CN102134444A - Temperature-resistance thermal-insulation heavy-duty anticorrosion coating - Google Patents
Temperature-resistance thermal-insulation heavy-duty anticorrosion coating Download PDFInfo
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- CN102134444A CN102134444A CN 201110045749 CN201110045749A CN102134444A CN 102134444 A CN102134444 A CN 102134444A CN 201110045749 CN201110045749 CN 201110045749 CN 201110045749 A CN201110045749 A CN 201110045749A CN 102134444 A CN102134444 A CN 102134444A
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- 238000000576 coating method Methods 0.000 title claims abstract description 42
- 239000011248 coating agent Substances 0.000 title claims abstract description 41
- 238000009413 insulation Methods 0.000 title claims abstract description 30
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 21
- 239000004593 Epoxy Substances 0.000 claims abstract description 20
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims abstract description 17
- TZCXTZWJZNENPQ-UHFFFAOYSA-L barium sulfate Chemical compound [Ba+2].[O-]S([O-])(=O)=O TZCXTZWJZNENPQ-UHFFFAOYSA-L 0.000 claims abstract description 17
- 229920001296 polysiloxane Polymers 0.000 claims abstract description 12
- 239000002994 raw material Substances 0.000 claims abstract description 10
- NJLLQSBAHIKGKF-UHFFFAOYSA-N dipotassium dioxido(oxo)titanium Chemical compound [K+].[K+].[O-][Ti]([O-])=O NJLLQSBAHIKGKF-UHFFFAOYSA-N 0.000 claims abstract description 9
- -1 polysiloxane Polymers 0.000 claims abstract description 9
- LRXTYHSAJDENHV-UHFFFAOYSA-H zinc phosphate Chemical compound [Zn+2].[Zn+2].[Zn+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O LRXTYHSAJDENHV-UHFFFAOYSA-H 0.000 claims abstract description 9
- 229910000165 zinc phosphate Inorganic materials 0.000 claims abstract description 9
- 150000001412 amines Chemical class 0.000 claims abstract description 8
- 239000006229 carbon black Substances 0.000 claims abstract description 8
- 239000007783 nanoporous material Substances 0.000 claims abstract description 7
- 229920000058 polyacrylate Polymers 0.000 claims abstract description 6
- 239000000463 material Substances 0.000 claims description 10
- PNEYBMLMFCGWSK-UHFFFAOYSA-N Alumina Chemical compound [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 9
- 229920003986 novolac Polymers 0.000 claims description 9
- 239000013078 crystal Substances 0.000 claims description 8
- 239000004408 titanium dioxide Substances 0.000 claims description 8
- 239000013530 defoamer Substances 0.000 claims description 7
- 229920002050 silicone resin Polymers 0.000 claims description 7
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 claims description 6
- 239000006185 dispersion Substances 0.000 claims description 5
- DMYOHQBLOZMDLP-UHFFFAOYSA-N 1-[2-(2-hydroxy-3-piperidin-1-ylpropoxy)phenyl]-3-phenylpropan-1-one Chemical compound C1CCCCN1CC(O)COC1=CC=CC=C1C(=O)CCC1=CC=CC=C1 DMYOHQBLOZMDLP-UHFFFAOYSA-N 0.000 claims description 3
- 229920013649 Paracril Polymers 0.000 claims description 3
- 239000005543 nano-size silicon particle Substances 0.000 claims description 3
- 239000002105 nanoparticle Substances 0.000 claims description 3
- 229920002635 polyurethane Polymers 0.000 claims description 3
- 239000004814 polyurethane Substances 0.000 claims description 3
- 229920005989 resin Polymers 0.000 abstract description 7
- 239000011347 resin Substances 0.000 abstract description 7
- 239000003822 epoxy resin Substances 0.000 abstract description 4
- 229920000647 polyepoxide Polymers 0.000 abstract description 4
- 239000002270 dispersing agent Substances 0.000 abstract description 3
- 239000004843 novolac epoxy resin Substances 0.000 abstract 2
- 239000002518 antifoaming agent Substances 0.000 abstract 1
- 230000007547 defect Effects 0.000 abstract 1
- 238000004321 preservation Methods 0.000 abstract 1
- 235000010215 titanium dioxide Nutrition 0.000 abstract 1
- 239000000126 substance Substances 0.000 description 8
- 238000002360 preparation method Methods 0.000 description 5
- 150000001875 compounds Chemical class 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 239000011521 glass Substances 0.000 description 3
- 239000003921 oil Substances 0.000 description 3
- 239000000049 pigment Substances 0.000 description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- 229920002125 Sokalan® Polymers 0.000 description 2
- 238000009775 high-speed stirring Methods 0.000 description 2
- 239000011806 microball Substances 0.000 description 2
- 239000004584 polyacrylic acid Substances 0.000 description 2
- KUBDPQJOLOUJRM-UHFFFAOYSA-N 2-(chloromethyl)oxirane;4-[2-(4-hydroxyphenyl)propan-2-yl]phenol Chemical compound ClCC1CO1.C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 KUBDPQJOLOUJRM-UHFFFAOYSA-N 0.000 description 1
- 229920000178 Acrylic resin Polymers 0.000 description 1
- 239000004925 Acrylic resin Substances 0.000 description 1
- 229910019142 PO4 Inorganic materials 0.000 description 1
