CN104000849A - Method for improving tastes and colors of Maoxijiao granules - Google Patents
Method for improving tastes and colors of Maoxijiao granules Download PDFInfo
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- CN104000849A CN104000849A CN201410246399.1A CN201410246399A CN104000849A CN 104000849 A CN104000849 A CN 104000849A CN 201410246399 A CN201410246399 A CN 201410246399A CN 104000849 A CN104000849 A CN 104000849A
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Abstract
The invention relates to a method for improving the tastes and colors of Maoxijiao granules. The method comprises the following steps: (1) cleaning the yak skin of the specific wildyak on the Tibetan Plateau, and then alkalizing and soaking the yak skin, thus obtaining the unhaired yak skin; (2) soaking and dealkalizing the unhaired yak skin, thus obtaining the dealkalized and unhaired yak skin; (3) blanching the dealkalized and unhaired yak skin, thus obtaining the degreased yak skin; (4) extracting the degreased yak skin with water to obtain filtrate A; (5) concentrating the filtrate A, then adding an alum solution, and standing and refrigerating to obtain filtrate B; (6) concentrating the filtrate B, and then extracting the foam, thus obtaining a Maoxijiao solution; (7) adding wine to the Maoxijiao solution, and then concentrating and drying the solution, thus obtaining Maoxijiao powder; (8) extracting prepared rehmannia root with water, thus obtaining filtrate C; (9) mixing radix astragali, angelica sinensis, Chinese dates, medlar and dried longan pulp, then extracting the mixture with water, and concentrating the mixture, thus obtaining a concentrated solution; (10) mixing the filtrate C with the concentrated solution, and then concentrating and drying the mixture, thus obtaining accessory powder; (11) mixing the Maoxijiao powder with the accessory powder uniformly, and granulating the mixture according to the conventional method, thus obtaining the Maoxijiao granules. The method is simple in process and low in cost.
Description
Technical field
The present invention relates to Chinese medicine composition preparing technical field, relate in particular to a kind of method of improving Yak skin glue granule mouthfeel, color and luster.
Background technology
Yak skin glue, taking yak skin as primary raw material, is aided with Qinghai-Tibet special medicinal material---and Radix Rehmanniae Preparata, the Radix Astragali, Radix Angelicae Sinensis, Fructus Jujubae, Fructus Lycii, Arillus Longan, can be made into the granule with blood tonification effect through extracting.Its production process is generally: pretreated yak skin dry product is put in multi-function extractor, first added the water of 1 ~ 2 times of weight, then add weight 1/300 ~ 1/1000NaOH defat, airtight extraction pot, heats, and boils 0.5 ~ 1 hour, pressure 0.11 ~ 0.12MPa, repeatedly adds water and rinses to pH value to neutral, puts water purification, add water again 1 ~ 2 times, heating, pressure 0.1 ~ 0.15MPa, extract, time is 8 ~ 20 hours, and extract filters, and filtrate is for subsequent use; Filtering residue adds 1 ~ 2 times of water of weight, second extraction, and 1 ~ 8 hour time, extract filters, merging filtrate, in extraction, once, 5 minutes time, 60 DEG C of concentrated medicaments are to density 1.074 ~ 1.091g/cm in aerofluxus per hour
3, after spraying is dry, obtain rubber powder.
But there is the micro-raw meat of abnormal smells from the patient in the Yak skin glue granule that adopts this explained hereafter, it is not good to take rear mouthfeel, the problem that aftertaste is turned sour.
Summary of the invention
Technical problem to be solved by this invention is to provide a kind of technique method of improving Yak skin glue granule mouthfeel, color and luster simple, with low cost.
For addressing the above problem, a kind of method of improving Yak skin glue granule mouthfeel, color and luster of the present invention, comprises the following steps:
(1) yak skin 3000 ~ 5000g is fresh or dry Qinghai-Tibet Platean peculiar cattle kind yak wild yak through infiltrating, after softening cleans up, then adding mass concentration by 2 ~ 3 times of its weight is 0.5 ~ 10% alkali, be to soak 24 ~ 72 hours under the condition of 20 ~ 38 DEG C in temperature, obtain the yak skin after depilation;
(2) the yak skin after described depilation being added to water by 3 ~ 5 times of its weight, is to soak dealkalize under the condition of 20 ~ 30 DEG C in water temperature, repeats 1 ~ 4 time, and each 10 ~ 30 minutes, then clear water rinsed, and cleaned remaining soft flocks, and measured pH value, obtained the yak skin of dealkalize depilation;
(3) the yak skin of described dealkalize depilation being cut into the fritter of 3 ~ 5cm, then add the water of 5 ~ 20 times of its weight, is the skin 2 ~ 3 times of scalding under the condition of 40 ~ 60 DEG C in temperature, obtains the yak skin after defat;
(4) the yak skin after described defat is extracted with the water of 8 ~ 12 times of its quality, after 2 ~ 10 hours, filter, discard residue, obtain filtrate A;
By described filtrate A 50 ~ 80 DEG C be concentrated into proportion and be 1:1.1 ~ 1:1.3 after, adding mass concentration is 2 ~ 10% alum solution, stirs, and leaves standstill 4 ~ 12h at 25 ~ 35 DEG C, then, at 5 ~ 10 DEG C of cold preservation 6 ~ 12h, removes by filter precipitate, obtains liquor B;
By described liquor B in the time that 60 ~ 80 DEG C are concentrated into proportion and are 1:1.3 ~ 1:1.5, add 0 ~ 10 DEG C of pure water to start to carry foam, repeatable operation 3 ~ 8 times, obtains the glue of Yak skin glue;
(7) in the glue of described Yak skin glue, add the yellow wine of its volume 3 ~ 6% or the mixture of barley wine or yellow wine-barley wine, stir, in the time being concentrated into proportion 1:1.0 ~ 1:1.3 for 50 ~ 70 DEG C, obtain glue, the spray-dried Yak skin glue powder that obtains of this glue;
(8) 20 ~ 500g Radix Rehmanniae Preparata being added water by 4 ~ 10 times of its quality, is to extract 2 times under the condition of 70 ~ 100 DEG C in temperature, and each extraction time is 2 ~ 4 hours, merges and obtains extracting solution A; The active carbon or kieselguhr or the active carbon-diatomaceous mixture that in described extracting solution A, add its volume 3 ~ 10%, stir evenly, and under room temperature, leaves standstill 6 ~ 12 hours, filters, and obtains liquor C;
(9) after 30 ~ 80g Radix Astragali, 50 ~ 400g Radix Angelicae Sinensis, 10 ~ 500g Fructus Jujubae, 10 ~ 300g Fructus Lycii, 20 ~ 400g Arillus Longan being mixed, add water by 3 ~ 10 times of mixture quality, be to extract 2 times under the condition of 70 ~ 100 DEG C in temperature, each extraction time is 1 ~ 4 hour, merge and obtain extracting solution B, it is 1:1.5 that this extracting solution B is concentrated into proportion at 60 ~ 90 DEG C, obtains concentrated solution;
(10) after described liquor C being mixed with described concentrated solution, stir, being concentrated into proportion at 60 ~ 90 DEG C is 1:1.5, the spray-dried ingredient powder that obtains;
(11) described Yak skin glue powder is mixed homogeneously with described ingredient powder, granulate according to a conventional method.
The alkali of described step in (1) refers to the one in sodium hydroxide solution, potassium hydroxide solution, sodium bicarbonate solution.
The described step (7) alcoholic strength of middle barley wine is 46 ~ 52 DEG C.
