CN104213402A - Wool fabric softener and preparation method thereof - Google Patents

Wool fabric softener and preparation method thereof Download PDF

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Publication number
CN104213402A
CN104213402A CN201410426406.6A CN201410426406A CN104213402A CN 104213402 A CN104213402 A CN 104213402A CN 201410426406 A CN201410426406 A CN 201410426406A CN 104213402 A CN104213402 A CN 104213402A
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CN
China
Prior art keywords
parts
softener
woolen
wool fabric
sodium bicarbonate
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Pending
Application number
CN201410426406.6A
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Chinese (zh)
Inventor
周敏
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WUXI QISHENG KNITTING GLOVES FACTORY
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WUXI QISHENG KNITTING GLOVES FACTORY
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Priority to CN201410426406.6A priority Critical patent/CN104213402A/en
Publication of CN104213402A publication Critical patent/CN104213402A/en
Pending legal-status Critical Current

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Abstract

The invention provides a wool fabric softener which is prepared from the following materials in parts by weight: 5 to 8 parts of alcohol ether phosphate ester sodium salt, 10 to 15 parts of polydimethylsiloxane, 50 to 60 parts of ethyl alcohol, 20 to 25 parts of stearamide, 3 to 5 parts of polyoxyethylene ether fatty acid ester, 1 to 3 parts of octadecyl dimethyl ammonium chloride, 3 to 5 parts of polypropylene glycol, 10 to 15 parts of liquid paraffin, 1 to 2 parts of sodium bicarbonate and 350 to 450 parts of water. The wool fabric softener is good in stability. After the wool fabric softener is used, wool fabric is soft and rich in elasticity. The experiment shows that the wool fabric softener also has a certain antistatic effect.

