CN104042449B - A kind of hydrogel mask sheet of high-temperature stable - Google Patents
A kind of hydrogel mask sheet of high-temperature stable Download PDFInfo
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Abstract
A hydrogel mask sheet for high-temperature stable, comprises carrier screen cloth and hydrogel; Described hydrogel is grouped into by the one-tenth of following percentage by weight: 0.1%-1% cellulose derivative water-soluble polymer, 0.5%-2% Sargassum extracts the natural water-soluble copolymer of class, the natural water-soluble copolymer of the extracellular polysaccharide class that 0.1%-2% fermentable generates, the natural water-soluble copolymer that 0.1%-2% plant seed or root extract, 0.1%-2% causes crosslinked required electrolyte; 0.5%-5% skin conditioning agent; 0.1%-1% Percutaneous absorption enhancer, 5%-20% polyalcohols, 0.1%-1% antiseptic, surplus pure water.High-temperature stable hydrogel mask sheet meets the requirement about mask physical and chemical index in People's Republic of China's light industry standard " QB-T2872-2007 facial film ".Hydrogel, on carrier screen cloth, keeps stable in the temperature range of-15 DEG C ~ 55 DEG C, improves the stability of product in transport and storage.
Description
Technical field:
This patent belongs to cosmetic field, is specifically related to a kind of hydrogel mask sheet and production technology thereof of high-temperature stable.
Background technology
At present with the hydrophilic hydrogel facial film that natural polymer cross linked polymer makes, because of its have that transparency is good, high, the moisture advantage such as abundant of All Pure Nature, safety and be more and more subject to the welcome of consumer.
Patent 200480023378.8 mentions thermally sensitive state-changing hydrogel composition and production method thereof, and this hydrogel is transformed into fluid state, because body temperature is transformed into fluid state when in contact skin at 10 DEG C ~ 50 DEG C.
Patent 201210485804.6 mentions a kind of temperature-sensitive hydrogel that can be used as nourishing pack and preparation method thereof, this hydrogel is temperature-sensitive hydrogel, and in 10 DEG C ~ 50 DEG C temperature ranges, this hydrogel is with the rising of temperature, its water suction saturation reduces, and moisture is from the release of gel inside.
According to the requirement about mask physical and chemical index in People's Republic of China's light industry standard " QB-T 2872-2007 facial film ", the text is as follows: heat-resisting, and (40 ± 1) DEG C keep 24h, no significant difference front with test after recovering room temperature; (-5 DEG C ~-10 DEG C) keep 24h, no significant difference front with experiment after recovering room temperature.Facial film a lot of hydrogel facial film of present stage circulation can not reach the middle requirement about " heat-resisting; (40 ± 1) DEG C keep 24h, no significant difference front with test after recovering room temperature " introduced of People's Republic of China's light industry standard " QB-T 2872-2007 facial film ".
Summary of the invention:
Object of the present invention is for the deficiencies in the prior art part, there is provided a kind of hydrogel mask sheet and production technology thereof of high-temperature stable, this high-temperature stable hydrogel mask sheet meets the requirement about mask physical and chemical index in People's Republic of China's light industry standard " QB-T 2872-2007 facial film ".
