CN104031771A - Gastroscope cleanser - Google Patents
Gastroscope cleanser Download PDFInfo
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- CN104031771A CN104031771A CN201410269729.9A CN201410269729A CN104031771A CN 104031771 A CN104031771 A CN 104031771A CN 201410269729 A CN201410269729 A CN 201410269729A CN 104031771 A CN104031771 A CN 104031771A
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- gastroscope
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Abstract
The invention relates to digestive endoscopy cleaning supplies and in particular relates to a gastroscope cleanser. The gastroscope cleanser is composed of the following raw materials: water, 3,9-divinyl-2,4,8,10-tetraoxaspiro[5,5] undecane, 3-(2-aminoethyl) benzpyrole-5-alcohol, 6-propyl-2-sulfo-2,3-dihydro-4(1H)-pyrimidone, 5-ethyl-5-(3-methyl butyl) barbituric acid, 2,3,4,5,6-pentacarbonyl-2-hexenoic acid-4-lactone, ethyl carbamate, 3-(10,11-dihydro-5H-dibenzo[a,d] cycloheptene-5-subunit)-N, N-dimethyl-1-propylamine, 2-hydroxy-N-(4-methoxyphenyl)-11H-benzo[a] carbazole-3-formamide and isobutyraldehyde. The gastroscope cleanser has good stain removal effect by utilizing mutual action and mutual effect among relative chemical components and has unique cleaning effect especially for food debris, blood clot, gastric juice, succus pancreaticus, bile, and the like.
Description
Technical field
The present invention relates to a kind of sanitising agent of digestive endoscopy cleaning supplies, particularly gastroscope.
background technology
Gastroscopy is the most reliable method of current diagnosis ESD disease, it utilizes the fiber-optic elongated pipe of black plastic parcel of one centimeter of a diameter, front end is equipped with endoscopy by the esophagus → stomach → duodenum that stretches into person under inspection in mouth, by the high light that light source device sent, can make light turn via optical fibers, allow doctor clearly observe the healthy state at each position in upper digestive tract from the other end.If desired, can stretch into clip by the duck eye on gastroscope and do cut sections for microscopic examination.
Because gastroscope will, through esophagus, stomach and duodenum, inevitably be subject to the pollution of swill, clot, gastric juice, pancreatic juice, bile etc., after inspection, be necessary it to wash targetedly clean, to ensure the each degree of cleaning that use of gastroscope.
Summary of the invention
The object of the present invention is to provide a kind of cleaning capacity high for the clean gastroscope sanitising agent of gastroscope.
Technical problem of the present invention, is achieved by following technical proposals:
Gastroscope sanitising agent, special character is to be made up of the raw material of following weight part proportioning: 80 parts, water, 3, 9-divinyl-2, 4, 8, 10-tetra-oxaspiros [5.5] undecane 18-20 part, 3-(2-amino-ethyl) indoles-5-alcohol 20-22 part, 6-propyl group-2-sulfo--2, 3-dihydro-4 (1H)-pyrimidone 10-12 part, 5-ethyl-5-(3-methyl butyl) barbituric acid 18-20 part, 2, 3, 4, 5, 6-penta hydroxy group-2-hexenoic acid-4-lactone 16-18 part, urethanum 14-16 part, 3-(10, 11-dihydro-5H-dibenzo [a, d] suberene-5-subunit)-N, N-dimethyl-1-propylamine 8-10 part, 2-hydroxy-n-(4-p-methoxy-phenyl)-11H-benzo [a] carbazole-3-methane amide 6-8 part, isobutyric aldehyde 5-7 part.
Preparation method of the present invention: add deionized water, add while stirring 3,9-divinyl-2,4,8,10-, tetra-oxaspiros [5.5] undecane, continues to be stirred to and be uniformly dispersed, and is then heated to 50-60 DEG C; Slowly add 3-(2-amino-ethyl) indoles-5-alcohol, 6-propyl group-2-sulfo--2,3-dihydro-4 (1H)-pyrimidone, stirs and makes it to dissolve; Add 5-ethyl-5-(3-methyl butyl) barbituric acid, 2,3,4,5,6-penta hydroxy group-2-hexenoic acid-4-lactone, urethanum, 3-(10,11-dihydro-5H-dibenzo [a, d] suberene-5-subunit)-N, N-dimethyl-1-propylamine, 2-hydroxy-n-(4-p-methoxy-phenyl)-11H-benzo [a] carbazole-3-methane amide, isobutyric aldehyde, stir; Be cooled to 30-35 DEG C, obtain required gastroscope sanitising agent.
This gastroscope sanitising agent, utilize interaction between related chemical constituents, influence each other, have good greasiness removal effect, especially have unique cleaning effect for spots such as the swill adhering on gastroscope, clot, gastric juice, pancreatic juice, bile, cleaning capacity is high.