Described step (7) in the mixture of yellow wine-barley wine refer to the mixture that yellow wine and barley wine are mixed in the ratio of 1mL:0.1 ~ 0.5mL.
(8) active carbon of described step-diatomaceous mixture refers to the mixture that active carbon and kieselguhr are mixed in the ratio of 1g:0.1 ~ 0.3g.
Described step (7) with described step (10) in spray-dired condition refer to mist flow 20 ~ 25mL/min, 35 ~ 45 DEG C of feeding temperatures, 170 ~ 180 DEG C of inlet temperature.
Replace step described in claim 1 (9) by following preparation method: after 30 ~ 80g Radix Astragali, 50 ~ 400g Radix Angelicae Sinensis, 10 ~ 500g Fructus Jujubae are mixed, add water by 3 ~ 10 times of its mixture quality, be to extract under the condition of 70 ~ 100 DEG C in temperature, after 1 ~ 4 hour, obtain extracting solution B; In described extracting solution B, adding 10 ~ 300g Fructus Lycii, 20 ~ 400g Arillus Longan, is to extract under the condition of 70 ~ 100 DEG C in temperature, obtains extracting solution C after 1 ~ 4 hour, and it is 1:1.5 that this extracting solution C is concentrated into proportion at 60 ~ 90 DEG C, obtains concentrated solution.
Replace step described in claim 1 (9) by following preparation method: after 50 ~ 400g Radix Angelicae Sinensis, 10 ~ 500g Fructus Jujubae, 10 ~ 300g Fructus Lycii are mixed, add water by 3 ~ 10 times of its mixture quality, be to extract under the condition of 70 ~ 100 DEG C in temperature, after 1 ~ 4 hour, obtain extracting solution B; In described extracting solution B, adding 30 ~ 80g Radix Astragali, 20 ~ 400g Arillus Longan, is to extract under the condition of 70 ~ 100 DEG C in temperature, obtains extracting solution C after 1 ~ 4 hour, and it is 1:1.5 that this extracting solution C is concentrated into proportion at 60 ~ 90 DEG C, obtains concentrated solution.
Replace step described in claim 1 (9) by following preparation method: after 10 ~ 300g Fructus Lycii, 20 ~ 400g Arillus Longan are mixed, adding water by 3 ~ 10 times of its mixture quality, is to extract under the condition of 70 ~ 100 DEG C in temperature, obtains extracting solution B after 1 ~ 4 hour; In described extracting solution B, adding 30 ~ 80g Radix Astragali, 10 ~ 500g Fructus Jujubae, 50 ~ 400g Radix Angelicae Sinensis, is to extract under the condition of 70 ~ 100 DEG C in temperature, obtains extracting solution C after 1 ~ 4 hour, and it is 1:1.5 that this extracting solution C is concentrated into proportion at 60 ~ 90 DEG C, obtains concentrated solution.
The present invention compared with prior art has the following advantages:
1, the present invention has increased except foreign protein operation, by adding 2 ~ 20% alum solutions effectively to remove impurity and foreign protein.
2, the present invention has increased and has put forward foam operation, by adding 0 ~ 10 DEG C of pure water repeatedly to carry foam, obtains shinny glue juice.
3, the present invention has increased taste masking operation, by add one or both mixture of 3 ~ 6% yellow wine or barley wine in glue, reaches the object of improving mouthfeel.
4, the present invention has increased bleaching process, by adopting active carbon, kieselguhr or active carbon, diatomaceous mixture, has effectively improved color and luster.
5, the present invention has increased unique abstraction process of adjuvant, in adjuvant extracts, has adopted and has been decocted first and rear lower technology, has effectively improved mouthfeel.
Detailed description of the invention
embodiment 1a method of improving Yak skin glue granule mouthfeel, color and luster, comprises the following steps:
(1) yak skin 3000g is fresh or dry Qinghai-Tibet Platean peculiar cattle kind yak wild yak through infiltrating, after softening cleans up, then adding mass concentration by 2 times of its weight is 0.5% alkali, be to soak 72 hours under the condition of 20 DEG C in temperature, obtain the yak skin after depilation.
Wherein: alkali refers to sodium hydroxide solution.
(2) the yak skin after depilation being added to water by 3 times of its weight, is to soak dealkalize 10 minutes under the condition of 20 DEG C in water temperature, and then clear water rinses, and cleans remaining soft flocks, and measures pH value, obtains the yak skin of dealkalize depilation.
(3) the yak skin of dealkalize depilation being cut into the fritter of 3cm, then add the water of 5 times of its weight, is the skin 2 times of scalding under the condition of 40 DEG C in temperature, obtains the yak skin after defat.
(4) the yak skin after defat is extracted with the water of 8 times of its quality, after 2 hours, filter, discard residue, obtain filtrate A.
By filtrate A 50 DEG C be concentrated into proportion and be 1:1.1 after, adding mass concentration is 2% alum solution, stirs, and leaves standstill 12h at 25 DEG C, then, at 5 DEG C of cold preservation 12h, removes by filter precipitate, obtains liquor B.
By liquor B in the time that 60 DEG C are concentrated into proportion and are 1:1.3, add 0 DEG C of pure water to start to carry foam, repeatable operation 3 times, obtains the glue of Yak skin glue.
(7) in the glue of Yak skin glue, add the yellow wine of its volume 3%, stir, in the time being concentrated into proportion 1:1.0 for 50 DEG C, obtain glue, this glue is the spray-dried Yak skin glue powder that obtains under the condition of mist flow 20mL/min, 35 DEG C of feeding temperatures, 170 DEG C of inlet temperature.
(8) 20g Radix Rehmanniae Preparata being added water by 4 times of its quality, is to extract 2 times under the condition of 70 DEG C in temperature, and each extraction time is 2 hours, merges and obtains extracting solution A; The active carbon that adds its volume 3% in extracting solution A, stirs evenly, and under room temperature, leaves standstill 6 hours, filters, and obtains liquor C.
(9) after the 30g Radix Astragali, 50g Radix Angelicae Sinensis, 10g Fructus Jujubae, 10g Fructus Lycii, 20g Arillus Longan being mixed, add water by 3 times of mixture quality, be to extract 2 times under the condition of 70 DEG C in temperature, each extraction time is 1 hour, merge and obtain extracting solution B, it is 1:1.5 that this extracting solution B is concentrated into proportion at 60 DEG C, obtains concentrated solution.
(10) after liquor C being mixed with concentrated solution, stir, being concentrated into proportion at 60 DEG C is 1:1.5, the spray-dried ingredient powder that obtains under the condition of mist flow 20mL/min, 35 DEG C of feeding temperatures, 170 DEG C of inlet temperature.
(11) Yak skin glue powder is mixed homogeneously with ingredient powder, granulate according to a conventional method.
embodiment 2a method of improving Yak skin glue granule mouthfeel, color and luster, comprises the following steps:
(1) yak skin 5000g is fresh or dry Qinghai-Tibet Platean peculiar cattle kind yak wild yak through infiltrating, after softening cleans up, then adding mass concentration by 3 times of its weight is 10% alkali, be to soak 24 hours under the condition of 38 DEG C in temperature, obtain the yak skin after depilation.
Wherein: alkali refers to potassium hydroxide solution.
(2) the yak skin after depilation being added to water by 5 times of its weight, is to soak dealkalize under the condition of 30 DEG C in water temperature, repeats 4 times, and each 30 minutes, then clear water rinsed, and cleaned remaining soft flocks, and measured pH value, obtained the yak skin that dealkalize is lost hair or feathers.
