CN103977917A - Hydrocyclone-centrifuge combined liquid-liquid separator - Google Patents

Hydrocyclone-centrifuge combined liquid-liquid separator Download PDF

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Publication number
CN103977917A
CN103977917A CN201410231631.4A CN201410231631A CN103977917A CN 103977917 A CN103977917 A CN 103977917A CN 201410231631 A CN201410231631 A CN 201410231631A CN 103977917 A CN103977917 A CN 103977917A
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China
Prior art keywords
centrifuge
cyclone
cylinder
rotary drum
liquid separator
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Pending
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CN201410231631.4A
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Chinese (zh)
Inventor
袁惠新
赵晓明
董译文
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Changzhou University
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Changzhou University
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Priority to CN201410231631.4A priority Critical patent/CN103977917A/en
Publication of CN103977917A publication Critical patent/CN103977917A/en
Pending legal-status Critical Current

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  • Centrifugal Separators (AREA)

Abstract

The invention relates to a hydrocyclone-centrifuge combined liquid-liquid separator. The separator is characterized by mainly comprising a hydrocyclone and a centrifuge. The hydrocyclone comprises a swirling cylinder, a feeding tube and a spill tube. The feeding tube is inserted tangentially on the left end side of the swirling cylinder, and the spill tube is arranged at the left end of the swirling cylinder and stretches out coaxially with the swirling cylinder. The hydrocyclone is fixed and does not rotation. The centrifuge comprises a left bearing, a drum and a right bearing. The centrifuge drum comprises a drum neck, a drum horn port, a drum large cylinder, a drum tapered cylinder and a drum small cylinder. The centrifuge drum is coaxial with the hydrocyclone, the centrifuge drum neck shares the same diameter with the swirling cylinder and is inserted in the swirling cylinder for certain distance, and a radial seal is arranged between the swirling cylinder and the centrifuge drum neck. The separator is simple in structure, convenient to manufacture and capable of separating high-concentration, high-viscosity or low-interfacial tension liquid-liquid mixtures.

