CN105176166A - Water-based paint with flame retarding function and preparation method of water-based paint - Google Patents
Water-based paint with flame retarding function and preparation method of water-based paint Download PDFInfo
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- CN105176166A CN105176166A CN201510682201.9A CN201510682201A CN105176166A CN 105176166 A CN105176166 A CN 105176166A CN 201510682201 A CN201510682201 A CN 201510682201A CN 105176166 A CN105176166 A CN 105176166A
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Abstract
The invention discloses water-based paint with a flame retarding function and a preparation method of the water-based paint. The water-based paint with the flame retarding function is prepared from the following raw materials in parts by weight: 70 to 75 parts of epoxy-modified organic silicon resin, 40 to 43 parts of hydroxyl bromic acid resin, 12 to 15 parts of decabromodiphenyl ethane, 22 to 25 parts of dodecyl acrylate, 2 to 4 parts of antimonous oxide, 7 to 9 parts of trichlorine propyl phosphate, 2 to 4 parts of forsterite, 60 to 65 parts of deionized water, 5 to 7 parts of fluorous rubber, 7 to 9 parts of crylic acid, 7 to 9 parts of titanium dioxide and 15 to 18 parts of assistant. The water-based paint disclosed by the invention is not only high in strength, anti-corrosion ability and anti-oxidation ability, but also has flame retardant property, the friction-resisting performance on the surface of the water-based paint is greatly increased, the friction of the water-based paint is reduced, the problems of bubbling, fracturing, whitening or even delaminating and the like cannot be caused during a long-term using process of the water-based paint, and the water-based paint can be used under a severe environment and has a wide using range and an environment protection effect.
Description
Technical field
The present invention relates to a kind of coating, specifically a kind of water-borne coatings with anti-flaming function and preparation method thereof.
Background technology
At present, along with the development of society, water-borne coatings can be widely used in the industries such as electrical equipment, metallurgy, oil, aviation field, chemical industry, medicine, food various in, because equipment is in the process of life-time service, and at high temperature or the place caught fire, coating burning-point is low, easily causes fire or aggravates spreading of the intensity of a fire, and giving out obnoxious flavour, bring about great losses, and at high temperature, easily come off, cause the inner rapid oxidation of coating, damage its structure, reduce its work-ing life, damage equipment, cause huge loss.
Summary of the invention
Technical problem to be solved by this invention is, for the shortcoming of above prior art, a kind of water-borne coatings with anti-flaming function and preparation method thereof is proposed, this water-borne coatings not only intensity is high, resistance to corrosion and resistance of oxidation extremely strong, also there is flame retardant properties, and the rub resistance ability on its surface improves greatly, reduce its wearing and tearing, this water-borne coatings life-time service can not bubble, be full of cracks, whiten the problems such as even delamination, and can use under rugged environment, use range is wide, and there is environment protecting, reduce costs, increase its work-ing life, and preparation method is provided, method is simple, cost is low, production efficiency is high.
