CN103993523A - Zeolite molecular sieve-added composite fuel oil filter paper and preparation method thereof - Google Patents
Zeolite molecular sieve-added composite fuel oil filter paper and preparation method thereof Download PDFInfo
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- CN103993523A CN103993523A CN201410170023.7A CN201410170023A CN103993523A CN 103993523 A CN103993523 A CN 103993523A CN 201410170023 A CN201410170023 A CN 201410170023A CN 103993523 A CN103993523 A CN 103993523A
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Abstract
The invention discloses a zeolite molecular sieve-added composite fuel oil filter paper. The composite fuel oil filter paper is characterized by being prepared from the following raw materials by weight: 56 to 59 parts of hardwood pulp, 35 to 38 parts of bagasse pulp, 2 to 3 parts of sugarcane peel, 3 to 4 parts of diatomite, 0.5 to 0.9 part of APG, 0.4 to 0.6 part of Tween-80, 0.7 to 0.9 part of polymeric aluminum, 2 to 3 parts of meerschaum, 2 to 3 parts of durian shell, 1 to 2 parts of a manganese sand filter, 1 to 2 parts of a cross-linking agent TAC, 1 to 2 parts of a zeolite molecular sieve, 6 to 8 parts of liquid silicone rubber, 4 to 5 parts of polyacryloyl, 1 to 2 parts of an auxiliary agent and a proper amount of water. According to the invention, crushed plant particles and the zeolite molecular sieve are added, so the filter paper has strong adsorption capability and a good filtering effect; a dipping liquid used in the invention is safe and nontoxic and has a good film forming effect, and the prepared filter paper has great toughness and is strong and durable; the auxiliary agent is added, which is safe and environment-friendly, small pores are formed in the surface of the filter paper, so adsorptivity is improved and the filter paper has water resistance.
Description
Technical field
The present invention relates to automobile filter field, particularly a kind of fuel oil composite filter paper that adds zeolite molecular sieve and preparation method thereof.
Background technology
Zeolite molecular sieve is the hydrate of crystalline aluminium metal silicate, and zeolite molecular sieve has structure and the feature of crystal, and surface is solid skeletal, and the effect of absorption molecule can be played in inner hole.Between hole, have duct to interconnect, molecule is passed through by duct.Due to the crystallographic property in hole, the pore-size distribution of molecular sieve is homogeneous very.Molecular sieve carries out selective absorption according to the size in its crystals hole to molecule, namely adsorbs a certain size molecule and repels the molecule of larger material, thereby being called visually " molecular sieve ".The suction-operated of zeolite molecular sieve has two features: (1) lip-deep Louis center polarity is very strong; (2) cage in zeolite or passage is small-sized, makes gravitational field wherein very strong.Therefore, it far surpasses the adsorbent of other types to the adsorption capacity of adsorption molecule.Even if the dividing potential drop of adsorbate (or concentration) is very low, adsorbance is still very considerable.
Modern Automobile Engine has entered the automatically controlled epoch, in all cases, engine is controlled stricter to fuel-injected, the quality requirements of fuel oil is improved increasingly, because containing the impurity such as water, pollutant in fuel oil, cause accounting for more than 80% of engine damage according to statistics.Fuel oil resembles the blood of automobile, and engine is exactly the heart of automobile, for engine provides high-quality fuel oil very important.In order to guarantee that internal combustion engine carries out safely and effectively, supporting filter material must possess good mechanical property and certain water resistant, fire resistant oil stability with it, with the strainability that guarantees that filter paper is good.
Summary of the invention
The object of this invention is to provide a kind of fuel oil composite filter paper that adds zeolite molecular sieve and preparation method thereof.