In order to realize the above object, a kind of hydrogel mask sheet of high-temperature stable, comprises carrier screen cloth and hydrogel; Described hydrogel is grouped into by the one-tenth of following percentage by weight:
0.1%-1% cellulose derivative water-soluble polymer, described cellulose derivative water-soluble polymer is one or several in sodium carboxymethyl cellulose, hydroxyethyl-cellulose and hydroxypropyl emthylcellulose;
0.5%-2% Sargassum extracts the natural water-soluble copolymer of class, the natural water-soluble copolymer that described Sargassum extracts class refer in carrageenan, sodium alginate, agar one or several;
The natural water-soluble copolymer of extracellular polysaccharide class that 0.1%-2% fermentable generates, the natural water-soluble copolymer of the extracellular polysaccharide class that described fermentable generates refer in xanthan gum, gellan gum one or several;
The natural water-soluble copolymer that 0.1%-2% plant seed or root extract, the natural water-soluble copolymer that described plant seed or root extract is one or several in guar gum, algaroba glue, Rhizoma amorphophalli root powder;
0.1%-2% causes crosslinked required electrolyte, described initiation be cross-linked that required electrolyte refers in potassium chloride, calcium chloride, sodium chloride, aluminum chloride one or several;
0.5%-5% skin conditioning agent, described skin conditioning agent refer in allantoin, hyaluronate sodium, Limax secretions filtrate, Aloe extraction solution, Flos Lonicerae extractive solution one or several;
0.1%-1% Percutaneous absorption enhancer, described Percutaneous absorption enhancer refer in tween 20, hydrolecithin, azone one or several;
5%-20% polyalcohols, described polyalcohols is one or several in glycerol, 1,3-PD, 1,3 butylene glycol;
0.1%-1% antiseptic, described antiseptic comprise in methyl hydroxybenzoate, propylparaben, DMDMH, phenoxyethanol, two imidazolidinyl urea one or several;
Surplus pure water.
The hydrogel mask sheet of described a kind of high-temperature stable, its special character is: the manufacture method of described hydrogel facial mask liquid comprises the following steps:
(1) prepare burden:
By 0.1%-1% cellulose derivative water-soluble polymer, 0.5%-2% Sargassum extracts the natural water-soluble copolymer of class, the natural water-soluble copolymer of the extracellular polysaccharide class that 0.1%-2% fermentable generates, the natural water-soluble copolymer that 0.1%-2% plant seed or root extract, 5%-20% polyalcohols, use bucket mix homogeneously, make uniform dispersion liquid; Then put in pure water, be heated to 85 DEG C, stir, then add 0.1%-2% and cause crosslinked required electrolyte, 0.5%-5% skin conditioning agent, 0.1%-1% Percutaneous absorption enhancer and 0.1%-1% antiseptic, be made into the hydrogel of temperature at the fluid state of 60 DEG C ~ 85 DEG C;
(2) be coated with:
The temperature that step (1) is obtained the fluid state of 60 DEG C ~ 85 DEG C hydrogel by hydrogel facial mask machine coating, compacting, make gel infiltration enter screen cloth, cooling after and screen cloth form gel slice, then utilize cutting die excision forming.
The hydrogel mask sheet of described a kind of high-temperature stable, its special character is: described hydrogel, on carrier screen cloth, keeps stable in the temperature range of-15 DEG C ~ 55 DEG C, improves the stability of product in transport and storage.
The hydrogel mask sheet of described a kind of high-temperature stable, its special character is: when described hydrogel mask sheet and contact skin, wherein contained skin conditioning agent rapid osmotic can enter skin due to the effect of Percutaneous absorption enhancer, reaches the effect of conditioning skin.
The natural water-soluble copolymer that the natural water-soluble copolymer of the extracellular polysaccharide class that described cellulose derivative water-soluble polymer, Sargassum extract the natural water-soluble copolymer of class, fermentable generates, plant seed or root extract is the base portion of this patent, and it is the collaborative carrier part forming hydrogel facial film mutually.
Wherein the cellulose derivative water-soluble polymer structure that hydrogel can be made to be formed is more fluffy, prevent hydrogel at low temperature (-15 DEG C) the larger ice crystal of generation by bursting by freezing, the hydrogel adding cellulose derivative water-soluble polymer forms finer and smoother ice crystal when low temperature (-15 DEG C), improves the low-temperature stability of product.
Crosslinked required electrolytical amount is caused by regulating, the gelling temp of hydrogel can be controlled, when causing crosslinked required electrolytical content at 0.1%-2%, the gelling temp of hydrogel is greater than 50 DEG C, if deviate from above-mentioned scope, gelling temp by < 50 DEG C, or can not form gel.
0.5%-5% skin conditioning agent, the skin conditioning agent told refer in allantoin, hyaluronate sodium, Limax secretions filtrate, Aloe extraction solution, Flos Lonicerae extractive solution one or several.
Skin conditioning agent be give product cosmetic result as moisturizing, releive, the composition of effect of compacting.