In order to solve the problems of the technologies described above, technical scheme of the present invention is achieved in the following ways: a kind of water-borne coatings with anti-flaming function, following raw material counted by weight by the water-borne coatings with anti-flaming function: epoxy modified silicone resin: 70-75 part, hydroxyl third bromic acid resin: 40-43 part, TDE: 12-15 part, dodecyl acrylate: 22-25 part, antimonous oxide: 2-4 part, trichlorine propyl phosphate: 7-9 part, forsterite: 2-4 part, deionized water: 60-65 part, viton: 5-7 part, vinylformic acid: 7-9 part, titanium dioxide: 7-9 part, auxiliary agent: 15-18 part,
The component of described auxiliary agent is counted by weight: zircon: 17-19 part, talcum powder: 13-15 part, deionized water: 10-15 part, kaolin: 12-14 part, Graphite Powder 99: 5-8 part;
The preparation method of described auxiliary agent is: by zircon and talcum powder co-grinding, cross 120 mesh sieves, obtain powders A, then kaolin and Graphite Powder 99 co-grinding, cross 40 mesh sieves, obtain powder B, powders A and powder B are uniformly mixed with the ratio of 3:2, stir 5-8 minute, then add deionized water and stirring reaction 15-20 minute, then filter, dry, pulverize, cross 120 mesh sieves, under nitrogen protection, after calcining 2-3 hour at being heated to 730-750 DEG C, air cooling, to room temperature, is then pulverized, cross 100 mesh sieves, can auxiliary agent be obtained; And use following method to obtain water-borne coatings that this has anti-flaming function:
Step (1): by raw material: epoxy modified silicone resin, hydroxyl third bromic acid resin, TDE are first put into stirring tank and mixed, temperature in control stirring tank is at 64-68 DEG C, setting stirring velocity 675-780r/min, churning time 40-45min, then putting into dodecyl acrylate successively, antimonous oxide, trichlorine propyl phosphate, forsterite mix, stirring velocity is 820-830r/min, keeps 40-45min;
Step (2): then by raw material: deionized water, viton, vinylformic acid, titanium dioxide, auxiliary agent are put into stirring tank and mixed, setting stirring velocity is 850-860r/min, churning time is 60-90min, modulation water-borne coatings pH value is 8-9, has the water-borne coatings of anti-flaming function described in can obtaining.
The technical scheme that the present invention limits further is:
The aforesaid water-borne coatings with anti-flaming function, following raw material counted by weight by the water-borne coatings with anti-flaming function: epoxy modified silicone resin: 70 parts, hydroxyl third bromic acid resin: 40 parts, TDE: 12 parts, dodecyl acrylate: 22 parts, antimonous oxide: 2 parts, trichlorine propyl phosphate: 7 parts, forsterite: 2 parts, deionized water: 60 parts, viton: 5 parts, vinylformic acid: 7 parts, titanium dioxide: 7 parts, auxiliary agent: 15 parts;
The component of described auxiliary agent is counted by weight: zircon: 17 parts, talcum powder: 13 parts, deionized water: 10 parts, kaolin: 12 parts, Graphite Powder 99: 5 parts;
The preparation method of described auxiliary agent is: by zircon and talcum powder co-grinding; cross 120 mesh sieves; obtain powders A, then kaolin and Graphite Powder 99 co-grinding, cross 40 mesh sieves; obtain powder B; powders A and powder B are uniformly mixed with the ratio of 3:2, stir 5 minutes, then add deionized water and stirring and react 15 minutes; then filter; dry, pulverize, cross 120 mesh sieves; under nitrogen protection; calcine after 2 hours at being heated to 730 DEG C, air cooling, to room temperature, is then pulverized; cross 100 mesh sieves, can auxiliary agent be obtained.
The aforesaid water-borne coatings with anti-flaming function, following raw material counted by weight by the water-borne coatings with anti-flaming function: epoxy modified silicone resin: 75 parts, hydroxyl third bromic acid resin: 43 parts, TDE: 15 parts, dodecyl acrylate: 25 parts, antimonous oxide: 4 parts, trichlorine propyl phosphate: 9 parts, forsterite: 4 parts, deionized water: 65 parts, viton: 7 parts, vinylformic acid: 9 parts, titanium dioxide: 9 parts, auxiliary agent: 18 parts;
The component of described auxiliary agent is counted by weight: zircon: 19 parts, talcum powder: 15 parts, deionized water: 15 parts, kaolin: 14 parts, Graphite Powder 99: 8 parts;
The preparation method of described auxiliary agent is: by zircon and talcum powder co-grinding; cross 120 mesh sieves; obtain powders A, then kaolin and Graphite Powder 99 co-grinding, cross 40 mesh sieves; obtain powder B; powders A and powder B are uniformly mixed with the ratio of 3:2, stir 8 minutes, then add deionized water and stirring and react 20 minutes; then filter; dry, pulverize, cross 120 mesh sieves; under nitrogen protection; calcine after 3 hours at being heated to 750 DEG C, air cooling, to room temperature, is then pulverized; cross 100 mesh sieves, can auxiliary agent be obtained.
