CN104130826A - 一种添加红磷阻燃剂的缓蚀型变压器油及其制备方法 - Google Patents
一种添加红磷阻燃剂的缓蚀型变压器油及其制备方法 Download PDFInfo
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- CN104130826A CN104130826A CN201410309124.8A CN201410309124A CN104130826A CN 104130826 A CN104130826 A CN 104130826A CN 201410309124 A CN201410309124 A CN 201410309124A CN 104130826 A CN104130826 A CN 104130826A
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- transformer oil
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- red phosphorus
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- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 title claims abstract description 21
- 238000002360 preparation method Methods 0.000 title claims description 8
- 239000003063 flame retardant Substances 0.000 title abstract description 7
- 238000005260 corrosion Methods 0.000 title abstract description 5
- 230000007797 corrosion Effects 0.000 title abstract description 5
- 230000002401 inhibitory effect Effects 0.000 title abstract 2
- 239000003921 oil Substances 0.000 claims abstract description 61
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 12
- 239000002199 base oil Substances 0.000 claims abstract description 10
- 239000004925 Acrylic resin Substances 0.000 claims abstract description 7
- 229920000178 Acrylic resin Polymers 0.000 claims abstract description 7
- 229910017083 AlN Inorganic materials 0.000 claims abstract description 7
- PIGFYZPCRLYGLF-UHFFFAOYSA-N Aluminum nitride Chemical compound [Al]#N PIGFYZPCRLYGLF-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 7
- 239000012535 impurity Substances 0.000 claims abstract description 4
- 238000002485 combustion reaction Methods 0.000 claims description 17
- 239000003112 inhibitor Substances 0.000 claims description 17
- -1 dodecenylsuccinic acid acid anhydride Chemical class 0.000 claims description 14
- SMWDFEZZVXVKRB-UHFFFAOYSA-N Quinoline Chemical compound N1=CC=CC2=CC=CC=C21 SMWDFEZZVXVKRB-UHFFFAOYSA-N 0.000 claims description 12
- 239000011858 nanopowder Substances 0.000 claims description 12
- 239000000843 powder Substances 0.000 claims description 12
- QELSKZZBTMNZEB-UHFFFAOYSA-N propylparaben Chemical compound CCCOC(=O)C1=CC=C(O)C=C1 QELSKZZBTMNZEB-UHFFFAOYSA-N 0.000 claims description 12
- 230000005764 inhibitory process Effects 0.000 claims description 10
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 9
- 239000000203 mixture Substances 0.000 claims description 7
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 6
- LRHPLDYGYMQRHN-UHFFFAOYSA-N butyl alcohol Substances CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 claims description 6
- 239000004405 propyl p-hydroxybenzoate Substances 0.000 claims description 6
- 235000010232 propyl p-hydroxybenzoate Nutrition 0.000 claims description 6
- 229960003415 propylparaben Drugs 0.000 claims description 6
- 239000000741 silica gel Substances 0.000 claims description 6
- 229910002027 silica gel Inorganic materials 0.000 claims description 6
- 229960001866 silicon dioxide Drugs 0.000 claims description 6
- XMVONEAAOPAGAO-UHFFFAOYSA-N sodium tungstate Chemical compound [Na+].[Na+].[O-][W]([O-])(=O)=O XMVONEAAOPAGAO-UHFFFAOYSA-N 0.000 claims description 6
- NGSFWBMYFKHRBD-UHFFFAOYSA-N sodium;2-hydroxypropanoic acid Chemical compound [Na+].CC(O)C(O)=O NGSFWBMYFKHRBD-UHFFFAOYSA-N 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 6
- 150000003852 triazoles Chemical class 0.000 claims description 6