Description

Cyclone-centrifuge combined liquid liquid separator
Technical field
The present invention relates to a kind of centrifugal separating device of multi-phase ingredients, particularly cyclone-centrifuge combined liquid liquid separator, belongs to the isolation technics of processing a large amount of, high concentration, high viscosity or low interfacial tension mixed liquor.
Background technology
The hypergravity equipment that conventional liquid liquid separates has cyclone and centrifuge.
For high concentration, full-bodied liquid liquid mixture, as former wet goods, the mixed form usually wrapping up mutually with liquid-liquid exists, and simple sedimentation separation process, as centrifuge separates, wrap up in mutually system and reach separation requirement because being difficult to break liquid liquid, and, if this mixed liquor continuous phase viscosity is large, the easy emulsification of mixed liquor, and decentralized photo sedimentation migration resistance is large, be difficult to reach separation requirement by cyclonic separation.In addition, the apparent viscosity of this liquid liquid mixture is often also large than the viscosity of any phase wherein, fast in the decay of cyclone inward eddy, and centrifugal sedimentation driving force is not enough and affect separating effect.Moreover, for the liquid liquid mixture of high concentration, low interfacial tension, as the mixed liquor of cyclohexane, cyclohexanone and water, in cyclone, tend to be difficult to separate because turbulent flow, shear action make liquid group, the breakup of drop, emulsification.If the treating capacity of this mixed liquor is large, the equipment investment of centrifuge and operating cost are large.
Current domestic dynamic hydrocyclone machine adopts the mode of axial admission mostly, this feeding manner makes rotary drum L/D ratio value larger, floor space is large and separative efficiency is lower, exist secondary to become a mandarin simultaneously, the defect such as energy consumption is high, bearing life is low, complex structure, therefore Dynamic Hydrocyclone Separation Technology is not promoted use so far.
For this reason, the present invention, in conjunction with the advantage of cyclone and centrifuge, has proposed a kind of cyclone-centrifuge combined liquid liquid separator.
Summary of the invention
The object of the present invention is to provide a kind of cyclone-centrifuge combined liquid liquid separator, it is simple in structure, easy to use, can break liquid-liquid and wrap mutually mixed system, and avoid the emulsion of low interfacial tension liquid, improves separative efficiency, reduces costs.
For achieving the above object, the invention discloses a kind of cyclone-centrifuge combined liquid liquid separator, described cyclone-centrifuge combined liquid liquid separator is mainly made up of cyclone and centrifuge.Described cyclone is mainly made up of whirl cylinder, feed pipe and overflow pipe, and feed pipe tangentially inserts in whirl cylinder left end side, and overflow pipe is positioned at whirl cylinder left end coaxially overhanging with whirl cylinder, forms light liquid outlet.Described centrifuge is mainly made up of rotary drum, left bearing and right bearing.Bowl is mainly made up of rotary drum neck, rotary drum horn mouth, rotary drum large cylinder, rotary drum cone cylinder and rotary drum roundlet cylinder.The little cylinder of rotary drum and heavy liquid exit join, and form heavy liquid exit.Bowl is coaxial with cyclone, and bowl neck and whirl cylinder are with footpath and insert whirl cylinder certain distance, have radial seal between the two.Cyclone maintains static, and centrifuge is supported on left bearing and right bearing, by the belt pulley driven rotary that is positioned at its right-hand member.
The operation principle of this device is as follows, and liquid liquid mixed liquor tangentially enters cyclone through charging aperture with certain speed, and produces eddy flow.Due to the mobile semi-free vortex that is mainly in cyclone, there is turbulent flow, shear property, liquid liquid mutually parcel system is broken, and is issued to the object of pre-separation at centrifugal action.Subsequently, mixed liquor enters centrifuge also further by the density contrast sedimentation layering of phase by neck and the horn mouth of rotary drum.Because turbulence intensity in centrifuge weakens, shearing force reduces, and drop can be not broken again.Underflow opening is moved and flowed to heavy phase to wall under the effect of centrifugal force, thereby discharge from underflow opening, and light liquid is assembled and flows to vertically cyclone at the effect Xia Xiang center of centrifugal force mutually, finally discharges from overfall.
Usefulness of the present invention is: 1) the mutual inclusion of liquid liquid system under the efficient separation of high-concentration of this device energy.2) this apparatus structure is simply compact, working stability.3) this plant energy consumption is little, long working life.
Brief description of the drawings
Fig. 1 is the schematic diagram of cyclone-centrifuge combined liquid liquid separator of the present invention;
Fig. 2 is the A-A cutaway view of cyclone-centrifuge combined liquid liquid separator forward spin flow device.
Wherein 1-cyclone overfall, 2-cyclone overflow pipe, 3-spigot stream charging aperture, 4-cyclone feed pipe, 5-seal, 6-centrifuge left bearing, 7-rotary drum horn mouth, 8-rotary drum large cylinder, 9-centrifuge, 10-rotary drum cone cylinder, 11-seperator case, 12-centrifuge right bearing, 13-belt pulley, 14-check washer, 15-clamp nut, 16-seperator heavy-fluid underflow opening, 17-seal, the little cylinder of 18-rotary drum, 19-spline, 20-rotary drum neck, 21-cyclone, 22-whirl cylinder.
Detailed description of the invention
With reference to Fig. 1, Fig. 2, this cyclone-centrifuge combined liquid liquid separator is mainly made up of cyclone 21 and centrifuge 9.The main body of described cyclone 21 is cylinder, and side is provided with cyclone charging aperture 3, and this cyclone charging aperture 3 is tangent with whirl cylinder 22, and cyclone overfall 1 is positioned at whirl cylinder 22 left ends coaxially overhanging with whirl cylinder 22.Described centrifuge 9 is mainly made up of left bearing 6, rotary drum neck 20, rotary drum horn mouth 7, rotary drum large cylinder 8, rotary drum cone cylinder 10, rotary drum roundlet cylinder 18 and right bearing 12.Rotary drum roundlet cylinder 18 right-hand members are seperator heavy-fluid underflow opening 16.Centrifuge 9 coaxially makes whole apparatus structure simple with cyclone 21, becomes a mandarin without secondary, and mixed liquor once steadily enters rotary drum, reduce the sudden contraction sudden expansion of liquid flow, flowed steadily, and then reduce turbulent flow, reduce the emulsification pretreatment to material, flow losses are less simultaneously, play energy-conservation effect.Bowl neck 20 and whirl cylinder 22 are with footpath and insert whirl cylinder 22 certain distances, there is radial seal 5 between the two, the Main Function of seal 5 is to prevent that mixed liquor from flowing out from the gap location of cyclone 21 and centrifuge 9 coupling parts, thereby plays the effect of sealing.Cyclone 21 maintains static, centrifuge 9 is supported on left bearing 6 and right bearing 12, drive rotary drum roundlet cylinder 18 to rotate by the belt pulley 13 that is positioned at its right-hand member, employing rotary drum cone end small end is that the benefit of rotary drum roundlet cylinder 18 place's input power modes is that axial dimension is little, compact conformation, stable, aspect supporting, the radial dimension of right bearing 12 is little, thereby make right bearing 12 rotational line speed little, long working life.
With reference to Fig. 1, Fig. 2, liquid liquid mixed liquor with certain speed from cyclone charging aperture 3 enters cyclone-centrifuge combined liquid liquid separator, at the interior generation eddy flow of cyclone 21.Due to the interior mobile turbulent flow of cyclone 21, shear action, liquid liquid phase mutually parcel system is broken, and be issued to pre-separation in the effect of centrifugal force, enter centrifuge 9 by rotary drum neck 20 and rotary drum horn mouth 7 subsequently, now turbulence intensity weakens, shearing force reduces, mixed liquor is further pressed density stratification under higher centrifugal action, heavy-fluid in opposite directions rotary drum wall is moved and is flowed out to seperator heavy-fluid underflow opening 16 along rotary drum cone wall, and light liquid Xiang Zexiang center is assembled and in axial direction flowed out by cyclone overfall 1.
Described cyclone-centrifuge combined liquid liquid separator is horizontal, can be also vertical.
Above-described embodiment only for exemplary purposes, is not intended to limit the scope of patent of the present invention.Within those skilled in the art have done according to teachings herein any amendment that does not exceed patent object of the present invention and intention or distortion are included in the application's scope.The scope of patent of the present invention is limited by claim.

