CN103790017B - A kind of antibacterial sheet finishing agent and preparation method thereof - Google Patents
A kind of antibacterial sheet finishing agent and preparation method thereof Download PDFInfo
- Publication number
- CN103790017B CN103790017B CN201310752903.0A CN201310752903A CN103790017B CN 103790017 B CN103790017 B CN 103790017B CN 201310752903 A CN201310752903 A CN 201310752903A CN 103790017 B CN103790017 B CN 103790017B
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- parts
- finishing agent
- antibacterial sheet
- sheet finishing
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- 230000000844 anti-bacterial effect Effects 0.000 title claims abstract description 19
- 238000002360 preparation method Methods 0.000 title claims abstract description 11
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 38
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 claims abstract description 29
- 238000003756 stirring Methods 0.000 claims abstract description 26
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims abstract description 20
- 239000000843 powder Substances 0.000 claims abstract description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 18
- 235000019739 Dicalciumphosphate Nutrition 0.000 claims abstract description 10
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims abstract description 10
- 239000001506 calcium phosphate Substances 0.000 claims abstract description 10
- 150000001732 carboxylic acid derivatives Chemical class 0.000 claims abstract description 10
- NEFBYIFKOOEVPA-UHFFFAOYSA-K dicalcium phosphate Chemical compound [Ca+2].[Ca+2].[O-]P([O-])([O-])=O NEFBYIFKOOEVPA-UHFFFAOYSA-K 0.000 claims abstract description 10
- 229940038472 dicalcium phosphate Drugs 0.000 claims abstract description 10
- 229910000390 dicalcium phosphate Inorganic materials 0.000 claims abstract description 10
- 229940051841 polyoxyethylene ether Drugs 0.000 claims abstract description 10
- 229920000056 polyoxyethylene ether Polymers 0.000 claims abstract description 10
- 239000011734 sodium Substances 0.000 claims abstract description 10
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 10
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000004110 Zinc silicate Substances 0.000 claims abstract description 8
- QWDJLDTYWNBUKE-UHFFFAOYSA-L magnesium bicarbonate Chemical compound [Mg+2].OC([O-])=O.OC([O-])=O QWDJLDTYWNBUKE-UHFFFAOYSA-L 0.000 claims abstract description 8
- 229910000022 magnesium bicarbonate Inorganic materials 0.000 claims abstract description 8
- 235000014824 magnesium bicarbonate Nutrition 0.000 claims abstract description 8
- 239000002370 magnesium bicarbonate Substances 0.000 claims abstract description 8
- XSMMCTCMFDWXIX-UHFFFAOYSA-N zinc silicate Chemical compound [Zn+2].[O-][Si]([O-])=O XSMMCTCMFDWXIX-UHFFFAOYSA-N 0.000 claims abstract description 8
- 235000019352 zinc silicate Nutrition 0.000 claims abstract description 8
- 239000000203 mixture Substances 0.000 claims abstract description 5
- 238000010438 heat treatment Methods 0.000 claims description 10
- 241000588724 Escherichia coli Species 0.000 abstract description 9
- 241000191967 Staphylococcus aureus Species 0.000 abstract description 9
- 230000000694 effects Effects 0.000 abstract description 3
- 238000001816 cooling Methods 0.000 abstract 1
- 230000002401 inhibitory effect Effects 0.000 description 4
- 229920000742 Cotton Polymers 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 1
- 230000001580 bacterial effect Effects 0.000 description 1
- 244000052616 bacterial pathogen Species 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000004166 bioassay Methods 0.000 description 1
- 238000009395 breeding Methods 0.000 description 1
- 230000001488 breeding effect Effects 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- 230000001629 suppression Effects 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
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- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
A kind of antibacterial sheet finishing agent and preparation method thereof, antibacterial sheet finishing agent is made up of according to weight ratio following composition: Dicalcium Phosphate is 3 ~ 7 parts, diatomite powder is 2 ~ 3 parts, titania powder is 1 ~ 2 part, zinc silicate is 3 ~ 5 parts, fatty alcohol-polyoxyethylene ether carboxylic acid sodium is 6 ~ 9 parts, diethylene glycol (DEG) is 3 ~ 5 parts, magnesium bicarbonate is 2 ~ 4 parts, water is 245 ~ 265 parts.Get each composition of finishing agent, mix again after being heated, strong stirring, cooling, prepare antibacterial sheet finishing agent, the sheet finishing agent prepared has the significant effect suppressing Escherichia coli and staphylococcus aureus.