The aforesaid water-borne coatings with anti-flaming function, following raw material counted by weight by the water-borne coatings with anti-flaming function: epoxy modified silicone resin: 72 parts, hydroxyl third bromic acid resin: 42 parts, TDE: 13 parts, dodecyl acrylate: 24 parts, antimonous oxide: 3 parts, trichlorine propyl phosphate: 8 parts, forsterite: 3 parts, deionized water: 62 parts, viton: 6 parts, vinylformic acid: 8 parts, titanium dioxide: 8 parts, auxiliary agent: 17 parts;
The component of described auxiliary agent is counted by weight: zircon: 18 parts, talcum powder: 14 parts, deionized water: 13 parts, kaolin: 13 parts, Graphite Powder 99: 7 parts;
The preparation method of described auxiliary agent is: by zircon and talcum powder co-grinding; cross 120 mesh sieves; obtain powders A, then kaolin and Graphite Powder 99 co-grinding, cross 40 mesh sieves; obtain powder B; powders A and powder B are uniformly mixed with the ratio of 3:2, stir 7 minutes, then add deionized water and stirring and react 18 minutes; then filter; dry, pulverize, cross 120 mesh sieves; under nitrogen protection; calcine after 2 hours at being heated to 740 DEG C, air cooling, to room temperature, is then pulverized; cross 100 mesh sieves, can auxiliary agent be obtained.
The invention has the beneficial effects as follows: this there is the water-borne coatings resistance to corrosion of anti-flaming function and resistance of oxidation extremely strong, also there is flame retardant properties, and the rub resistance ability on its surface improves greatly, reduce its wearing and tearing, increase its work-ing life, and provide preparation method, method is simple, cost is low, and production efficiency is high; Wherein add TDE, antimonous oxide and trichlorine propyl phosphate fire retardant material, the flame retardant properties of water-borne coatings can not only be improved, water-borne coatings can also be made to have self-extinguishing, and weathering resistance, winter hardiness, static resistance etc., improve the over-all properties of water-borne coatings; Security when improving the work-ing life of water-borne coatings and use; This water-borne coatings adhesive property is excellent, and elasticity, flexible resistance and tear strength are high, and oil resistant, heat-resisting, winter hardiness good, good seal performance, long service life.
Embodiment
The present invention is described in further detail below:
embodiment 1
A kind of water-borne coatings with anti-flaming function that the present embodiment provides, following raw material counted by weight by the water-borne coatings with anti-flaming function: epoxy modified silicone resin: 70 parts, hydroxyl third bromic acid resin: 40 parts, TDE: 12 parts, dodecyl acrylate: 22 parts, antimonous oxide: 2 parts, trichlorine propyl phosphate: 7 parts, forsterite: 2 parts, deionized water: 60 parts, viton: 5 parts, vinylformic acid: 7 parts, titanium dioxide: 7 parts, auxiliary agent: 15 parts;
The component of described auxiliary agent is counted by weight: zircon: 17 parts, talcum powder: 13 parts, deionized water: 10 parts, kaolin: 12 parts, Graphite Powder 99: 5 parts;
The preparation method of described auxiliary agent is: by zircon and talcum powder co-grinding, cross 120 mesh sieves, obtain powders A, then kaolin and Graphite Powder 99 co-grinding, cross 40 mesh sieves, obtain powder B, powders A and powder B are uniformly mixed with the ratio of 3:2, stir 5 minutes, then add deionized water and stirring and react 15 minutes, then filter, dry, pulverize, cross 120 mesh sieves, under nitrogen protection, calcine after 2 hours at being heated to 730 DEG C, air cooling, to room temperature, is then pulverized, cross 100 mesh sieves, can auxiliary agent be obtained; And use following method to obtain water-borne coatings that this has anti-flaming function:
Step (1): by raw material: epoxy modified silicone resin, hydroxyl third bromic acid resin, TDE are first put into stirring tank and mixed, temperature in control stirring tank is at 64 DEG C, setting stirring velocity 675r/min, churning time 40min, then putting into dodecyl acrylate successively, antimonous oxide, trichlorine propyl phosphate, forsterite mix, stirring velocity is 820r/min, keeps 40min;
Step (2): then by raw material: deionized water, viton, vinylformic acid, titanium dioxide, auxiliary agent are put into stirring tank and mixed, setting stirring velocity is 850r/min, churning time is 60min, and modulation water-borne coatings pH value is 8, has the water-borne coatings of anti-flaming function described in can obtaining.