(3) the yak skin of dealkalize depilation being cut into the fritter of 5cm, then add the water of 20 times of its weight, is the skin 3 times of scalding under the condition of 60 DEG C in temperature, obtains the yak skin after defat.
(4) the yak skin after defat is extracted with the water of 12 times of its quality, after 10 hours, filter, discard residue, obtain filtrate A.
By filtrate A 80 DEG C be concentrated into proportion and be 1:1.3 after, adding mass concentration is 10% alum solution, stirs, and leaves standstill 4h at 35 DEG C, then, at 10 DEG C of cold preservation 6h, removes by filter precipitate, obtains liquor B.
By liquor B in the time that 80 DEG C are concentrated into proportion and are 1:1.5, add 10 DEG C of pure water to start to carry foam, repeatable operation 8 times, obtains the glue of Yak skin glue.
(7) in the glue of Yak skin glue, add the barley wine of its volume 6%, stir, in the time being concentrated into proportion 1:1.3 for 70 DEG C, obtain glue, this glue is the spray-dried Yak skin glue powder that obtains under the condition of mist flow 25mL/min, 45 DEG C of feeding temperatures, 180 DEG C of inlet temperature.
Wherein: the alcoholic strength of barley wine is 46 DEG C.
(8) 500g Radix Rehmanniae Preparata being added water by 10 times of its quality, is to extract 2 times under the condition of 100 DEG C in temperature, and each extraction time is 4 hours, merges and obtains extracting solution A; The kieselguhr that adds its volume 10% in extracting solution A, stirs evenly, and under room temperature, leaves standstill 12 hours, filters, and obtains liquor C.
(9) after the 80g Radix Astragali, 400g Radix Angelicae Sinensis, 500g Fructus Jujubae, 300g Fructus Lycii, 400g Arillus Longan being mixed, add water by 10 times of mixture quality, be to extract 2 times under the condition of 100 DEG C in temperature, each extraction time is 4 hours, merge and obtain extracting solution B, it is 1:1.5 that this extracting solution B is concentrated into proportion at 90 DEG C, obtains concentrated solution.
(10) after liquor C being mixed with concentrated solution, stir, being concentrated into proportion at 90 DEG C is 1:1.5, the spray-dried ingredient powder that obtains under the condition of mist flow 25mL/min, 45 DEG C of feeding temperatures, 180 DEG C of inlet temperature.
(11) Yak skin glue powder is mixed homogeneously with ingredient powder, granulate according to a conventional method.
embodiment 3a method of improving Yak skin glue granule mouthfeel, color and luster, comprises the following steps:
(1) yak skin 4000g is fresh or dry Qinghai-Tibet Platean peculiar cattle kind yak wild yak through infiltrating, after softening cleans up, then adding mass concentration by 2.5 times of its weight is 1% alkali, be to soak 36 hours under the condition of 25 DEG C in temperature, obtain the yak skin after depilation.
Wherein: alkali refers to sodium bicarbonate solution.
(2) the yak skin after depilation being added to water by 4 times of its weight, is to soak dealkalize under the condition of 25 DEG C in water temperature, repeats 2 times, and each 20 minutes, then clear water rinsed, and cleaned remaining soft flocks, and measured pH value, obtained the yak skin that dealkalize is lost hair or feathers.
(3) the yak skin of dealkalize depilation being cut into the fritter of 4cm, then add the water of 10 times of its weight, is the skin 2 times of scalding under the condition of 50 DEG C in temperature, obtains the yak skin after defat.
(4) the yak skin after defat is extracted with the water of 10 times of its quality, after 6 hours, filter, discard residue, obtain filtrate A.
By filtrate A 60 DEG C be concentrated into proportion and be 1:1.2 after, adding mass concentration is 6% alum solution, stirs, and leaves standstill 8h at 30 DEG C, then, at 8 DEG C of cold preservation 8h, removes by filter precipitate, obtains liquor B.
By liquor B in the time that 70 DEG C are concentrated into proportion and are 1:1.4, add 5 DEG C of pure water to start to carry foam, repeatable operation 5 times, obtains the glue of Yak skin glue.
(7) in the glue of Yak skin glue, add the mixture of the yellow wine-barley wine of its volume 5%, stir, in the time being concentrated into proportion 1:1.1 for 60 DEG C, obtain glue, this glue is the spray-dried Yak skin glue powder that obtains under the condition of mist flow 23mL/min, 40 DEG C of feeding temperatures, 175 DEG C of inlet temperature.
Wherein: the alcoholic strength of barley wine is 46 DEG C.
The mixture of yellow wine-barley wine refers to the mixture that yellow wine and barley wine are mixed in the ratio of 1mL:0.1mL.
(8) 100g Radix Rehmanniae Preparata being added water by 7 times of its quality, is to extract 2 times under the condition of 80 DEG C in temperature, and each extraction time is 3 hours, merges and obtains extracting solution A; Active carbon-diatomaceous the mixture that adds its volume 6% in extracting solution A, stirs evenly, and under room temperature, leaves standstill 8 hours, filters, and obtains liquor C.
Wherein: active carbon-diatomaceous mixture refers to the mixture that active carbon and kieselguhr are mixed in the ratio of 1g:0.1g.
(9) after the 50g Radix Astragali, 100g Radix Angelicae Sinensis, 100g Fructus Jujubae, 100g Fructus Lycii, 100g Arillus Longan being mixed, add water by 5 times of mixture quality, be to extract 2 times under the condition of 80 DEG C in temperature, each extraction time is 2 hours, merge and obtain extracting solution B, it is 1:1.5 that this extracting solution B is concentrated into proportion at 80 DEG C, obtains concentrated solution.
(10) after liquor C being mixed with concentrated solution, stir, being concentrated into proportion at 80 DEG C is 1:1.5, the spray-dried ingredient powder that obtains under the condition of mist flow 23mL/min, 40 DEG C of feeding temperatures, 175 DEG C of inlet temperature.
(11) Yak skin glue powder is mixed homogeneously with ingredient powder, granulate according to a conventional method.
embodiment 4a method of improving Yak skin glue granule mouthfeel, color and luster, comprises the following steps:
(1) yak skin 3200g is fresh or dry Qinghai-Tibet Platean peculiar cattle kind yak wild yak through infiltrating, after softening cleans up, then adding mass concentration by 2 times of its weight is 1.5% alkali, be to soak 26 hours under the condition of 22 DEG C in temperature, obtain the yak skin after depilation.
Wherein: alkali refers to sodium hydroxide solution.
(2) the yak skin after depilation being added to water by 3.5 times of its weight, is to soak dealkalize under the condition of 22 DEG C in water temperature, repeats 3 times, and each 15 minutes, then clear water rinsed, and cleaned remaining soft flocks, and measured pH value, obtained the yak skin that dealkalize is lost hair or feathers.
(3) the yak skin of dealkalize depilation being cut into the fritter of 3cm, then add the water of 6 times of its weight, is the skin 2 times of scalding under the condition of 42 DEG C in temperature, obtains the yak skin after defat.
(4) the yak skin after defat is extracted with the water of 8.5 times of its quality, after 3 hours, filter, discard residue, obtain filtrate A.
By filtrate A 55 DEG C be concentrated into proportion and be 1:1.1 after, adding mass concentration is 3% alum solution, stirs, and leaves standstill 6h at 28 DEG C, then, at 6 DEG C of cold preservation 7h, removes by filter precipitate, obtains liquor B.
By liquor B in the time that 65 DEG C are concentrated into proportion and are 1:1.3, add 2 DEG C of pure water to start to carry foam, repeatable operation 4 times, obtains the glue of Yak skin glue.
