CN104193233A - Thermal insulation masonry mortar and preparation method thereof - Google Patents

Thermal insulation masonry mortar and preparation method thereof Download PDF

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Publication number
CN104193233A
CN104193233A CN201410353318.8A CN201410353318A CN104193233A CN 104193233 A CN104193233 A CN 104193233A CN 201410353318 A CN201410353318 A CN 201410353318A CN 104193233 A CN104193233 A CN 104193233A
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parts
masonry mortar
water
minute
mortar
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CN201410353318.8A
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CN104193233B (en
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张洪滨
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Shandong Shengyang New Building Materials Co ltd
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BENGBU HONGAN PRECISION MACHINERY Co Ltd
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/50Reuse, recycling or recovery technologies
    • Y02W30/91Use of waste materials as fillers for mortars or concrete

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  • Curing Cements, Concrete, And Artificial Stone (AREA)

Abstract

The invention relates to thermal insulation masonry mortar which is prepared from the following raw materials in parts by weight: 15 to 20 parts of pure acrylic emulsion, 8 to 12 parts of emulsified silicone oil, 2 to 3 parts of paraffin, 10 to 14 parts of rice hull ash, 240 to 270 parts of expanded perlite, 2 to 4 parts of ethylene glycol octylphenol ether, 5 to 8 parts of zinc carbonate, 150 to 170 parts of cement, 40 to 50 parts of microsilica powder, 10 to 14 parts of sodium metasilicate, a proper amount of water, 20 to 25 parts of auxiliaries and 5 to 6 parts of calcium nitrite. The masonry mortar is good in thermal insulation, and is also good in compactness and high in bonding strength due to the added rice hull ash and microsilica powder; the water resistance of the masonry mortar is improved due to the added pure acrylic emulsion, emulsified silicone oil and paraffin; the masonry mortar can be rapidly hardened, so that the corrosion of a steel bar is effectively prevented, i.e., the service life of the steel bar is prolonged; and by virtue of the auxiliaries, the compressive strength and the rupture strength of the masonry mortar are enhanced while the workability, the sagging resistance, the thixotropy and the sedimentation resistance of the masonry mortar are improved.

