CN104152188A - Plant pinene fuel oil - Google Patents
Plant pinene fuel oil Download PDFInfo
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- CN104152188A CN104152188A CN201410153832.7A CN201410153832A CN104152188A CN 104152188 A CN104152188 A CN 104152188A CN 201410153832 A CN201410153832 A CN 201410153832A CN 104152188 A CN104152188 A CN 104152188A
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- Prior art keywords
- plant
- pinene
- fuel oil
- oil
- firpene
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- 239000000295 fuel oil Substances 0.000 title abstract description 15
- XMGQYMWWDOXHJM-UHFFFAOYSA-N limonene Chemical compound CC(=C)C1CCC(C)=CC1 XMGQYMWWDOXHJM-UHFFFAOYSA-N 0.000 claims abstract description 24
- 239000000463 material Substances 0.000 claims abstract description 22
- 239000000446 fuel Substances 0.000 claims abstract description 19
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical group CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 claims abstract description 12
- HZAXFHJVJLSVMW-UHFFFAOYSA-N 2-Aminoethan-1-ol Chemical compound NCCO HZAXFHJVJLSVMW-UHFFFAOYSA-N 0.000 claims abstract description 10
- 238000004519 manufacturing process Methods 0.000 claims abstract description 10
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 claims abstract description 8
- KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 claims abstract description 8
- 239000006227 byproduct Substances 0.000 claims abstract description 8
- KHPCPRHQVVSZAH-UHFFFAOYSA-N trans-cinnamyl beta-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OCC=CC1=CC=CC=C1 KHPCPRHQVVSZAH-UHFFFAOYSA-N 0.000 claims abstract description 8
- 230000018044 dehydration Effects 0.000 claims abstract description 4
- 238000006297 dehydration reaction Methods 0.000 claims abstract description 4
- 238000001914 filtration Methods 0.000 claims abstract description 4
- 238000002156 mixing Methods 0.000 claims abstract description 4
- 238000006386 neutralization reaction Methods 0.000 claims abstract description 4
- XOKSLPVRUOBDEW-UHFFFAOYSA-N pinane Chemical compound CC1CCC2C(C)(C)C1C2 XOKSLPVRUOBDEW-UHFFFAOYSA-N 0.000 claims description 34
- 229930006728 pinane Natural products 0.000 claims description 17
- 238000003756 stirring Methods 0.000 claims description 6
- 238000012545 processing Methods 0.000 claims description 5
- 239000002253 acid Substances 0.000 claims description 4
- BTANRVKWQNVYAZ-UHFFFAOYSA-N butan-2-ol Chemical compound CCC(C)O BTANRVKWQNVYAZ-UHFFFAOYSA-N 0.000 claims description 4
- ZBCBWPMODOFKDW-UHFFFAOYSA-N diethanolamine Chemical compound OCCNCCO ZBCBWPMODOFKDW-UHFFFAOYSA-N 0.000 claims description 4
- WUOACPNHFRMFPN-UHFFFAOYSA-N alpha-terpineol Chemical compound CC1=CCC(C(C)(C)O)CC1 WUOACPNHFRMFPN-UHFFFAOYSA-N 0.000 claims description 3
- 230000036571 hydration Effects 0.000 claims description 3
- 238000006703 hydration reaction Methods 0.000 claims description 3
- DKGAVHZHDRPRBM-UHFFFAOYSA-N Tert-Butanol Chemical compound CC(C)(C)O DKGAVHZHDRPRBM-UHFFFAOYSA-N 0.000 claims description 2
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims description 2
- ZXEKIIBDNHEJCQ-UHFFFAOYSA-N isobutanol Chemical compound CC(C)CO ZXEKIIBDNHEJCQ-UHFFFAOYSA-N 0.000 claims description 2
- 229960004418 trolamine Drugs 0.000 claims description 2
- 239000003921 oil Substances 0.000 abstract description 27
- 238000002485 combustion reaction Methods 0.000 abstract description 4
- 238000003912 environmental pollution Methods 0.000 abstract description 4
- 239000000047 product Substances 0.000 abstract description 3
- 241000196324 Embryophyta Species 0.000 abstract 5
- HICYDYJTCDBHMZ-UHFFFAOYSA-N (+)-alpha-Longipinen Natural products C12C3C(C)=CCC1C3(C)CCCC2(C)C HICYDYJTCDBHMZ-UHFFFAOYSA-N 0.000 abstract 4
- HICYDYJTCDBHMZ-COMQUAJESA-N (+)-alpha-longipinene Chemical compound CC1(C)CCC[C@]2(C)[C@]3([H])[C@@]1([H])[C@@]2([H])CC=C3C HICYDYJTCDBHMZ-COMQUAJESA-N 0.000 abstract 4
- 229930004728 longipinene Natural products 0.000 abstract 4
- 241000779819 Syncarpia glomulifera Species 0.000 abstract 3
- 239000001739 pinus spp. Substances 0.000 abstract 3
- 229940036248 turpentine Drugs 0.000 abstract 3
- 239000002283 diesel fuel Substances 0.000 description 5
- 239000000284 extract Substances 0.000 description 5
