CN103981714B - Medicated clothing resist printing colour fixative and its preparation method and application - Google Patents
Medicated clothing resist printing colour fixative and its preparation method and application Download PDFInfo
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- CN103981714B CN103981714B CN201410217181.3A CN201410217181A CN103981714B CN 103981714 B CN103981714 B CN 103981714B CN 201410217181 A CN201410217181 A CN 201410217181A CN 103981714 B CN103981714 B CN 103981714B
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- medicated clothing
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Abstract
The present invention provides a kind of medicated clothing resist printing colour fixative, and this resist printing colour fixative is formulated by high molecular weight water soluble polymer, Polyethylene Glycol, organic phosphoric acid, sodium gluconate, potassium hydroxide, preservative and water. It is characterized in that the various materials in component each play the effect of oneself and produce good cooperative effect. This resist printing colour fixative and plain edition detergent with the use of, there is anti-dyeing, low energy consumption, easy to use and dimensionally stable after using, do not lose hair or feathers, the feature such as medicated clothing gloss color constant (color fixative). Present invention also offers the preparation method and application of this medicated clothing resist printing colour fixative.
Description
Technical field
The present invention relates to chemical field, especially a kind of medicated clothing resist printing colour fixative and its preparation method and application.
Background technology
Medicated clothing is colourful, and dyeing is different with material used causes in washing process discolouration phenomena in various degree. In home laundry thing process, when washing put together by the medicated clothing of different colours, pigment above medicated clothing can come off, owing to laundry water is in alkalescence, pigment can contaminate above fabric again, causes mixing medicated clothing string dye, affect clean result, more seriously, greatly destroying quality and the class of product, this is undesirable in life at home.
Chinese patent CN1096051 discloses a kind of without phosphorous liquid detergent capable of resisting cross talk and preparation method thereof. Wherein detergent is formulated by surfactant and inorganic and organic additive and water. It is characterized in that the glacial acetic acid containing 1.6��4% in component, make pH value between 5��6.5. This detergent, compared with plain edition detergent, has without crossing extensive use of chemical fertilizer pollution, anti-colour contamination, low energy consumption, the feature such as easy to use.
Chinese patent CN1354244 discloses a kind of liquid detergent capable of resisting cross talk, and formula is made up of raw materials such as 6��40% surfactants, 0.1��10% anti-colour contamination high polymers, and properties of product are stable, and anti-colour contamination effect is obvious. It is mainly technically characterized ny the employing surfactant such as anion, amphion 6��40%, anti-colour contamination high polymer 0.1��10%, additionally can add the raw material such as cationic surfactant, washing assisant, makes product have the function of washing and anti-colour contamination.
Chinese patent CN102453620 discloses a kind of multifunctional laundry liquid, the percentage by weight composition of this liquid detergent includes: anion surfactant 1%��50%, nonionic surfactant 1%��40%, high molecular polymer 0%��30%, disinfection sanitizer 0%��2%, fluorescent whitening agent 0%��0.5%, acid-base modifier: 0%��10%, enzyme: 0%��2%, 0%��0.5%, pigment 0%��0.0005%. Utilize the absorption of high molecular polymer long-chain, parcel dirt, there is removal stain, anti-colour contamination, realize the multi-functionals such as clean, submissive, antistatic, and be applicable to various medicated clothings, bedding, towel etc.
But what these documents were directed to is resist printing (colour contamination) detergent, and they at least exist inferior position in cost, effect and operating aspect compared with the medicated clothing resist printing colour fixative of the present invention. This area remains a need for that development and operation is simple, excellent effect, cost are low, the resist printing colour fixative of applied range.
