CN104073058B - Method for plastic soft package water-based intaglio printing ink - Google Patents
Method for plastic soft package water-based intaglio printing ink Download PDFInfo
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- CN104073058B CN104073058B CN201410335422.4A CN201410335422A CN104073058B CN 104073058 B CN104073058 B CN 104073058B CN 201410335422 A CN201410335422 A CN 201410335422A CN 104073058 B CN104073058 B CN 104073058B
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- deionized water
- resin liquid
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 56
- 229920003023 plastic Polymers 0.000 title claims abstract description 9
- 239000004033 plastic Substances 0.000 title claims abstract description 9
- 238000000034 method Methods 0.000 title abstract 6
- 239000007788 liquid Substances 0.000 claims abstract description 25
- 239000011347 resin Substances 0.000 claims abstract description 24
- 229920005989 resin Polymers 0.000 claims abstract description 24
- 238000005576 amination reaction Methods 0.000 claims abstract description 10
- 239000004925 Acrylic resin Substances 0.000 claims abstract description 8
- 229920000178 Acrylic resin Polymers 0.000 claims abstract description 8
- 238000004519 manufacturing process Methods 0.000 claims abstract description 7
- 239000002904 solvent Substances 0.000 claims abstract description 6
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims abstract description 5
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 27
- 239000008367 deionised water Substances 0.000 claims description 21
- 229910021641 deionized water Inorganic materials 0.000 claims description 21
- HZAXFHJVJLSVMW-UHFFFAOYSA-N 2-Aminoethan-1-ol Chemical compound NCCO HZAXFHJVJLSVMW-UHFFFAOYSA-N 0.000 claims description 15
- 239000000463 material Substances 0.000 claims description 13
- 238000002360 preparation method Methods 0.000 claims description 13
- 239000013530 defoamer Substances 0.000 claims description 11
- 239000002270 dispersing agent Substances 0.000 claims description 11
- 238000011017 operating method Methods 0.000 claims description 11
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 9
- 235000021388 linseed oil Nutrition 0.000 claims description 8
- 239000000944 linseed oil Substances 0.000 claims description 8
- 239000006185 dispersion Substances 0.000 claims description 7
- 239000002002 slurry Substances 0.000 claims description 7
- 239000000843 powder Substances 0.000 claims description 5
- 229920003015 aliphatic polyurethane dispersion Polymers 0.000 claims description 4
- 239000000839 emulsion Substances 0.000 claims description 4
- 239000000049 pigment Substances 0.000 claims description 4
- 229920002635 polyurethane Polymers 0.000 claims description 4
- 239000004814 polyurethane Substances 0.000 claims description 4
- 239000004334 sorbic acid Substances 0.000 claims description 4
- ARXJGSRGQADJSQ-UHFFFAOYSA-N 1-methoxypropan-2-ol Chemical compound COCC(C)O ARXJGSRGQADJSQ-UHFFFAOYSA-N 0.000 claims description 3
- 238000009826 distribution Methods 0.000 claims description 3
- 238000000227 grinding Methods 0.000 claims description 3
- 239000006210 lotion Substances 0.000 claims description 3
- 239000004576 sand Substances 0.000 claims description 3
- 238000005406 washing Methods 0.000 claims description 3
- 229920002472 Starch Polymers 0.000 claims description 2
- 235000019698 starch Nutrition 0.000 claims description 2
- 238000001035 drying Methods 0.000 abstract description 8
- 239000002966 varnish Substances 0.000 abstract 3
- 239000000853 adhesive Substances 0.000 abstract 1
- 230000001070 adhesive effect Effects 0.000 abstract 1
- 239000002131 composite material Substances 0.000 abstract 1