- 230000000694 effects Effects 0.000 description 4
- 239000002803 fossil fuel Substances 0.000 description 4
- 238000011161 development Methods 0.000 description 3
- 230000018109 developmental process Effects 0.000 description 3
- 230000008676 import Effects 0.000 description 3
- GRWFGVWFFZKLTI-IUCAKERBSA-N (-)-α-pinene Chemical compound CC1=CC[C@@H]2C(C)(C)[C@H]1C2 GRWFGVWFFZKLTI-IUCAKERBSA-N 0.000 description 2
- 239000010779 crude oil Substances 0.000 description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000003208 petroleum Substances 0.000 description 2
- WTARULDDTDQWMU-RKDXNWHRSA-N (+)-β-pinene Chemical compound C1[C@H]2C(C)(C)[C@@H]1CCC2=C WTARULDDTDQWMU-RKDXNWHRSA-N 0.000 description 1
- WTARULDDTDQWMU-IUCAKERBSA-N (-)-Nopinene Natural products C1[C@@H]2C(C)(C)[C@H]1CCC2=C WTARULDDTDQWMU-IUCAKERBSA-N 0.000 description 1
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 1
- WTARULDDTDQWMU-UHFFFAOYSA-N Pseudopinene Natural products C1C2C(C)(C)C1CCC2=C WTARULDDTDQWMU-UHFFFAOYSA-N 0.000 description 1
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 description 1
- XCPQUQHBVVXMRQ-UHFFFAOYSA-N alpha-Fenchene Natural products C1CC2C(=C)CC1C2(C)C XCPQUQHBVVXMRQ-UHFFFAOYSA-N 0.000 description 1
- MVNCAPSFBDBCGF-UHFFFAOYSA-N alpha-pinene Natural products CC1=CCC23C1CC2C3(C)C MVNCAPSFBDBCGF-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 229930006722 beta-pinene Natural products 0.000 description 1
- 235000011089 carbon dioxide Nutrition 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 230000002860 competitive effect Effects 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 125000004122 cyclic group Chemical group 0.000 description 1
- 238000005474 detonation Methods 0.000 description 1
- 230000001804 emulsifying effect Effects 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000010304 firing Methods 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- LCWMKIHBLJLORW-UHFFFAOYSA-N gamma-carene Natural products C1CC(=C)CC2C(C)(C)C21 LCWMKIHBLJLORW-UHFFFAOYSA-N 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 230000004630 mental health Effects 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000003345 natural gas Substances 0.000 description 1
- 239000005445 natural material Substances 0.000 description 1
- 239000000419 plant extract Substances 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- GRWFGVWFFZKLTI-UHFFFAOYSA-N rac-alpha-Pinene Natural products CC1=CCC2C(C)(C)C1C2 GRWFGVWFFZKLTI-UHFFFAOYSA-N 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- -1 removes moisture Substances 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 239000004576 sand Substances 0.000 description 1
- 238000012216 screening Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000004083 survival effect Effects 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
Landscapes
- Solid Fuels And Fuel-Associated Substances (AREA)
- Liquid Carbonaceous Fuels (AREA)
Abstract
The invention relates to plant pinene fuel oil in the fuel fabrication field. The plant pinene fuel oil is prepared by mixing 65-75% of pinene-containing oil, 26-34% of dipentene and 2-3% of auxiliary, wherein the pinene-containing oil is originated from a byproduct in production of rosin, turpentine and pinene: a longipinene material. The plant pinene fuel oil is prepared by the following steps: 1) dehydration: adding 0.3% of monoethanolamine into the longipinene material; 2) neutralization: adding monoethanolamine to adjust the pH value to 7.0; and 3) filtration: removing filter residues. Dipentene is originated from a byproduct in production of terpilenol by hydratation of turpentine, and a combustion improver is normal butanol. Dipentene and normal butanol are added to reduce the density, viscosity and flash point of the fuel oil, so that the fuel oil is easy to ignite. According to the fuel oil, the problem of treating the plenty of byproduct longipinene material after pinene is extracted from turpentine is solved, so that the longipinene material becomes an environment-friendly clean energy product with a high heat value, the environmental pollution caused by the fuel oil in the combustion process is overcome, and the plant pinene fuel oil is an existing energy-saving and emission-reducing renewable plant fuel.