In order to realize object of the present invention, the present invention passes through following scheme implementation:
Add a fuel oil composite filter paper for zeolite molecular sieve, its raw material by following weight portion is made: hardwood pulp 56-59, bagasse pulp 35-38, sugarcane skin 2-3, diatomite 3-4, APG 0.5-0.9, Tween 80 0.4-0.6, aluminium polychloride 0.7-0.9, sepiolite 2-3, durian shell 2-3, manganese sand filtering material 1-2, crosslinking agent TAC 1-2, zeolite molecular sieve 1-2, liquid silastic 6-8, polyacrylamide 4-5, auxiliary agent 1-2, water are appropriate;
Described auxiliary agent is made by the raw material of following weight portion: fruit of glossy privet 2-3, castor bean shell 1-2, carboxymethyl cellulose 1-2, zirconium English powder 3-5, nano titanium oxide 2-3, xanthans 3-5, Ludox 2-3, sodium alginate 1-2, water 50-60; First preparation method puts into the fruit of glossy privet pulverizer to be ground into 120-140 object mixed-powder stand-by together with castor bean shell; Then xanthans, Ludox, sodium alginate are mixed, add appropriate water to stir, be heated to 30-35 ℃ of continuation stirring and add carboxymethyl cellulose, zirconium English powder, nano titanium oxide after 10-15 minute, continue insulation 24-29 minute, finally add mixed-powder to stir, form turbid liquid.
A kind of fuel oil composite filter paper that adds zeolite molecular sieve of the present invention, by following concrete steps, made:
(1) sugarcane skin, durian shell, diatomite, sepiolite, zeolite molecular sieve are mixed, grind to form 50-100 object powder, add crosslinking agent TAC, with the speed of 850-950 rev/min, stir 25-30 minute, then 50-60 ℃ dry 1.5-2.5 hour stand-by;
(2) hardwood pulp, bagasse pulp are put into hydrabrusher size degradation, then through beater, beating consistency is controlled at 5.3-6.3%, makes slurry;
(3) compound of step (1) is added in slurry, add APG, Tween 80, be heated to 65-75 ℃, stir, add appropriate water size mixing to solid content be 2.5-3.5%, the slurry mixing up, after forming web moulding, aspirates dehydration to the l Water Paper after moulding under the vacuum condition of 0.05-0.08Mpa;
(4) by all the other the residual components mixing and stirring except auxiliary agent, the water that adds 2-3 doubly to measure, then heating, temperature is controlled at 60-70 ℃, boils 50-60 minute, insulation 25-30 minute, be warming up to 70-75 ℃, stir and make maceration extract and put into dipping tank;
(5) body paper after step (3) dehydration is passed through to dipping tank with the speed of 3-3.5m/s, maceration extract is uniformly coated on body paper, in electric drying oven with forced convection, dries 4-5min, then auxiliary agent is coated on the body paper of oven dry, dry 6-10min on last ray machine, after taking-up and get final product.
The invention has the beneficial effects as follows: the present invention adds plant and pulverizes particulate and zeolite molecular sieve, high adsorption capacity, filtering is effective; Maceration extract of the present invention, safety non-toxic, film-formation result is good, and toughness is large, durable; Add auxiliary agent, safety and environmental protection, the small hole forming on filter paper surface, has increased adsorptivity, has a water resisting property.
Specific embodiments
Below by instantiation, the present invention is described in detail.
Add a fuel oil composite filter paper for zeolite molecular sieve, its by following weight portion (kilogram) raw material make: hardwood pulp 56, bagasse pulp 35, sugarcane skin 2, diatomite 3, APG 0.5, Tween 80 0.4, aluminium polychloride 0.7, sepiolite 2, durian shell 2, manganese sand filtering material 1, crosslinking agent TAC 1, zeolite molecular sieve 1, liquid silastic 6, polyacrylamide 4, auxiliary agent 1, water are appropriate;
Described auxiliary agent by following weight portion (kilogram) raw material make: the fruit of glossy privet 2, castor bean shell 1, carboxymethyl cellulose 1, zirconium English powder 3, nano titanium oxide 2, xanthans 3, Ludox 2, sodium alginate 1, water 50; First preparation method puts into the fruit of glossy privet pulverizer to be ground into 120-140 object mixed-powder stand-by together with castor bean shell; Then xanthans, Ludox, sodium alginate are mixed, add appropriate water to stir, be heated to 30-35 ℃ of continuation stirring and add carboxymethyl cellulose, zirconium English powder, nano titanium oxide after 10-15 minute, continue insulation 24-29 minute, finally add mixed-powder to stir, form turbid liquid.