embodiment 2
A kind of water-borne coatings with anti-flaming function that the present embodiment provides, following raw material counted by weight by the water-borne coatings with anti-flaming function: epoxy modified silicone resin: 75 parts, hydroxyl third bromic acid resin: 43 parts, TDE: 15 parts, dodecyl acrylate: 25 parts, antimonous oxide: 4 parts, trichlorine propyl phosphate: 9 parts, forsterite: 4 parts, deionized water: 65 parts, viton: 7 parts, vinylformic acid: 9 parts, titanium dioxide: 9 parts, auxiliary agent: 18 parts;
The component of described auxiliary agent is counted by weight: zircon: 19 parts, talcum powder: 15 parts, deionized water: 15 parts, kaolin: 14 parts, Graphite Powder 99: 8 parts;
The preparation method of described auxiliary agent is: by zircon and talcum powder co-grinding, cross 120 mesh sieves, obtain powders A, then kaolin and Graphite Powder 99 co-grinding, cross 40 mesh sieves, obtain powder B, powders A and powder B are uniformly mixed with the ratio of 3:2, stir 8 minutes, then add deionized water and stirring and react 20 minutes, then filter, dry, pulverize, cross 120 mesh sieves, under nitrogen protection, calcine after 3 hours at being heated to 750 DEG C, air cooling, to room temperature, is then pulverized, cross 100 mesh sieves, can auxiliary agent be obtained; And use following method to obtain water-borne coatings that this has anti-flaming function:
Step (1): by raw material: epoxy modified silicone resin, hydroxyl third bromic acid resin, TDE are first put into stirring tank and mixed, temperature in control stirring tank is at 68 DEG C, setting stirring velocity 780r/min, churning time 45min, then putting into dodecyl acrylate successively, antimonous oxide, trichlorine propyl phosphate, forsterite mix, stirring velocity is 830r/min, keeps 45min;
Step (2): then by raw material: deionized water, viton, vinylformic acid, titanium dioxide, auxiliary agent are put into stirring tank and mixed, setting stirring velocity is 860r/min, churning time is 90min, and modulation water-borne coatings pH value is 9, has the water-borne coatings of anti-flaming function described in can obtaining.
embodiment 3
A kind of water-borne coatings with anti-flaming function that the present embodiment provides, following raw material counted by weight by the water-borne coatings with anti-flaming function: epoxy modified silicone resin: 72 parts, hydroxyl third bromic acid resin: 42 parts, TDE: 13 parts, dodecyl acrylate: 24 parts, antimonous oxide: 3 parts, trichlorine propyl phosphate: 8 parts, forsterite: 3 parts, deionized water: 62 parts, viton: 6 parts, vinylformic acid: 8 parts, titanium dioxide: 8 parts, auxiliary agent: 17 parts;
The component of described auxiliary agent is counted by weight: zircon: 18 parts, talcum powder: 14 parts, deionized water: 13 parts, kaolin: 13 parts, Graphite Powder 99: 7 parts;
The preparation method of described auxiliary agent is: by zircon and talcum powder co-grinding, cross 120 mesh sieves, obtain powders A, then kaolin and Graphite Powder 99 co-grinding, cross 40 mesh sieves, obtain powder B, powders A and powder B are uniformly mixed with the ratio of 3:2, stir 7 minutes, then add deionized water and stirring and react 18 minutes, then filter, dry, pulverize, cross 120 mesh sieves, under nitrogen protection, calcine after 2 hours at being heated to 740 DEG C, air cooling, to room temperature, is then pulverized, cross 100 mesh sieves, can auxiliary agent be obtained; And use following method to obtain water-borne coatings that this has anti-flaming function:
Step (1): by raw material: epoxy modified silicone resin, hydroxyl third bromic acid resin, TDE are first put into stirring tank and mixed, temperature in control stirring tank is at 65 DEG C, setting stirring velocity 678r/min, churning time 42min, then putting into dodecyl acrylate successively, antimonous oxide, trichlorine propyl phosphate, forsterite mix, stirring velocity is 825r/min, keeps 42min;
Step (2): then by raw material: deionized water, viton, vinylformic acid, titanium dioxide, auxiliary agent are put into stirring tank and mixed, setting stirring velocity is 855r/min, churning time is 80min, and modulation water-borne coatings pH value is 8, has the water-borne coatings of anti-flaming function described in can obtaining.