0.1%-1% Percutaneous absorption enhancer, the Percutaneous absorption enhancer told refer in tween 20, hydrogenation ovum lipoid, azone one or several.By the osmosis of Percutaneous absorption enhancer to skin, the skin conditioning agent in hydrogel can be absorbed by the skin faster, reaches the effect of fast skin conditioning.
Accompanying drawing explanation
Fig. 1 is the gel strength-temperature profile of hydrogel of the present invention.
Detailed description of the invention:
Below in conjunction with embodiment, the invention will be further described:
Embodiment 1
A hydrogel mask sheet for high-temperature stable, comprises carrier screen cloth and hydrogel; Described hydrogel is grouped into by the one-tenth of following percentage by weight:
Cellulose derivative water-soluble polymer 0.1%,
Sargassum extracts the natural water-soluble copolymer 0.5% of class,
The natural water-soluble copolymer 0.1% of the extracellular polysaccharide class that fermentable generates,
The natural water-soluble copolymer 0.1% that plant seed or root extract,
Cause crosslinked required electrolyte 0.1%,
Skin conditioning agent 0.5%,
Percutaneous absorption enhancer 0.1%,
Polyalcohols 5%,
Antiseptic 0.1%,
Surplus pure water.
Described cellulose derivative water-soluble polymer is sodium carboxymethyl cellulose;
The natural water-soluble copolymer that described Sargassum extracts class is carrageenan,
The natural water-soluble copolymer of the extracellular polysaccharide class that described fermentable generates is xanthan gum,
The natural water-soluble copolymer that described plant seed or root extract is guar gum,
It is potassium chloride that described initiation is cross-linked required electrolyte,
Described skin conditioning agent is allantoin,
Described Percutaneous absorption enhancer tween 20,
Described polyalcohols is glycerol,
Described antiseptic is methyl hydroxybenzoate,
Surplus pure water.
The manufacture method of described hydrogel facial mask liquid comprises the following steps:
(1) prepare burden:
By sodium carboxymethyl cellulose, carrageenan, xanthan gum, guar gum, glycerol bucket mix homogeneously, make uniform dispersion liquid.Then put in pure water, be heated to 85 DEG C, stir, then add potassium chloride, allantoin, tween 20 and methyl hydroxybenzoate, be made into the hydrogel of temperature at the fluid state of 60 DEG C ~ 85 DEG C;
(2) be coated with:
The temperature that step (1) is obtained at the hydrogel of the fluid state of 60 DEG C ~ 85 DEG C, by hydrogel facial mask machine coating, compacting, make gel infiltration enter screen cloth, cooling after and screen cloth form gel slice, then utilize cutting die excision forming.
Described hydrogel facial mask liquid, on carrier screen cloth, keeps stable in the temperature range of-15 DEG C ~ 55 DEG C, improves the stability of product in transport and storage.
When described hydrogel facial mask liquid and contact skin, wherein contained skin conditioning agent rapid osmotic can enter skin due to the effect of Percutaneous absorption enhancer, reaches the effect of conditioning skin.
Embodiment 2
A hydrogel mask sheet for high-temperature stable, comprises carrier screen cloth and hydrogel; Described hydrogel is grouped into by the one-tenth of following percentage by weight:
Cellulose derivative water-soluble polymer 1%,
Sargassum extracts the natural water-soluble copolymer 2% of class,
The natural water-soluble copolymer 2% of the extracellular polysaccharide class that fermentable generates,
The natural water-soluble copolymer 2% that plant seed or root extract,
Cause crosslinked required electrolyte 2%,
Skin conditioning agent 5%,
Percutaneous absorption enhancer 1%,
Polyalcohols 20%,
Antiseptic 1%,
Surplus pure water.