Embodiment
Below provide the specific embodiment of the present invention, be used for the present invention to be further described.In the present invention, if no special instructions, each raw material is all taking working substance content as 100%.
In following examples and comparative example, raw material introduction:
3,9-divinyl-2,4,8,10-, tetra-oxaspiros [5.5] undecane, CAS accession number is: 78-19-3;
3-(2-amino-ethyl) indoles-5-alcohol, CAS accession number is: 50-67-9;
6-propyl group-2-sulfo--2,3-dihydro-4 (1H)-pyrimidone, CAS accession number is: 51-52-5;
5-ethyl-5-(3-methyl butyl) barbituric acid, CAS accession number is: 57-43-2;
2,3,4,5,6-penta hydroxy group-2-hexenoic acid-4-lactone, CAS accession number is: 50-81-7;
Urethanum, CAS accession number is: 51-79-6;
3-(10,11-dihydro-5H-dibenzo [a, d] suberene-5-subunit)-N, N-dimethyl-1-propylamine, CAS accession number is: 50-48-6;
2-hydroxy-n-(4-p-methoxy-phenyl)-11H-benzo [a] carbazole-3-methane amide, CAS accession number is: 86-19-1;
Isobutyric aldehyde, CAS accession number is: 78-84-2.
Embodiment 1
Weigh: water 80kg, 3, 9-divinyl-2, 4, 8, 10-tetra-oxaspiros [5.5] undecane 18kg, 3-(2-amino-ethyl) indoles-5-alcohol 22kg, 6-propyl group-2-sulfo--2, 3-dihydro-4 (1H)-pyrimidone 11kg, 5-ethyl-5-(3-methyl butyl) barbituric acid 18kg, 2, 3, 4, 5, 6-penta hydroxy group-2-hexenoic acid-4-lactone 16kg, urethanum 16kg, 3-(10, 11-dihydro-5H-dibenzo [a, d] suberene-5-subunit)-N, N-dimethyl-1-propylamine 10kg, 2-hydroxy-n-(4-p-methoxy-phenyl)-11H-benzo [a] carbazole-3-methane amide 6kg, isobutyric aldehyde 7kg.
The preparation method of this embodiment gastroscope sanitising agent: add deionized water, add while stirring 3,9-divinyl-2,4,8,10-, tetra-oxaspiros [5.5] undecane, continues to be stirred to and be uniformly dispersed, and is then heated to 50-60 DEG C; Slowly add 3-(2-amino-ethyl) indoles-5-alcohol, 6-propyl group-2-sulfo--2,3-dihydro-4 (1H)-pyrimidone, stirs and makes it to dissolve; Add 5-ethyl-5-(3-methyl butyl) barbituric acid, 2,3,4,5,6-penta hydroxy group-2-hexenoic acid-4-lactone, urethanum, 3-(10,11-dihydro-5H-dibenzo [a, d] suberene-5-subunit)-N, N-dimethyl-1-propylamine, 2-hydroxy-n-(4-p-methoxy-phenyl)-11H-benzo [a] carbazole-3-methane amide, isobutyric aldehyde, stir; Be cooled to 30-35 DEG C, obtain required gastroscope sanitising agent.
Embodiment 2
Weigh: water 80kg, 3, 9-divinyl-2, 4, 8, 10-tetra-oxaspiros [5.5] undecane 20kg, 3-(2-amino-ethyl) indoles-5-alcohol 20kg, 6-propyl group-2-sulfo--2, 3-dihydro-4 (1H)-pyrimidone 12kg, 5-ethyl-5-(3-methyl butyl) barbituric acid 20kg, 2, 3, 4, 5, 6-penta hydroxy group-2-hexenoic acid-4-lactone 17kg, urethanum 14kg, 3-(10, 11-dihydro-5H-dibenzo [a, d] suberene-5-subunit)-N, N-dimethyl-1-propylamine 9kg, 2-hydroxy-n-(4-p-methoxy-phenyl)-11H-benzo [a] carbazole-3-methane amide 8kg, isobutyric aldehyde 6kg.
The preparation method of this embodiment gastroscope sanitising agent is with embodiment 1.
Embodiment 3
Weigh: water 80kg, 3, 9-divinyl-2, 4, 8, 10-tetra-oxaspiros [5.5] undecane 19kg, 3-(2-amino-ethyl) indoles-5-alcohol 21kg, 6-propyl group-2-sulfo--2, 3-dihydro-4 (1H)-pyrimidone 10kg, 5-ethyl-5-(3-methyl butyl) barbituric acid 19kg, 2, 3, 4, 5, 6-penta hydroxy group-2-hexenoic acid-4-lactone 18kg, urethanum 15kg, 3-(10, 11-dihydro-5H-dibenzo [a, d] suberene-5-subunit)-N, N-dimethyl-1-propylamine 8kg, 2-hydroxy-n-(4-p-methoxy-phenyl)-11H-benzo [a] carbazole-3-methane amide 7kg, isobutyric aldehyde 5kg.