- 229920000058 polyacrylate Polymers 0.000 abstract 1
- 238000012360 testing method Methods 0.000 description 4
- 239000011248 coating agent Substances 0.000 description 3
- 238000000576 coating method Methods 0.000 description 3
- 238000004806 packaging method and process Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- IAFBRPFISOTXSO-UHFFFAOYSA-N 2-[[2-chloro-4-[3-chloro-4-[[1-(2,4-dimethylanilino)-1,3-dioxobutan-2-yl]diazenyl]phenyl]phenyl]diazenyl]-n-(2,4-dimethylphenyl)-3-oxobutanamide Chemical compound C=1C=C(C)C=C(C)C=1NC(=O)C(C(=O)C)N=NC(C(=C1)Cl)=CC=C1C(C=C1Cl)=CC=C1N=NC(C(C)=O)C(=O)NC1=CC=C(C)C=C1C IAFBRPFISOTXSO-UHFFFAOYSA-N 0.000 description 1
- 244000283207 Indigofera tinctoria Species 0.000 description 1
- 229920006243 acrylic copolymer Polymers 0.000 description 1
- 239000005030 aluminium foil Substances 0.000 description 1
- 239000006229 carbon black Substances 0.000 description 1
- 239000011111 cardboard Substances 0.000 description 1
- 229920001577 copolymer Polymers 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000010977 jade Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000000123 paper Substances 0.000 description 1
- 239000011087 paperboard Substances 0.000 description 1
- 239000002985 plastic film Substances 0.000 description 1
- 229920006255 plastic film Polymers 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
Landscapes
- Inks, Pencil-Leads, Or Crayons (AREA)
- Paints Or Removers (AREA)
Abstract
The invention relates to a method for plastic soft package water-based intaglio printing ink. The method comprises the following steps: (1) preparing water-based resin liquid; (2) preparing water-based ink color paste; (3) preparing water-based varnish; (4) preparing water-based ink. As the method adopts the amination of modified acrylic polymer water-based acrylic resin SR-630 to prepare the water-based resin liquid; then, the water-based resin liquid is utilized to prepare the water-based ink color paste and the water-based varnish respectively; the plastic soft package water-based intaglio printing ink is prepared through mixing the water-based ink color paste with the water-based varnish according to the required water-based ink. The method has the advantages that the technological requirements are low, the production efficiency is high, and the quality of products is stable; the printing ink produced by the method is the most ideal substitute for solvent-based ink because of the advantages of the ink, such as light smell, good drying balance equality, excellent drying speed, bright color, good glossiness, excellent adhesive force and excellent composite strength.
Description
Technical field
The present invention relates to a kind of production method of plastic flexible package aqueous intaglio printing ink.
Background technology
Solvent type ink is traditional ink, has technical maturity, the advantages such as steady quality.But the pollution of its volatile matter to environment and the harm to HUMAN HEALTH serious.The development of current water color ink is maked rapid progress, and is comprising on paper, cardboard, paperboard, plastics film, the multiple base material of aluminium foil and can print.But still there is the shortcomings such as rate of drying is slow, quality stability is poor for the water-base gravure ink of plastic film printing.
Summary of the invention
The object of the present invention is to provide a kind of smell little, desiccated balance and rate of drying good, bright in colour, glossiness is good, the production method of the plastic flexible package aqueous intaglio printing ink of sticking power and combined strength bination excellence.
