CN104016702A - Imitating rock surface ceramic brick capable of insulating and damping as well as production method thereof - Google Patents
Imitating rock surface ceramic brick capable of insulating and damping as well as production method thereof Download PDFInfo
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- CN104016702A CN104016702A CN201410221476.8A CN201410221476A CN104016702A CN 104016702 A CN104016702 A CN 104016702A CN 201410221476 A CN201410221476 A CN 201410221476A CN 104016702 A CN104016702 A CN 104016702A
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- perlite
- ceramic tile
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Abstract
The invention discloses an imitating rock surface ceramic brick capable of insulating and damping, which comprises the following raw materials by weight: 50-90% of perlite micropowder, 5-35% of perlite vitreous bead micropowder, 1-20% of foaming agent, 3-20% of flux and a liquid binder prepared according to weight ratio of main raw materials. According to the invention, perlite deep processing industrial mine tailing-perlite micropowder and perlite vitreous bead micropowder are employed, under the low temperature of 1020-1060 DEG C, an indoor decoration material which is characterized in that the water absorption is greater than 300%, the volume density is between 650-850kg/m<3>, fracture modulus is greater than 3 MPa, heat conduction coefficient is less than 0.20W/(m.k), combustion grade is grade A1, thickness is between 30-60 mm, and the indoor decoration material has decorative effect of rock surface and has damping and insulation functions can be produced. The imitating rock surface ceramic brick can be widely used for damping and insulating decoration in public occasions such as conference room, cinema, hospital and pub as well as family room.
Description
Technical field
The present invention relates to heat preservation humidity conditioning building materials field, is exactly a kind of waste material of ore in sand form process of manufacture for pearlstone that utilizes specifically---ceramic tile and the production method thereof with heat preservation humidity conditioning function and hole stone scar decorative effect that perlite powder and pearlstone micro mist are produced.
Background technology
City on the south China Huaihe River, due to climate reasons, causes following three problems: (1) is cold winter, and dry air causes pulmonary bacterial, such as SARS pneumonia, influenza etc.; (2) summer damp and hot, atmospheric moisture is large, causes furniture clothing mouldy, also easily causes bacterial derivation, endangers healthy; (3) spring and autumn, humidity temperature suitable can, but but encouraged a large amount of procreations of mould, flea, worm lice, health risk not only, the harm of also capturing repeatedly life, such as the case that tick worm is taken people's life by force occurs repeatedly in Xinyang in recent years.
Therefore, special procure and will invent a kind of building ceramics that regulates humidity, adjusting room temp, the growth of mould fungus inhibition worm lice and kill bacteria that has.
The adjustable technical products of disclosed humidity is divided into two classes: a class be can not roasting gelled material product as plastering, concrete product etc.; Another kind of be can roasting ceramic, particularly, the adjustable building ceramics of diatom soil series humidity proposing on Japanese patent laid-open 4-354514 communique, the zeolite that Japanese patent laid-open 3-109244 communique proposes is the adjustable building ceramics of humidity, the adjustable building ceramics of glaze surface humidity that the raw material wet processes high-temperature firing with damping effect that Chinese patent CN99103601.8 proposes forms.
In above-mentioned prior art, all have the following disadvantages: (1) does not have the comprehensive action of heat preservation humidity conditioning, bactericidal; (2) there is the ceramic of damping effect, all adopt wet ball grinding complete processing, greatly wasted electric energy and fuel energy; (3) all adopt the natural mineral raw of capable of adjusting humidity, not only production cost is higher, and waste resource.
Summary of the invention
In order to overcome above-mentioned deficiency of the prior art; the invention provides a kind of waste material of ore in sand form process of manufacture for pearlstone that utilizes---perlite powder and perlite glass bead micro mist are main raw material; adopt dry process, produced and there is imitative hole stone scar ceramic tile and the production method thereof that good insulation temperature adjustment, bactericidal and decorative effect are good.