- 235000019354 vermiculite Nutrition 0.000 claims description 6
- 229910052902 vermiculite Inorganic materials 0.000 claims description 6
- 239000010455 vermiculite Substances 0.000 claims description 6
- 229920002545 silicone oil Polymers 0.000 claims description 4
- AZJQQNWSSLCLJN-UHFFFAOYSA-N 2-ethoxyquinoline Chemical compound C1=CC=CC2=NC(OCC)=CC=C21 AZJQQNWSSLCLJN-UHFFFAOYSA-N 0.000 claims description 3
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 claims description 3
- 238000000498 ball milling Methods 0.000 claims description 3
- PMHQVHHXPFUNSP-UHFFFAOYSA-M copper(1+);methylsulfanylmethane;bromide Chemical compound Br[Cu].CSC PMHQVHHXPFUNSP-UHFFFAOYSA-M 0.000 claims description 3
- 229960000935 dehydrated alcohol Drugs 0.000 claims description 3
- 125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 claims description 3
- 229960004756 ethanol Drugs 0.000 claims description 3
- 239000007788 liquid Substances 0.000 claims description 3
- 239000002245 particle Substances 0.000 claims description 3
- AOHJOMMDDJHIJH-UHFFFAOYSA-N propylenediamine Chemical compound CC(N)CN AOHJOMMDDJHIJH-UHFFFAOYSA-N 0.000 claims description 3
- 239000011347 resin Substances 0.000 claims description 3
- 229920005989 resin Polymers 0.000 claims description 3
- 229910000077 silane Inorganic materials 0.000 claims description 3
- 238000010025 steaming Methods 0.000 claims description 3
- WVRNUXJQQFPNMN-VAWYXSNFSA-N 3-[(e)-dodec-1-enyl]oxolane-2,5-dione Chemical compound CCCCCCCCCC\C=C\C1CC(=O)OC1=O WVRNUXJQQFPNMN-VAWYXSNFSA-N 0.000 abstract 2
- OSASVXMJTNOKOY-UHFFFAOYSA-N chlorobutanol Chemical compound CC(C)(O)C(Cl)(Cl)Cl OSASVXMJTNOKOY-UHFFFAOYSA-N 0.000 abstract 2
- 230000003647 oxidation Effects 0.000 abstract 2
- 238000007254 oxidation reaction Methods 0.000 abstract 2
- HNVIQLPOGUDBSU-UHFFFAOYSA-N 2,6-dimethylmorpholine Chemical compound CC1CNCC(C)O1 HNVIQLPOGUDBSU-UHFFFAOYSA-N 0.000 abstract 1
- CYDQOEWLBCCFJZ-UHFFFAOYSA-N 4-(4-fluorophenyl)oxane-4-carboxylic acid Chemical compound C=1C=C(F)C=CC=1C1(C(=O)O)CCOCC1 CYDQOEWLBCCFJZ-UHFFFAOYSA-N 0.000 abstract 1
- QRUDEWIWKLJBPS-UHFFFAOYSA-N benzotriazole Chemical compound C1=CC=C2N[N][N]C2=C1 QRUDEWIWKLJBPS-UHFFFAOYSA-N 0.000 abstract 1
- 239000012964 benzotriazole Substances 0.000 abstract 1
- 229960004926 chlorobutanol Drugs 0.000 abstract 1
- 125000000753 cycloalkyl group Chemical group 0.000 abstract 1
- 230000002035 prolonged effect Effects 0.000 abstract 1
- 229940005581 sodium lactate Drugs 0.000 abstract 1
- 235000011088 sodium lactate Nutrition 0.000 abstract 1
- 239000001540 sodium lactate Substances 0.000 abstract 1
- 239000000295 fuel oil Substances 0.000 description 4
- 238000009413 insulation Methods 0.000 description 4
- 150000003071 polychlorinated biphenyls Chemical group 0.000 description 3
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 description 2
- 230000015556 catabolic process Effects 0.000 description 2
- NBVXSUQYWXRMNV-UHFFFAOYSA-N fluoromethane Chemical compound FC NBVXSUQYWXRMNV-UHFFFAOYSA-N 0.000 description 2
- 230000003245 working effect Effects 0.000 description 2
- 150000001336 alkenes Chemical class 0.000 description 1
- 230000000711 cancerogenic effect Effects 0.000 description 1
- 239000003990 capacitor Substances 0.000 description 1
- 231100000315 carcinogenic Toxicity 0.000 description 1
- 238000005352 clarification Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000001934 delay Effects 0.000 description 1