A kind of fuel oil composite filter paper that adds zeolite molecular sieve of the present invention, by following concrete steps, made:
(1) sugarcane skin, durian shell, diatomite, sepiolite, zeolite molecular sieve are mixed, grind to form 50-100 object powder, add crosslinking agent TAC, with the speed of 850-950 rev/min, stir 25-30 minute, then 50-60 ℃ dry 1.5-2.5 hour stand-by;
(2) hardwood pulp, bagasse pulp are put into hydrabrusher size degradation, then through beater, beating consistency is controlled at 5.3-6.3%, makes slurry;
(3) compound of step (1) is added in slurry, add APG, Tween 80, be heated to 65-75 ℃, stir, add appropriate water size mixing to solid content be 2.5-3.5%, the slurry mixing up, after forming web moulding, aspirates dehydration to the l Water Paper after moulding under the vacuum condition of 0.05-0.08Mpa;
(4) by all the other the residual components mixing and stirring except auxiliary agent, the water that adds 2-3 doubly to measure, then heating, temperature is controlled at 60-70 ℃, boils 50-60 minute, insulation 25-30 minute, be warming up to 70-75 ℃, stir and make maceration extract and put into dipping tank;
(5) body paper after step (3) dehydration is passed through to dipping tank with the speed of 3-3.5m/s, maceration extract is uniformly coated on body paper, in electric drying oven with forced convection, dries 4-5min, then auxiliary agent is coated on the body paper of oven dry, dry 6-10min on last ray machine, after taking-up and get final product.
The Air permenbility 85-90 L/m of the filter paper that after testing, the present invention makes
2between s, maximum diameter of hole is 53-55 μ m, and average pore size is 45 μ m.
Claims (2)
1. a fuel oil composite filter paper that adds zeolite molecular sieve, it is characterized in that, by the raw material of following weight portion, made: hardwood pulp 56-59, bagasse pulp 35-38, sugarcane skin 2-3, diatomite 3-4, APG 0.5-0.9, Tween 80 0.4-0.6, aluminium polychloride 0.7-0.9, sepiolite 2-3, durian shell 2-3, manganese sand filtering material 1-2, crosslinking agent TAC 1-2, zeolite molecular sieve 1-2, liquid silastic 6-8, polyacrylamide 4-5, auxiliary agent 1-2, water are appropriate;
Described auxiliary agent is made by the raw material of following weight portion: fruit of glossy privet 2-3, castor bean shell 1-2, carboxymethyl cellulose 1-2, zirconium English powder 3-5, nano titanium oxide 2-3, xanthans 3-5, Ludox 2-3, sodium alginate 1-2, water 50-60; First preparation method puts into the fruit of glossy privet pulverizer to be ground into 120-140 object mixed-powder stand-by together with castor bean shell; Then xanthans, Ludox, sodium alginate are mixed, add appropriate water to stir, be heated to 30-35 ℃ of continuation stirring and add carboxymethyl cellulose, zirconium English powder, nano titanium oxide after 10-15 minute, continue insulation 24-29 minute, finally add mixed-powder to stir, form turbid liquid.
2. a kind of fuel oil composite filter paper that adds zeolite molecular sieve according to claim 1, is characterized in that, by following concrete steps, is made:
(1) sugarcane skin, durian shell, diatomite, sepiolite, zeolite molecular sieve are mixed, grind to form 50-100 object powder, add crosslinking agent TAC, with the speed of 850-950 rev/min, stir 25-30 minute, then 50-60 ℃ dry 1.5-2.5 hour stand-by;
(2) hardwood pulp, bagasse pulp are put into hydrabrusher size degradation, then through beater, beating consistency is controlled at 5.3-6.3%, makes slurry;
(3) compound of step (1) is added in slurry, add APG, Tween 80, be heated to 65-75 ℃, stir, add appropriate water size mixing to solid content be 2.5-3.5%, the slurry mixing up, after forming web moulding, aspirates dehydration to the l Water Paper after moulding under the vacuum condition of 0.05-0.08Mpa;
(4) by all the other the residual components mixing and stirring except auxiliary agent, the water that adds 2-3 doubly to measure, then heating, temperature is controlled at 60-70 ℃, boils 50-60 minute, insulation 25-30 minute, be warming up to 70-75 ℃, stir and make maceration extract and put into dipping tank;
(5) body paper after step (3) dehydration is passed through to dipping tank with the speed of 3-3.5m/s, maceration extract is uniformly coated on body paper, in electric drying oven with forced convection, dries 4-5min, then auxiliary agent is coated on the body paper of oven dry, dry 6-10min on last ray machine, after taking-up and get final product.