Summary of the invention
The present invention provides a kind of medicated clothing resist printing colour fixative, and it comprises the component (by weight) with following content:
In a preferred embodiment, the present invention provides a kind of medicated clothing resist printing colour fixative, and it comprises the component (by weight) with following content:
In another preferred embodiment, the present invention provides a kind of medicated clothing resist printing colour fixative, and it comprises the component (by weight) with following content:
In still another preferred embodiment, the present invention provides a kind of medicated clothing resist printing colour fixative, and it comprises the component (by weight) with following content:
In one embodiment, the preparation method that the present invention provides medicated clothing resist printing colour fixative, the method includes
(1) accurately metering deionized water is in reactor, and under agitation (600 revs/min) add sodium gluconate, Polyethylene Glycol, organic phosphoric acid (ATMP), potassium hydroxide, stirring more 10 minutes.
(2) under fast stirring (1500 revs/min) rapidly join the high molecular weight water soluble polymer measured, and stir 30 minutes and stop stirring, soak about 2 hours, open stirring, see whether to dissolve completely. After being completely dissolved, adding preservative agent also filters discharging packaging after stirring 10 minutes.
The medicated clothing resist printing colour fixative of the present invention is a kind of colourless to light yellow clear liquid, and in weak anionic, density is 1.050 �� 0.1g/cm3(20 DEG C), PH (stock solution), at 7 �� 1 (20 DEG C), can mix with arbitrary proportion with water and viscosity does not increase, and hard water, salt, different PH and temperature is all stable.
The Polyethylene Glycol used in the present invention is Liquid Macrogol, PEG400, Polyethylene Glycol 500, Macrogol 600, Polyethylene Glycol 700, polyethylene glycol-800 or two or more mixture in them. PEG400 is preferably used.
The high molecular weight water soluble polymer used in the present invention is cellulose, cellulose ether, such as methylcellulose, hydroxyethylmethyl-cellulose, hydroxypropyl methyl cellulose, hydroxy butyl methyl cellulose, hydroxyethyl cellulose, hydroxypropyl cellulose, hydroxybutyl cellulose, sodium carboxymethyl cellulose etc., polyvinyl alcohol, polysaccharide such as amylopectin or pullulan, polyvinylpyrrolidone, alginic acid or its salt, sodium chondroitin sulfate, chrondroitin heparin etc., or two or more mixture in them. Preferred pullulan or sodium chondroitin sulfate.
The preservative used in the present invention is sodium benzoate, potassium sorbate, isothiazolone, P-hydroxybenzoic acid sodium, dimethyl hydantoin etc., or two or more mixture in them.
Present invention also offers a kind of medicated clothing resist printing colour fixative for preventing the purposes of medicated clothing dyeing (altering color).
The medicated clothing resist printing colour fixative of the present invention has following characteristic and advantage:
�� parent's dye-type polymer, without fiber-reactive
�� after coordinating this product to wash one or two times the medicated clothing that easily fades, medicated clothing no longer fades substantially
�� from medicated clothing, adsorb the dyestuff being dissolved in the water or pigment
�� the dyestuff being dissolved in water from medicated clothing is retained in water, it is prevented that returning of medicated clothing is stained with (returning dye) by dyestuff
�� resist printing process is not by the impact of PH
�� resist printing process is by the impact of salt (detergent and in liquid detergent all containing more salt) concentration
�� all there is good result at ambient and elevated temperatures
�� to the textured medicated clothing different with color all effective
�� outstanding dispersive property, effectively prevent the formation of deposition of dye and redeposition
�� resist printing colour fixative will not make medicated clothing fade, sparkling clean after washing, and has certain dirt-removing power concurrently simultaneously
The invention solves colouring problem when puzzlement people wash medicated clothing for a long time, disclose a kind of medicated clothing resist printing colour fixative and preparation method thereof.This resist printing colour fixative is formulated by high molecular weight water soluble polymer, Polyethylene Glycol, organic phosphoric acid, sodium gluconate, potassium hydroxide, preservative and water. It is characterized in that the various materials in component each play the effect of oneself and produce good cooperative effect. This resist printing colour fixative and plain edition detergent with the use of, there is anti-dyeing, low energy consumption, easy to use and dimensionally stable after using, do not lose hair or feathers, the feature such as medicated clothing gloss color constant (color fixative).