The present invention, its step comprises following operation:
(1) preparation of water-base resin liquid: formula: water-borne acrylic resin SR-630 35-38wt%; Deionized water 48-52 wt%; Ethanol 4 wt%; Monoethanolamine MEA BASF 8-12 wt%; Defoamer 1 wt%; Add up to 100 wt%, operating procedure: first deionized water, alcohol solvent are dropped in reactor in proportion, water-borne acrylic resin is slowly dropped in unlatching dispersion machine and heat riser, dispersion limit, limit, disperse after temperature rises to 65 DEG C, slowly to drip Monoethanolamine MEA BASF in 20 minutes, carry out resin constant temperature amination reaction, amination two hours;
(2) preparation of water color ink mill base: formula: water-base resin liquid 30-35 wt%; Deionized water A20.5-25.5 wt%; Ethylene glycol 4 wt%; Monoethanolamine MEA BASF 10 wt%; Water-borne wax starches 0.5 wt%; Aqueous dispersant 0.3-0.5 wt%; Pigment powder 25 wt%; Defoamer 0.3 wt%; Deionized water B4.4 wt%; Add up to 100 wt%, operating procedure: water-base resin liquid, deionized water A, ethylene glycol, Monoethanolamine MEA BASF, water-borne wax slurry and aqueous dispersant are dropped in Scattered Kettle, disperse within 10 minutes, slowly to drop into powder colo(u)rant dispersion again to wash out after 30 minutes, Scattered Kettle is gone to sand mill and carry out material grinding distribution, finally wash machine and Scattered Kettle with deionized water B, washing lotion is poured in material and is mixed;
(3) preparation of water-based stand linseed oil: formula: water-base resin liquid 5-6 wt%; NeoCeylA-1120 ACRYLIC EMULSION 62-68 wt%; NeoPac E-200 polyurethane acroleic acid 15-18 wt%; Propylene glycol monomethyl ether 3 wt%; Monoethanolamine MEA BASF 2 wt%; W-18 aqueous dispersant 0.5 wt%; NeoRez R-650 aliphatic polyurethane dispersion liquid 2 wt%; W-0506 defoamer 0.2 wt%; Deionized water 4 wt%; Ethylene glycol 3 wt%; Add up to: 100 wt%, operating procedure: material is dropped in Scattered Kettle and is uniformly dispersed;
(4) preparation of water color ink: formula: water-based stand linseed oil 60-70 wt%; Water color ink mill base 30-40 wt%, adds up to: 100 wt%, operating procedure: dropped in Scattered Kettle by material and be uniformly dispersed.
The present invention, water-base resin liquid is obtained owing to adopting the acrylate copolymer water-borne acrylic resin SR-630 amination of modification, and then by water-base resin liquid obtained water color ink mill base and water-based stand linseed oil respectively, again according to required water color ink, gained is allocated by water color ink mill base and water-based stand linseed oil, there is processing requirement low, the advantages such as production efficiency is high, constant product quality.The ink produced by it, smell is little, desiccated balance and rate of drying good, bright in colour, glossiness is good, sticking power and combined strength bination excellent, be the optimal substitute of solvent type ink.
Embodiment
A production method for plastic flexible package aqueous intaglio printing ink, its step comprises following operation:
(1) preparation of water-base resin liquid: formula (wt%, lower same):
Water-borne acrylic resin SR-630 35-38;
Deionized water 48-52;
Ethanol 4;
Monoethanolamine MEA BASF 8-12;
Defoamer 1;
Add up to: 100.
Preparation method: first deionized water, alcohol solvent are dropped in reactor in proportion, Alkali-soluble acrylic's copolymer resins is slowly dropped on unlatching dispersion machine and heat riser, dispersion limit, limit, disperse after temperature rises to 65 DEG C, slowly to drip Monoethanolamine MEA BASF in 20 minutes, carry out resin constant temperature amination reaction, amination two hours, the pH value of aminated resin liquid is constantly detected during amination, the pH value of resin liquid is controlled between 9.0-9.5, carries out detecting, filtering and packaging after qualified after resin dissolves safety and pH value amination up to standard complete.
Testing index:
Outward appearance: colourless transparent liquid;
Viscosity: 65-90 " (25 DEG C, coating No. 4 cups);
PH value: 9.0-9.5;
Solid content: 35-38%.