Description
Technical field
The present invention relates to finishing agent of a kind of sheet and preparation method thereof, particularly relate to a kind of have significant suppress Escherichia coli and the sheet finishing agent of staphylococcus aureus and the preparation method of sheet finishing agent.
Background technology
The material of sheet mostly is cotton, after a number of uses, and in long-time unwashed situation, sheet can grow a certain amount of bacterium, and wherein Escherichia coli are exactly a very large harm.Grow in a large number if Escherichia coli obtain, human body can be caused to produce some diseases.Equally, the amount reproduction of staphylococcus aureus, also can increase the ill risk of people.When arranging sheet, allowing sheet possess stronger significant suppression staphylococcus aureus and colibacillary effect, the probability that people are ill can be reduced.The current kind of finishing agent is more, in these finishing agents, the finishing agent of these two kinds of pathogenic bacteria can be suppressed significantly also less, need us and continues research and development.
Summary of the invention
The technical problem solved: common sheet does not have the effect suppressing Escherichia coli and staphylococcus aureus, can increase the risk of people after Long-Time Service.
Technical scheme: the invention discloses a kind of antibacterial sheet finishing agent, antibacterial sheet finishing agent is made up of according to weight ratio following composition: Dicalcium Phosphate is 3 ~ 7 parts, diatomite powder is 2 ~ 3 parts, titania powder is 1 ~ 2 part, zinc silicate is 3 ~ 5 parts, fatty alcohol-polyoxyethylene ether carboxylic acid sodium is 6 ~ 9 parts, diethylene glycol (DEG) is 3 ~ 5 parts, magnesium bicarbonate is 2 ~ 4 parts, water is 245 ~ 265 parts.
A preparation method for antibacterial sheet finishing agent, preparation method comprises the following steps: water temperature in finishing agent reactor heating jacket is adjusted to 62 DEG C ~ 68 DEG C by (1); (2) in question response still heating jacket after water temperature stability, in reactor, drop into water is 245 ~ 265 parts, and stir with paddle, speed of agitator is 200rpm, adds that fatty alcohol-polyoxyethylene ether carboxylic acid sodium is 6 ~ 9 parts, diethylene glycol (DEG) is 3 ~ 5 parts during stirring, stirs; (3) in reactor, add that Dicalcium Phosphate is 3 ~ 7 parts, diatomite powder is 2 ~ 3 parts, titania powder is 1 ~ 2 part, zinc silicate is 3 ~ 5 parts, magnesium bicarbonate is 2 ~ 4 parts again, high-speed stirred is carried out again with paddle, speed of agitator is 400rpm, till stirring; (4) finishing agent after stirring is cooled naturally, obtain antibacterial finishing agent.
Described fatty alcohol-polyoxyethylene ether carboxylic acid sodium is preferably 9 parts.Described Dicalcium Phosphate order number is preferably 400 orders.Described titania powder is preferably 2 parts.
Beneficial effect: by the sheet of pure-cotton fabric after finishing agent of the present invention arranges, the Escherichia coli inhibiting rate of sheet is 74% to 78%, and the inhibiting rate of staphylococcus aureus is 81% to 87%.