Description
Technical field
The present invention relates to New-type fuel and manufacture field, specifically a kind of plant firpene oil fuel.
Background technology
The energy is the lifeblood of national economy, the mankind's the survival and development are more and more higher to the degree of dependence of the energy, the energy using at present has 85% to be that fossil oil oil, Sweet natural gas and coal by burning non-renewable obtains, and the fossil fuel resource in the whole world just progressively moves towards exhaustion.Oil is the energy being most widely used.According to up-to-date estimation, on the earth, oil stable supplying can not exceed 20 years, and dry spells is only 50 years, and energy dilemma is the huge challenge that the mankind are about to face the middle of this century.China is the relatively poor countries of petroleum resources, and reserves are only 12% of the world per capita.Along with the rapid growth of national economy, the petroleum resources of China are increasingly in short supply, and since China in 1993 becomes net import of oil state, crude oil import quantity increases year by year, and crude oil import has accounted for national oil aggregate supply more than 50% at present.
In fossil oil is played a great role in human society modernization development, also bring serious ecological environmental pollution problem.Data shows, 70% carbonic acid gas in atmosphere, 80% sulfide and 70% oxynitride come from the product after combustion of fossil fuel, cause the severe contamination of atmosphere.In recent years, all there is big area, large-scale haze weather in China various places, has worsened living environment, serious threat people physical and mental health.
Fossil energy is gradually exhausted, energy consumption constantly increases, severe environmental pollution in the situation that, advocate protection of the environment, Sustainable development and recycling economy, become the only selection of people.People are novel in the urgent need to develop and useining, clean energy.
Nuclear energy except fossil energy, can be applied to maturely generating, but since Fukushima, Japan Nuclear power plants is due to earthquake reason, produce nuclear leakage, jeopardize the multiple countries of periphery, so people have had and re-recognized nuclear energy, think that it is also dangerous, and sun power utilization, because its utilising efficiency is low, can't large-scale application.
Therefore, the utilization of plant energy progresses into people's sight line, and it is clean energy, be a kind of form of earth plant storage sun power, plant fuel oil is topmost plant energy, and it is from plant, and plant can cyclic regeneration, atmosphere pollution not after plant fuel oil firing.
China's plant resources is abundant, can be used as setting up mass-producing plant fuel oil raw material site, utilizes deserted mountain, sand ground etc. to afforest suitable for afforestationly.China produces more than 60 ten thousand tons, rosin per year, and wherein Guangdong has more than ten ten thousand tons of rosin every year, and it makes rosin and turps, extracts the long pinane material of a large amount of byproducts after the firpene (being α-pinene and beta-pinene) of high value from turps, has pending.Past is just added in the 180# heavy oil of high pollution, uses as fuel, can not make the best use of everything and contaminate environment.The applicant is through research and development for many years, find out a new way, make to extract from turps after the product of firpene and so on high value, remaining long pinane material, through being treated as containing firpene oil, add again other component, produce plant firpene oil fuel, as a kind of green reproducible, fossil fuel ordinary diesel oil substitute, calorific value is high, free from environmental pollution, achieves many things at one stroke.Other plant fuel oil on existing market, calorific value is low, and cost is high, difficult universal.
Summary of the invention
The problems referred to above that exist in order to solve prior art plant fuel oil, the present invention proposes a kind of plant firpene oil fuel.
The technical scheme that the present invention uses is as follows:
One kind of plant firpene oil fuel, the material that it comprises following weight percent: containing firpene oil 60-80%, kautschin 20-40%, ignition dope 1-5%, through mixing.Screening formulation: containing firpene oil 65-75%, kautschin 26-34%, ignition dope 2-3%.