(7) in the glue of Yak skin glue, add the barley wine of its volume 4%, stir, in the time being concentrated into proportion 1:1.2 for 50 ~ 70 DEG C, obtain glue, this glue is the spray-dried Yak skin glue powder that obtains under the condition of mist flow 20mL/min, 35 DEG C of feeding temperatures, 170 DEG C of inlet temperature.
Wherein: the alcoholic strength of barley wine is 52 DEG C.
(8) 50g Radix Rehmanniae Preparata being added water by 5 times of its quality, is to extract 2 times under the condition of 75 DEG C in temperature, and each extraction time is 2.5 hours, merges and obtains extracting solution A; Active carbon-diatomaceous the mixture that adds its volume 4% in extracting solution A, stirs evenly, and under room temperature, leaves standstill 10 hours, filters, and obtains liquor C.
Wherein: active carbon-diatomaceous mixture refers to the mixture that active carbon and kieselguhr are mixed in the ratio of 1g:0.3g.
(9) after the 40g Radix Astragali, 150g Radix Angelicae Sinensis, 50g Fructus Jujubae being mixed, adding water by 4 times of its mixture quality, is to extract under the condition of 75 DEG C in temperature, obtains extracting solution B after 3 hours; In extracting solution B, adding 50g Fructus Lycii, 50g Arillus Longan, is to extract under the condition of 75 DEG C in temperature, obtains extracting solution C after 3 hours, and it is 1:1.5 that this extracting solution C is concentrated into proportion at 65 DEG C, obtains concentrated solution.
(10) after liquor C being mixed with concentrated solution, stir, being concentrated into proportion at 65 DEG C is 1:1.5, the spray-dried ingredient powder that obtains under the condition of mist flow 20mL/min, 35 DEG C of feeding temperatures, 170 DEG C of inlet temperature.
(11) Yak skin glue powder is mixed homogeneously with ingredient powder, granulate according to a conventional method.
embodiment 5a method of improving Yak skin glue granule mouthfeel, color and luster, comprises the following steps:
(1) yak skin 3400g is fresh or dry Qinghai-Tibet Platean peculiar cattle kind yak wild yak through infiltrating, after softening cleans up, then adding mass concentration by 3 times of its weight is 2.5% alkali, be to soak 48 hours under the condition of 28 DEG C in temperature, obtain the yak skin after depilation.
Wherein: alkali refers to potassium hydroxide solution.
(2) the yak skin after depilation being added to water by 4.5 times of its weight, is to soak dealkalize under the condition of 24 DEG C in water temperature, repeats 2 times, and each 25 minutes, then clear water rinsed, and cleaned remaining soft flocks, and measured pH value, obtained the yak skin that dealkalize is lost hair or feathers.
(3) the yak skin of dealkalize depilation being cut into the fritter of 5cm, then add the water of 8 times of its weight, is the skin 3 times of scalding under the condition of 45 DEG C in temperature, obtains the yak skin after defat.
(4) the yak skin after defat is extracted with the water of 9 times of its quality, after 4 hours, filter, discard residue, obtain filtrate A.
By filtrate A 50 ~ 80 DEG C be concentrated into proportion and be 1:1.3 after, adding mass concentration is 5% alum solution, stirs, and leaves standstill 10h at 32 DEG C, then, at 6 DEG C of cold preservation 10h, removes by filter precipitate, obtains liquor B.
By liquor B in the time that 75 DEG C are concentrated into proportion and are 1:1.5, add 4 DEG C of pure water to start to carry foam, repeatable operation 6 times, obtains the glue of Yak skin glue.
(7) in the glue of Yak skin glue, add the barley wine of its volume 3.5%, stir, in the time being concentrated into proportion 1:1.0 for 55 DEG C, obtain glue, this glue is the spray-dried Yak skin glue powder that obtains under the condition of mist flow 25mL/min, 45 DEG C of feeding temperatures, 180 DEG C of inlet temperature.
Wherein: the alcoholic strength of barley wine is 49 DEG C.
(8) 150g Radix Rehmanniae Preparata being added water by 6 times of its quality, is to extract 2 times under the condition of 85 DEG C in temperature, and each extraction time is 3.5 hours, merges and obtains extracting solution A; Active carbon-diatomaceous the mixture that adds its volume 8% in extracting solution A, stirs evenly, and under room temperature, leaves standstill 6 hours, filters, and obtains liquor C.
Wherein: active carbon-diatomaceous mixture refers to the mixture that active carbon and kieselguhr are mixed in the ratio of 1g:0.2g.
(9) after the 60g Radix Astragali, 200g Radix Angelicae Sinensis, 150g Fructus Jujubae being mixed, adding water by 6 times of its mixture quality, is to extract under the condition of 85 DEG C in temperature, obtains extracting solution B after 1 hour; In extracting solution B, adding 150g Fructus Lycii, 150g Arillus Longan, is to extract under the condition of 85 DEG C in temperature, obtains extracting solution C after 1 hour, and it is 1:1.5 that this extracting solution C is concentrated into proportion at 70 DEG C, obtains concentrated solution.
(10) after liquor C being mixed with concentrated solution, stir, being concentrated into proportion at 70 DEG C is 1:1.5, the spray-dried ingredient powder that obtains under the condition of mist flow 25mL/min, 45 DEG C of feeding temperatures, 180 DEG C of inlet temperature.
(11) Yak skin glue powder is mixed homogeneously with ingredient powder, granulate according to a conventional method.
embodiment 6a method of improving Yak skin glue granule mouthfeel, color and luster, comprises the following steps:
(1) yak skin 3600g is fresh or dry Qinghai-Tibet Platean peculiar cattle kind yak wild yak through infiltrating, after softening cleans up, then adding mass concentration by 2.5 times of its weight is 3% alkali, be to soak 60 hours under the condition of 35 DEG C in temperature, obtain the yak skin after depilation.
Wherein: alkali refers to sodium bicarbonate solution.
(2) the yak skin after depilation being added to water by 4 times of its weight, is to soak dealkalize under the condition of 28 DEG C in water temperature, repeats 4 times, and each 10 minutes, then clear water rinsed, and cleaned remaining soft flocks, and measured pH value, obtained the yak skin that dealkalize is lost hair or feathers.
(3) the yak skin of dealkalize depilation being cut into the fritter of 4cm, then add the water of 15 times of its weight, is the skin 3 times of scalding under the condition of 55 DEG C in temperature, obtains the yak skin after defat.
(4) the yak skin after defat is extracted with the water of 8 times of its quality, after 10 hours, filter, discard residue, obtain filtrate A.
By filtrate A 50 DEG C be concentrated into proportion and be 1:1.3 after, adding mass concentration is 8% alum solution, stirs, and leaves standstill 12h at 25 DEG C, then, at 5 DEG C of cold preservation 12h, removes by filter precipitate, obtains liquor B.
By liquor B in the time that 60 DEG C are concentrated into proportion and are 1:1.3, add 0 DEG C of pure water to start to carry foam, repeatable operation 3 times, obtains the glue of Yak skin glue.
(7) in the glue of Yak skin glue, add the mixture of the yellow wine-barley wine of its volume 3%, stir, in the time being concentrated into proportion 1:1.0 for 50 DEG C, obtain glue, this glue is the spray-dried Yak skin glue powder that obtains under the condition of mist flow 23mL/min, 40 DEG C of feeding temperatures, 175 DEG C of inlet temperature.
Wherein: the alcoholic strength of barley wine is 52 DEG C.