Description

A kind of building heat insulation mortar and preparation method thereof
Technical field
The invention belongs to building material field, particularly a kind of building heat insulation mortar and preparation method thereof.
Background technology
Mortar is common material for building, belongs to the indispensable material in building operation.According to performance, divide, mortar is divided into a variety of, has in conjunction with mortar, filleting mortar, thermal insulation mortar etc.; By purposes, be divided into masonry mortar, plastering mortar (comprising decoration mortar, waterproof mortar), adhesive mortar etc.
The performance quality of mortar differs at present, affects use.Specifically the factor that affects mortar performance comprises the workability of fresh mortar, mobility, water-retentivity, is exactly the intensity of hardened mortar in addition.Need to study new mortar, make it have excellent application property and processibility, sag resistance, thixotropy, anti-settling, package stability, improve pumping and shear-thinning, also need to find new material, to improve its use properties and intensity, and reduce comprehensive cost.
Summary of the invention
The object of the present invention is to provide a kind of building heat insulation mortar and preparation method thereof, this mortar is good heat insulating not only, and cohesive strength is high, good waterproof performance, and sclerosis is fast, can effectively prevent reinforcement corrosion, extends the work-ing life of reinforcing bar.
Technical scheme of the present invention is as follows:
A building heat insulation mortar, is characterized in that being made by the raw material of following weight part: pure-acrylic emulsion 15-20, silicone emulsion 8-12, paraffin 2-3, rice hull ash 10-14, pearlstone 240-270, ethylene glycol octyl phenyl ether 2-4, zinc carbonate 5-8, cement 150-170, SILICA FUME 40-50, Starso 10-14, water are appropriate, auxiliary agent 20-25, calcium nitrite 5-6;
Described auxiliary agent is made by the raw material of following weight part: attapulgite 2-3, wilkinite 2-3, steel fiber 6-7, urethane acrylate 4-5, E-12 epoxy resin 2-3, epoxy acrylate 3-4, peroxidized t-butyl perbenzoate 0.2-0.3, vinylbenzene 1-2, dipropylene glycol 3-4, TriMethylolPropane(TMP) 2-3, Calucium Silicate powder 3-4, mandarin oil 0.8-1.2, benzotriazole 0.6-0.9, trimeric cyanamide 1-2, 10-15% sodium hydroxide solution 6-8, sodium oleate 0.2-0.3, ammonium persulphate 0.1-0.2, water 17-20, preparation method is: attapulgite, wilkinite are put into calcining furnace, at 670-700 ℃, calcine 3-4 hour, taking-up, puts into 10-15% sodium hydroxide solution and be ground to 20-40 μ m slurry, and the material pH value of sizing mixing is for neutral, and spraying is dried to obtain powder, water, sodium oleate, urethane acrylate, E-12 epoxy resin, epoxy acrylate, vinylbenzene, dipropylene glycol, TriMethylolPropane(TMP) are mixed, be heated to 60-70 ℃, add peroxidized t-butyl perbenzoate, stirring reaction 20-30 minute, add again described powder and other composition, continue to be warming up to 80-90 ℃, stirring reaction 50-60 minute, obtains.
The preparation method of described building heat insulation mortar, is characterized in that comprising the following steps:
(1) silicone emulsion, paraffin, rice hull ash are mixed, grind 20-30 minute;
(2) pure-acrylic emulsion, ethylene glycol octyl phenyl ether, zinc carbonate, calcium nitrite, Starso, water are mixed, stir and obtain slurry;
(3) auxiliary agent, SILICA FUME are mixed, dispersion grinding 20-30 minute, obtains mixture;
(4) mixing of materials other remaining components and (1) step, (2) step, (3) step being obtained is even, and stirring reaction 10-15 minute, obtains.
Beneficial effect of the present invention
Mortar of the present invention is good heat insulating not only, and has added rice hull ash, SILICA FUME, and compactness is good, cohesive strength is high, by adding pure-acrylic emulsion, silicone emulsion, paraffin, has improved water-repellancy, this mortar hardening is fast, can effectively prevent reinforcement corrosion, extends the work-ing life of reinforcing bar; The application of the invention auxiliary agent, has improved resistance to compression, the folding strength of mortar, has improved workability, sag resistance, thixotropy and anti-settling.
Embodiment
A building heat insulation mortar, by following weight part (kilogram) raw material make: pure-acrylic emulsion 18, silicone emulsion 10, paraffin 2.5, rice hull ash 12, pearlstone 260, ethylene glycol octyl phenyl ether 3, zinc carbonate 6, cement 160, SILICA FUME 45, Starso 12, water are appropriate, auxiliary agent 23, calcium nitrite 5.5;
Described auxiliary agent by following weight part (kilogram) raw material make: attapulgite 2.5, wilkinite 2.5, steel fiber 6.5, urethane acrylate 4.5, E-12 epoxy resin 2.5, epoxy acrylate 3.5, peroxidized t-butyl perbenzoate 0.5, vinylbenzene 1.5, dipropylene glycol 3.5, TriMethylolPropane(TMP) 2.5, Calucium Silicate powder 3.5, mandarin oil 1, benzotriazole 0.8, trimeric cyanamide 1.5,3% sodium hydroxide solution 7, sodium oleate 0.3, ammonium persulphate 0.2, water 19; Preparation method is: attapulgite, wilkinite are put into calcining furnace, calcine 3.5 hours at 69 ℃, taking-up, puts into 13% sodium hydroxide solution and be ground to 30 μ m slurries, and the material pH value of sizing mixing is for neutral, and spraying is dried to obtain powder; Water, sodium oleate, urethane acrylate, E-12 epoxy resin, epoxy acrylate, vinylbenzene, dipropylene glycol, TriMethylolPropane(TMP) are mixed, be heated to 65 ℃, add peroxidized t-butyl perbenzoate, stirring reaction 25 minutes, add again described powder and other composition, continue to be warming up to 85 ℃, stirring reaction 55 minutes, obtains.
The preparation method of described building heat insulation mortar, comprises the following steps:
(1) silicone emulsion, paraffin, rice hull ash are mixed, grind 25 minutes;
(2) pure-acrylic emulsion, ethylene glycol octyl phenyl ether, zinc carbonate, calcium nitrite, Starso, water are mixed, stir and obtain slurry;
(3) auxiliary agent, SILICA FUME are mixed, dispersion grinding 25 minutes, obtains mixture;
(4) mixing of materials other remaining components and (1) step, (2) step, (3) step being obtained is even, and stirring reaction 12 minutes, obtains.
Experimental data:
The ultimate compression strength of the mortar 28d of this embodiment is 44MPa, folding strength 14MPa, and water-intake rate 1.6%, thermal conductivity is 0.06W/mk.