Although having several about anti-colour contamination detergent patent with one section of periodical research report domestic, commodity are not seen in market. Another its belongs to detergent and the present invention is a kind of resist agent, without the property compared. Abroad (Germany) has a kind of anti-dyeing towel (" Beckman doctor " anti-dyeing towel) to apply comparatively maturation abroad, we test on year-on-year basis with " Beckman doctor " anti-dyeing towel by product, and this medicated clothing resist printing colour fixative effect is substantially dominant.
Accompanying drawing explanation
Fig. 1 is the test effect comparison diagram of resist printing colour fixative Piglet s colibacillosis I.
Fig. 2 is the product figure of " Beckman doctor " anti-dyeing towel.
Fig. 3 is the test effect comparison diagram of resist printing colour fixative and " Beckman doctor " anti-dyeing towel Piglet s colibacillosis II.
Embodiment
Embodiment 1
Measuring 23.5 parts by weight of deionized water in reactor, under agitation (600 revs/min) add sodium gluconate 7 weight portion, PEG400 42 weight portion, organic phosphoric acid 8 weight portion, potassium hydroxide 4 weight portion, stirring more 10 minutes. (1500 revs/min) rapidly join high molecular weight water soluble polymer hydroxyethylmethyl-cellulose 15 weight portion under fast stirring, stir 30 minutes and stop stirring, soak about 2 hours, open stirring, see whether to dissolve completely. After being completely dissolved, adding preservative agent sodium benzoate 0.5 weight portion also filters discharging packaging after stirring 10 minutes.
Embodiment 2
Measuring 24.5 parts by weight of deionized water in reactor, under agitation (600 revs/min) add sodium gluconate 6 weight portion, PEG400 39 weight portion, organic phosphoric acid 8 weight portion, potassium hydroxide 4 weight portion, stirring more 10 minutes. (1500 revs/min) rapidly join high molecular weight water soluble polymer sodium carboxymethyl cellulose 18 weight portion under fast stirring, stir 30 minutes and stop stirring, soak about 2 hours, open stirring, see whether to dissolve completely. After being completely dissolved, adding preservative agent sodium benzoate 0.5 weight portion also filters discharging packaging after stirring 10 minutes.
Embodiment 3
Measuring 23.5 parts by weight of deionized water in reactor, under agitation (600 revs/min) add sodium gluconate 7 weight portion, Macrogol 600 42 weight portion, organic phosphoric acid 8 weight portion, potassium hydroxide 4 weight portion, stirring more 10 minutes. (1500 revs/min) rapidly join high molecular weight water soluble polymer polyvinyl alcohol 15 weight portion under fast stirring, stir 30 minutes and stop stirring, soak about 2 hours, open stirring, see whether to dissolve completely. After being completely dissolved, adding preservative agent potassium sorbate 0.5 weight portion also filters discharging packaging after stirring 10 minutes.
Embodiment 4
Measuring 24.5 parts by weight of deionized water in reactor, under agitation (600 revs/min) add sodium gluconate 6 weight portion, Macrogol 600 39 weight portion, organic phosphoric acid 8 weight portion, potassium hydroxide 4 weight portion, stirring more 10 minutes. (1500 revs/min) rapidly join high molecular weight water soluble polymer pullulan 18 weight portion under fast stirring, stir 30 minutes and stop stirring, soak about 2 hours, open stirring, see whether to dissolve completely.After being completely dissolved, adding preservative agent potassium sorbate 0.5 weight portion also filters discharging packaging after stirring 10 minutes.
Embodiment 5
Measuring 27.5 parts by weight of deionized water in reactor, under agitation (600 revs/min) add sodium gluconate 8 weight portion, PEG400 40 weight portion, organic phosphoric acid 8 weight portion, potassium hydroxide 4 weight portion, stirring more 10 minutes. (1500 revs/min) rapidly join high molecular weight water soluble polymer polyvinylpyrrolidone 12 weight portion under fast stirring, stir 30 minutes and stop stirring, soak about 2 hours, open stirring, see whether to dissolve completely. After being completely dissolved, adding preservative agent isothiazolone 0.5 weight portion also filters discharging packaging after stirring 10 minutes.
