CN104017651B - A kind of preparation method of Tree Peony flower Rose mediation essential oil and device - Google Patents
A kind of preparation method of Tree Peony flower Rose mediation essential oil and device Download PDFInfo
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- CN104017651B CN104017651B CN201310104579.1A CN201310104579A CN104017651B CN 104017651 B CN104017651 B CN 104017651B CN 201310104579 A CN201310104579 A CN 201310104579A CN 104017651 B CN104017651 B CN 104017651B
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Abstract
The present invention relates to a kind of preparation method of essential oil, specifically a kind of Tree Peony flower Rose is in harmonious proportion the preparation method of essential oil and device, the present invention adopts alcohol vapour to circulate and extracts, and filtering membrane is set in extraction chamber, by containing spices alcohol vapour direct filtration after condensation collection and treatment, simplify technological process, save mass energy; Tree Peony flower to be extracted and Rose can be extracted by the present invention as required in proportion simultaneously, and technique is simple, and is conducive to mixing, and strengthen the synergy between Tree Peony flower and rose ethereal oil.
Description
Technical field
The present invention relates to a kind of preparation method of essential oil, specifically a kind of Tree Peony flower Rose is in harmonious proportion the preparation method of essential oil and device.
Background technology
Essential oil originates from scented plants AromaticHerbst.Not all plant can output essential oil, only has those to contain the plant of face cream gland, just likely output essential oil.The face cream gland of different plant is distributed with difference, has plenty of on petal, leaf, rhizome or trunk.After sachet is refined extraction, namely become " plants essential oil " alleged by us.Essential oil has lipotropy, is easy to be dissolved in grease, because the molecular chain of essential oil is usually shorter, this makes them very easily permeate in skin, and enters in body through capillary vessel abundant under subcutaneous lipids.Essential oil is made up of some very little molecules, these high volatile matters, can enter health, message is directly delivered to brain by nose breathing road, by the limbic system of brain, regulates the physiological function of mood and health.So in aromatotherapy, essential oil can strengthen the function of physiology and psychology.The chemical structure that has each plants essential oil decides the mode of its fragrance, color, mobility and it and System Operation, also makes each plants essential oil respectively have a set of special function speciality.
The title that essential oil has " Chinese medicine in west ", is can enter blood circulation by Cutaneous permeation, effectively can nurses one's health health, reach releive, the effect such as purification.
Essential oil essence can anti-communicable disease, to antibacterium, virus, mould, can anti-inflammation, anti-spasm, promotes cell metabolism and cell regeneration function, makes life finer.And some essential oil energy endocrine regulation organ, promote hormone secretion, allow the physiology of human body and psychological activity, obtain good development.
Compound essential oil is allocated according to its different feature character by various plants essential oil, according to the concrete symptom of human body, with suitable folk prescription essential oil and substrate oil and the control of dosage, does certain collocation and just can get a desired effect.The effect of compound essential oil is often greater than the summation of each folk prescription essential oil, namely produces synergy, and such as: add among chamomile essential oil by appropriate lavender essential oil, the antiinflammation of Flos Matricariae chamomillae just can promote greatly; In folk prescription essential oil, jasmin quintessence oil has scar effect of dispelling preferably, but folk prescription jasmin quintessence oil price is high, is not easily received by consumers in general.
In prior art, the making method of compound essential oil mostly is single plants essential oil after organic solvent soak extraction, and filter, distill and carry out mix and match again, complex process, and not easily mix, synergy is not good.
Summary of the invention
Single plants essential oil mostly is after organic solvent soak extraction for the making method of compound essential oil in prior art, filter, distill and carry out mix and match again, complex process, and not easily mix, the problem that synergy is not good, the invention provides preparation method and the device of a kind of Tree Peony flower Rose mediation essential oil.
For solving the problems of the technologies described above, the technical solution used in the present invention is:
A preparation method for Tree Peony flower Rose mediation essential oil, comprises the following steps:
Step one: fresh Tree Peony flower and Rose are loaded in the flower stand in extraction chamber, flower layer thickness is 10 ~ 30cm;
Step 2: alcohol vapour is entered by flower stand bottom and upwards continues to flow through Tree Peony flower and Rose layer, the fragrance ingredient of Tree Peony flower and Rose is extracted in condensation, and backflow is collected after membrane filtration after filtration afterwards, and wherein alcohol vapour flow velocity is 10 ~ 50L/Kg fresh flower min;
Step 3: after above-mentioned step cycle extraction 5 ~ 24h, the ethanol extract distillation and concentration under 70 ~ 80 DEG C of conditions collected is slipped out to absence of liquid;
Step 4: by step 3 gained concentrated solution processed, obtains Tree Peony flower Rose mediation essential oil;
Described Tree Peony flower and Rose alternatively layered load in flower stand.
A kind of Tree Peony flower Rose mediation essential oil, is made up of peony essential oil and rose ethereal oil.