Claims (2)

1. a building heat insulation mortar, is characterized in that being made by the raw material of following weight part: pure-acrylic emulsion 15-20, silicone emulsion 8-12, paraffin 2-3, rice hull ash 10-14, pearlstone 240-270, ethylene glycol octyl phenyl ether 2-4, zinc carbonate 5-8, cement 150-170, SILICA FUME 40-50, Starso 10-14, water are appropriate, auxiliary agent 20-25, calcium nitrite 5-6;
Described auxiliary agent is made by the raw material of following weight part: attapulgite 2-3, wilkinite 2-3, steel fiber 6-7, urethane acrylate 4-5, E-12 epoxy resin 2-3, epoxy acrylate 3-4, peroxidized t-butyl perbenzoate 0.2-0.3, vinylbenzene 1-2, dipropylene glycol 3-4, TriMethylolPropane(TMP) 2-3, Calucium Silicate powder 3-4, mandarin oil 0.8-1.2, benzotriazole 0.6-0.9, trimeric cyanamide 1-2, 10-15% sodium hydroxide solution 6-8, sodium oleate 0.2-0.3, ammonium persulphate 0.1-0.2, water 17-20, preparation method is: attapulgite, wilkinite are put into calcining furnace, at 670-700 ℃, calcine 3-4 hour, taking-up, puts into 10-15% sodium hydroxide solution and be ground to 20-40 μ m slurry, and the material pH value of sizing mixing is for neutral, and spraying is dried to obtain powder, water, sodium oleate, urethane acrylate, E-12 epoxy resin, epoxy acrylate, vinylbenzene, dipropylene glycol, TriMethylolPropane(TMP) are mixed, be heated to 60-70 ℃, add peroxidized t-butyl perbenzoate, stirring reaction 20-30 minute, add again described powder and other composition, continue to be warming up to 80-90 ℃, stirring reaction 50-60 minute, obtains.
2. the preparation method of building heat insulation mortar according to claim 1, is characterized in that comprising the following steps:
(1) silicone emulsion, paraffin, rice hull ash are mixed, grind 20-30 minute;
(2) pure-acrylic emulsion, ethylene glycol octyl phenyl ether, zinc carbonate, calcium nitrite, Starso, water are mixed, stir and obtain slurry;
(3) auxiliary agent, SILICA FUME are mixed, dispersion grinding 20-30 minute, obtains mixture;
(4) mixing of materials other remaining components and (1) step, (2) step, (3) step being obtained is even, and stirring reaction 10-15 minute, obtains.
CN201410353318.8A 2014-07-24 2014-07-24 A kind of building heat insulation mortar and preparation method thereof Active CN104193233B (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104529293A (en) * 2014-12-20 2015-04-22 魏超产 Waterproof heat insulation environment-friendly mortar and preparation method thereof
CN104529291A (en) * 2014-12-20 2015-04-22 魏超产 Masonry mortar and preparation method thereof
CN104529295A (en) * 2014-12-20 2015-04-22 王小波 Fiber surface mortar and preparation method thereof
CN109796164A (en) * 2019-04-02 2019-05-24 东北林业大学 A kind of preparation method of double-doped rice hull ash and silicon ash antifreezing cement mortar
CN110951237A (en) * 2019-12-09 2020-04-03 西安鼎蓝通信技术有限公司 Preparation method of noise reduction material for sound equipment

