CN104212342A - Heat insulation and corrosion prevention coating and preparation method thereof - Google Patents
Heat insulation and corrosion prevention coating and preparation method thereof Download PDFInfo
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- CN104212342A CN104212342A CN201410478245.5A CN201410478245A CN104212342A CN 104212342 A CN104212342 A CN 104212342A CN 201410478245 A CN201410478245 A CN 201410478245A CN 104212342 A CN104212342 A CN 104212342A
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Abstract
The invention discloses a heat insulation and corrosion prevention coating. The heat insulation and corrosion prevention coating comprises the following components in percentage by mass: 35-45% of epoxy-modified organic silicon resin, 6-8% of hollow microspheres, 12-18% of composite flame retardant, 14-18% of hydrotalcite, 10-12% of titanium dioxide, 2-5% of toughener, 1-3% of defoamer and 3-5% of drier. The invention further discloses a preparation method of the heat insulation and corrosion prevention coating. The product disclosed by the invention has excellent weather resistance, aging resistance, radiation resistance, wear resistance, impact resistance, resistance to high temperature and low temperature, stable electric conductivity and strong adhesion; the resistivity can meet the anti-static requirements and further ensure the long service life of the coating; simultaneously, the product is efficient, convenient and simple to construct, and can really realize self-curing of the inorganic coating at normal temperature and realize excellent resistance to salt fog and aging resistance; the coating has self-repair property, local scratches caused by external force can be still protected, the coating can not be damaged by cutting or welding, and the welding quality is not affected by welding with the coating.
Description
Technical field
The invention belongs to chemical field, relate to a kind of protective system, specifically a kind of heat-insulating anti-corrosive coating and preparation method thereof.
Background technology
Protective system has become the important fresh combatants of paint field, and protective system plays increasing effect, and development prospect is considerable.But traditional product is improved perfect gradually, new product constantly researches and develops appearance, adapt to new standard and requirement in anticorrosion market and environmental regulation development, still need proactive, Continuous Innovation.Analyze according to expert personage: protective system price is obviously taken advantage of a favourable situation in rising now, and this is to marine finish, and ocean exploitation is relevant.Country was strengthening dynamics of investment to the ocean of the earth 7/10ths always in recent years, and wherein protective system is exactly a projecting point in this part.
Chemical pollution and neurotoxic injury, solvent based coating products itself has certain chemical hazard.In the work of Xu's dress, it should be noted that solvent in coating, thinner cause air pollution on human to have harm; Fire, explosion hazard, solvent based coating, and the thinner etc. used in painting operation are inflammable and explosive material mostly, Gu this painting operation itself also exists the hidden danger of fire and blast.Cause fire and the possible reason of blast to have during electrostatic coating and do not observe working specification, easily produce discharge spark; Useless paint, the keeping such as the useless rag of coating cloud, coating material and solvent is not good at, and is deposited in and easily produces spontaneous combustion together and light; Electric installation is selected or improper use, or does not have on-call maintenance after infringement, and anti-hazard classification is inadequate; Thunderstorm season lightning hazards.
Summary of the invention
Technical problem to be solved by this invention is, overcomes the shortcoming of prior art, provides a kind of heat-insulating anti-corrosive coating and preparation method thereof, product of the present invention has remarkable weathering resistance, anti-aging, radioprotective, wear-resisting, shock-resistant, high temperature resistant, low temperature, stable conductivity, strong adhesion; Its resistivity can meet anti-electrostatic requirement, can ensure again the long lifetime of coating.
In order to solve above technical problem, the invention provides a kind of heat-insulating anti-corrosive coating, the component of its each composition forms by following mass percent proportioning:
Epoxy modified silicone resin: 35-45%
Tiny balloon: 6-8%
Composite flame-retardant agent: 12-18%
Hydrotalcite: 14-18%
Titanium dioxide: 10-12%
Toughner: 2-5%
Defoamer: 1-3%
Siccative: 3-5%.