The object of the present invention is achieved like this:
The imitative hole of a heat preservation humidity conditioning stone scar ceramic tile, its main raw material comprises and being made into according to weight percent: perlite powder 50～90%, perlite glass bead micro mist 5～35%, whipping agent 1～20%, fusing assistant 3～20%; And according to the liquid-containing binder of main raw material weight proportion;
Described liquid-containing binder comprises liquid-containing binder A, the 10l/100kg of consumption proportion main raw material weight; Liquid-containing binder B, the 10l/100kg of consumption proportion main raw material weight;
Described liquid-containing binder A is alkaline binding agent, comprises the aqueous solution of high concentration water's glass, metasilicate pentahydrate sodium and non-hydrate sodium metasilicate; Liquid-containing binder B is acid binding agent, comprises the phosphoric acid emulsion of phosphaljel solution, aluminum oxide;
Described whipping agent comprises calcium carbonate, saltcake and graphite, is wherein at least one, and fusing assistant comprises fluorite, soda ash, silicon partially, is wherein at least one;
Described perlite powder and perlite glass bead micro mist be for adopting the dry process following raw material obtaining of 80 orders that sieves, whipping agent and the fusing assistant agent raw material for adopting 100 mesh sieves that dry ground is crossed to obtain;
The described imitative hole of heat preservation humidity conditioning stone scar ceramic tile, its production method step is as follows:
Raw material is prepared; To comprise that by perlite powder, perlite glass bead micro mist, whipping agent, solubility promoter be the powdery below 80 orders, above powder is added in mixer and mixed in component ratio, be then sequentially added into liquid-containing binder A and liquid-containing binder B 10～20 mesh sieves, standby after old 24 hours that are uniformly mixed, sieve; Powder after old adds in press, and according to the pressure low-pressure moulding of 10～25MPa, the product after moulding is dry through mesh belt dry kiln drying, enter in ceramic roller kiln or pushed bat kiln after the glazing of glaze line and burn till, and firing temperature is 1020～1060, the cycle is 35～60min.The hole lithosporic line that product decoration relies on the decorative pattern of press press distributing mode, mould and burns till rear appearance is realized, and obtains having the ceramic tile of damping heat insulation function and imitative hole stone scar decorative effect.
positive beneficial effect:the present invention relates to damping thermal insulation decorative material technical field; refer in particular to and utilize perlite deep processing industries mine tailing---perlite powder and perlite glass bead micro mist; as shown in Figure 1; under 1020～1060 ℃ of temperature production conditions; produce water-intake rate and be greater than 300%, volume density is at 650～850kg/m
3between, the modulus of rupture is greater than 3MPa, thermal conductivity is less than 0.20W/ (m.k), burning rank is A1 level, thickness 30～60mm, the house decorative material with hole stone scar decorative effect and damping and heat insulation function, the damping insulation and decoration finishing of the public situation such as it can widespread use meeting room, cinema, hospital, bar or family room.
Accompanying drawing explanation
Fig. 1 produces the schema of solid waste in perlite deep-processing process;
Fig. 2 is production method process flow sheet of the present invention.
Embodiment
Below in conjunction with the drawings and specific embodiments, the present invention is described further:
The imitative hole of a heat preservation humidity conditioning stone scar ceramic tile, its main raw material comprises and being made into according to weight percent: perlite powder 50～90%, perlite glass bead micro mist 5～35%, whipping agent 1～20%, fusing assistant 3～20%; And according to the liquid-containing binder of main raw material weight proportion;
Described liquid-containing binder comprises liquid-containing binder A, the 10L/100kg of consumption proportion main raw material weight; Liquid-containing binder B, the 10L/100kg of consumption proportion main raw material weight;
Described liquid-containing binder A is alkaline binding agent, comprises the aqueous solution of high concentration water's glass, metasilicate pentahydrate sodium and non-hydrate sodium metasilicate; Liquid-containing binder B is acid binding agent, comprises the phosphoric acid emulsion of phosphaljel solution, aluminum oxide;
Described whipping agent comprises calcium carbonate, saltcake and graphite, is wherein at least one, and fusing assistant comprises fluorite, soda ash, is wherein at least one;
Described perlite powder and perlite glass bead micro mist be for adopting the dry process following raw material obtaining of 80 orders that sieves, whipping agent and the fusing assistant agent raw material for adopting 100 mesh sieves that dry ground is crossed to obtain;
The described imitative hole of heat preservation humidity conditioning stone scar ceramic tile, its production method step is as follows:
As shown in Figure 2, raw material is prepared; To comprise that by perlite powder, perlite glass bead micro mist, whipping agent, solubility promoter be the powdery below 80 orders, above powder is added in mixer and mixed in component ratio, be then sequentially added into liquid-containing binder A and liquid-containing binder B 10～20 mesh sieves, standby after old 24 hours that are uniformly mixed, sieve; Powder after old adds in press, according to the pressure low-pressure moulding of 10～25MPa, product after moulding is dry through mesh belt dry kiln drying, enter in ceramic roller kiln or pushed bat kiln after the glazing of glaze line and burn till, and firing temperature is that 1020～1060 ℃, cycle are 35～60min.The hole lithosporic line that product decoration relies on the decorative pattern of press press distributing mode, mould and burns till rear appearance is realized, and obtains having the ceramic tile of damping heat insulation function and imitative hole stone scar decorative effect.