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2001058823A1 (en) * 2000-02-08 2001-08-16 Rha Technology, Inc. Method for producing a blended cementitious composition
CN101182178A (en) * 2007-11-29 2008-05-21 武汉莱克利安科技有限公司 Special masonry mortar for self-insulating wall
CN101538136A (en) * 2009-04-29 2009-09-23 华南理工大学 Premixing mortar with high moisture retention and production method thereof
CN102674778A (en) * 2012-06-04 2012-09-19 同济大学 Self-leveling mortar doped with low-temperature rice hull ash
GB2500744A (en) * 2011-11-24 2013-10-02 Fibrelime Ltd A pliable building material
CN103387365A (en) * 2013-07-24 2013-11-13 安徽英柯建材有限公司 Thermal mortar in wall construction

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2001058823A1 (en) * 2000-02-08 2001-08-16 Rha Technology, Inc. Method for producing a blended cementitious composition
CN101182178A (en) * 2007-11-29 2008-05-21 武汉莱克利安科技有限公司 Special masonry mortar for self-insulating wall
CN101538136A (en) * 2009-04-29 2009-09-23 华南理工大学 Premixing mortar with high moisture retention and production method thereof
GB2500744A (en) * 2011-11-24 2013-10-02 Fibrelime Ltd A pliable building material
CN102674778A (en) * 2012-06-04 2012-09-19 同济大学 Self-leveling mortar doped with low-temperature rice hull ash
CN103387365A (en) * 2013-07-24 2013-11-13 安徽英柯建材有限公司 Thermal mortar in wall construction

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104529293A (en) * 2014-12-20 2015-04-22 魏超产 Waterproof heat insulation environment-friendly mortar and preparation method thereof
CN104529291A (en) * 2014-12-20 2015-04-22 魏超产 Masonry mortar and preparation method thereof
CN104529295A (en) * 2014-12-20 2015-04-22 王小波 Fiber surface mortar and preparation method thereof
CN109796164A (en) * 2019-04-02 2019-05-24 东北林业大学 A kind of preparation method of double-doped rice hull ash and silicon ash antifreezing cement mortar
CN110951237A (en) * 2019-12-09 2020-04-03 西安鼎蓝通信技术有限公司 Preparation method of noise reduction material for sound equipment

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Effective date of registration: 20190715

Address after: 257 400 Yongxi Road 288, Lijin County, Dongying City, Shandong Province

Patentee after: Shandong Shengyang New Building Materials Co.,Ltd.

Address before: 233000 Anhui city of Bengbu province high tech District Road No. 168

Patentee before: BENGBU HONGAN PRECISION MACHINERY Co.,Ltd.

PE01 Entry into force of the registration of the contract for pledge of patent right
PE01 Entry into force of the registration of the contract for pledge of patent right

Denomination of invention: A masonry insulation mortar and its preparation method

Effective date of registration: 20220629

Granted publication date: 20160629

Pledgee: Industrial and Commercial Bank of China Limited Lijin sub branch

Pledgor: Shandong Shengyang New Building Materials Co.,Ltd.

Registration number: Y2022980009436

PC01 Cancellation of the registration of the contract for pledge of patent right
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Date of cancellation: 20231123

Granted publication date: 20160629

Pledgee: Industrial and Commercial Bank of China Limited Lijin sub branch

Pledgor: Shandong Shengyang New Building Materials Co.,Ltd.

Registration number: Y2022980009436