(2) preparation of water color ink mill base: formula:
Yellow red blue-black
Water-base resin liquid 33 30 35 35;
Deionized water A 22.5 25.5 20.5 20.5;
Ethylene glycol 4444;
Monoethanolamine MEA BASF 10 10 10 10;
Water-borne wax slurry 0.5 0.5 0.5 0.5;
Aqueous dispersant W-18 0.3 0.3 0.3 0.3;
P-Y-12 diarylide yellow 25;
P-R-21 red 25;
PB15:3 indigo plant 25;
Colour carbon black 25;
Defoamer 0.3 0.3 0.3 0.3;
Deionized water B 4.4 4.4 4.4 4.4;
Add up to: 100 100 100 100.
Operating procedure: water-base resin liquid, deionized water A, ethylene glycol, Monoethanolamine MEA BASF, water-borne wax slurry and aqueous dispersant are dropped in Scattered Kettle, disperse within 10 minutes, slowly to drop into again after pigment powder disperses 30 minutes and wash out, Scattered Kettle is gone to sand mill and carry out material grinding distribution, finally wash machine and Scattered Kettle with deionized water B, washing lotion is poured in material and is mixed.
Testing index:
Form and aspect: approximate test;
Depth of shade: 95-110%;
Fineness :≤10 μ;
PH value: 8.5-9.0.
(3) preparation of water-based stand linseed oil: formula:
Water-base resin liquid 5;
NeoCeylA-1120 ACRYLIC EMULSION 65;
NeoPac E-200 polyurethane acroleic acid 15.3;
Propylene glycol monomethyl ether 3;
Monoethanolamine MEA BASF 2;
Aqueous dispersant W-18 0.5;
NeoRez R-650 aliphatic polyurethane dispersion liquid 2;
Defoamer W-0506 0.2;
Deionized water 4;
Ethylene glycol 3;
Add up to: 100.
Operating procedure: material is dropped into censorship packaging after being uniformly dispersed in Scattered Kettle.
Testing index:
Outward appearance: milky white liquid;
Viscosity: 25-30 " (25 DEG C, coating No. 4 cups).
(4) preparation of water color ink: formula:
Yellow red blue-black;
Water-based stand linseed oil 70 60 62 60;
Yellow pulp 30;
Red slurry 40;
Blue slurry 38;
Black slurry 40;
Add up to: 100 100 100 100.
Operating procedure: material is dropped into censorship after being uniformly dispersed in Scattered Kettle.
The yellow red blue-black of standard;
Fineness≤10≤10≤10≤10≤10;
Viscosity (being coated with 4 glasss 25 DEG C) 20 "-30 " 25 " 27 " 22 " 20 ";
Form and aspect are up to standard to standard color sample;
Depth of shade 95-110% is up to standard;
Sticking power >=95 do not come off up to standard;
First dryness 3 '-5 ' 3 ' 20 " 4 ' 35 " 3 ' 58 " 4 ' 52 ";
Thorough dryness 8 '-12 ' 8 ' 50 " 11 ' 12 " 10 ' 27 " 11 ' 43 ".
Note: 1, fineness adopts the Hegman grind gage of 0-50mm range to measure;
2, viscosity measures when adopting 25 DEG C, domestic coating No. 4 cups;
3, form and aspect and survey concentration are range estimation;
4, sticking power is that the wide pulling force belt of employing 1 centimetre is measured;
5, rate of drying adopts the Hegman grind gage of double flute 0-100MM range to measure, and the standard of first dryness is the time of drying of 0-50MM; Thorough dryness is the time of drying of 0-100MM.
In the present invention, water-borne acrylic resin SR-630 can Trade Co., Ltd. be provided by Qingdao beautiful jade; Defoamer adopts the defoamer W-0506 provided by Taiwan De Qian chemical company; The aqueous dispersant W-18 that aqueous dispersant adopts Taiwan De Qian chemical company to provide; NeoCeylA-1120 ACRYLIC EMULSION, NeoPac E-200 polyurethane acroleic acid and NeoRez R-650 aliphatic polyurethane dispersion liquid are provided by Wei Laihui south group company.