The mixture of yellow wine-barley wine refers to the mixture that yellow wine and barley wine are mixed in the ratio of 1mL:0.5mL.
(8) 200g Radix Rehmanniae Preparata being added water by 6 times of its quality, is to extract 2 times under the condition of 70 DEG C in temperature, and each extraction time is 4 hours, merges and obtains extracting solution A; The active carbon that adds its volume 3% in extracting solution A, stirs evenly, and under room temperature, leaves standstill 6 hours, filters, and obtains liquor C.
(9) after the 60g Radix Astragali, 200g Radix Angelicae Sinensis, 200g Fructus Jujubae being mixed, adding water by 3 times of its mixture quality, is to extract under the condition of 70 DEG C in temperature, obtains extracting solution B after 4 hours; In extracting solution B, adding 200g Fructus Lycii, 200g Arillus Longan, is to extract under the condition of 70 DEG C in temperature, obtains extracting solution C after 4 hours, and it is 1:1.5 that this extracting solution C is concentrated into proportion at 60 DEG C, obtains concentrated solution.
(10) after liquor C being mixed with concentrated solution, stir, being concentrated into proportion at 60 DEG C is 1:1.5, the spray-dried ingredient powder that obtains under the condition of mist flow 23mL/min, 40 DEG C of feeding temperatures, 175 DEG C of inlet temperature.
(11) Yak skin glue powder is mixed homogeneously with ingredient powder, granulate according to a conventional method.
embodiment 7a method of improving Yak skin glue granule mouthfeel, color and luster, comprises the following steps:
(1) yak skin 3800g is fresh or dry Qinghai-Tibet Platean peculiar cattle kind yak wild yak through infiltrating, after softening cleans up, then adding mass concentration by 2 times of its weight is 3.5% alkali, be to soak 24 hours under the condition of 38 DEG C in temperature, obtain the yak skin after depilation.
Wherein: alkali refers to sodium hydroxide solution.
(2) the yak skin after depilation being added to water by 3 times of its weight, is to soak dealkalize under the condition of 30 DEG C in water temperature, repeats 2 times, and each 20 minutes, then clear water rinsed, and cleaned remaining soft flocks, and measured pH value, obtained the yak skin that dealkalize is lost hair or feathers.
(3) the yak skin of dealkalize depilation being cut into the fritter of 4cm, then add the water of 10 times of its weight, is the skin 3 times of scalding under the condition of 50 DEG C in temperature, obtains the yak skin after defat.
(4) the yak skin after defat is extracted with the water of 12 times of its quality, after 6 hours, filter, discard residue, obtain filtrate A.
By filtrate A 80 DEG C be concentrated into proportion and be 1:1.3 after, adding mass concentration is 10% alum solution, stirs, and leaves standstill 4h at 35 DEG C, then, at 10 DEG C of cold preservation 6h, removes by filter precipitate, obtains liquor B.
By liquor B in the time that 80 DEG C are concentrated into proportion and are 1:1.5, add 10 DEG C of pure water to start to carry foam, repeatable operation 8 times, obtains the glue of Yak skin glue.
(7) in the glue of Yak skin glue, add the mixture of the yellow wine-barley wine of its volume 6%, stir, in the time being concentrated into proportion 1:1.3 for 70 DEG C, obtain glue, this glue is the spray-dried Yak skin glue powder that obtains under the condition of mist flow 20mL/min, 35 DEG C of feeding temperatures, 170 DEG C of inlet temperature.
Wherein: the alcoholic strength of barley wine is 49 DEG C.
The mixture of yellow wine-barley wine refers to the mixture that yellow wine and barley wine are mixed in the ratio of 1mL:0.3mL.
(8) 300g Radix Rehmanniae Preparata being added water by 5 times of its quality, is to extract 2 times under the condition of 90 DEG C in temperature, and each extraction time is 3 hours, merges and obtains extracting solution A; The active carbon that adds its volume 8% in extracting solution A, stirs evenly, and under room temperature, leaves standstill 8 hours, filters, and obtains liquor C.
(9) after 250g Radix Angelicae Sinensis, 250g Fructus Jujubae, 250g Fructus Lycii being mixed, adding water by 8 times of its mixture quality, is to extract under the condition of 90 DEG C in temperature, obtains extracting solution B after 1 hour; In extracting solution B, adding the 80g Radix Astragali, 250g Arillus Longan, is to extract under the condition of 90 DEG C in temperature, obtains extracting solution C after 1 hour, and it is 1:1.5 that this extracting solution C is concentrated into proportion at 80 DEG C, obtains concentrated solution.
(10) after liquor C being mixed with concentrated solution, stir, being concentrated into proportion at 80 DEG C is 1:1.5, the spray-dried ingredient powder that obtains under the condition of mist flow 20mL/min, 35 DEG C of feeding temperatures, 170 DEG C of inlet temperature.
(11) Yak skin glue powder is mixed homogeneously with ingredient powder, granulate according to a conventional method.
embodiment 8a method of improving Yak skin glue granule mouthfeel, color and luster, comprises the following steps:
(1) yak skin 4200g is fresh or dry Qinghai-Tibet Platean peculiar cattle kind yak wild yak through infiltrating, after softening cleans up, then adding mass concentration by 3 times of its weight is 4% alkali, be to soak 40 hours under the condition of 30 DEG C in temperature, obtain the yak skin after depilation.
Wherein: alkali refers to potassium hydroxide solution.
(2) the yak skin after depilation being added to water by 5 times of its weight, is to soak dealkalize 10 minutes under the condition of 20 DEG C in water temperature, and then clear water rinses, and cleans remaining soft flocks, and measures pH value, obtains the yak skin of dealkalize depilation.
(3) the yak skin of dealkalize depilation being cut into the fritter of 5cm, then add the water of 20 times of its weight, is the skin 2 times of scalding under the condition of 60 DEG C in temperature, obtains the yak skin after defat.
(4) the yak skin after defat is extracted with the water of 10 times of its quality, after 8 hours, filter, discard residue, obtain filtrate A.
By filtrate A 60 DEG C be concentrated into proportion and be 1:1.2 after, adding mass concentration is 6% alum solution, stirs, and leaves standstill 8h at 30 DEG C, then, at 8 DEG C of cold preservation 10h, removes by filter precipitate, obtains liquor B.
By liquor B in the time that 75 DEG C are concentrated into proportion and are 1:1.4, add 5 DEG C of pure water to start to carry foam, repeatable operation 4 times, obtains the glue of Yak skin glue.
(7) in the glue of Yak skin glue, add the yellow wine of its volume 5%, stir, in the time being concentrated into proportion 1:1.2 for 55 DEG C, obtain glue, this glue is the spray-dried Yak skin glue powder that obtains under the condition of mist flow 25mL/min, 45 DEG C of feeding temperatures, 180 DEG C of inlet temperature.
(8) 400g Radix Rehmanniae Preparata being added water by 10 times of its quality, is to extract 2 times under the condition of 100 DEG C in temperature, and each extraction time is 2 hours, merges and obtains extracting solution A; The kieselguhr that adds its volume 3% in extracting solution A, stirs evenly, and under room temperature, leaves standstill 6 hours, filters, and obtains liquor C.
(9) after 400g Radix Angelicae Sinensis, 500g Fructus Jujubae, 300g Fructus Lycii being mixed, adding water by 10 times of its mixture quality, is to extract under the condition of 100 DEG C in temperature, obtains extracting solution B after 1 hour; In extracting solution B, adding the 80g Radix Astragali, 400g Arillus Longan, is to extract under the condition of 100 DEG C in temperature, obtains extracting solution C after 1 hour, and it is 1:1.5 that this extracting solution C is concentrated into proportion at 90 DEG C, obtains concentrated solution.