- 229920004482 WACKER® Polymers 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- FPAFDBFIGPHWGO-UHFFFAOYSA-N dioxosilane;oxomagnesium;hydrate Chemical compound O.[Mg]=O.[Mg]=O.[Mg]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O FPAFDBFIGPHWGO-UHFFFAOYSA-N 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- NBVXSUQYWXRMNV-UHFFFAOYSA-N fluoromethane Chemical compound FC NBVXSUQYWXRMNV-UHFFFAOYSA-N 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000011325 microbead Substances 0.000 description 1
- 239000004005 microsphere Substances 0.000 description 1
- 241000345420 miki group Species 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 229920002803 thermoplastic polyurethane Polymers 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
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- Paints Or Removers (AREA)
Abstract
The invention relates to the technical field of coating, in particular to temperature-resistance thermal-insulation heavy-duty anticorrosion coating, which comprises the following raw material components in percentage by mass: 10 to 40 percent of epoxy modified organosilicon resin, 5 to 20 percent of novolac epoxy resin, 8 to 20 percent of modified amine curing agent, 2 to 10 percent of flexibilizer, 0.1 to 1 percent of modified polysiloxane flatting agent, 0.01 to 0.1 percent of polysiloxane defoaming agent, 0.1 to 1 percent of polyacrylate dispersant, 4 to 11 percent of zinc phosphate, 4 to 10 percent of barite powder, 3 to 8 percent of titanium white, 0.01 to 0.1 percent of carbon black, 15 to 40 percent of potassium titanate whiskers and 2 to 20 percent of nano porous material. The organosilicon-modified epoxy resin adopted by the invention combines the high performance of epoxy resin and organosilicon resin, and the organosilicon-modified epoxy resin and the novolac epoxy resin compensate for respective defects. The coating has high anticorrosion performance, high high-temperature-resistance performance and high insulating performance, and the adhesion force, medium-resistance performance and thermal-insulation and heat-preservation performance of the coating are improved considerably.
Description
Technical field
The present invention relates to the technical field of coatings of chemical industry technology, specifically, relate to the heat insulation heavy-duty coating of a kind of heatproof.
Background technology
Thermal insulating coating is a kind of effective heat insulation means, and its research is originated from needs to the aircraft temperature control.Now, the application (be used for shell that oil product store equipment and transport pipeline) of thermal insulating coating in petroleum industry obtained good effect, and it has reduced the volatilization of oil product, has guaranteed the safety of basin.But high temperature resistant heat insulation coating is a kind of special coating, and it not only will have the characteristic of general coating, also should possess high temperature resistant and heat insulation function.Because the development of new technology and the increase of demand, people have proposed more and more higher requirement to high temperature resistant heat insulation coating at present, and the economic worth of high temperature resistant heat insulation coating is more and more obvious.
Chinese patent CN101230223A discloses a kind of " vacuum micro-ball ultra-thin insulating coating and preparation method thereof ", this thermal insulating coating is a film forming matter with fluorocarbon resin, acrylic resin, urethane resin, with the vacuum micro-ball is weighting material, and processability is thermal insulating coating preferably.In addition, people such as Liu Chengbo are film forming matter with the epoxy modified silicone resin, add heat-resisting tinting pigment, sial ceramic hollow microballon etc. and prepare the heatproof thermal insulating coating.Chinese patent CN1990799A discloses a kind of " high temperature insulating mould coating ", and it is base-material with the heat stable resin, is lagging material with hollow microsphere and nanoporous weighting material, prepares the thermal insulating coating of better performances.Above-described thermal insulating coating one is not mention this important index of thermal conductivity; The 2nd, in the preparation method, all used hollow glass microbead, this makes the surface of paint film be easy to generate unfairness, influences the sticking power of thermal insulating coating.
Summary of the invention
The objective of the invention is to overcome the deficiencies in the prior art, for high temperature resistant heat insulation coating increases a kind of good heat-insulation effect, low, the heat insulation heavy rot-resistant new variety of heatproof of thermal conductivity, can be in the chemical plant, the shell of the high-temperature pipe in power station, boiler, kiln and oil product stores equipment and the transport pipeline shell is used.