Described cellulose derivative water-soluble polymer is two kinds of 1:1 preparations by weight in sodium carboxymethyl cellulose, hydroxyethyl-cellulose and hydroxypropyl emthylcellulose; As sodium carboxymethyl cellulose, hydroxyethyl-cellulose mixture by weight;
Described Sargassum extracts the natural water-soluble copolymer of class, is kind of the 1:1 preparation by weight of two in carrageenan, sodium alginate, agar; As: carrageenan, sodium alginate mixture by weight
The natural water-soluble copolymer of the extracellular polysaccharide class that described fermentable generates is two kinds of 1:1 preparations by weight in xanthan gum, gellan gum;
The natural water-soluble copolymer that described plant seed or root extract is two kinds of 1:1 preparations by weight in guar gum, algaroba glue, Rhizoma amorphophalli root powder; As guar gum, algaroba glue 1:1 mixture by weight
Described initiation is cross-linked required electrolyte and refers in potassium chloride, calcium chloride, sodium chloride, aluminum chloride two kinds 1:1 preparations by weight; As potassium chloride, calcium chloride 1:1 mixture by weight;
Described skin conditioning agent refers to two kinds of 1:1 preparations by weight in allantoin, hyaluronate sodium, Limax secretions filtrate, Aloe extraction solution, Flos Lonicerae extractive solution; As allantoin and hyaluronate sodium 1:1 mixture by weight
Described Percutaneous absorption enhancer refers to two kinds of 1:1 preparations by weight in tween 20, hydrolecithin, azone; As tween 20 and hydrolecithin mixture;
Described polyalcohols is two kinds of 1:1 preparations by weight in glycerol, 1,3-PD, 1,3 butylene glycol; As glycerol, 1,3-PD mixture;
Described antiseptic is two kinds of 1:1 preparations by weight in methyl hydroxybenzoate, propylparaben, DMDMH, phenoxyethanol, two imidazolidinyl urea, Sensiva SC50; As methyl hydroxybenzoate and propylparaben mixture.
Embodiment 3
A hydrogel mask sheet for high-temperature stable, comprises carrier screen cloth and hydrogel; Described hydrogel is grouped into by the one-tenth of following percentage by weight:
A hydrogel mask sheet for high-temperature stable, comprises carrier screen cloth and hydrogel facial mask liquid; It is characterized in that described hydrogel facial mask liquid is grouped into by the one-tenth of following percentage by weight:
Cellulose derivative water-soluble polymer 0.5%,
Sargassum extracts the natural water-soluble copolymer 1.3% of class,
The natural water-soluble copolymer 1.2% of the extracellular polysaccharide class that fermentable generates,
The natural water-soluble copolymer 1.1% that plant seed or root extract,
Cause crosslinked required electrolyte 1.4%,
Skin conditioning agent 2.5%,
Percutaneous absorption enhancer 0.7%,
Polyalcohols 12%,
Antiseptic 0.7%,
Surplus pure water.
Described cellulose derivative water-soluble polymer is the 1:1:1 preparation by weight of sodium carboxymethyl cellulose, hydroxyethyl-cellulose and hydroxypropyl emthylcellulose;
Described Sargassum extracts the natural water-soluble copolymer of class, is carrageenan, sodium alginate and agar 1:1:1 mixture by weight;
The natural water-soluble copolymer of the extracellular polysaccharide class that described fermentable generates is xanthan gum, gellan gum 1:1 mixture by weight;
The natural water-soluble copolymer that described plant seed or root extract is the 1:1:1 preparation by weight of guar gum, algaroba glue and Rhizoma amorphophalli root powder;
Described initiation is cross-linked required electrolyte and refers in potassium chloride, calcium chloride, sodium chloride, aluminum chloride three kinds 1:1:1 mixtures by weight; As potassium chloride, calcium chloride and sodium chloride mixture;
Described skin conditioning agent refers to three kinds of 1:1:1 preparations by weight in allantoin, hyaluronate sodium, Limax secretions filtrate, Aloe extraction solution, Flos Lonicerae extractive solution; As allantoin, hyaluronate sodium and Limax secretions filtrate mixture;
Described Percutaneous absorption enhancer refers to the 1:1:1 preparation by weight of tween 20, hydrolecithin and azone; ;
Described polyalcohols is glycerol, 1,3-PD, 1,3 butylene glycol 1:1:1 mixture by weight;
Described antiseptic is three kinds of 1:1:1 preparations by weight in methyl hydroxybenzoate, propylparaben, DMDMH, phenoxyethanol, two imidazolidinyl urea; As methyl hydroxybenzoate, propylparaben, DMDMH and phenoxyethanol mixture.