(10) after liquor C being mixed with concentrated solution, stir, being concentrated into proportion at 90 DEG C is 1:1.5, the spray-dried ingredient powder that obtains under the condition of mist flow 25mL/min, 45 DEG C of feeding temperatures, 180 DEG C of inlet temperature.
(11) Yak skin glue powder is mixed homogeneously with ingredient powder, granulate according to a conventional method.
embodiment 9a method of improving Yak skin glue granule mouthfeel, color and luster, comprises the following steps:
(1) yak skin 4400g is fresh or dry Qinghai-Tibet Platean peculiar cattle kind yak wild yak through infiltrating, after softening cleans up, then adding mass concentration by 2.5 times of its weight is 4.5% alkali, be to soak 24 hours under the condition of 32 DEG C in temperature, obtain the yak skin after depilation.
Wherein: alkali refers to sodium bicarbonate solution.
(2) the yak skin after depilation being added to water by 3 times of its weight, is to soak dealkalize under the condition of 20 DEG C in water temperature, repeats 4 times, and each 10 minutes, then clear water rinsed, and cleaned remaining soft flocks, and measured pH value, obtained the yak skin that dealkalize is lost hair or feathers.
(3) the yak skin of dealkalize depilation being cut into the fritter of 3cm, then add the water of 5 times of its weight, is the skin 3 times of scalding under the condition of 40 DEG C in temperature, obtains the yak skin after defat.
(4) the yak skin after defat is extracted with the water of 8 times of its quality, after 10 hours, filter, discard residue, obtain filtrate A.
By filtrate A 50 DEG C be concentrated into proportion and be 1:1.1 after, adding mass concentration is 2% alum solution, stirs, and leaves standstill 12h at 25 DEG C, then, at 10 DEG C of cold preservation 6h, removes by filter precipitate, obtains liquor B.
By liquor B in the time that 60 DEG C are concentrated into proportion and are 1:1.3, add 0 DEG C of pure water to start to carry foam, repeatable operation 3 times, obtains the glue of Yak skin glue.
(7) in the glue of Yak skin glue, add the barley wine of its volume 3%, stir, in the time being concentrated into proportion 1:1.0 for 50 DEG C, obtain glue, this glue is the spray-dried Yak skin glue powder that obtains under the condition of mist flow 23mL/min, 40 DEG C of feeding temperatures, 175 DEG C of inlet temperature.
Wherein: the alcoholic strength of barley wine is 50 DEG C.
(8) 20g Radix Rehmanniae Preparata being added water by 4 times of its quality, is to extract 2 times under the condition of 70 DEG C in temperature, and each extraction time is 2 hours, merges and obtains extracting solution A; Active carbon-diatomaceous the mixture that adds its volume 3% in extracting solution A, stirs evenly, and under room temperature, leaves standstill 6 hours, filters, and obtains liquor C.
Wherein: active carbon-diatomaceous mixture refers to the mixture that active carbon and kieselguhr are mixed in the ratio of 1g:0.1g.
(9) after 50g Radix Angelicae Sinensis, 10g Fructus Jujubae, 10g Fructus Lycii being mixed, adding water by 3 times of its mixture quality, is to extract under the condition of 70 DEG C in temperature, obtains extracting solution B after 4 hours; In extracting solution B, adding the 30g Radix Astragali, 20g Arillus Longan, is to extract under the condition of 70 DEG C in temperature, obtains extracting solution C after 4 hours, and it is 1:1.5 that this extracting solution C is concentrated into proportion at 60 DEG C, obtains concentrated solution.
(10) after liquor C being mixed with concentrated solution, stir, being concentrated into proportion at 60 DEG C is 1:1.5, the spray-dried ingredient powder that obtains under the condition of mist flow 23mL/min, 40 DEG C of feeding temperatures, 175 DEG C of inlet temperature.
(11) Yak skin glue powder is mixed homogeneously with ingredient powder, granulate according to a conventional method.
embodiment 10a method of improving Yak skin glue granule mouthfeel, color and luster, comprises the following steps:
(1) yak skin 4600g is fresh or dry Qinghai-Tibet Platean peculiar cattle kind yak wild yak through infiltrating, after softening cleans up, then adding mass concentration by 2 times of its weight is 5% alkali, be to soak 36 hours under the condition of 38 DEG C in temperature, obtain the yak skin after depilation.
Wherein: alkali refers to sodium hydroxide solution.
(2) the yak skin after depilation being added to water by 5 times of its weight, is to soak dealkalize under the condition of 30 DEG C in water temperature, repeats 2 times, and each 20 minutes, then clear water rinsed, and cleaned remaining soft flocks, and measured pH value, obtained the yak skin that dealkalize is lost hair or feathers.
(3) the yak skin of dealkalize depilation being cut into the fritter of 5cm, then add the water of 20 times of its weight, is the skin 2 times of scalding under the condition of 60 DEG C in temperature, obtains the yak skin after defat.
(4) the yak skin after defat is extracted with the water of 12 times of its quality, after 10 hours, filter, discard residue, obtain filtrate A.
By filtrate A 80 DEG C be concentrated into proportion and be 1:1.3 after, adding mass concentration is 10% alum solution, stirs, and leaves standstill 4h at 35 DEG C, then, at 5 DEG C of cold preservation 12h, removes by filter precipitate, obtains liquor B.
By liquor B in the time that 80 DEG C are concentrated into proportion and are 1:1.5, add 0 DEG C of pure water to start to carry foam, repeatable operation 3 times, obtains the glue of Yak skin glue.
(7) in the glue of Yak skin glue, add the yellow wine of its volume 6%, stir, in the time being concentrated into proportion 1:1.3 for 70 DEG C, obtain glue, this glue is the spray-dried Yak skin glue powder that obtains under the condition of mist flow 20mL/min, 35 DEG C of feeding temperatures, 170 DEG C of inlet temperature.
(8) 500g Radix Rehmanniae Preparata being added water by 10 times of its quality, is to extract 2 times under the condition of 100 DEG C in temperature, and each extraction time is 4 hours, merges and obtains extracting solution A; The active carbon that adds its volume 10% in extracting solution A, stirs evenly, and under room temperature, leaves standstill 12 hours, filters, and obtains liquor C.
(9) after 300g Fructus Lycii, 400g Arillus Longan being mixed, adding water by 10 times of its mixture quality, is to extract under the condition of 100 DEG C in temperature, obtains extracting solution B after 4 hours; In extracting solution B, adding the 80g Radix Astragali, 500g Fructus Jujubae, 400g Radix Angelicae Sinensis, is to extract under the condition of 100 DEG C in temperature, obtains extracting solution C after 4 hours, and it is 1:1.5 that this extracting solution C is concentrated into proportion at 90 DEG C, obtains concentrated solution.
(10) after liquor C being mixed with concentrated solution, stir, being concentrated into proportion at 90 DEG C is 1:1.5, the spray-dried ingredient powder that obtains under the condition of mist flow 20mL/min, 35 DEG C of feeding temperatures, 170 DEG C of inlet temperature.
(11) Yak skin glue powder is mixed homogeneously with ingredient powder, granulate according to a conventional method.
embodiment 11a method of improving Yak skin glue granule mouthfeel, color and luster, comprises the following steps:
(1) yak skin 4800g is fresh or dry Qinghai-Tibet Platean peculiar cattle kind yak wild yak through infiltrating, after softening cleans up, then adding mass concentration by 3 times of its weight is 6% alkali, be to soak 24 hours under the condition of 20 DEG C in temperature, obtain the yak skin after depilation.