The preparation method of this embodiment gastroscope sanitising agent is with embodiment 1.
Comparative example 1
Weigh: water 80kg, 3,9-divinyl-2,4,8,10-, tetra-oxaspiros [5.5] undecane 18kg, 3-(2-amino-ethyl) indoles-5-alcohol 22kg, 5-ethyl-5-(3-methyl butyl) barbituric acid 18kg, 2,3,4,5,6-penta hydroxy group-2-hexenoic acid-4-lactone 16kg, urethanum 16kg, 3-(10,11-dihydro-5H-dibenzo [a, d] suberene-5-subunit)-N, N-dimethyl-1-propylamine 10kg, isobutyric aldehyde 7kg.
The preparation method of this comparative example gastroscope sanitising agent: add deionized water, add while stirring 3,9-divinyl-2,4,8,10-, tetra-oxaspiros [5.5] undecane, continues to be stirred to and be uniformly dispersed, and is then heated to 50-60 DEG C; Slowly add 3-(2-amino-ethyl) indoles-5-alcohol, stir and make it to dissolve; Add 5-ethyl-5-(3-methyl butyl) barbituric acid, 2,3,4,5,6-penta hydroxy group-2-hexenoic acid-4-lactone, urethanum, 3-(10,11-dihydro-5H-dibenzo [a, d] suberene-5-subunit)-N, N-dimethyl-1-propylamine, isobutyric aldehyde, stir; Be cooled to 30-35 DEG C, obtain required gastroscope sanitising agent.
Comparative example 2
Weigh: water 80kg, 3-(2-amino-ethyl) indoles-5-alcohol 20-22kg, 6-propyl group-2-sulfo--2,3-dihydro-4 (1H)-pyrimidone 10-12kg, 5-ethyl-5-(3-methyl butyl) barbituric acid 18-20kg, urethanum 14-16kg, 3-(10,11-dihydro-5H-dibenzo [a, d] suberene-5-subunit)-N, N-dimethyl-1-propylamine 8-10kg, 2-hydroxy-n-(4-p-methoxy-phenyl)-11H-benzo [a] carbazole-3-methane amide 6-8kg, isobutyric aldehyde 5-7kg.
The preparation method of this embodiment gastroscope sanitising agent: add deionized water, be then heated to 50-60 DEG C; Slowly add 3-(2-amino-ethyl) indoles-5-alcohol, 6-propyl group-2-sulfo--2,3-dihydro-4 (1H)-pyrimidone, stirs and makes it to dissolve; Add 5-ethyl-5-(3-methyl butyl) barbituric acid, urethanum, 3-(10,11-dihydro-5H-dibenzo [a, d] suberene-5-subunit)-N, N-dimethyl-1-propylamine, 2-hydroxy-n-(4-p-methoxy-phenyl)-11H-benzo [a] carbazole-3-methane amide, isobutyric aldehyde, stir; Be cooled to 30-35 DEG C, obtain required gastroscope sanitising agent.
Carry out detergency test with embodiment 1-3 and comparative example 1-2 gained finished product, concrete steps are as follows:
1) preparation of artificial dirt
Mixing oil formula: taking butter, lard, vegetables oil mass ratio as 0.3:0.7:1 configuration, and add the glyceryl monostearate of its total mass 6%, this is artificial dirt.
Artificial dirt is put on electric furnace and is heated to 250 DEG C, stir and keep this temperature 15min, beaker is moved to magnetic stirrer and stir, naturally cool to temperature required for subsequent use.The temperature reference of defiling: in the time that room temperature is 20 DEG C, need 80 DEG C of oil temperatures; When room temperature is 25 DEG C, need 45 DEG C of oil temperatures; When room temperature is lower than 17 DEG C or during higher than 27 DEG C, test should not be carried out, and need under temperature adapt circumstance, carry out.Should use if desired the Terg-O-Tometer of attached freezing plant.
2) defile
Clean gastroscope is put and weighed on frame taking five as one group, be accurately weighed as W0 with balance, the gastroscope after weighing is placed on rack one by one.
In the time that greasy dirt remains in stable temperature, one by one gastroscope is got on to take off from rack, all immerse in greasy dirt and keep 2-3s, slowly take out, after the lower speed of greasy dirt is slack-off, put back to original rack, prepare successively dirty mould bases.After the greasy dirt on gastroscope solidifies, gastroscope is taken off and corner or the unnecessary greasy dirt of side wiped with filter paper or absorbent cotton.Under room temperature, leaving standstill after 4h, is W1 weighing on frame with balance accurate weighing.