- 230000003111 delayed effect Effects 0.000 description 1
- 238000007598 dipping method Methods 0.000 description 1
- 238000006073 displacement reaction Methods 0.000 description 1
- KWKXNDCHNDYVRT-UHFFFAOYSA-N dodecylbenzene Chemical compound CCCCCCCCCCCCC1=CC=CC=C1 KWKXNDCHNDYVRT-UHFFFAOYSA-N 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 230000007096 poisonous effect Effects 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
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CN201410309124.8A CN104130826B (zh) | 2014-07-02 | 2014-07-02 | 一种添加红磷阻燃剂的缓蚀型变压器油及其制备方法 |
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CN201410309124.8A CN104130826B (zh) | 2014-07-02 | 2014-07-02 | 一种添加红磷阻燃剂的缓蚀型变压器油及其制备方法 |
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Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105296100A (zh) * | 2015-10-22 | 2016-02-03 | 铜陵三佳变压器有限责任公司 | 一种高燃点变压器油 |
CN105296099A (zh) * | 2015-10-22 | 2016-02-03 | 铜陵三佳变压器有限责任公司 | 一种稳定性高的变压器油 |
CN107201264A (zh) * | 2017-06-07 | 2017-09-26 | 合肥励仙电力工程有限公司 | 一种高稳定性导热阻燃变压器用油及其制备方法 |
CN107312603A (zh) * | 2017-07-12 | 2017-11-03 | 合肥轻风飏电气科技有限责任公司 | 一种绝缘消弧纳米材料改性变压器油及其制备方法 |
CN111286396A (zh) * | 2020-03-30 | 2020-06-16 | 国网湖南省电力有限公司 | 改性高燃点变压器油及其制备方法 |
CN113150853A (zh) * | 2021-03-24 | 2021-07-23 | 西南大学 | 一种APTES表面改性纳米SiO2绝缘油的制备方法 |
CN115851336A (zh) * | 2022-11-30 | 2023-03-28 | 清华大学 | 紫磷晶体及其制备方法与应用、润滑油及其制备方法与应用 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20120172641A1 (en) * | 2009-08-10 | 2012-07-05 | Chevron U.S.A. Inc. | Base oil having high kinematic viscosity and low pour point |
CN102660363A (zh) * | 2012-05-23 | 2012-09-12 | 上海中孚特种油品有限公司 | 一种变压器油及其制备方法 |
CN103113963A (zh) * | 2013-01-29 | 2013-05-22 | 安徽凯奥润滑油科技有限公司 | 一种超高压变压器油及其生产工艺 |
-
2014
- 2014-07-02 CN CN201410309124.8A patent/CN104130826B/zh active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20120172641A1 (en) * | 2009-08-10 | 2012-07-05 | Chevron U.S.A. Inc. | Base oil having high kinematic viscosity and low pour point |
CN102660363A (zh) * | 2012-05-23 | 2012-09-12 | 上海中孚特种油品有限公司 | 一种变压器油及其制备方法 |
CN103113963A (zh) * | 2013-01-29 | 2013-05-22 | 安徽凯奥润滑油科技有限公司 | 一种超高压变压器油及其生产工艺 |
Cited By (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105296100A (zh) * | 2015-10-22 | 2016-02-03 | 铜陵三佳变压器有限责任公司 | 一种高燃点变压器油 |
CN105296099A (zh) * | 2015-10-22 | 2016-02-03 | 铜陵三佳变压器有限责任公司 | 一种稳定性高的变压器油 |
CN107201264A (zh) * | 2017-06-07 | 2017-09-26 | 合肥励仙电力工程有限公司 | 一种高稳定性导热阻燃变压器用油及其制备方法 |
CN107312603A (zh) * | 2017-07-12 | 2017-11-03 | 合肥轻风飏电气科技有限责任公司 | 一种绝缘消弧纳米材料改性变压器油及其制备方法 |
CN111286396A (zh) * | 2020-03-30 | 2020-06-16 | 国网湖南省电力有限公司 | 改性高燃点变压器油及其制备方法 |
CN111286396B (zh) * | 2020-03-30 | 2022-06-21 | 国网湖南省电力有限公司 | 改性高燃点变压器油及其制备方法 |
CN113150853A (zh) * | 2021-03-24 | 2021-07-23 | 西南大学 | 一种APTES表面改性纳米SiO2绝缘油的制备方法 |
CN115851336A (zh) * | 2022-11-30 | 2023-03-28 | 清华大学 | 紫磷晶体及其制备方法与应用、润滑油及其制备方法与应用 |
CN115851336B (zh) * | 2022-11-30 | 2023-08-18 | 清华大学 | 紫磷晶体及其制备方法与应用、润滑油及其制备方法与应用 |
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Effective date of registration: 20230105 Address after: 314500 2 buildings, 1680 development road, Wutong street, Tongxiang, Jiaxing, Zhejiang Patentee after: Baozhichuan Electrical Equipment Co.,Ltd. Address before: 314500 1 buildings, 1680 development road, Wutong street, Tongxiang, Jiaxing, Zhejiang Patentee before: Jiaxing Ping'an Electrical Engineering Co.,Ltd. |