Wherein: alkali refers to potassium hydroxide solution.
(2) the yak skin after depilation being added to water by 4 times of its weight, is to soak dealkalize under the condition of 25 DEG C in water temperature, repeats 3 times, and each 25 minutes, then clear water rinsed, and cleaned remaining soft flocks, and measured pH value, obtained the yak skin that dealkalize is lost hair or feathers.
(3) the yak skin of dealkalize depilation being cut into the fritter of 4cm, then add the water of 15 times of its weight, is the skin 3 times of scalding under the condition of 55 DEG C in temperature, obtains the yak skin after defat.
(4) the yak skin after defat is extracted with the water of 10 times of its quality, after 6 hours, filter, discard residue, obtain filtrate A.
By filtrate A 75 DEG C be concentrated into proportion and be 1:1.2 after, adding mass concentration is 5% alum solution, stirs, and leaves standstill 10h at 30 DEG C, then, at 8 DEG C of cold preservation 8h, removes by filter precipitate, obtains liquor B.
By liquor B in the time that 70 DEG C are concentrated into proportion and are 1:1.4, add 10 DEG C of pure water to start to carry foam, repeatable operation 8 times, obtains the glue of Yak skin glue.
(7) in the glue of Yak skin glue, add the mixture of the yellow wine-barley wine of its volume 6%, stir, in the time being concentrated into proportion 1:1.1 for 70 DEG C, obtain glue, this glue is the spray-dried Yak skin glue powder that obtains under the condition of mist flow 25mL/min, 45 DEG C of feeding temperatures, 180 DEG C of inlet temperature.
Wherein: the alcoholic strength of barley wine is 46 DEG C.
The mixture of yellow wine-barley wine refers to the mixture that yellow wine and barley wine are mixed in the ratio of 1mL:0.1mL.
(8) 100g Radix Rehmanniae Preparata being added water by 6 times of its quality, is to extract 2 times under the condition of 80 DEG C in temperature, and each extraction time is 3 hours, merges and obtains extracting solution A; Active carbon-diatomaceous the mixture that adds its volume 4% in extracting solution A, stirs evenly, and under room temperature, leaves standstill 6 hours, filters, and obtains liquor C.
Wherein: active carbon-diatomaceous mixture refers to the mixture that active carbon and kieselguhr are mixed in the ratio of 1g:0.3g.
(9) after 100g Fructus Lycii, 100g Arillus Longan being mixed, adding water by 4 times of its mixture quality, is to extract under the condition of 80 DEG C in temperature, obtains extracting solution B after 1 hour; In extracting solution B, adding the 40g Radix Astragali, 100g Fructus Jujubae, 100g Radix Angelicae Sinensis, is to extract under the condition of 80 DEG C in temperature, obtains extracting solution C after 1 hour, and it is 1:1.5 that this extracting solution C is concentrated into proportion at 70 DEG C, obtains concentrated solution.
(10) after liquor C being mixed with concentrated solution, stir, being concentrated into proportion at 70 DEG C is 1:1.5, the spray-dried ingredient powder that obtains under the condition of mist flow 25mL/min, 45 DEG C of feeding temperatures, 180 DEG C of inlet temperature.
(11) Yak skin glue powder is mixed homogeneously with ingredient powder, granulate according to a conventional method.
embodiment 12a method of improving Yak skin glue granule mouthfeel, color and luster, comprises the following steps:
(1) yak skin 5000g is fresh or dry Qinghai-Tibet Platean peculiar cattle kind yak wild yak through infiltrating, after softening cleans up, then adding mass concentration by 2.5 times of its weight is 8% alkali, be to soak 24 hours under the condition of 38 DEG C in temperature, obtain the yak skin after depilation.
Wherein: alkali refers to sodium bicarbonate solution.
(2) the yak skin after depilation being added to water by 5 times of its weight, is to soak dealkalize under the condition of 30 DEG C in water temperature, repeats 4 times, and each 30 minutes, then clear water rinsed, and cleaned remaining soft flocks, and measured pH value, obtained the yak skin that dealkalize is lost hair or feathers.
(3) the yak skin of dealkalize depilation being cut into the fritter of 5cm, then add the water of 20 times of its weight, is the skin 3 times of scalding under the condition of 60 DEG C in temperature, obtains the yak skin after defat.
(4) the yak skin after defat is extracted with the water of 12 times of its quality, after 10 hours, filter, discard residue, obtain filtrate A.
By filtrate A 80 DEG C be concentrated into proportion and be 1:1.3 after, adding mass concentration is 10% alum solution, stirs, and leaves standstill 4h at 35 DEG C, then, at 10 DEG C of cold preservation 6h, removes by filter precipitate, obtains liquor B.
By liquor B in the time that 80 DEG C are concentrated into proportion and are 1:1.5, add 10 DEG C of pure water to start to carry foam, repeatable operation 8 times, obtains the glue of Yak skin glue.
(7) in the glue of Yak skin glue, add the yellow wine of its volume 6%, stir, in the time being concentrated into proportion 1:1.3 for 70 DEG C, obtain glue, this glue is the spray-dried Yak skin glue powder that obtains under the condition of mist flow 25mL/min, 45 DEG C of feeding temperatures, 180 DEG C of inlet temperature.
(8) 500g Radix Rehmanniae Preparata being added water by 10 times of its quality, is to extract 2 times under the condition of 100 DEG C in temperature, and each extraction time is 4 hours, merges and obtains extracting solution A; The kieselguhr that adds its volume 10% in extracting solution A, stirs evenly, and under room temperature, leaves standstill 12 hours, filters, and obtains liquor C.
(9) after 300g Fructus Lycii, 400g Arillus Longan being mixed, adding water by 10 times of its mixture quality, is to extract under the condition of 100 DEG C in temperature, obtains extracting solution B after 4 hours; In extracting solution B, adding the 80g Radix Astragali, 500g Fructus Jujubae, 400g Radix Angelicae Sinensis, is to extract under the condition of 100 DEG C in temperature, obtains extracting solution C after 4 hours, and it is 1:1.5 that this extracting solution C is concentrated into proportion at 90 DEG C, obtains concentrated solution.
(10) after liquor C being mixed with concentrated solution, stir, being concentrated into proportion at 90 DEG C is 1:1.5, the spray-dried ingredient powder that obtains under the condition of mist flow 25mL/min, 45 DEG C of feeding temperatures, 180 DEG C of inlet temperature.
(11) Yak skin glue powder is mixed homogeneously with ingredient powder, granulate according to a conventional method.