Detailed description of the invention
Embodiment 1
(1) water temperature in finishing agent reactor heating jacket is adjusted to 68 DEG C; (2) in question response still heating jacket after water temperature stability, in reactor, drop into water is 245kg, and stir with paddle, speed of agitator is 200rpm, adds that fatty alcohol-polyoxyethylene ether carboxylic acid sodium is 6kg, diethylene glycol (DEG) is 5kg during stirring, stirs; (3) in reactor, add that 400 object Dicalcium Phosphate are 7kg, diatomite powder is 2kg, titania powder is 2kg, zinc silicate is 3kg, magnesium bicarbonate is 4kg again, high-speed stirred is carried out again with paddle, speed of agitator is 400rpm, till stirring; (4) finishing agent after stirring is cooled naturally, obtain antibacterial finishing agent.
Embodiment 2
(1) water temperature in finishing agent reactor heating jacket is adjusted to 64 DEG C; (2) in question response still heating jacket after water temperature stability, in reactor, drop into water is 255kg, and stir with paddle, speed of agitator is 200rpm, adds that fatty alcohol-polyoxyethylene ether carboxylic acid sodium is 7kg, diethylene glycol (DEG) is 3kg during stirring, stirs; (3) in reactor, add that 400 object Dicalcium Phosphate are 3kg, diatomite powder is 3kg, titania powder is 2kg, zinc silicate is 4kg, magnesium bicarbonate is 2kg again, high-speed stirred is carried out again with paddle, speed of agitator is 400rpm, till stirring; (4) finishing agent after stirring is cooled naturally, obtain antibacterial finishing agent.
Embodiment 3
(1) water temperature in finishing agent reactor heating jacket is adjusted to 62 DEG C; (2) in question response still heating jacket after water temperature stability, in reactor, drop into water is 265kg, and stir with paddle, speed of agitator is 200rpm, adds that fatty alcohol-polyoxyethylene ether carboxylic acid sodium is 9kg, diethylene glycol (DEG) is 4kg during stirring, stirs; (3) in reactor, add that 400 object Dicalcium Phosphate are 5kg, diatomite powder is 2kg, titania powder is 1kg, zinc silicate is 5kg, magnesium bicarbonate is 3kg again, high-speed stirred is carried out again with paddle, speed of agitator is 400rpm, till stirring; (4) finishing agent after stirring is cooled naturally, obtain antibacterial finishing agent.
Get textile sheet, soak 2h with the finishing agent of embodiment 1, embodiment 2, embodiment 3, naturally dry after soaking.Measure the bacteriostasis rate of the sheet after arranging.Bacterial classification is Escherichia coli and staphylococcus aureus, and bioassay standard is FZ/T73023-2006, and test result is as follows.
| Embodiment 1 | Embodiment 2 | Embodiment 3 | |
| Escherichia coli inhibiting rate | 77% | 78% | 74% |
| Staphylococcus aureus inhibiting rate | 87% | 81% | 85% |
After arrangement, the bacteriostasis rate of sheet is higher, can suppress growing and breeding of Escherichia coli and staphylococcus aureus significantly, has the sanitation and hygiene utilizing and keep sheet.
Claims (4)
1. an antibacterial sheet finishing agent, is characterized in that antibacterial sheet finishing agent is made up of according to weight ratio following composition: Dicalcium Phosphate is 3 ~ 7 parts, diatomite powder is 2 ~ 3 parts, titania powder is 1 ~ 2 part, zinc silicate is 3 ~ 5 parts, fatty alcohol-polyoxyethylene ether carboxylic acid sodium is 6 ~ 9 parts, diethylene glycol (DEG) is 3 ~ 5 parts, magnesium bicarbonate is 2 ~ 4 parts, water is 245 ~ 265 parts;
The preparation method of described a kind of antibacterial sheet finishing agent, preparation method comprises the following steps: water temperature in finishing agent reactor heating jacket is adjusted to 62 DEG C ~ 68 DEG C by (1); (2) in question response still heating jacket after water temperature stability, in reactor, drop into water is 245 ~ 265 parts, and stir with paddle, speed of agitator is 200rpm, adds that fatty alcohol-polyoxyethylene ether carboxylic acid sodium is 6 ~ 9 parts, diethylene glycol (DEG) is 3 ~ 5 parts during stirring, stirs; (3) in reactor, add that Dicalcium Phosphate is 3 ~ 7 parts, diatomite powder is 2 ~ 3 parts, titania powder is 1 ~ 2 part, zinc silicate is 3 ~ 5 parts, magnesium bicarbonate is 2 ~ 4 parts again, high-speed stirred is carried out again with paddle, speed of agitator is 400rpm, till stirring; (4) finishing agent after stirring is cooled naturally, obtain antibacterial finishing agent.