Like this by technical scheme of the present invention, this water-borne coatings not only intensity is high, resistance to corrosion and resistance of oxidation extremely strong, also there is flame retardant properties, and the rub resistance ability on its surface improves greatly, reduce its wearing and tearing, this water-borne coatings life-time service can not bubble, chap, whiten the problems such as even delamination, and can use under rugged environment, use range is wide, and there is environment protecting, reduce costs, increase its work-ing life, and preparation method is provided, method is simple, and cost is low, and production efficiency is high.
Above embodiment is only and technological thought of the present invention is described, can not limit protection scope of the present invention with this, and every technological thought proposed according to the present invention, any change that technical scheme basis is done, all falls within scope.
Claims (5)
1. there is a water-borne coatings for anti-flaming function, it is characterized in that: described in there is anti-flaming function water-borne coatings count following raw material by weight: epoxy modified silicone resin: 70-75 part, hydroxyl third bromic acid resin: 40-43 part, TDE: 12-15 part, dodecyl acrylate: 22-25 part, antimonous oxide: 2-4 part, trichlorine propyl phosphate: 7-9 part, forsterite: 2-4 part, deionized water: 60-65 part, viton: 5-7 part, vinylformic acid: 7-9 part, titanium dioxide: 7-9 part, auxiliary agent: 15-18 part;
The component of described auxiliary agent is counted by weight: zircon: 17-19 part, talcum powder: 13-15 part, deionized water: 10-15 part, kaolin: 12-14 part, Graphite Powder 99: 5-8 part;
The preparation method of described auxiliary agent is: by zircon and talcum powder co-grinding; cross 120 mesh sieves; obtain powders A, then kaolin and Graphite Powder 99 co-grinding, cross 40 mesh sieves; obtain powder B; powders A and powder B are uniformly mixed with the ratio of 3:2, stir 5-8 minute, then add deionized water and stirring reaction 15-20 minute; then filter; dry, pulverize, cross 120 mesh sieves; under nitrogen protection; after calcining 2-3 hour at being heated to 730-750 DEG C, air cooling, to room temperature, is then pulverized; cross 100 mesh sieves, can auxiliary agent be obtained.
2. the water-borne coatings with anti-flaming function according to claim 1, is characterized in that: described in there is anti-flaming function water-borne coatings count following raw material by weight: epoxy modified silicone resin: 70 parts, hydroxyl third bromic acid resin: 40 parts, TDE: 12 parts, dodecyl acrylate: 22 parts, antimonous oxide: 2 parts, trichlorine propyl phosphate: 7 parts, forsterite: 2 parts, deionized water: 60 parts, viton: 5 parts, vinylformic acid: 7 parts, titanium dioxide: 7 parts, auxiliary agent: 15 parts;
The component of described auxiliary agent is counted by weight: zircon: 17 parts, talcum powder: 13 parts, deionized water: 10 parts, kaolin: 12 parts, Graphite Powder 99: 5 parts;
The preparation method of described auxiliary agent is: by zircon and talcum powder co-grinding; cross 120 mesh sieves; obtain powders A, then kaolin and Graphite Powder 99 co-grinding, cross 40 mesh sieves; obtain powder B; powders A and powder B are uniformly mixed with the ratio of 3:2, stir 5 minutes, then add deionized water and stirring and react 15 minutes; then filter; dry, pulverize, cross 120 mesh sieves; under nitrogen protection; calcine after 2 hours at being heated to 730 DEG C, air cooling, to room temperature, is then pulverized; cross 100 mesh sieves, can auxiliary agent be obtained.