A kind of device for the preparation of Tree Peony flower Rose mediation essential oil, comprise extraction chamber and the stilling chamber of sealing, flower stand is provided with in extraction chamber, in extraction chamber, the both sides up and down of flower stand are respectively equipped with filtering membrane, the bottom of extraction chamber is communicated with the top of stilling chamber by pipeline I, the top of extraction chamber is communicated with the upper and lower of stilling chamber respectively by the Liang Ge branch of pipeline II, the bottom of extraction chamber is communicated with the bottom of stilling chamber by pipeline III, the bottom of stilling chamber is provided with pipeline IV, control valve is equipped with on each pipeline and in the branch of pipeline, pipeline II is provided with prolong,
Described flower stand is multilayer.
Beneficial effect of the present invention:
The present invention adopts alcohol vapour to circulate and extracts, and the infiltration being more conducive to treating extract is extracted, and arranges filtering membrane in extraction chamber, by containing condensation collection and treatment after the alcohol vapour direct filtration of spices, simplifies technological process, has saved mass energy;
Tree Peony flower to be extracted and Rose can be extracted by the present invention as required in proportion simultaneously, and technique is simple, and is conducive to mixing, and strengthen the synergy between Tree Peony flower and rose ethereal oil;
Preparation facilities provided by the invention, by opening pipelines different between extraction chamber and stilling chamber, can realize extracting and distillation and concentration two kinds of functions, and whole technological process is uninterrupted continuously, simplifies equipment, has saved mass energy, and simple to operate, convenient and practical.
Accompanying drawing explanation
Fig. 1 Tree Peony flower Rose mediation essential oil preparation facilities structural representation;
Reference numeral: 1, extraction chamber, 2, stilling chamber, 3, pipeline I, 4, pipeline II, 5, pipeline III, 6, pipeline IV, 7, flower stand, 8, filtering membrane, 9, prolong, 10, control valve I, 11, control valve II, 12, control valve III, 13, control valve IV, 14, control valve V, 15, control valve VI.
Embodiment
Below in conjunction with embodiment, the present invention is further elaborated.
A kind of Tree Peony flower Rose mediation essential oil, is made up of peony essential oil and rose ethereal oil.
A preparation method for Tree Peony flower Rose mediation essential oil, comprises the following steps:
Step one: fresh Tree Peony flower and Rose are loaded in the flower stand in extraction chamber, flower layer thickness is 10 ~ 30cm;
Step 2: alcohol vapour is entered by flower stand bottom and upwards continues to flow through Tree Peony flower and Rose layer, the fragrance ingredient of Tree Peony flower and Rose is extracted in condensation, and backflow is collected after membrane filtration after filtration afterwards, and wherein alcohol vapour flow velocity is 10 ~ 50L/Kg fresh flower min;
Step 3: after above-mentioned step cycle extraction 5 ~ 24h, the ethanol extract distillation and concentration under 70 ~ 80 DEG C of conditions collected is slipped out to absence of liquid;
Step 4: by step 3 gained concentrated solution processed, obtains Tree Peony flower Rose mediation essential oil.
A kind of device for the preparation of Tree Peony flower Rose mediation essential oil, comprise extraction chamber 1 and the stilling chamber 2 of sealing, flower stand 7 is provided with in extraction chamber 1, in extraction chamber 1, the both sides up and down of flower stand 7 are respectively equipped with filtering membrane 8, the bottom of extraction chamber 1 is communicated with the top of stilling chamber 2 by pipeline I 3, the top of extraction chamber 1 is communicated with the upper and lower of stilling chamber 2 respectively by the Liang Ge branch of pipeline II 4, the bottom of extraction chamber 1 is communicated with the bottom of stilling chamber 2 by pipeline III 5, the bottom of stilling chamber 2 is provided with pipeline IV 6, control valve is equipped with on each pipeline and in the branch of pipeline, pipeline II 4 is provided with prolong 9.
As shown in the figure, for Tree Peony flower Rose mediation essential oil preparation facilities structural representation, Tree Peony flower and Rose alternatively layered are loaded in the flower stand 7 in extraction chamber, flower layer thickness is 10 ~ 30cm, seal extraction chamber 1 afterwards, appropriate ethanol will be injected in stilling chamber, open control valve I 10, control valve IV 13 and control valve VI 15, the lateral that connecting pipe I 3 and extraction chamber 1 are communicated with stilling chamber 2 bottom by pipeline II 4, closed control valve II 11, control valve III 12 and control valve 14 V, circulating condensing liquid is injected by prolong, then stilling chamber 2 temperature is made to rise to 70 ~ 80 DEG C, steam in stilling chamber 2 enters bottom, extraction chamber 1 by pipeline I 3, flow through the Tree Peony flower on flower stand 7 and Rose layer from bottom to top, the fragrance ingredient of Tree Peony flower and Rose is extracted in condensation, be back to bottom extraction chamber 1 after filter membrane 8 filters afterwards, connecting pipe III 5 is guided to stilling chamber 2, uncooled alcohol vapour is back to stilling chamber 2 by pipeline II 4 after filter membrane 8 filters, circulation extraction like this 5 ~ 24h, closed control valve I 10, control valve IV 13 and control valve VI 15, open control valve 14 V, be communicated with extraction chamber 1 by the lateral of pipeline II 4 with stilling chamber 2 top, Tree Peony flower after extraction and rose slag are cleaned out extraction chamber 1, close extraction chamber 1 afterwards, slipped out to absence of liquid by ethanol extract distillation and concentration in stilling chamber 2, open control valve III 12, concentrated solution is derived by pipeline IV 6, then gained concentrated solution is carried out processed, obtains Tree Peony flower Rose mediation essential oil.