Embodiment 6
Measuring 27.5 parts by weight of deionized water in reactor, under agitation (600 revs/min) add sodium gluconate 8 weight portion, PEG400 40 weight portion, organic phosphoric acid 8 weight portion, potassium hydroxide 4 weight portion, stirring more 10 minutes. (1500 revs/min) rapidly join high molecular weight water soluble polymer alginate 12 weight portion under fast stirring, stir 30 minutes and stop stirring, soak about 2 hours, open stirring, see whether to dissolve completely. After being completely dissolved, adding preservative agent P-hydroxybenzoic acid sodium 0.5 weight portion also filters discharging packaging after stirring 10 minutes.
Embodiment 7
Measuring 27.5 parts by weight of deionized water in reactor, under agitation (600 revs/min) add sodium gluconate 8 weight portion, Macrogol 600 40 weight portion, organic phosphoric acid 8 weight portion, potassium hydroxide 4 weight portion, stirring more 10 minutes. (1500 revs/min) rapidly join high molecular weight water soluble polymer sodium chondroitin sulfate 12 weight portion under fast stirring, stir 30 minutes and stop stirring, soak about 2 hours, open stirring, see whether to dissolve completely. After being completely dissolved, adding preservative agent P-hydroxybenzoic acid sodium 0.5 weight portion also filters discharging packaging after stirring 10 minutes.
Embodiment 8
Measuring 27.5 parts by weight of deionized water in reactor, under agitation (600 revs/min) add sodium gluconate 8 weight portion, PEG400 40 weight portion, organic phosphoric acid 8 weight portion, potassium hydroxide 4 weight portion, stirring more 10 minutes. (1500 revs/min) rapidly join high molecular weight water soluble polymer chrondroitin heparin 12 weight portion under fast stirring, stir 30 minutes and stop stirring, soak about 2 hours, open stirring, see whether to dissolve completely. After being completely dissolved, adding preservative agent dimethyl hydantoin 0.5 weight portion also filters discharging packaging after stirring 10 minutes.
Embodiment 9
Measuring 27.5 parts by weight of deionized water in reactor, under agitation (600 revs/min) add sodium gluconate 8 weight portion, PEG400 40 weight portion, organic phosphoric acid 8 weight portion, potassium hydroxide 4 weight portion, stirring more 10 minutes. (1500 revs/min) rapidly join high molecular weight water soluble polymer pullulan 12 weight portion under fast stirring, stir 30 minutes and stop stirring, soak about 2 hours, open stirring, see whether to dissolve completely. After being completely dissolved, adding preservative agent dimethyl hydantoin 0.5 weight portion also filters discharging packaging after stirring 10 minutes.
Resist printing colour fixative Piglet s colibacillosis I
One, test apparatus
Two, test method
1. each addition 100ml tap water in A, B beaker (200ml);
2. (1) adds 4 grams of regular powders in A beaker, stirs with Glass rod;
(2) in B beaker, add 4 grams of regular powders and 10 milliliters of resist printing colour fixative, stir with another Glass rod;
3. in A beaker, put into 1 piece of white pure cotton cloth (A) and 2 pieces of color cloth; In B beaker, in like manner put into 1 piece of white pure cotton cloth (B) and 2 pieces of painting cloths, be stirred continuously with Glass rod, make cloth be completely immersed in aqueous solution, timing simultaneously;
4. outwell aqueous solution after about three to five minutes, take out painting cloth, then in A, B beaker, respectively add 100ml tap water, after being sufficiently stirred for Glass rod, take out white pure cotton cloth A, B, extract water;
5. even up A, B cloth, contrast color.
Three, result of the test
Detect by an unaided eye A, B cloth. As shown in Fig. 1 result, A cloth and B cloth have obvious aberration, and B cloth is almost without staining, illustrates that resist printing colour fixative has good resist printing effect.