Description

A kind of woolen softener and preparation method thereof
Technical field
The invention belongs to textile auxiliary technical field, be specifically related to a kind of woolen softener.
Background technology
Because softener can be given fabric with soft, comfortable feel, therefore can improve quality and the surcharge of fabric, become the main auxiliary agent of after-finishing of textile products.Along with the raising of people's living standard, the enhancing of the awareness of environment protection and health, requirement to weaving special material is also more and more higher, require fabric to have certain softness, the characteristic such as crease-resistant, also more and more higher to the quality requirements of softener, this has also promoted the fast development of softener kind.
Summary of the invention
The invention provides a kind of woolen softener, apply after woolen softener of the present invention, wool fabric is soft, high resilience.
The invention provides a kind of woolen softener, described woolen softener is comprised of each material of following parts by mass: alcohol ether phosphide sodium salt 5-8 part, dimethyl silicone polymer 10-15 part, ethanol 70-80 part, stearmide 20-25 part, aliphatic acid polyethenoxy ether ester 3-5 part, octadecyl alkyl dimethyl ammonium chloride 1-3 part, polypropylene glycol 3-5 part, atoleine 10-15 part, sodium bicarbonate 1-2 part, water 350-450 part.
Preferably, described woolen softener is comprised of each material of following parts by mass: 6 parts of alcohol ether phosphide sodium salts, 12 parts of dimethyl silicone polymers, 75 parts of ethanol, 22 parts of stearmides, 4 parts of aliphatic acid polyethenoxy ether esters, 2 parts of octadecyl alkyl dimethyl ammonium chlorides, 4 parts of polypropylene glycols, 12 parts of atoleines, 1 part of sodium bicarbonate, 400 parts, water.
The invention provides the preparation method that above-mentioned woolen softener is also provided, step is as follows:
1) by proportioning, water, alcohol ether phosphide sodium salt, dimethyl silicone polymer, stearmide, aliphatic acid polyethenoxy ether ester are heated to 70-80 ℃, stir, reaction 1-2 hour;
2) add octadecyl alkyl dimethyl ammonium chloride, ethanol, polypropylene glycol, insulated and stirred, reaction 2-3 hour;
3) be cooled to room temperature, add atoleine, sodium bicarbonate, after being uniformly mixed and get final product.
Softener of the present invention has good stability, applies after softener of the present invention, and wool fabric is soft, high resilience.Through test, softener of the present invention also has certain antistatic effect.
The specific embodiment
Following embodiment is convenient to understand better the present invention, but does not limit the present invention.Experimental technique in following embodiment, if no special instructions, is conventional method.
embodiment 1
The formula of woolen softener of the present invention is as follows:
Alcohol ether phosphide sodium salt 6kg, dimethyl silicone polymer 12kg, ethanol 75kg, stearmide 22kg, aliphatic acid polyethenoxy ether ester 4kg, octadecyl alkyl dimethyl ammonium chloride 2kg, polypropylene glycol 4kg, atoleine 12kg, sodium bicarbonate 1kg, water 400kg.
The preparation method of woolen softener of the present invention is as follows:
1) by proportioning, water, alcohol ether phosphide sodium salt, dimethyl silicone polymer, stearmide, aliphatic acid polyethenoxy ether ester are heated to 75 ℃, stir, react 1.5 hours;
2) add octadecyl alkyl dimethyl ammonium chloride, ethanol, polypropylene glycol, insulated and stirred, reacts 2.5 hours;
3) be cooled to room temperature, add atoleine, sodium bicarbonate, after being uniformly mixed and get final product.
embodiment 2
The formula of woolen softener of the present invention is as follows:
Alcohol ether phosphide sodium salt 5kg, dimethyl silicone polymer 15kg, ethanol 70kg, stearmide 25kg, aliphatic acid polyethenoxy ether ester 5kg, octadecyl alkyl dimethyl ammonium chloride 1kg, polypropylene glycol 5kg, atoleine 10kg, sodium bicarbonate 1.5kg, water 450kg.
The preparation method of woolen softener of the present invention is as follows:
1) by proportioning, water, alcohol ether phosphide sodium salt, dimethyl silicone polymer, stearmide, aliphatic acid polyethenoxy ether ester are heated to 75 ℃, stir, react 2 hours;
2) add octadecyl alkyl dimethyl ammonium chloride, ethanol, polypropylene glycol, insulated and stirred, reacts 2 hours;
3) be cooled to room temperature, add atoleine, sodium bicarbonate, after being uniformly mixed and get final product.
embodiment 3
The formula of woolen softener of the present invention is as follows:
Alcohol ether phosphide sodium salt 8kg, dimethyl silicone polymer 10kg, ethanol 80kg, stearmide 20kg, aliphatic acid polyethenoxy ether ester 3kg, octadecyl alkyl dimethyl ammonium chloride 3kg, polypropylene glycol 3kg, atoleine 15kg, sodium bicarbonate 2kg, water 350kg.
The preparation method of woolen softener of the present invention is as follows:
1) by proportioning, water, alcohol ether phosphide sodium salt, dimethyl silicone polymer, stearmide, aliphatic acid polyethenoxy ether ester are heated to 75 ℃, stir, react 1 hour;
2) add octadecyl alkyl dimethyl ammonium chloride, ethanol, polypropylene glycol, insulated and stirred, reacts 3 hours;
3) be cooled to room temperature, add atoleine, sodium bicarbonate, after being uniformly mixed and get final product.
embodiment 4
The formula of woolen softener of the present invention is as follows:
Alcohol ether phosphide sodium salt 6kg, dimethyl silicone polymer 10kg, ethanol 75kg, stearmide 25kg, aliphatic acid polyethenoxy ether ester 3kg, octadecyl alkyl dimethyl ammonium chloride 3kg, polypropylene glycol 4kg, atoleine 15kg, sodium bicarbonate 2kg, water 380kg.
The preparation method of woolen softener of the present invention is as follows:
1) by proportioning, water, alcohol ether phosphide sodium salt, dimethyl silicone polymer, stearmide, aliphatic acid polyethenoxy ether ester are heated to 75 ℃, stir, react 1.5 hours;
2) add octadecyl alkyl dimethyl ammonium chloride, ethanol, polypropylene glycol, insulated and stirred, reacts 2.5 hours;
3) be cooled to room temperature, add atoleine, sodium bicarbonate, after being uniformly mixed and get final product.
Finally it should be noted that: the foregoing is only the preferred embodiments of the present invention, be not limited to the present invention, although the present invention is had been described in detail with reference to previous embodiment, for a person skilled in the art, its technical scheme that still can record aforementioned each embodiment is modified, or part technical characterictic is wherein equal to replacement.Within the spirit and principles in the present invention all, any modification of doing, be equal to replacement, improvement etc., within all should being included in protection scope of the present invention.