Described containing firpene oil, byproduct--the long pinane material while deriving from rosin, turps and firpene production, through the following step, processing forms.
1) dehydration: will long pinane material with in pump delivery to the first reactor, add the one in Monoethanolamine MEA BASF, diethanolamine, trolamine, preferably Monoethanolamine MEA BASF, its effect is to reduce viscosity, impels profit layering, addition is 0.2-0.6%, stir 60-90 minute, then leave standstill 4-6 hour, profit natural layering, the moisture content of reactor bottom is emitted, then by long pinane mass transport to the second reactor on top.
2) neutralization: measure acid number, add the one in Monoethanolamine MEA BASF, diethanolamine, preferably Monoethanolamine MEA BASF, its effect is to reduce acid number, neutralizes, and adjusts pH value to 6.5-7.5, then stirs 40-80 minute, leaves standstill 3-5 hour, then is delivered in the 3rd reactor.
3) filter: by the long pinane material in the 3rd reactor, deliver to pressure filter and carry out press filtration, remove filter residue, gained is containing firpene oil.
By product when described kautschin derives from turps hydration manufacture Terpineol 350, its content is 80-95%.
Described ignition dope is butanols, comprises propyl carbinol, isopropylcarbinol, the trimethyl carbinol, sec-butyl alcohol, and content is more than 93%, preferably propyl carbinol.
Above-mentioned long pinane material also can extract from trunk, branch, leaf, pulverizes by it, therefrom obtains liquid substance, removes moisture, extracts rosin and turps, then from turps, extracts after firpene, remaining is long pinane material.
The invention has the beneficial effects as follows:
1) solve the processing problem of the long pinane material of a large amount of byproducts extracting in turps after firpene, made it become high heating value, environmentally friendly, reproducible plant fuel, become the substitute of non-renewable fossil fuel ordinary diesel oil.
2) in formula, adding the effect of kautschin is to reduce density of the present invention and flash-point, make it easily to light, and burning completely; The effect that adds propyl carbinol is to reduce viscosity of the present invention and flash-point, and there is emulsifying effect, prevent that the micro-moisture existing in the present invention from producing detonation, also makes various compositions in the present invention evenly be mixed into one, prevent contingent demixing phenomenon, and burning is incomplete.
3) can be directly from the trunk of plant, branch, leaf, extract long pinane material, for making plant firpene oil fuel, and the quantity that above-mentioned plant goes out of use every year is in the wild surprising, can utilize, and will benefit future generations all ages.
4) the present invention's kautschin, propyl carbinol etc. used is the natural material of plant extract, and processing and making process of the present invention does not produce any pollutent yet.
5) plant firpene oil fuel of the present invention is higher by approximately 15% than ordinary diesel oil calorific value, and flash-point is high by 40%, and price is low by 10%, and consumption saves 24%, safe and reliable, super quality and competitive price, energy-conserving and environment-protective.
Embodiment
One kind of plant firpene oil fuel, the material that comprises following weight percent: containing firpene oil 65-75%, kautschin 26-34%, ignition dope 2-3%, through mixing.
Containing firpene oil, byproduct--the long pinane material while deriving from rosin, turps and firpene production, through the following step, processing forms.
1) dehydration: add Monoethanolamine MEA BASF in long pinane material, addition is 0.3%, stirs 70 minutes, leaves standstill 5 hours, and profit natural layering, emits the moisture content of bottom.
2) neutralization: measure acid number, add Monoethanolamine MEA BASF to neutralize, adjust pH value to 7.0, then stir 60 minutes, leave standstill 4 hours.
3) filter: will long pinane material, deliver to pressure filter and carry out press filtration, remove filter residue, gained is containing firpene oil.
By product when kautschin derives from turps hydration manufacture Terpineol 350, its content is 90-95%.Ignition dope is propyl carbinol, and content is more than 95%.
Each formula of the present invention and performance are as following table:
Plant firpene oil fuel of the present invention and ordinary diesel oil performance comparison table
Plant firpene oil fuel of the present invention and ordinary diesel oil combustion testing contrast table
(3# of engineering department of Yuan Da company steam oven)
Claims (4)
1. a kind of plant firpene oil fuel, is characterized in that the material that comprises following weight percent: containing firpene oil 60-80%, and kautschin 20-40%, ignition dope 1-5%, through mixing.