The technical scheme that the present invention limits further is:
Tiny balloon is SiO 2 hollow microsphere, particle size range 120-150 micron; Composite flame-retardant agent is antimonous oxide, magnesium hydroxide, aluminium hydroxide, primary ammonium phosphate, primary ammonium phosphate, and its mass ratio is 2:1:1:1:1; The particle size range 100-300 order of hydrotalcite and titanium dioxide; Toughner is the one of epoxy resin or resol; Defoamer is silicone oil; Siccative is dibutyl tin laurate.
Further,
A kind of preparation method of heat-insulating anti-corrosive coating is also provided, comprises following concrete steps:
Step (1): by epoxy modified silicone resin, toughner, defoamer, siccative is put in dispersion cylinder respectively, and turn on agitator slowly stirs, and stirring velocity is that 240-280 turns/min, stirs 25-29 minute, to homogeneous transparent, for subsequent use;
Step (2): the homogeneous transparent material obtained in step (2) is added tiny balloon, composite flame-retardant agent under whipped state, adjusting rotary speed is that 550-570 turns/min, and churning time is 33-35 minute, controls dispersion cylinder temperature≤35 DEG C;
Step (3): obtain adding hydrotalcite in mixture, titanium dioxide by step (3), stir while adding equally, adjusting rotary speed is that 900-940 turns/min, stirs and examines viscosimetric≤80s after one hour, Gu containing amount≤68%, obtain finished product.
A kind of preparation method of heat-insulating anti-corrosive coating is also provided, comprises following concrete steps:
Step (1): by epoxy modified silicone resin, toughner, defoamer, siccative is put in dispersion cylinder respectively, and turn on agitator slowly stirs, and stirring velocity is 240 turns/min, stirs 29 minutes, to homogeneous transparent, for subsequent use;
Step (2): the homogeneous transparent material obtained in step (2) is added tiny balloon, composite flame-retardant agent under whipped state, adjusting rotary speed is 550 turns/min, and churning time is 35 minutes, controls dispersion cylinder temperature≤35 DEG C;
Step (3): obtain adding hydrotalcite in mixture, titanium dioxide by step (3), stir while adding equally, adjusting rotary speed is 900 turns/min, stirs and examines viscosimetric≤80s after one hour, Gu containing amount≤68%, obtain finished product.
A kind of preparation method of heat-insulating anti-corrosive coating is also provided, comprises following concrete steps:
Step (1): by epoxy modified silicone resin, toughner, defoamer, siccative is put in dispersion cylinder respectively, and turn on agitator slowly stirs, and stirring velocity is 280 turns/min, stirs 25 minutes, to homogeneous transparent, for subsequent use;
Step (2): the homogeneous transparent material obtained in step (2) is added tiny balloon, composite flame-retardant agent under whipped state, adjusting rotary speed is 570 turns/min, and churning time is 33 minutes, controls dispersion cylinder temperature≤35 DEG C;
Step (3): obtain adding hydrotalcite in mixture, titanium dioxide by step (3), stir while adding equally, adjusting rotary speed is 940 turns/min, stirs and examines viscosimetric≤80s after one hour, Gu containing amount≤68%, obtain finished product.
A kind of preparation method of heat-insulating anti-corrosive coating is also provided, comprises following concrete steps:
Step (1): by epoxy modified silicone resin, toughner, defoamer, siccative is put in dispersion cylinder respectively, and turn on agitator slowly stirs, and stirring velocity is 260 turns/min, stirs 27 minutes, to homogeneous transparent, for subsequent use;
Step (2): the homogeneous transparent material obtained in step (2) is added tiny balloon, composite flame-retardant agent under whipped state, adjusting rotary speed is 560 turns/min, and churning time is 34 minutes, controls dispersion cylinder temperature≤35 DEG C;
Step (3): obtain adding hydrotalcite in mixture, titanium dioxide by step (3), stir while adding equally, adjusting rotary speed is 920 turns/min, stirs and examines viscosimetric≤80s after one hour, Gu containing amount≤68%, obtain finished product.