Perlite glass bead micro mist, its chemical composition quality percentage composition is as follows: SiO
274～78%, Al
2o
313～16%, Fe
2o
30.6～2.8%, TiO
20.2～0.6%, K
2o 2～5%, and CaO 1～2%, and MgO 0.5～2%, Na
2o 1～2%.
Pearlite tail sand, its chemical composition quality percentage composition is as follows: SiO
272～75%, Al
2o
312～14%, Fe
2o
30.5～1.5% TiO
20.2～1.5%, K
2o 2～5%, and CaO 0～1%, and MgO 0～1%, Na
2o 3～10%, and IL 3～8%.
Fluorite, its chemical composition quality percentage composition is as follows: SiO
20～30%, Al
2o
30.1～1%, Fe
2o
30.5～2% TiO
20.5～2%, K
2o 1～2%, and CaO 5～45%, and MgO 1～10%, Na
2o 0.1～1%, P
2o
50.5～30%, IL 0～20%.
Fluorite is powdery, sand shape or granular.Raw ore outward appearance is white, green or transparence.
Water glass: transparent liquid, mother-in-law Mei Shi degree 45～60 degree.
Wingdale: purity is not less than 95%.
Graphite: purity is not less than 95%.
Saltcake: purity is not less than 95%; .
Biphosphate Al binding agent: transparence liquid, its chemical composition quality percentage composition scope is as follows: P
2o
530～33%, Al
2o
36～8%, Fe
2o
3be less than 0.5%; Other character are as follows: volume density is at 1450～1470kg/m
3between, pH value 1.4.
[interpretation of result]
After product of the present invention burns till, water-intake rate is greater than 300%, and volume density is at 650～850kg/m
3between, the modulus of rupture is greater than 3MPa, and thermal conductivity is less than 0.25W/ (m.k), and burning rank is A1 level, belongs to damping heat preservation decoration integrative ceramic plate.
embodiment 1
The perlite glass bead micro mist of the perlite powder by weight 59%, weight 20%, the Wingdale of weight 5%, the soda ash of the Fluorspar Powder of weight 6%, weight 5%,, the 500Kg admixtion that the graphite of the saltcake of weight 4%, weight 1% forms adds in mixer is dry mixed, and are added the biphosphate Al binding agent of weight 60L and the water glass bonding agent of weight 50L heavily to drop into be uniformly mixed and to cross 20 order reciprocating sieves successively.Powder through being mixed with, after in feed bin old 24 hours, carries out cloth decoration dry-pressing formed, and wherein pressure is 10～25bar, and it is dry that the product after moulding enters mesh-belt kiln through rotary conveyor, and dry tenacity is not less than 0.5MPa.After dry, enter in ceramic roller kiln or pushed bat kiln and burn till, firing temperature is that 1020～1060 ℃, cycle are 35min.After burning till, can make and there is hole lithosporic line damping thermal insulation inner wall board.Its water suction is 313%, and volume density is at 673kg/m
3between, the modulus of rupture is 3.15MPa, and thermal conductivity is 0.20W/ (m.k), and burning rank is A1 level.
embodiment 2
The perlite glass bead micro mist of the perlite powder by weight 65%, weight 20%, the Wingdale of weight 2%, the soda ash of the Fluorspar Powder of weight 5%, weight 3%,, the 500kg admixtion that the graphite of the saltcake of weight 4%, weight 1% forms adds in mixer is dry mixed, and are added the biphosphate Al binding agent of weight 60L and the water glass bonding agent of weight 50L heavily to drop into be uniformly mixed and to cross 20 order reciprocating sieves successively.Powder through being mixed with, after in feed bin old 24 hours, carries out cloth decoration dry-pressing formed, and wherein pressure is 15～25bar, and it is dry that the product after moulding enters mesh-belt kiln through rotary conveyor, and dry tenacity is not less than 0.5MPa.After dry, enter in ceramic roller kiln or pushed bat kiln and burn till, firing temperature is that 1020～1060 ℃, cycle are 35min.After burning till, can make and there is hole lithosporic line damping thermal insulation inner wall board.Its water suction is 325%, and volume density is at 756kg/m
3between, the modulus of rupture is 4.15MPa, and thermal conductivity is 0.25W/ (m.k), and burning rank is A1 level.