Claims (9)
1. a method of improving Yak skin glue granule mouthfeel, color and luster, comprises the following steps:
(1) yak skin 3000 ~ 5000g is fresh or dry Qinghai-Tibet Platean peculiar cattle kind yak wild yak through infiltrating, after softening cleans up, then adding mass concentration by 2 ~ 3 times of its weight is 0.5 ~ 10% alkali, be to soak 24 ~ 72 hours under the condition of 20 ~ 38 DEG C in temperature, obtain the yak skin after depilation;
(2) the yak skin after described depilation being added to water by 3 ~ 5 times of its weight, is to soak dealkalize under the condition of 20 ~ 30 DEG C in water temperature, repeats 1 ~ 4 time, and each 10 ~ 30 minutes, then clear water rinsed, and cleaned remaining soft flocks, and measured pH value, obtained the yak skin of dealkalize depilation;
(3) the yak skin of described dealkalize depilation being cut into the fritter of 3 ~ 5cm, then add the water of 5 ~ 20 times of its weight, is the skin 2 ~ 3 times of scalding under the condition of 40 ~ 60 DEG C in temperature, obtains the yak skin after defat;
(4) the yak skin after described defat is extracted with the water of 8 ~ 12 times of its quality, after 2 ~ 10 hours, filter, discard residue, obtain filtrate A;
By described filtrate A 50 ~ 80 DEG C be concentrated into proportion and be 1:1.1 ~ 1:1.3 after, adding mass concentration is 2 ~ 10% alum solution, stirs, and leaves standstill 4 ~ 12h at 25 ~ 35 DEG C, then, at 5 ~ 10 DEG C of cold preservation 6 ~ 12h, removes by filter precipitate, obtains liquor B;
By described liquor B in the time that 60 ~ 80 DEG C are concentrated into proportion and are 1:1.3 ~ 1:1.5, add 0 ~ 10 DEG C of pure water to start to carry foam, repeatable operation 3 ~ 8 times, obtains the glue of Yak skin glue;
(7) in the glue of described Yak skin glue, add the yellow wine of its volume 3 ~ 6% or the mixture of barley wine or yellow wine-barley wine, stir, in the time being concentrated into proportion 1:1.0 ~ 1:1.3 for 50 ~ 70 DEG C, obtain glue, the spray-dried Yak skin glue powder that obtains of this glue;
(8) 20 ~ 500g Radix Rehmanniae Preparata being added water by 4 ~ 10 times of its quality, is to extract 2 times under the condition of 70 ~ 100 DEG C in temperature, and each extraction time is 2 ~ 4 hours, merges and obtains extracting solution A; The active carbon or kieselguhr or the active carbon-diatomaceous mixture that in described extracting solution A, add its volume 3 ~ 10%, stir evenly, and under room temperature, leaves standstill 6 ~ 12 hours, filters, and obtains liquor C;
(9) after 30 ~ 80g Radix Astragali, 50 ~ 400g Radix Angelicae Sinensis, 10 ~ 500g Fructus Jujubae, 10 ~ 300g Fructus Lycii, 20 ~ 400g Arillus Longan being mixed, add water by 3 ~ 10 times of mixture quality, be to extract 2 times under the condition of 70 ~ 100 DEG C in temperature, each extraction time is 1 ~ 4 hour, merge and obtain extracting solution B, it is 1:1.5 that this extracting solution B is concentrated into proportion at 60 ~ 90 DEG C, obtains concentrated solution;
(10) after described liquor C being mixed with described concentrated solution, stir, being concentrated into proportion at 60 ~ 90 DEG C is 1:1.5, the spray-dried ingredient powder that obtains;
(11) described Yak skin glue powder is mixed homogeneously with described ingredient powder, granulate according to a conventional method.
2. a kind of method of improving Yak skin glue granule mouthfeel, color and luster as claimed in claim 1, is characterized in that: the alkali of described step in (1) refers to the one in sodium hydroxide solution, potassium hydroxide solution, sodium bicarbonate solution.
3. a kind of method of improving Yak skin glue granule mouthfeel, color and luster as claimed in claim 1, is characterized in that: the described step (7) alcoholic strength of middle barley wine is 46 ~ 52 DEG C.
4. a kind of method of improving Yak skin glue granule mouthfeel, color and luster as claimed in claim 1, is characterized in that: described step (7) in the mixture of yellow wine-barley wine refer to the mixture that yellow wine and barley wine are mixed in the ratio of 1mL:0.1 ~ 0.5mL.
5. a kind of method of improving Yak skin glue granule mouthfeel, color and luster as claimed in claim 1, is characterized in that: (8) active carbon of described step-diatomaceous mixture refers to the mixture that active carbon and kieselguhr are mixed in the ratio of 1g:0.1 ~ 0.3g.
6. a kind of method of improving Yak skin glue granule mouthfeel, color and luster as claimed in claim 1, it is characterized in that: described step (7) with described step (10) in spray-dired condition refer to mist flow 20 ~ 25mL/min, 35 ~ 45 DEG C of feeding temperatures, 170 ~ 180 DEG C of inlet temperature.
7. a kind of method of improving Yak skin glue granule mouthfeel, color and luster as claimed in claim 1, it is characterized in that: replace step described in claim 1 (9) by following preparation method: after 30 ~ 80g Radix Astragali, 50 ~ 400g Radix Angelicae Sinensis, 10 ~ 500g Fructus Jujubae are mixed, add water by 3 ~ 10 times of its mixture quality, be to extract under the condition of 70 ~ 100 DEG C in temperature, after 1 ~ 4 hour, obtain extracting solution B; In described extracting solution B, adding 10 ~ 300g Fructus Lycii, 20 ~ 400g Arillus Longan, is to extract under the condition of 70 ~ 100 DEG C in temperature, obtains extracting solution C after 1 ~ 4 hour, and it is 1:1.5 that this extracting solution C is concentrated into proportion at 60 ~ 90 DEG C, obtains concentrated solution.
8. a kind of method of improving Yak skin glue granule mouthfeel, color and luster as claimed in claim 1, it is characterized in that: replace step described in claim 1 (9) by following preparation method: after 50 ~ 400g Radix Angelicae Sinensis, 10 ~ 500g Fructus Jujubae, 10 ~ 300g Fructus Lycii are mixed, add water by 3 ~ 10 times of its mixture quality, be to extract under the condition of 70 ~ 100 DEG C in temperature, after 1 ~ 4 hour, obtain extracting solution B; In described extracting solution B, adding 30 ~ 80g Radix Astragali, 20 ~ 400g Arillus Longan, is to extract under the condition of 70 ~ 100 DEG C in temperature, obtains extracting solution C after 1 ~ 4 hour, and it is 1:1.5 that this extracting solution C is concentrated into proportion at 60 ~ 90 DEG C, obtains concentrated solution.
9. a kind of method of improving Yak skin glue granule mouthfeel, color and luster as claimed in claim 1, it is characterized in that: replace step described in claim 1 (9) by following preparation method: after 10 ~ 300g Fructus Lycii, 20 ~ 400g Arillus Longan are mixed, add water by 3 ~ 10 times of its mixture quality, be to extract under the condition of 70 ~ 100 DEG C in temperature, after 1 ~ 4 hour, obtain extracting solution B; In described extracting solution B, adding 30 ~ 80g Radix Astragali, 10 ~ 500g Fructus Jujubae, 50 ~ 400g Radix Angelicae Sinensis, is to extract under the condition of 70 ~ 100 DEG C in temperature, obtains extracting solution C after 1 ~ 4 hour, and it is 1:1.5 that this extracting solution C is concentrated into proportion at 60 ~ 90 DEG C, obtains concentrated solution.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107412268A (en) * | 2016-12-29 | 2017-12-01 | 青海高原红绿色保健制品有限公司 | A kind of Yak skin glue and preparation method thereof |
| CN112335882A (en) * | 2020-12-03 | 2021-02-09 | 中国科学院西北高原生物研究所 | Yak skin glue compound product with blood replenishing and bleeding stopping effects and preparation method thereof |
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| CN107412268A (en) * | 2016-12-29 | 2017-12-01 | 青海高原红绿色保健制品有限公司 | A kind of Yak skin glue and preparation method thereof |
| CN112335882A (en) * | 2020-12-03 | 2021-02-09 | 中国科学院西北高原生物研究所 | Yak skin glue compound product with blood replenishing and bleeding stopping effects and preparation method thereof |
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