Claims (3)

1. a woolen softener, it is characterized in that: described woolen softener is comprised of each material of following parts by mass: alcohol ether phosphide sodium salt 5-8 part, dimethyl silicone polymer 10-15 part, ethanol 70-80 part, stearmide 20-25 part, aliphatic acid polyethenoxy ether ester 3-5 part, octadecyl alkyl dimethyl ammonium chloride 1-3 part, polypropylene glycol 3-5 part, atoleine 10-15 part, sodium bicarbonate 1-2 part, water 350-450 part.
2. woolen softener according to claim 1, it is characterized in that: described woolen softener is comprised of each material of following parts by mass: 6 parts of alcohol ether phosphide sodium salts, 12 parts of dimethyl silicone polymers, 75 parts of ethanol, 22 parts of stearmides, 4 parts of aliphatic acid polyethenoxy ether esters, 2 parts of octadecyl alkyl dimethyl ammonium chlorides, 4 parts of polypropylene glycols, 12 parts of atoleines, 1 part of sodium bicarbonate, 400 parts, water.
3. the preparation method of the woolen softener described in claim 1 or 2, is characterized in that: step is as follows:
(1) by proportioning, water, alcohol ether phosphide sodium salt, dimethyl silicone polymer, stearmide, aliphatic acid polyethenoxy ether ester are heated to 70-80 ℃, stir, reaction 1-2 hour;
(2) add octadecyl alkyl dimethyl ammonium chloride, ethanol, polypropylene glycol, insulated and stirred, reaction 2-3 hour;
(3) be cooled to room temperature, add atoleine, sodium bicarbonate, after being uniformly mixed and get final product.
CN201410426406.6A 2014-08-27 2014-08-27 Wool fabric softener and preparation method thereof Pending CN104213402A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201410426406.6A CN104213402A (en) 2014-08-27 2014-08-27 Wool fabric softener and preparation method thereof

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Application Number Priority Date Filing Date Title
CN201410426406.6A CN104213402A (en) 2014-08-27 2014-08-27 Wool fabric softener and preparation method thereof

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CN104213402A true CN104213402A (en) 2014-12-17

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104674555A (en) * 2015-03-06 2015-06-03 苏州爱立方服饰有限公司 Anti-static finishing agent for fabric and preparation method of anti-static finishing agent
CN105350323A (en) * 2015-09-25 2016-02-24 桐乡市新艺虹电气有限公司 Cotton thread softening additive
CN105441211A (en) * 2015-11-16 2016-03-30 胡光明 Compound softening agent and preparation method thereof
CN105463852A (en) * 2016-01-08 2016-04-06 湖州市千金丝织厂 Novel soft finishing agent and preparation method thereof
CN106120347A (en) * 2016-08-29 2016-11-16 枣阳市金鹏化工有限公司 A kind of softening agent containing dimethicone and preparation method thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101003947A (en) * 2006-01-18 2007-07-25 丹东恒星精细化工有限公司 Finishing agent of polysiloxane fiber, and producing method
CN102839537A (en) * 2012-09-19 2012-12-26 吴江市意胜纺织有限公司 Fabric softening agent
CN102877312A (en) * 2012-09-05 2013-01-16 吴江涵辉纺织有限公司 Fabric softener
CN103266484A (en) * 2013-05-16 2013-08-28 湖州厉华妤婕联合纺织有限公司 Fabric softening agent

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101003947A (en) * 2006-01-18 2007-07-25 丹东恒星精细化工有限公司 Finishing agent of polysiloxane fiber, and producing method
CN102877312A (en) * 2012-09-05 2013-01-16 吴江涵辉纺织有限公司 Fabric softener
CN102839537A (en) * 2012-09-19 2012-12-26 吴江市意胜纺织有限公司 Fabric softening agent
CN103266484A (en) * 2013-05-16 2013-08-28 湖州厉华妤婕联合纺织有限公司 Fabric softening agent

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Title
杨原梅等: "一种复配有机硅羊毛织物柔软剂", 《染整技术》 *

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104674555A (en) * 2015-03-06 2015-06-03 苏州爱立方服饰有限公司 Anti-static finishing agent for fabric and preparation method of anti-static finishing agent
CN104674555B (en) * 2015-03-06 2016-09-21 苏州爱立方服饰有限公司 A kind of fabric antistatic treatment agent and preparation method thereof
CN105350323A (en) * 2015-09-25 2016-02-24 桐乡市新艺虹电气有限公司 Cotton thread softening additive
CN105441211A (en) * 2015-11-16 2016-03-30 胡光明 Compound softening agent and preparation method thereof
CN105463852A (en) * 2016-01-08 2016-04-06 湖州市千金丝织厂 Novel soft finishing agent and preparation method thereof
CN106120347A (en) * 2016-08-29 2016-11-16 枣阳市金鹏化工有限公司 A kind of softening agent containing dimethicone and preparation method thereof

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Application publication date: 20141217