Claims (1)
1. a production method for plastic flexible package aqueous intaglio printing ink, its step comprises following operation:
(1) preparation of water-base resin liquid: formula: water-borne acrylic resin SR-630 35-38wt%; Deionized water 48-52 wt%; Ethanol 4 wt%; Monoethanolamine MEA BASF 8-12 wt%; Defoamer 1 wt%; Add up to 100 wt%, operating procedure: first deionized water, alcohol solvent are dropped in reactor in proportion, water-borne acrylic resin SR-630 is slowly dropped on unlatching dispersion machine and heat riser, dispersion limit, limit, disperse after temperature rises to 65 DEG C, slowly to drip Monoethanolamine MEA BASF in 20 minutes, carry out resin constant temperature amination reaction, amination two hours;
(2) preparation of water color ink mill base: formula: the water-base resin liquid 30-35 wt% prepared by operation (1); Deionized water A20.5-25.5 wt%; Ethylene glycol 4 wt%; Monoethanolamine MEA BASF 10 wt%; Water-borne wax starches 0.5 wt%; Aqueous dispersant 0.3-0.5 wt%; Pigment powder 25 wt%; Defoamer 0.3 wt%; Deionized water B4.4 wt%; Add up to 100 wt%, operating procedure: water-base resin liquid, deionized water A, ethylene glycol, Monoethanolamine MEA BASF, water-borne wax slurry and aqueous dispersant are dropped in Scattered Kettle, disperse within 10 minutes, slowly to drop into again after pigment powder disperses 30 minutes and wash out, Scattered Kettle is gone to sand mill and carry out material grinding distribution, finally wash machine and Scattered Kettle with deionized water B, washing lotion is poured in material and is mixed;
(3) preparation of water-based stand linseed oil: formula: the water-base resin liquid 5-6 wt% prepared by operation (1); NeocrylA-1120 ACRYLIC EMULSION 62-68 wt%; NeoPac E-200 polyurethane acroleic acid 15-18 wt%; Propylene glycol monomethyl ether 3 wt%; Monoethanolamine MEA BASF 2 wt%; W-18 aqueous dispersant 0.5 wt%; NeoRez R-650 aliphatic polyurethane dispersion liquid 2 wt%; W-0506 defoamer 0.2 wt%; Deionized water 4 wt%; Ethylene glycol 3 wt%; Add up to: 100 wt%, operating procedure: material is dropped in Scattered Kettle and is uniformly dispersed;
(4) preparation of water color ink: formula: the water-based stand linseed oil 60-70 wt% prepared by operation (3); Water color ink mill base 30-40 wt% prepared by operation (2), adds up to: 100 wt%, operating procedure: dropped in Scattered Kettle by material and be uniformly dispersed.
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| CN201410335422.4A CN104073058B (en) | 2014-07-15 | 2014-07-15 | Method for plastic soft package water-based intaglio printing ink |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410335422.4A CN104073058B (en) | 2014-07-15 | 2014-07-15 | Method for plastic soft package water-based intaglio printing ink |
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| CN104073058A CN104073058A (en) | 2014-10-01 |
| CN104073058B true CN104073058B (en) | 2015-07-08 |
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Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104672982A (en) * | 2015-03-15 | 2015-06-03 | 随州市三庆水性印刷材料有限公司 | Preparation method of environmentally-friendly water-based ink |
| CN104804521A (en) * | 2015-04-24 | 2015-07-29 | 郭小曼 | Toning process of ink for environment-friendly water-based paint |
| CN104987773A (en) * | 2015-07-17 | 2015-10-21 | 合肥忠豪新材料有限公司 | Environment-friendly water-based printing ink and preparation method thereof |