3) testing sequence
The gastroscope of known greasy dirt amount is inserted in corresponding wash stand and prepared to wash.
Spotter is switched on power, and wash temperature is set to 28 DEG C, and velocity of rotation is set to 160r/min, and washing time is set to 5min.
Take 5.0g sample to be tested in 2500ml hard water, after shaking up, measure respectively 800ml test solution in five washing becks of Terg-O-Tometer, in the time that test solution temperature rises to 28 DEG C, rapidly the gastroscope of known weight is put into washing beck accordingly together with wash stand, after putting into washing beck, last gastroscope starts to count soak time, rapidly agitator is installed simultaneously, while soaking 1min, start spotter, start washing, when 5min, machine auto stop, rapidly agitator is taken off, take out wash stand, to wash rear gastroscope is placed on rack one by one, after standing 3h, mould bases being put to corresponding weighing frame weighs as W2.
Result represents
Soil removal efficiency=[(W1-W2)/(W1-W0)] * 100%
| ? | Soil removal efficiency, % |
| Embodiment 1 | 98.6 |
| Embodiment 2 | 98.3 |
| Embodiment 3 | 97.9 |
| Comparative example 1 | 80.2 |
| Comparative example 2 | 68.4 |
Claims (1)
1. gastroscope sanitising agent, it is characterized in that being formed by the raw material of following weight part proportioning: 80 parts, water, 3, 9-divinyl-2, 4, 8, 10-tetra-oxaspiros [5.5] undecane 18-20 part, 3-(2-amino-ethyl) indoles-5-alcohol 20-22 part, 6-propyl group-2-sulfo--2, 3-dihydro-4 (1H)-pyrimidone 10-12 part, 5-ethyl-5-(3-methyl butyl) barbituric acid 18-20 part, 2, 3, 4, 5, 6-penta hydroxy group-2-hexenoic acid-4-lactone 16-18 part, urethanum 14-16 part, 3-(10, 11-dihydro-5H-dibenzo [a, d] suberene-5-subunit)-N, N-dimethyl-1-propylamine 8-10 part, 2-hydroxy-n-(4-p-methoxy-phenyl)-11H-benzo [a] carbazole-3-methane amide 6-8 part, isobutyric aldehyde 5-7 part.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410269729.9A CN104031771A (en) | 2014-06-17 | 2014-06-17 | Gastroscope cleanser |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410269729.9A CN104031771A (en) | 2014-06-17 | 2014-06-17 | Gastroscope cleanser |
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| Publication Number | Publication Date |
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| CN104031771A true CN104031771A (en) | 2014-09-10 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201410269729.9A Pending CN104031771A (en) | 2014-06-17 | 2014-06-17 | Gastroscope cleanser |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104498228A (en) * | 2014-12-02 | 2015-04-08 | 林大利 | Detergent for fibro-colonoscope |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2002086045A1 (en) * | 2001-04-19 | 2002-10-31 | Esc, Inc. | Cleaning compositions |
| CN1705735A (en) * | 2002-10-14 | 2005-12-07 | 阿科尼亚有限公司 | Composition |
| CN1786134A (en) * | 2004-12-07 | 2006-06-14 | 雷金丰 | Multifunction antiseptic sterilizing cleaning agent composition and its preparation method |
| CN102071113A (en) * | 2011-02-05 | 2011-05-25 | 徐宏汇 | Condensed multi-enzyme medical cleaning agent |
| CN102133155A (en) * | 2010-01-22 | 2011-07-27 | 和光交易株式会社 | Skin cleaning agent having excellent water solublility |
-
2014
- 2014-06-17 CN CN201410269729.9A patent/CN104031771A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2002086045A1 (en) * | 2001-04-19 | 2002-10-31 | Esc, Inc. | Cleaning compositions |
| CN1705735A (en) * | 2002-10-14 | 2005-12-07 | 阿科尼亚有限公司 | Composition |
| CN1786134A (en) * | 2004-12-07 | 2006-06-14 | 雷金丰 | Multifunction antiseptic sterilizing cleaning agent composition and its preparation method |
| CN102133155A (en) * | 2010-01-22 | 2011-07-27 | 和光交易株式会社 | Skin cleaning agent having excellent water solublility |
| CN102071113A (en) * | 2011-02-05 | 2011-05-25 | 徐宏汇 | Condensed multi-enzyme medical cleaning agent |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104498228A (en) * | 2014-12-02 | 2015-04-08 | 林大利 | Detergent for fibro-colonoscope |
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Application publication date: 20140910 |
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