Resist printing colour fixative Piglet s colibacillosis II
One, test apparatus
Two, test method
1. each addition 100ml tap water in A, B beaker (200ml);
2. (1) adds 4 grams of regular powders in A beaker, stirs with Glass rod;
(2) in B beaker, add 4 grams of regular powders and 10 milliliters of resist printing colour fixative, stir with another Glass rod;
3. in A beaker, put into 1 piece of white pure cotton cloth (A) and 2 pieces of color cloth; In B beaker, in like manner put into 1 piece of white pure cotton cloth (B) and 2 pieces of painting cloths, be stirred continuously with Glass rod, make cloth be completely immersed in aqueous solution, timing simultaneously;
4. outwell aqueous solution after about three to five minutes, take out painting cloth, then in A, B beaker, respectively add 100ml tap water, after being sufficiently stirred for Glass rod, take out white pure cotton cloth A, B, extract water;
5. even up A, B cloth, contrast color.
Three, result of the test
Detect by an unaided eye A, B cloth. As shown in Fig. 3 result, A cloth and B cloth have obvious aberration, and B cloth is without staining, illustrates that resist printing colour fixative has extraordinary resist printing effect.
Resist printing colour fixative and " Beckman doctor " anti-dyeing towel Piglet s colibacillosis I
One, test apparatus
Two, test method
1. each addition 100ml tap water in A, B beaker (200ml);
2. (1) adds 4 grams of regular powders and a piece of " Beckman doctor " anti-dyeing towel in A beaker, stirs with Glass rod;
(2) in B beaker, add 4 grams of regular powders and 10 milliliters of resist printing colour fixative, stir with another Glass rod;
3. in A beaker, put into 1 piece of white pure cotton cloth (A) and 2 pieces of color cloth; In B beaker, in like manner put into 1 piece of white pure cotton cloth (B) and 2 pieces of painting cloths, be stirred continuously with Glass rod, make cloth be completely immersed in aqueous solution, timing simultaneously;
4. outwell aqueous solution after about three to five minutes, take out painting cloth, then in A, B beaker, respectively add 100ml tap water, after being sufficiently stirred for Glass rod, take out white pure cotton cloth A, B, extract water;
5. even up A, B cloth, contrast color.
Three, result of the test
Detect by an unaided eye A, B cloth. A cloth and B cloth have obvious aberration, and B cloth is almost without staining, illustrates that resist printing colour fixative has good resist printing effect.
Resist printing colour fixative and " Beckman doctor " anti-dyeing towel Piglet s colibacillosis II
Test by " resist printing colour fixative and " Beckman doctor " anti-dyeing towel Piglet s colibacillosis I " identical mode with above, simply the product of embodiment 6-9 is used as resist printing colour fixative, result of the test display A cloth has obvious aberration with B cloth, and B cloth is without staining, illustrate that resist printing colour fixative has extraordinary resist printing effect.
Detect by an unaided eye A, B cloth. A cloth and B cloth have obvious aberration, and B cloth is almost without staining, illustrates that resist printing colour fixative has good resist printing effect.
Although disclosing the preferred embodiment of the present invention for illustrative purposes, it will be understood by those skilled in the art that under the scope and spirit without departing from such as appended claim present invention disclosed, it is all possible for carrying out various modification, interpolation and replacement.
Claims (12)
1. a medicated clothing resist printing colour fixative, it is characterised in that comprise the component with following content, by weight,
2. the medicated clothing resist printing colour fixative of claim 1, it is characterised in that comprise the component with following content, by weight,
3. the medicated clothing resist printing colour fixative of claim 2, it is characterised in that comprise the component with following content, by weight,
4. the medicated clothing resist printing colour fixative of claim 3, it is characterised in that comprise the component with following content, by weight,
5. the medicated clothing resist printing colour fixative of claim 1, it is characterised in that described Polyethylene Glycol is Liquid Macrogol, PEG400, Polyethylene Glycol 500, Macrogol 600, Polyethylene Glycol 700, polyethylene glycol-800 or two or more mixture in them.