3. the water-borne coatings with anti-flaming function according to claim 1, is characterized in that: described in there is anti-flaming function water-borne coatings count following raw material by weight: epoxy modified silicone resin: 75 parts, hydroxyl third bromic acid resin: 43 parts, TDE: 15 parts, dodecyl acrylate: 25 parts, antimonous oxide: 4 parts, trichlorine propyl phosphate: 9 parts, forsterite: 4 parts, deionized water: 65 parts, viton: 7 parts, vinylformic acid: 9 parts, titanium dioxide: 9 parts, auxiliary agent: 18 parts;
The component of described auxiliary agent is counted by weight: zircon: 19 parts, talcum powder: 15 parts, deionized water: 15 parts, kaolin: 14 parts, Graphite Powder 99: 8 parts;
The preparation method of described auxiliary agent is: by zircon and talcum powder co-grinding; cross 120 mesh sieves; obtain powders A, then kaolin and Graphite Powder 99 co-grinding, cross 40 mesh sieves; obtain powder B; powders A and powder B are uniformly mixed with the ratio of 3:2, stir 8 minutes, then add deionized water and stirring and react 20 minutes; then filter; dry, pulverize, cross 120 mesh sieves; under nitrogen protection; calcine after 3 hours at being heated to 750 DEG C, air cooling, to room temperature, is then pulverized; cross 100 mesh sieves, can auxiliary agent be obtained.
4. the water-borne coatings with anti-flaming function according to claim 1, is characterized in that: described in there is anti-flaming function water-borne coatings count following raw material by weight: epoxy modified silicone resin: 72 parts, hydroxyl third bromic acid resin: 42 parts, TDE: 13 parts, dodecyl acrylate: 24 parts, antimonous oxide: 3 parts, trichlorine propyl phosphate: 8 parts, forsterite: 3 parts, deionized water: 62 parts, viton: 6 parts, vinylformic acid: 8 parts, titanium dioxide: 8 parts, auxiliary agent: 17 parts;
The component of described auxiliary agent is counted by weight: zircon: 18 parts, talcum powder: 14 parts, deionized water: 13 parts, kaolin: 13 parts, Graphite Powder 99: 7 parts;
The preparation method of described auxiliary agent is: by zircon and talcum powder co-grinding; cross 120 mesh sieves; obtain powders A, then kaolin and Graphite Powder 99 co-grinding, cross 40 mesh sieves; obtain powder B; powders A and powder B are uniformly mixed with the ratio of 3:2, stir 7 minutes, then add deionized water and stirring and react 18 minutes; then filter; dry, pulverize, cross 120 mesh sieves; under nitrogen protection; calcine after 2 hours at being heated to 740 DEG C, air cooling, to room temperature, is then pulverized; cross 100 mesh sieves, can auxiliary agent be obtained.
5. there is a preparation method for the water-borne coatings of anti-flaming function, it is characterized in that: the method is carried out according to the following steps:
Step (1): by raw material: epoxy modified silicone resin, hydroxyl third bromic acid resin, TDE are first put into stirring tank and mixed, temperature in control stirring tank is at 64-68 DEG C, setting stirring velocity 675-780r/min, churning time 40-45min, then putting into dodecyl acrylate successively, antimonous oxide, trichlorine propyl phosphate, forsterite mix, stirring velocity is 820-830r/min, keeps 40-45min;
Step (2): then by raw material: deionized water, viton, vinylformic acid, titanium dioxide, auxiliary agent are put into stirring tank and mixed, setting stirring velocity is 850-860r/min, churning time is 60-90min, modulation water-borne coatings pH value is 8-9, has the water-borne coatings of anti-flaming function described in can obtaining.
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN107556840A (en) * | 2017-09-05 | 2018-01-09 | 绍兴思安阻燃科技有限公司 | A kind of chemical fibre sofa fabric flame retardant |
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CN104592894A (en) * | 2013-10-30 | 2015-05-06 | 烟台纳克环保科技有限公司 | Fireproof paint |
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CN102850881A (en) * | 2012-09-12 | 2013-01-02 | 山东长星集团有限公司 | Environment-friendly fire-retardant paint |
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