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
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CN105986527A (en) * | 2016-01-29 | 2016-10-05 | 蚌埠首创滤清器有限公司 | Hydraulic filter filtering paper with modified rosin for water resistance improvement |
CN105986528A (en) * | 2016-01-29 | 2016-10-05 | 蚌埠首创滤清器有限公司 | Hydraulic oil filter paper capable of separating oil from water efficiently |
CN106631126A (en) * | 2016-12-16 | 2017-05-10 | 朱海东 | Method for processing concrete for walls in tropical marine climate areas |
CN107675550A (en) * | 2017-10-10 | 2018-02-09 | 枣庄市恒宇纸业有限公司 | A kind of parchment and preparation method thereof |
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CN102533032A (en) * | 2010-12-10 | 2012-07-04 | 深圳市嘉达高科产业发展有限公司 | Automatic indoor humidity adjusting coating |
CN102888784A (en) * | 2012-09-20 | 2013-01-23 | 蚌埠凤凰滤清器有限责任公司 | Environment-friendly efficient filter filtering paper and preparation method thereof |
CN102912677A (en) * | 2012-09-20 | 2013-02-06 | 蚌埠凤凰滤清器有限责任公司 | Air-filtration paper for automobile engine filter and preparation method of air-filtration paper |
CN103382687A (en) * | 2013-06-26 | 2013-11-06 | 蚌埠首创滤清器有限公司 | Heat-resistance filter paper and preparation method thereof |
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2014
- 2014-04-25 CN CN201410170023.7A patent/CN103993523A/en active Pending
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
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CN102533032A (en) * | 2010-12-10 | 2012-07-04 | 深圳市嘉达高科产业发展有限公司 | Automatic indoor humidity adjusting coating |
CN102888784A (en) * | 2012-09-20 | 2013-01-23 | 蚌埠凤凰滤清器有限责任公司 | Environment-friendly efficient filter filtering paper and preparation method thereof |
CN102912677A (en) * | 2012-09-20 | 2013-02-06 | 蚌埠凤凰滤清器有限责任公司 | Air-filtration paper for automobile engine filter and preparation method of air-filtration paper |
CN103382687A (en) * | 2013-06-26 | 2013-11-06 | 蚌埠首创滤清器有限公司 | Heat-resistance filter paper and preparation method thereof |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
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CN105986527A (en) * | 2016-01-29 | 2016-10-05 | 蚌埠首创滤清器有限公司 | Hydraulic filter filtering paper with modified rosin for water resistance improvement |
CN105986528A (en) * | 2016-01-29 | 2016-10-05 | 蚌埠首创滤清器有限公司 | Hydraulic oil filter paper capable of separating oil from water efficiently |
CN106631126A (en) * | 2016-12-16 | 2017-05-10 | 朱海东 | Method for processing concrete for walls in tropical marine climate areas |
CN107675550A (en) * | 2017-10-10 | 2018-02-09 | 枣庄市恒宇纸业有限公司 | A kind of parchment and preparation method thereof |
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Address after: 233000 Mount Huangshan Road, Bengbu high tech Zone, Anhui, No. 8028 Applicant after: ANHUI PHOENIX FILTER CO., LTD. Address before: 233000 Mount Huangshan Road, Bengbu high tech Zone, Anhui, No. 8028 Applicant before: Bengbu Fenghuang Filters Co., Ltd. |
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Free format text: CORRECT: APPLICANT; FROM: BENGBU FENGHUANG FILTERS CO., LTD. TO: ANHUI PHOENIX INTERNATIONAL CO., LTD. |
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Application publication date: 20140820 |
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