6. the medicated clothing resist printing colour fixative of claim 5, it is characterised in that described Polyethylene Glycol is PEG400.
7. the medicated clothing resist printing colour fixative of claim 1, it is characterized in that described high molecular weight water soluble polymer is cellulose, cellulose ether, amylopectin, pullulan, polyvinyl alcohol, polyvinylpyrrolidone, alginic acid or its salt, sodium chondroitin sulfate, chrondroitin heparin or two or more mixture in them.
8. the medicated clothing resist printing colour fixative of claim 7, it is characterised in that described cellulose is methylcellulose, hydroxyethylmethyl-cellulose, hydroxypropyl methyl cellulose, hydroxy butyl methyl cellulose, hydroxyethyl cellulose, hydroxypropyl cellulose, hydroxybutyl cellulose or sodium carboxymethyl cellulose.
9. the medicated clothing resist printing colour fixative described in any one of claim 1-6, it is characterised in that described high molecular weight water soluble polymer is pullulan or sodium chondroitin sulfate.
10. the medicated clothing resist printing colour fixative of claim 9, it is characterised in that described preservative is sodium benzoate, potassium sorbate, isothiazolone, P-hydroxybenzoic acid sodium, dimethyl hydantoin, or two or more mixture in them.
11. the preparation method of the medicated clothing resist printing colour fixative described in any one of claim 1-10, it is characterised in that the method includes:
(1) accurately metering deionized water is in reactor, under agitation, 600 revs/min, adds sodium gluconate, Polyethylene Glycol, organic phosphoric acid, potassium hydroxide, stirs 10 minutes,
(2) under fast stirring, 1500 revs/min, rapidly join the high molecular weight water soluble polymer measured, stir 30 minutes and stop stirring, soak 2 hours, open stirring, see whether to dissolve completely; After being completely dissolved, adding preservative agent also filters discharging packaging after stirring 10 minutes.
12. the medicated clothing resist printing colour fixative described in any one of claim 1-10 prevents the purposes that medicated clothing dyes.
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Families Citing this family (3)
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| CN105064085A (en) * | 2015-09-08 | 2015-11-18 | 湖州南浔宏亮纺织有限公司 | Novel levelling agent for dyeing pure cotton and dyeing method thereof |
| CN105296191A (en) * | 2015-11-19 | 2016-02-03 | 黑龙江大学 | Efficient decontaminating and color-protecting laundry detergent and preparation method therefor |
| CN111519455A (en) * | 2020-04-17 | 2020-08-11 | 广州科丰达新材料科技有限公司 | Anti-ballistic and anti-dyeing powder and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP3087909B2 (en) * | 1991-07-23 | 2000-09-18 | イーストマン ケミカル カンパニー | Method for producing lubricant-impregnated fiber |
| CN102493234A (en) * | 2011-12-22 | 2012-06-13 | 东莞市广利行洗涤原料有限公司 | Reserving agent for washing jean garments and preparation method thereof |
| CN103276615A (en) * | 2011-12-22 | 2013-09-04 | 东莞市广利行洗涤原料有限公司 | Resist agent for jeans wear washing and preparation method of resist agent |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| TW200540263A (en) * | 2004-02-13 | 2005-12-16 | Kao Corp | Process for washing |
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP3087909B2 (en) * | 1991-07-23 | 2000-09-18 | イーストマン ケミカル カンパニー | Method for producing lubricant-impregnated fiber |
| CN102493234A (en) * | 2011-12-22 | 2012-06-13 | 东莞市广利行洗涤原料有限公司 | Reserving agent for washing jean garments and preparation method thereof |
| CN103276615A (en) * | 2011-12-22 | 2013-09-04 | 东莞市广利行洗涤原料有限公司 | Resist agent for jeans wear washing and preparation method of resist agent |
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