2. a kind of plant firpene oil fuel according to claim 1, is characterized in that: described containing firpene oil, and byproduct--the long pinane material while deriving from rosin, turps and firpene production, through the following step, processing forms:
1) dehydration: will long pinane material with in pump delivery to the first reactor, add the one in Monoethanolamine MEA BASF, diethanolamine, trolamine, addition is 0.2-0.6%, stir 60-90 minute, then leave standstill 4-6 hour, profit natural layering, emits the moisture content of reactor bottom, then by long pinane mass transport to the second reactor on top;
2) neutralization: measure acid number, add the one in Monoethanolamine MEA BASF, diethanolamine, neutralize, adjust pH value to 6.5-7.5, then stir 40-80 minute, leave standstill 3-5 hour, then be delivered in the 3rd reactor;
3) filter: by the long pinane material in the 3rd reactor, deliver to pressure filter and carry out press filtration, remove filter residue, gained is containing firpene oil.
3. a kind of plant firpene oil fuel according to claim 1, is characterized in that: by product when described kautschin derives from turps hydration manufacture Terpineol 350, its content is 80-95%.
4. a kind of plant firpene oil fuel according to claim 1, is characterized in that: described ignition dope is butanols, and comprise propyl carbinol, isopropylcarbinol, the trimethyl carbinol, sec-butyl alcohol, content is more than 93%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410153832.7A CN104152188B (en) | 2014-04-16 | 2014-04-16 | One kind of plant firpene oil fuel |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410153832.7A CN104152188B (en) | 2014-04-16 | 2014-04-16 | One kind of plant firpene oil fuel |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104152188A true CN104152188A (en) | 2014-11-19 |
| CN104152188B CN104152188B (en) | 2015-09-09 |
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ID=51877820
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410153832.7A Expired - Fee Related CN104152188B (en) | 2014-04-16 | 2014-04-16 | One kind of plant firpene oil fuel |
Country Status (1)
| Country | Link |
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| CN (1) | CN104152188B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106906014A (en) * | 2017-03-31 | 2017-06-30 | 兰州燚能生物科技有限责任公司 | Biological alcohol-based light Fuel flash-point Improve agent |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101353603A (en) * | 2008-09-10 | 2009-01-28 | 刘鹏 | Artificially synthesized fuel oil and production method thereof |
| CN102229823A (en) * | 2011-06-10 | 2011-11-02 | 西安万德科技有限公司 | Terpene isopropyl carbonate gasoline antiknock |
| CN103122263A (en) * | 2013-01-30 | 2013-05-29 | 秦如新 | Fuel additive and clean low-carbon fuel with same |
| CN103415600A (en) * | 2011-03-10 | 2013-11-27 | 国际壳牌研究有限公司 | Improvements relating to gasoline fuel formulations |
-
2014
- 2014-04-16 CN CN201410153832.7A patent/CN104152188B/en not_active Expired - Fee Related
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101353603A (en) * | 2008-09-10 | 2009-01-28 | 刘鹏 | Artificially synthesized fuel oil and production method thereof |
| CN103415600A (en) * | 2011-03-10 | 2013-11-27 | 国际壳牌研究有限公司 | Improvements relating to gasoline fuel formulations |
| CN102229823A (en) * | 2011-06-10 | 2011-11-02 | 西安万德科技有限公司 | Terpene isopropyl carbonate gasoline antiknock |
| CN103122263A (en) * | 2013-01-30 | 2013-05-29 | 秦如新 | Fuel additive and clean low-carbon fuel with same |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106906014A (en) * | 2017-03-31 | 2017-06-30 | 兰州燚能生物科技有限责任公司 | Biological alcohol-based light Fuel flash-point Improve agent |
| CN106906014B (en) * | 2017-03-31 | 2020-09-01 | 兰州燚能生物科技有限责任公司 | Flash point improver for biological alcohol-based light fuel |
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| Publication number | Publication date |
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| CN104152188B (en) | 2015-09-09 |
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Effective date of registration: 20160818 Address after: 526020, Guangdong 40, Duanzhou Province, Zhaoqing Road Star Cui Bridge Company Patentee after: Jiang Caiqing Address before: 526020, No. 15, No. four, village two, Chu Gang Town, Duanzhou District, Guangdong, Zhaoqing Patentee before: ZHAOQING XINDIXIN BIOLOGICAL ENERGY Co.,Ltd. |
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Granted publication date: 20150909 |