The raw material sources that this patent uses are as follows:
Above-described is only preferred embodiments of the present invention.It should be pointed out that for the person of ordinary skill of the art, without departing from the principles of the present invention, can also make some improvement and modification, this is also considered as protection scope of the present invention.
Claims (4)
1. a hydrogel mask sheet for high-temperature stable, comprises carrier screen cloth and hydrogel; It is characterized in that described hydrogel is grouped into by the one-tenth of following percentage by weight:
0.1%-1% cellulose derivative water-soluble polymer, described cellulose derivative water-soluble polymer is one or several in sodium carboxymethyl cellulose, hydroxyethyl-cellulose and hydroxypropyl emthylcellulose;
0.5%-2% Sargassum extracts the natural water-soluble copolymer of class, the natural water-soluble copolymer that described Sargassum extracts class refer in carrageenan, sodium alginate, agar one or several;
The natural water-soluble copolymer of extracellular polysaccharide class that 0.1%-2% fermentable generates, the natural water-soluble copolymer of the extracellular polysaccharide class that described fermentable generates refer in xanthan gum, gellan gum one or several;
The natural water-soluble copolymer that 0.1%-2% plant seed or root extract, the natural water-soluble copolymer that described plant seed or root extract is one or several in guar gum, algaroba glue, Rhizoma amorphophalli root powder;
0.1%-2% causes crosslinked required electrolyte, described initiation be cross-linked that required electrolyte refers in potassium chloride, calcium chloride, sodium chloride, aluminum chloride one or several;
0.5%-5% skin conditioning agent, described skin conditioning agent refer in allantoin, hyaluronate sodium, Limax secretions filtrate, Aloe extraction solution, Flos Lonicerae extractive solution one or several;
0.1%-1% Percutaneous absorption enhancer, described Percutaneous absorption enhancer refer in tween 20, hydrolecithin, azone one or several;
5%-20% polyalcohols, described polyalcohols is one or several in glycerol, 1,3-PD, 1,3 butylene glycol;
0.1%-1% antiseptic, described antiseptic comprise in methyl hydroxybenzoate, propylparaben, DMDMH, phenoxyethanol, two imidazolidinyl urea one or several;
Surplus pure water.
2. the hydrogel mask sheet of a kind of high-temperature stable according to claim 1, is characterized in that: the manufacture method of described hydrogel facial mask liquid comprises the following steps:
(1) prepare burden:
By 0.1%-1% cellulose derivative water-soluble polymer, 0.5%-2% Sargassum extracts the natural water-soluble copolymer of class, the natural water-soluble copolymer of the extracellular polysaccharide class that 0.1%-2% fermentable generates, the natural water-soluble copolymer that 0.1%-2% plant seed or root extract, 5%-20% polyalcohols, use bucket mix homogeneously, make uniform dispersion liquid; Then put in pure water, be heated to 85 DEG C, stir, then add 0.1%-2% and cause crosslinked required electrolyte, 0.5%-5% skin conditioning agent, 0.1%-1% Percutaneous absorption enhancer and 0.1%-1% antiseptic, be made into the hydrogel of temperature at the fluid state of 60 DEG C ~ 85 DEG C;
(2) be coated with:
The temperature that step (1) is obtained the fluid state of 60 DEG C ~ 85 DEG C hydrogel by hydrogel facial mask machine coating, compacting, make gel infiltration enter screen cloth, cooling after and screen cloth form gel slice, then utilize cutting die excision forming.
3. the hydrogel mask sheet of a kind of high-temperature stable according to claim 1 and 2, is characterized in that: described hydrogel, on carrier screen cloth, keeps stable in the temperature range of-15 DEG C ~ 55 DEG C, improves the stability of product in transport and storage.
4. the hydrogel mask sheet of a kind of high-temperature stable according to claim 1 and 2, it is characterized in that: when described hydrogel mask sheet and contact skin, wherein contained skin conditioning agent rapid osmotic can enter skin due to the effect of Percutaneous absorption enhancer, reaches the effect of conditioning skin.
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