The invention has the beneficial effects as follows:
There is remarkable weathering resistance, anti-aging, radioprotective, wear-resisting, shock-resistant, high temperature resistant, low temperature, stable conductivity, strong adhesion; Its resistivity can meet anti-electrostatic requirement, can ensure again the long lifetime of coating; Simultaneously efficient convenient: easy construction, really realizes the normal temperature self cure of inorganic paint, can realize excellent salt fog resistance, ageing-resistant; Coating has self-repair, and the local cut that external force causes still can be protected, and coating is not cut and welding damage, and band coating welding does not affect welding quality.
Embodiment
embodiment 1
The present embodiment provides a kind of heat-insulating anti-corrosive coating, and the component of its each composition forms by following mass percent proportioning:
Epoxy modified silicone resin: 35%
Tiny balloon: 8%
Composite flame-retardant agent: 18%
Hydrotalcite: 18%
Titanium dioxide: 12%
Toughner: 5%
Defoamer: 1%
Siccative: 3%.
Wherein, tiny balloon is SiO 2 hollow microsphere, particle size range 120 microns; Composite flame-retardant agent is antimonous oxide, magnesium hydroxide, aluminium hydroxide, primary ammonium phosphate, primary ammonium phosphate, and its mass ratio is 2:1:1:1:1; Particle size range 100 order of hydrotalcite and titanium dioxide; Toughner is epoxy resin; Defoamer is silicone oil; Siccative is dibutyl tin laurate.
The present embodiment also provides a kind of preparation method of heat-insulating anti-corrosive coating, comprises following concrete steps:
Step (1): by epoxy modified silicone resin, toughner, defoamer, siccative is put in dispersion cylinder respectively, and turn on agitator slowly stirs, and stirring velocity is 240 turns/min, stirs 29 minutes, to homogeneous transparent, for subsequent use;
Step (2): the homogeneous transparent material obtained in step (2) is added tiny balloon, composite flame-retardant agent under whipped state, adjusting rotary speed is 550 turns/min, and churning time is 35 minutes, controls dispersion cylinder temperature≤35 DEG C;
Step (3): obtain adding hydrotalcite in mixture, titanium dioxide by step (3), stir while adding equally, adjusting rotary speed is 900 turns/min, stirs and examines viscosimetric≤80s after one hour, Gu containing amount≤68%, obtain finished product.
Be coated in by above-mentioned gained finished product on 4 pieces of test plate (panel)s, film thickness, at 300um-400um, after paint film maintains 7 days, carries out performance test to it.
Wherein will directly carry out performance test by one piece of test plate (panel), result is as follows:
End properties data obtained by table 1 embodiment 1
| Test performance | Project | Unit | Numerical value/effect |
| Mechanical property | Sticking power | Mpa | 6.2 |
| Flexility | Elongation | % | 3.3 |
Other three pieces of test plate (panel)s are placed on respectively in the different mixing acid of three kinds of concentration, three kinds of acid concentrations are respectively nitration mixture 80%+ water 20%, nitration mixture 60%+ water 40%, nitration mixture 40%+ water 60%, described nitration mixture by 50% sulfuric acid, 30% hydrochloric acid, 15% nitric acid, four kinds of 5% hydrofluoric acid mix, through the observation of 30d, there is about about 10, bubble in test plate (panel) surface.Taken out by test plate (panel) after immersion and carry out performance test to it, result is as follows:
Performance data after the pickling of finished product obtained by table 2 embodiment 1
| Test performance | Project | Unit | Numerical value/effect |
| Mechanical property | Sticking power | Mpa | 4.1 |
| Flexility | Elongation | % | 1.8 |
embodiment 2
The present embodiment provides a kind of heat-insulating anti-corrosive coating, and the component of its each composition forms by following mass percent proportioning:
Epoxy modified silicone resin: 45%
Tiny balloon: 6%
Composite flame-retardant agent: 14%
Hydrotalcite: 15%
Titanium dioxide: 10%
Toughner: 2%
Defoamer: 3%
Siccative: 5%.