embodiment 3
The perlite glass bead micro mist of the perlite powder by weight 50%, weight 35%, the Wingdale of weight 5%, the saltcake of the Fluorspar Powder of weight 5%, weight 4%,, the 500kg admixtion that the graphite of weight 1% forms adds in mixer is dry mixed, and are added the biphosphate Al binding agent of weight 60L and the water glass bonding agent of weight 50L heavily to drop into be uniformly mixed and to cross 20 order reciprocating sieves successively.Powder through being mixed with, after in feed bin old 24 hours, carries out cloth decoration dry-pressing formed, and wherein pressure is 15～25bar, and it is dry that the product after moulding enters mesh-belt kiln through rotary conveyor, and dry tenacity is not less than 0.5MPa.After dry, enter in ceramic roller kiln or pushed bat kiln and burn till, firing temperature is that 1020～1060 ℃, cycle are 35min.After burning till, can make and there is hole lithosporic line damping thermal insulation inner wall board.Its water suction is 425%, and volume density is at 651kg/m
3between, the modulus of rupture is 3.15MPa, and thermal conductivity is 0.165W/ (m.k), and burning rank is A1 level.
embodiment 4
The perlite glass bead micro mist of the perlite powder by weight 80%, weight 10%, the Wingdale of weight 5%,, the 500kg admixtion that the graphite of the saltcake of weight 4%, weight 1% forms adds in mixer is dry mixed, and are added the biphosphate Al binding agent of weight 60L and the water glass bonding agent of weight 50L heavily to drop into be uniformly mixed and to cross 20 order reciprocating sieves successively.Powder through being mixed with, after in feed bin old 24 hours, carries out cloth decoration dry-pressing formed, and wherein pressure is 15～25bar, and it is dry that the product after moulding enters mesh-belt kiln through rotary conveyor, and dry tenacity is not less than 0.5MPa.After dry, enter in ceramic roller kiln or pushed bat kiln and burn till, firing temperature is that 1020～1060 ℃, cycle are 35min.After burning till, can make and there is hole lithosporic line damping thermal insulation inner wall board.Its water suction is 305%, and volume density is at 751kg/m
3between, the modulus of rupture is 3.05MPa, and thermal conductivity is 0.173W/ (m.k), and burning rank is A1 level.
The present invention relates to damping thermal insulation decorative material technical field; refer in particular to and utilize perlite deep processing industries mine tailing---perlite powder and perlite glass bead micro mist; as shown in Figure 1; under 1020～1060 ℃ of temperature production conditions; produce water-intake rate and be greater than 300%, volume density is at 650～850kg/m
3between, the modulus of rupture is greater than 3MPa, thermal conductivity is less than 0.20W/ (m.k), burning rank is A1 level, thickness 30～60mm, the house decorative material with hole stone scar decorative effect and damping and heat insulation function, the damping insulation and decoration finishing of the public situation such as it can widespread use meeting room, cinema, hospital, bar or family room.
Above case study on implementation is only for illustrating the preferred embodiment of the present invention; but the present invention is not limited to above-mentioned embodiment; in the ken possessing at described field those of ordinary skill; any modification of doing within the spirit and principles in the present invention, be equal to and substitute and improvement etc., all should be considered as the application's protection domain.
Claims (7)
1. the imitative hole of a heat preservation humidity conditioning stone scar ceramic tile, is characterized in that: its main raw material comprises and being made into according to weight percent: perlite powder 50～90%, perlite glass bead micro mist 5～35%, whipping agent 1～20%, fusing assistant 3～20%; And according to the liquid-containing binder of main raw material weight proportion.
2. according to the imitative hole of a kind of heat preservation humidity conditioning described in claim stone scar ceramic tile, it is characterized in that: described liquid-containing binder according to claim 1 comprises liquid-containing binder A, the 10l/100kg of consumption proportion main raw material weight; Liquid-containing binder B, the 10l/100kg of consumption proportion main raw material weight.
3. according to the imitative hole of a kind of heat preservation humidity conditioning described in claim stone scar ceramic tile, it is characterized in that: described liquid-containing binder A is alkaline binding agent, comprises the aqueous solution of high concentration water's glass, metasilicate pentahydrate sodium and non-hydrate sodium metasilicate; Liquid-containing binder B is acid binding agent, comprises the phosphoric acid emulsion of phosphaljel solution, aluminum oxide.
4. according to the imitative hole of a kind of heat preservation humidity conditioning described in claim stone scar ceramic tile, it is characterized in that: described whipping agent comprises calcium carbonate, saltcake and graphite, is wherein at least one, and fusing assistant comprises fluorite, soda ash, silicon partially, is wherein at least one.