For achieving the above object, the technical scheme taked of the present invention is:
The heat insulation heavy-duty coating of a kind of heatproof is characterized in that, the mass percent that its raw material is formed is:
Epoxy modified silicone resin 10～40%;
Novolac epoxy 5～20%;
Modified amine curing agent 8～20%;
Toughner 2～10%;
Modified polyorganosiloxane class flow agent 0.1～1%;
Polysiloxane defoamer 0.01～0.1%;
Polyacrylate(s) dispersion agent 0.1～1%;
Zinc phosphate 4～11%;
Ground barium sulfate 4～10%;
Titanium dioxide 3～8%;
Carbon black 0.01～0.1%;
Crystal whisker of hexa potassium titanate 15～40%;
Nanoporous material 2～20%.
The heat insulation heavy-duty coating of a kind of heatproof is characterized in that, the mass percent that its raw material is formed is:
Epoxy modified silicone resin 10～25%;
Novolac epoxy 5～15%;
Modified amine curing agent 5～15%;
Toughner 3～6%;
Modified polyorganosiloxane class flow agent 0.4～0.7%;
Polysiloxane defoamer 0.05～0.08%;
Polyacrylate(s) dispersion agent 0.5～0.8%;
Zinc phosphate 6～9%;
Ground barium sulfate 5～8%;
Titanium dioxide 5～7%;
Carbon black 0.02～0.05%;
Crystal whisker of hexa potassium titanate 20～35%;
Nanoporous material 5～12%.
Described toughner is one or more in paracril, thiorubber, the epoxy-terminated polyurethane.
Described nanoporous weighting material is one or more in nano aluminium oxide, nano-sized iron oxide, nano zircite, the nano silicon.
The positively effect of the heat insulation heavy-duty coating of a kind of heatproof of the present invention is:
(1) adopting the organic-silicon-modified Resins, epoxy collection Resins, epoxy and the premium properties of silicone resin is one, add novolac epoxy, remedied defective separately, have good protection against corrosion, high temperature resistant and point insulating performance, particularly sticking power, the medium-resistance to ground improves a lot than silicone resin;
(2) select for use nanoporous weighting material, whisker shape pigment as thermal insulating filling, intercepted the transmission of heat effectively, played function of heat insulation preferably, thermal resistance coefficient can reach 0.06w/m ﹒ k;
(3) prospect of applying is preferably arranged.
Embodiment
Below provide the embodiment of the heat insulation heavy-duty coating of a kind of heatproof of the present invention, provide 3 embodiment.But should be pointed out that enforcement of the present invention is not limited to following embodiment.
Embodiment 1
The heat insulation heavy-duty coating of a kind of heatproof, the mass percent that its raw material is formed is:
Epoxy modified silicone 25% can adopt the product of good promise organosilicon company limited in Jiangsu Miki Group or DOW CORNING or Degussa or Changzhou or Wacker Chemical Co.,Ltd;
Novolac epoxy 8% adopts the 638S product of 438 or South Asia Resins, epoxy company limited of Dow Chemical;
Modified amine curing agent 12% adopts the product of U.S. Ka Delai company;
Modified polyorganosiloxane class flow agent 0.7%, employing moral modest (Shanghai) chemical company model are 435 product;
Polysiloxane defoamer 0.01%, employing moral modest (Shanghai) chemical company model are 6800 product;
Polyacrylate(s) dispersion agent 0.5%, adopting Bi Ke company model is the product of BYK-354;
Toughner 3% adopts paracril, thiorubber, one or more in the epoxy-terminated polyurethane etc.;
Zinc phosphate 6.77%, its chemical formula are Zn (PO4) 22H2O;
Carbon black 0.02%, adopting sky, Qingdao and graphite company limited model is the product of C612;
Ground barium sulfate 5%, adopting Shanghai Shuan Run chemical industry company limited model is the product of LB-800, its kind and consumption are decided according to required color and colourity;
Titanium dioxide 5%, adopting Shanghai suitable should chemical company's model be the product of R902;
Potassium titanate crystal whisker 24% is minute hand shape barred body, adopts the product of Shanghai Jingxu Composite Material Co., Ltd.;
Nanoporous material 10%, one or more in employing nano aluminium oxide, nano-sized iron oxide, nano zircite, the nano silicon.
The preparation process of the heat insulation heavy-duty coating of described a kind of heatproof is:
(1) novolac epoxy is joined in the modifying epoxy resin by organosilicon, add solvent then, high-speed stirring is fully dissolved, with this as base-material;
(2) in the base-material of step (1), add various auxiliary agents, high-speed stirring by mass percentage; Add various pigment and filler again,, fully disperse, obtain compound, then compound is ground to required fineness as zinc phosphate, talcum powder, titanium dioxide, ground barium sulfate and lagging material potassium titanate crystal whisker;
(3) in step (2) levigated compound, add hollow glass micropearl, be uniformly dispersed then and promptly get the heatproof heat-insulating anti-corrosive coating.