Wherein, tiny balloon is SiO 2 hollow microsphere, particle size range 150 microns; Composite flame-retardant agent is antimonous oxide, magnesium hydroxide, aluminium hydroxide, primary ammonium phosphate, primary ammonium phosphate, and its mass ratio is 2:1:1:1:1; Particle size range 300 order of hydrotalcite and titanium dioxide; Toughner is resol; Defoamer is silicone oil; Siccative is dibutyl tin laurate.
A kind of preparation method of heat-insulating anti-corrosive coating is also provided, comprises following concrete steps:
Step (1): by epoxy modified silicone resin, toughner, defoamer, siccative is put in dispersion cylinder respectively, and turn on agitator slowly stirs, and stirring velocity is 280 turns/min, stirs 25 minutes, to homogeneous transparent, for subsequent use;
Step (2): the homogeneous transparent material obtained in step (2) is added tiny balloon, composite flame-retardant agent under whipped state, adjusting rotary speed is 570 turns/min, and churning time is 33 minutes, controls dispersion cylinder temperature≤35 DEG C;
Step (3): obtain adding hydrotalcite in mixture, titanium dioxide by step (3), stir while adding equally, adjusting rotary speed is 940 turns/min, stirs and examines viscosimetric≤80s after one hour, Gu containing amount≤68%, obtain finished product.
Be coated in by above-mentioned gained finished product on 4 pieces of test plate (panel)s, film thickness, at 300um-400um, after paint film maintains 7 days, carries out performance test to it.
Wherein will directly carry out performance test by one piece of test plate (panel), result is as follows:
End properties data obtained by table 3 embodiment 2
| Test performance | Project | Unit | Numerical value/effect |
| Mechanical property | Sticking power | Mpa | 4.9 |
| Flexility | Elongation | % | 2.5 |
Other three pieces of test plate (panel)s are placed on respectively in the different mixing acid of three kinds of concentration, three kinds of acid concentrations are respectively nitration mixture 80%+ water 20%, nitration mixture 60%+ water 40%, nitration mixture 40%+ water 60%, described nitration mixture by 50% sulfuric acid, 30% hydrochloric acid, 15% nitric acid, four kinds of 5% hydrofluoric acid mix, through the observation of 30d, there is about about 10, bubble in test plate (panel) surface.Taken out by test plate (panel) after immersion and carry out performance test to it, result is as follows:
Performance data after the pickling of finished product obtained by table 4 embodiment 2
| Test performance | Project | Unit | Numerical value/effect |
| Mechanical property | Sticking power | Mpa | 3.0 |
| Flexility | Elongation | % | 1.3 |
embodiment 3
The present embodiment provides a kind of heat-insulating anti-corrosive coating, and the component of its each composition forms by following mass percent proportioning:
Epoxy modified silicone resin: 40%
Tiny balloon: 5%
Composite flame-retardant agent: 12%
Hydrotalcite: 18%
Titanium dioxide: 12%
Toughner: 5%
Defoamer: 3%
Siccative: 5%.
Wherein, tiny balloon is SiO 2 hollow microsphere, particle size range 135 microns; Composite flame-retardant agent is antimonous oxide, magnesium hydroxide, aluminium hydroxide, primary ammonium phosphate, primary ammonium phosphate, and its mass ratio is 2:1:1:1:1; Particle size range 200 order of hydrotalcite and titanium dioxide; Toughner is epoxy resin; Defoamer is silicone oil; Siccative is dibutyl tin laurate.
A kind of preparation method of heat-insulating anti-corrosive coating is also provided, comprises following concrete steps:
Step (1): by epoxy modified silicone resin, toughner, defoamer, siccative is put in dispersion cylinder respectively, and turn on agitator slowly stirs, and stirring velocity is 260 turns/min, stirs 27 minutes, to homogeneous transparent, for subsequent use;
Step (2): the homogeneous transparent material obtained in step (2) is added tiny balloon, composite flame-retardant agent under whipped state, adjusting rotary speed is 560 turns/min, and churning time is 34 minutes, controls dispersion cylinder temperature≤35 DEG C;
Step (3): obtain adding hydrotalcite in mixture, titanium dioxide by step (3), stir while adding equally, adjusting rotary speed is 920 turns/min, stirs and examines viscosimetric≤80s after one hour, Gu containing amount≤68%, obtain finished product.