5. according to the imitative hole of a kind of heat preservation humidity conditioning described in claim stone scar ceramic tile; it is characterized in that: described perlite powder and perlite glass bead micro mist be for adopting the dry process following raw material obtaining of 80 orders that sieves whipping agent and the fusing assistant agent raw material for adopting 100 mesh sieves that dry ground is crossed to obtain.
6. according to the imitative hole of a kind of heat preservation humidity conditioning described in claim stone scar ceramic tile, it is characterized in that: the described imitative hole of heat preservation humidity conditioning stone scar ceramic tile, its production method step is as follows:
The imitative hole of a heat preservation humidity conditioning stone scar ceramic tile, is characterized in that preparation method as claimed in claim 1, specific as follows:
Raw material is prepared; To comprise that by perlite powder, perlite glass bead micro mist, whipping agent, solubility promoter be the powdery below 80 orders, above powder is added in mixer and mixed in component ratio, be then sequentially added into liquid-containing binder A and liquid-containing binder B 10～20 mesh sieves, standby after old 24 hours that are uniformly mixed, sieve; Powder after old adds in press, according to the pressure low-pressure moulding of 10～25MPa, product after moulding is dry through mesh belt dry kiln drying, enter in ceramic roller kiln or pushed bat kiln after the glazing of glaze line and burn till, and firing temperature is that 1020～1060 ℃, cycle are 35～60min.
7. the hole lithosporic line that product decoration relies on the decorative pattern of press press distributing mode, mould and burns till rear appearance is realized, and obtains having the ceramic tile of damping heat insulation function and imitative hole stone scar decorative effect.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410221476.8A CN104016702B (en) | 2014-05-26 | 2014-05-26 | The imitative hole stone scar ceramic tile of a kind of heat preservation humidity conditioning and production method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410221476.8A CN104016702B (en) | 2014-05-26 | 2014-05-26 | The imitative hole stone scar ceramic tile of a kind of heat preservation humidity conditioning and production method thereof |
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| CN104016702A true CN104016702A (en) | 2014-09-03 |
| CN104016702B CN104016702B (en) | 2016-06-15 |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104725029A (en) * | 2015-03-22 | 2015-06-24 | 周光惠 | Composite ceramic toughened ceramic brick with humidity adjusting function and production method thereof |
| CN105399336A (en) * | 2015-12-30 | 2016-03-16 | 信阳科美新型材料有限公司 | Perlite foam glass product and production method thereof |
| CN105669173A (en) * | 2016-01-11 | 2016-06-15 | 信阳科美新型材料有限公司 | Thermal insulating decorative ceramic plate produced by comprehensive utilization of perlite waste and production method thereof |
| CN106587640A (en) * | 2016-12-13 | 2017-04-26 | 信阳科美新型材料有限公司 | Light heat insulation and hydrophobic glass bead used for construction and preparation method of light heat insulation and hydrophobic glass bead |
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| CN101234872A (en) * | 2008-03-07 | 2008-08-06 | 张辉 | Vitrification micro-sphere thermal insulating mortar with self humidity-conditioning function |
| CN103626476A (en) * | 2013-12-03 | 2014-03-12 | 信阳方浩实业有限公司 | Method for producing light-weight heat-insulating decorative ceramic plate by using solid waste in production and processing course of expanded pearlite |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104725029A (en) * | 2015-03-22 | 2015-06-24 | 周光惠 | Composite ceramic toughened ceramic brick with humidity adjusting function and production method thereof |
| CN105399336A (en) * | 2015-12-30 | 2016-03-16 | 信阳科美新型材料有限公司 | Perlite foam glass product and production method thereof |
| CN105669173A (en) * | 2016-01-11 | 2016-06-15 | 信阳科美新型材料有限公司 | Thermal insulating decorative ceramic plate produced by comprehensive utilization of perlite waste and production method thereof |
| CN106587640A (en) * | 2016-12-13 | 2017-04-26 | 信阳科美新型材料有限公司 | Light heat insulation and hydrophobic glass bead used for construction and preparation method of light heat insulation and hydrophobic glass bead |
| CN106587640B (en) * | 2016-12-13 | 2019-07-02 | 信阳科美新型材料有限公司 | Light thermal insulation hydrophobic glass pearl for building and preparation method thereof |
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|---|---|
| CN104016702B (en) | 2016-06-15 |
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Effective date of registration: 20220708 Address after: 233500 west of Anchi Avenue, Letu Town, Mengcheng County, Bozhou City, Anhui Province Patentee after: Anhui ruimeng Technology Co.,Ltd. Address before: 464117 Hongguang Industrial Park, Shangtianti Management District, Xinyang City, Henan Province Patentee before: Xinyang Fanghao Industrial Co.,Ltd. |