| CN105111818A (en) * | 2015-07-21 | 2015-12-02 | 漳州市芳远印务有限公司 | Tangle film with excellent printing adhesion |
| CN107922763B (en) * | 2015-09-18 | 2021-05-14 | 株式会社新克 | Water-based gravure ink |
| CN107177234A (en) * | 2017-06-23 | 2017-09-19 | 福建东南艺术纸品股份有限公司 | A kind of ink and its production technology |
| CN108546452A (en) * | 2018-04-17 | 2018-09-18 | 中山创美涂料有限公司 | A kind of aqueous gravure Yellow ink of flexible PVC decorating film and preparation method thereof |
| CN109321030B (en) * | 2018-11-07 | 2021-12-07 | 顾洪杰 | Water-based plastic inner printing ink and water-based plastic surface printing ink |
| CN110760221A (en) * | 2019-12-12 | 2020-02-07 | 惠州德斯坤化工有限公司 | Water-based plastic gravure ink and preparation method thereof |
| CN111500113B (en) * | 2020-06-05 | 2022-04-19 | 杭州海维特化工科技有限公司 | Copper plate paper gravure water-based ink and preparation method thereof |
| CN112812684A (en) * | 2020-12-31 | 2021-05-18 | 惠州乐印水性科技有限公司 | Varnish and ink for gravure printing with same |
| CN112778825A (en) * | 2020-12-31 | 2021-05-11 | 惠州乐印水性科技有限公司 | Ink for gravure printing and preparation method thereof |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH10152639A (en) * | 1996-11-25 | 1998-06-09 | Toyo Ink Mfg Co Ltd | Water-base printing ink |
| JP4469479B2 (en) * | 2000-09-14 | 2010-05-26 | 中央理化工業株式会社 | Aqueous emulsion resin composition |
| CN101029194B (en) * | 2006-02-28 | 2010-08-04 | 北京英科凡化工产品有限公司 | Plastic-film water intaglio printing ink |
| CN101134864A (en) * | 2007-10-15 | 2008-03-05 | 山西精华科工贸有限公司 | Cigarette label high-speed intaglio printing water-based ink |
| CN101429359A (en) * | 2008-12-08 | 2009-05-13 | 山西鹰鲲科技有限公司 | Water-based plastic composite inner-printing ink |
| CN101717596B (en) * | 2009-12-08 | 2012-05-23 | 湖州杭华油墨科技有限公司 | Water-based ink for package printing of high-adhesion film and manufacturing method thereof |
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Address after: 515561, Guangdong, Jieyang Airport Economic Zone, Jieyang Town, Mei Hua Village Network Hill Applicant after: JIEDONG COUNTY FUDE PRINTING MATERIAL CO.,LTD. Address before: 515561, Jieyang City, Guangdong province Jiedong County town of Huamei village network Hill Applicant before: JIEDONG COUNTY FUDE PRINTING MATERIAL Co.,Ltd. |
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Effective date of registration: 20181217 Address after: 521000 Zhongshan (Chaozhou) Industrial Transfer Park, Xiangqiao District, Chaozhou City, Guangdong Province, northeast of Fengquan Road, South Branch of the Industrial Park Path (JN07-16-3-2 Block) Patentee after: GUANGDONG FUTE CHEMICAL Co.,Ltd. Address before: 515561 Huamei Village Netshan, Didu Town, Jieyang Airport Economic Zone, Jieyang City, Guangdong Province Patentee before: JIEDONG COUNTY FUDE PRINTING MATERIAL CO.,LTD. |
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Address after: 521000 northeast of Fengquan Road, Jingnan sub Park, Zhongshan (Chaozhou) industrial transfer park, Chaozhou City, Guangdong Province (plot jn07-16-3-2) Patentee after: Guangdong Fude Industrial Co.,Ltd. Address before: 521000 Zhongshan (Chaozhou) Industrial Transfer Park, Xiangqiao District, Chaozhou City, Guangdong Province, northeast of Fengquan Road, South Branch of the Industrial Park Path (JN07-16-3-2 Block) Patentee before: GUANGDONG FUTE CHEMICAL Co.,Ltd. |