Be coated in by above-mentioned gained finished product on 4 pieces of test plate (panel)s, film thickness, at 300um-400um, after paint film maintains 7 days, carries out performance test to it.
Wherein will directly carry out performance test by one piece of test plate (panel), result is as follows:
End properties data obtained by table 5 embodiment 3
| Test performance | Project | Unit | Numerical value/effect |
| Mechanical property | Sticking power | Mpa | 5.8 |
| Flexility | Elongation | % | 4.7 |
Other three pieces of test plate (panel)s are placed on respectively in the different mixing acid of three kinds of concentration, three kinds of acid concentrations are respectively nitration mixture 80%+ water 20%, nitration mixture 60%+ water 40%, nitration mixture 40%+ water 60%, described nitration mixture by 50% sulfuric acid, 30% hydrochloric acid, 15% nitric acid, four kinds of 5% hydrofluoric acid mix, through the observation of 30d, there is about about 10, bubble in test plate (panel) surface.Taken out by test plate (panel) after immersion and carry out performance test to it, result is as follows:
Performance data after the pickling of finished product obtained by table 6 embodiment 3
| Test performance | Project | Unit | Numerical value/effect |
| Mechanical property | Sticking power | Mpa | 2.6 |
| Flexility | Elongation | % | 2.1 |
Above embodiment is only and technological thought of the present invention is described, can not limit protection scope of the present invention with this, and every technological thought proposed according to the present invention, any change that technical scheme basis is done, all falls within scope.
Claims (9)
1. a heat-insulating anti-corrosive coating, the component of its each composition forms by following mass percent proportioning:
Epoxy modified silicone resin: 35-45%
Tiny balloon: 6-8%
Composite flame-retardant agent: 12-18%
Hydrotalcite: 14-18%
Titanium dioxide: 10-12%
Toughner: 2-5%
Defoamer: 1-3%
Siccative: 3-5%.
2. heat-insulating anti-corrosive coating according to claim 1, is characterized in that, described tiny balloon is SiO 2 hollow microsphere, particle size range 120-150 micron.
3. heat-insulating anti-corrosive coating according to claim 1, is characterized in that, described composite flame-retardant agent is antimonous oxide, magnesium hydroxide, aluminium hydroxide, primary ammonium phosphate, primary ammonium phosphate, and its mass ratio is 2:1:1:1:1.
4. heat-insulating anti-corrosive coating according to claim 1, is characterized in that, the particle size range 100-300 order of described hydrotalcite and titanium dioxide.
5. heat-insulating anti-corrosive coating according to claim 1, is characterized in that, described toughner is the one of epoxy resin or resol; Defoamer is silicone oil; Siccative is dibutyl tin laurate.
6. a preparation method for heat-insulating anti-corrosive coating, is characterized in that, comprises following concrete steps:
Step (1): by epoxy modified silicone resin, toughner, defoamer, siccative is put in dispersion cylinder respectively, and turn on agitator slowly stirs, and stirring velocity is that 240-280 turns/min, stirs 25-29 minute, to homogeneous transparent, for subsequent use;
Step (2): the homogeneous transparent material obtained in step (2) is added tiny balloon, composite flame-retardant agent under whipped state, adjusting rotary speed is that 550-570 turns/min, and churning time is 33-35 minute, controls dispersion cylinder temperature≤35 DEG C;
Step (3): obtain adding hydrotalcite in mixture, titanium dioxide by step (3), stir while adding equally, adjusting rotary speed is that 900-940 turns/min, stirs and examines viscosimetric≤80s after one hour, Gu containing amount≤68%, obtain finished product.