Embodiment 2
The heat insulation heavy-duty coating of a kind of heatproof, the mass percent that its raw material is formed is:
Epoxy modified silicone 20%;
Novolac epoxy 10%;
Modified amine curing agent 10%;
Modified polyorganosiloxane class flow agent 1%;
Polysiloxane defoamer 0.05%;
Polyacrylic acid dispersant 1%;
Toughner 6%;
Zinc phosphate 7.9%;
Carbon black 0.05%;
Ground barium sulfate 4%;
Titanium dioxide 7%;
Potassium titanate crystal whisker 28%;
Nanoporous material 5%; The source of above-mentioned raw materials is with embodiment 1.
The preparation process of the heat insulation heavy-duty coating of above-mentioned a kind of heatproof is with embodiment 1.
Embodiment 3
The heat insulation heavy-duty coating of a kind of heatproof, the mass percent that its raw material is formed is:
Epoxy modified silicone 15%;
Novolac epoxy 15%;
Modified amine curing agent 6%;
Modified polyorganosiloxane class flow agent 0.5%;
Polysiloxane defoamer 0.08%;
Polyacrylic acid dispersant 0.8%;
Toughner 9%;
Zinc phosphate 8%;
Carbon black 0.01%;
Ground barium sulfate 7%;
Titanium dioxide 6%;
Potassium titanate crystal whisker 18.61%;
Hollow glass micropearl 14%; The source of above-mentioned raw materials is with embodiment 1.
The preparation process of the heat insulation heavy-duty coating of above-mentioned a kind of heatproof is with embodiment 1.
The performance index of heat insulation heavy-duty coating of a kind of heatproof of the present invention and coating are as shown in the table:
Table. the heat insulation heavy-duty coating heatproof of a kind of heatproof heat-proof quality test chart
Claims (4)
1. the heat insulation heavy-duty coating of heatproof is characterized in that, the mass percent that its raw material is formed is:
Epoxy modified silicone resin 10～40%;
Novolac epoxy 5～20%;
Modified amine curing agent 8～20%;
Toughner 2～10%;
Modified polyorganosiloxane class flow agent 0.1～1%;
Polysiloxane defoamer 0.01～0.1%;
Polyacrylate(s) dispersion agent 0.1～1%;
Zinc phosphate 4～11%;
Ground barium sulfate 4～10%;
Titanium dioxide 3～8%;
Carbon black 0.01～0.1%;
Crystal whisker of hexa potassium titanate 15～40%;
Nanoporous material 2～20%.
2. according to the heat insulation heavy-duty coating of right 1 described a kind of heatproof, it is characterized in that the mass percent that its raw material is formed is:
Epoxy modified silicone resin 10～25%;
Novolac epoxy 5～15%;
Modified amine curing agent 5～15%;
Toughner 3～6%;
Modified polyorganosiloxane class flow agent 0.4～0.7%;
Polysiloxane defoamer 0.05～0.08%;
Polyacrylate(s) dispersion agent 0.5～0.8%;
Zinc phosphate 6～9%;
Ground barium sulfate 5～8%;
Titanium dioxide 5～7%;
Carbon black 0.02～0.05%;
Crystal whisker of hexa potassium titanate 20～35%;
Nanoporous material 5～12%.
3. according to the heat insulation heavy-duty coating of right 1 described a kind of heatproof, it is characterized in that described toughner is one or more in paracril, thiorubber, the epoxy-terminated polyurethane.
4. according to the heat insulation heavy-duty coating of right 1 described a kind of heatproof, it is characterized in that described nanoporous weighting material is one or more in nano aluminium oxide, nano-sized iron oxide, nano zircite, the nano silicon.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201110045749 CN102134444A (en) | 2011-02-25 | 2011-02-25 | Temperature-resistance thermal-insulation heavy-duty anticorrosion coating |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201110045749 CN102134444A (en) | 2011-02-25 | 2011-02-25 | Temperature-resistance thermal-insulation heavy-duty anticorrosion coating |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN102134444A true CN102134444A (en) | 2011-07-27 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201110045749 Pending CN102134444A (en) | 2011-02-25 | 2011-02-25 | Temperature-resistance thermal-insulation heavy-duty anticorrosion coating |
Country Status (1)
| Country | Link |
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| 《上海涂料》 20080530 何德泉 耐热环氧粉末涂料 第46卷, 第05期 * |
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Application publication date: 20110727 |