江市建科工程质量检测中心有限公司 A kind of detection method of cement stabilized macadam grading
CN111537385A (en) * 2020-04-26 2020-08-14 山东莱钢永锋钢铁有限公司 Cement fineness inspection method
CN114804688A (en) * 2022-06-27 2022-07-29 山西工程科技职业大学 Method for determining gradation and mixing ratio of regenerated mixed fine aggregate
CN114804688B (en) * 2022-06-27 2022-09-16 山西工程科技职业大学 Method for determining gradation and mixing ratio of regenerated mixed fine aggregate

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