7. the preparation method of heat-insulating anti-corrosive coating according to claim 6, is characterized in that, comprises following concrete steps:
Step (1): by epoxy modified silicone resin, toughner, defoamer, siccative is put in dispersion cylinder respectively, and turn on agitator slowly stirs, and stirring velocity is 240 turns/min, stirs 29 minutes, to homogeneous transparent, for subsequent use;
Step (2): the homogeneous transparent material obtained in step (2) is added tiny balloon, composite flame-retardant agent under whipped state, adjusting rotary speed is 550 turns/min, and churning time is 35 minutes, controls dispersion cylinder temperature≤35 DEG C;
Step (3): obtain adding hydrotalcite in mixture, titanium dioxide by step (3), stir while adding equally, adjusting rotary speed is 900 turns/min, stirs and examines viscosimetric≤80s after one hour, Gu containing amount≤68%, obtain finished product.
8. the preparation method of heat-insulating anti-corrosive coating according to claim 6, is characterized in that, comprises following concrete steps:
Step (1): by epoxy modified silicone resin, toughner, defoamer, siccative is put in dispersion cylinder respectively, and turn on agitator slowly stirs, and stirring velocity is 280 turns/min, stirs 25 minutes, to homogeneous transparent, for subsequent use;
Step (2): the homogeneous transparent material obtained in step (2) is added tiny balloon, composite flame-retardant agent under whipped state, adjusting rotary speed is 570 turns/min, and churning time is 33 minutes, controls dispersion cylinder temperature≤35 DEG C;
Step (3): obtain adding hydrotalcite in mixture, titanium dioxide by step (3), stir while adding equally, adjusting rotary speed is 940 turns/min, stirs and examines viscosimetric≤80s after one hour, Gu containing amount≤68%, obtain finished product.
9. the preparation method of heat-insulating anti-corrosive coating according to claim 6, is characterized in that, comprises following concrete steps:
Step (1): by epoxy modified silicone resin, toughner, defoamer, siccative is put in dispersion cylinder respectively, and turn on agitator slowly stirs, and stirring velocity is 260 turns/min, stirs 27 minutes, to homogeneous transparent, for subsequent use;
Step (2): the homogeneous transparent material obtained in step (2) is added tiny balloon, composite flame-retardant agent under whipped state, adjusting rotary speed is 560 turns/min, and churning time is 34 minutes, controls dispersion cylinder temperature≤35 DEG C;
Step (3): obtain adding hydrotalcite in mixture, titanium dioxide by step (3), stir while adding equally, adjusting rotary speed is 920 turns/min, stirs and examines viscosimetric≤80s after one hour, Gu containing amount≤68%, obtain finished product.
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| CN104893486A (en) * | 2015-05-21 | 2015-09-09 | 芜湖蒲草电子商务有限公司 | Antistatic and heat-resistant coating for corrugated carton and preparation method of antistatic and heat-resistant coating |
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| CN105694632A (en) * | 2016-04-11 | 2016-06-22 | 浙江新乐造船有限公司 | Fireproof coating for bulkheads of ships, method for preparing fireproof coating and application thereof |
| CN111793437A (en) * | 2020-08-04 | 2020-10-20 | 营口嘉宸防火科技有限公司 | Special coating with corrosion resistance, fire resistance, heat insulation and heat preservation functions and preparation method thereof |
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Cited By (5)
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| CN104893486A (en) * | 2015-05-21 | 2015-09-09 | 芜湖蒲草电子商务有限公司 | Antistatic and heat-resistant coating for corrugated carton and preparation method of antistatic and heat-resistant coating |
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| CN105694632A (en) * | 2016-04-11 | 2016-06-22 | 浙江新乐造船有限公司 | Fireproof coating for bulkheads of ships, method for preparing fireproof coating and application thereof |
| CN105694632B (en) * | 2016-04-11 | 2017-10-13 | 浙江新乐造船有限公司 | It is a kind of for fire resistant coating of ship bulkhead and its preparation method and application |
| CN111793437A (en) * | 2020-08-04 | 2020-10-20 | 营口嘉宸防火科技有限公司 | Special coating with corrosion resistance, fire resistance, heat insulation and heat preservation functions and preparation method thereof |
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Application publication date: 20141217 |
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