Claims (4)
1. a preparation method for Tree Peony flower Rose mediation essential oil, is characterized in that, comprise the following steps:
Step one: fresh Tree Peony flower and Rose are loaded in the flower stand in extraction chamber, flower layer thickness is 10 ~ 30cm;
Step 2: alcohol vapour is entered by flower stand bottom and upwards continues to flow through Tree Peony flower and Rose layer, the fragrance ingredient of Tree Peony flower and Rose is extracted in condensation, backflow is collected after membrane filtration after filtration afterwards, and wherein alcohol vapour flow velocity is 10 ~ 50L/(Kg fresh flower min);
Step 3: after above-mentioned step cycle extraction 5 ~ 24h, the ethanol extract distillation and concentration under 70 ~ 80 DEG C of conditions collected is slipped out to absence of liquid;
Step 4: by step 3 gained concentrated solution processed, obtains Tree Peony flower Rose mediation essential oil.
2. the preparation method of Tree Peony flower Rose mediation essential oil as claimed in claim 1, is characterized in that: described Tree Peony flower and Rose alternatively layered load in flower stand.
3. the device for the preparation method of Tree Peony flower Rose mediation essential oil as claimed in claim 1, comprise extraction chamber (1) and the stilling chamber (2) of sealing, flower stand (7) is provided with in extraction chamber (1), it is characterized in that: the both sides up and down of extraction chamber (1) interior flower stand (7) are respectively equipped with filtering membrane (8), the bottom of extraction chamber (1) is communicated with the top of stilling chamber (2) by pipeline I (3), the top of extraction chamber (1) is communicated with the upper and lower of stilling chamber (2) respectively by the Liang Ge branch of pipeline II (4), the bottom of extraction chamber (1) is communicated with the bottom of stilling chamber (2) by pipeline III (5), the bottom of stilling chamber (2) is provided with pipeline IV (6), control valve is equipped with on each pipeline and in the branch of pipeline, pipeline II (4) is provided with prolong (9).
4., as claimed in claim 3 for the device of the preparation method of Tree Peony flower Rose mediation essential oil, it is characterized in that: described flower stand (7) is multilayer.
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| CN201310104579.1A CN104017651B (en) | 2013-03-29 | 2013-03-29 | A kind of preparation method of Tree Peony flower Rose mediation essential oil and device |
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| CN201310104579.1A CN104017651B (en) | 2013-03-29 | 2013-03-29 | A kind of preparation method of Tree Peony flower Rose mediation essential oil and device |
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| CN104017651B true CN104017651B (en) | 2016-03-16 |
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Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104017649B (en) * | 2013-03-29 | 2016-03-16 | 洛阳春魁农业开发有限公司 | A kind of preparation method of Tree Peony flower Flower of Arabian Jasmine mediation essential oil and device |
| CN104017650B (en) * | 2013-03-29 | 2016-03-02 | 洛阳春魁农业开发有限公司 | A kind of preparation method of Tree Peony flower lavandula angustifolia mediation essential oil and device |
| CN107746750A (en) * | 2017-11-13 | 2018-03-02 | 莱州百士通玫瑰业开发股份有限公司 | The preparation method of rosebud water |
| CN110419765B (en) * | 2019-08-12 | 2022-04-19 | 四川三联新材料有限公司 | Preparation method and preparation device of electronic cigarette tobacco tar |
| CN113842667B (en) * | 2020-09-17 | 2023-01-24 | 湖北鄂达生物科技有限公司 | Sealwort extract product preparation equipment |
| CN112772895A (en) * | 2021-01-28 | 2021-05-11 | 东莞市永益食品有限公司 | Preparation process of composite seasoning cooking wine |
| CN115161114A (en) * | 2022-06-07 | 2022-10-11 | 厦门健康工程与创新研究院 | Method for extracting hydrolat from spliced roses of different varieties |
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Effective date of registration: 20180118 Address after: Xiang Yiyang County 471000 city of Luoyang province Henan Weiyi deer town Xiangshan No. 7 Lido Patentee after: Luoyang city peony industry development Co.,Ltd. Address before: 471003 Henan province Luoyang Xigong Mill Road Wangcheng Avenue on the west side of Mill Road 89, two floor No. 01-02001 Patentee before: LUOYANG CHUNKUI AGRICULTURAL DEVELOPMENT Co.,Ltd. |
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Effective date of registration: 20200630 Address after: No.1 yard, Heming Road, Tianhu Town, Song County, Luoyang City, Henan Province Patentee after: Luoyang red peony industry technology development Co.,Ltd. Address before: Xiang Yiyang County 471000 city of Luoyang province Henan Weiyi deer town Xiangshan No. 7 Lido Patentee before: Luoyang city peony industry development Co.,Ltd. |
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