2. a kind of antibacterial sheet finishing agent according to claim 1, is characterized in that described fatty alcohol-polyoxyethylene ether carboxylic acid sodium is 9 parts.
3. the preparation method of a kind of antibacterial sheet finishing agent according to claim 1, is characterized in that described Dicalcium Phosphate order number is 400 orders.
4. the preparation method of a kind of antibacterial sheet finishing agent according to claim 1, is characterized in that described titania powder is 2 parts.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310752903.0A CN103790017B (en) | 2013-12-31 | 2013-12-31 | A kind of antibacterial sheet finishing agent and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310752903.0A CN103790017B (en) | 2013-12-31 | 2013-12-31 | A kind of antibacterial sheet finishing agent and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103790017A CN103790017A (en) | 2014-05-14 |
| CN103790017B true CN103790017B (en) | 2015-12-30 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201310752903.0A Expired - Fee Related CN103790017B (en) | 2013-12-31 | 2013-12-31 | A kind of antibacterial sheet finishing agent and preparation method thereof |
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Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104264482B (en) * | 2014-09-26 | 2016-11-30 | 枝江大江纺织有限责任公司 | A kind of crease-resistant nursing agent of antibacterial fabric and preparation method thereof |
| CN104328657B (en) * | 2014-10-20 | 2016-08-31 | 苏州庄爵服饰有限公司 | Antibiotic finishing method for clothes |
| CN105369629A (en) * | 2015-12-22 | 2016-03-02 | 常熟市博凡针纺织有限公司 | Dyeing and finishing process for double-sided plush |
| CN107938355A (en) * | 2017-11-30 | 2018-04-20 | 英泰时尚服饰（苏州）有限公司 | A kind of preparation method of antibacterial soft type sheet finishing agent |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1155750C (en) * | 1999-07-20 | 2004-06-30 | 王景毅 | Health-care multi-element fabric and its preparing process |
| CN1751577A (en) * | 2004-09-24 | 2006-03-29 | 深圳市清华源兴生物医药科技有限公司 | Composite sterilizing agent contg. silver and zinc, prepn. method and application thereof |
| CN102094319A (en) * | 2009-12-11 | 2011-06-15 | 国家纳米技术与工程研究院 | Antibacterial agent for textiles and preparation and application thereof |
| CN102094323A (en) * | 2009-12-11 | 2011-06-15 | 国家纳米技术与工程研究院 | Composite antibacterial textile finishing agent and application thereof |
| CN102535176A (en) * | 2010-12-27 | 2012-07-04 | 国家纳米技术与工程研究院 | Moisture-absorbing and quick-drying antibacterial composite finishing agent, preparation method and use method thereof |
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| CN103790017A (en) | 2014-05-14 |
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| SE01 | Entry into force of request for substantive examination | ||
| CB03 | Change of inventor or designer information |
Inventor after: Xue Xincai Inventor after: Chen Guoqing Inventor after: Lei Caihong Inventor before: Zhang Dexuan |
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| COR | Change of bibliographic data | ||
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| TR01 | Transfer of patent right |
Effective date of registration: 20191231 Address after: 224300 group 1, xintanzi neighborhood committee, Xintan Town, Sheyang County, Yancheng City, Jiangsu Province Patentee after: YANCHENG RUIJIA TEXTILE FABRIC Co.,Ltd. Address before: 7 groups of friendship village Songling town of Wujiang District of Suzhou City, Jiangsu province 215200 split eight community Patentee before: SUZHOU XUANDE TEXTILE SCIENCE & TECHNOLOGY Co.,Ltd. |
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| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20151230 |