Claims (9)

1. cyclone-centrifuge combined liquid liquid separator, it is characterized in that, described cyclone-centrifuge combined liquid liquid separator is mainly made up of cyclone (21) and centrifuge (9), described cyclone (21) is by whirl cylinder (22), cyclone feed pipe (4) and cyclone overflow pipe (2) composition, cyclone feed pipe (4) tangentially inserts in whirl cylinder (22) left end side, cyclone overflow pipe (2) is positioned at whirl cylinder (22) left end coaxially overhanging with whirl cylinder (22), described centrifuge (9) is mainly by centrifuge left bearing (6), rotary drum neck (20), rotary drum horn mouth (7), rotary drum large cylinder (8), rotary drum cone cylinder (10), the little cylinder of rotary drum (18) and centrifuge right bearing (12) composition, centrifuge (9) is coaxial with cyclone (21), bowl neck (20) and whirl cylinder (22) are with footpath and insert whirl cylinder (22) certain distance, there is radial seal (5) between the two, cyclone (21) maintains static, centrifuge (9) is supported on centrifuge left bearing (6) and centrifuge right bearing (12), centrifuge (9) is by belt pulley (13) driven rotary that is positioned at its right-hand member.
2. cyclone-centrifuge combined liquid liquid separator according to claim 1, is characterized in that, described cyclone charging aperture (3) and cyclone (21) tangent connection of inner chamber, also can adopt the tangent connection of evolvent type.
3. cyclone-centrifuge combined liquid liquid separator according to claim 1, is characterized in that, described whirl cylinder (22) is cylindrical drum, and draw ratio is 1.5~2.
4. cyclone-centrifuge combined liquid liquid separator according to claim 1, it is characterized in that, the ratio that described cyclone overflow pipe (2) inserts the degree of depth of whirl cylinder (22) and the intracavity diameter of whirl cylinder (22) is 0.5-3.0.
5. cyclone-centrifuge combined liquid liquid separator according to claim 1, it is characterized in that, centrifuge (9) is by each section of rotary drum neck (20), rotary drum horn mouth (7), rotary drum large cylinder (8), rotary drum cone cylinder (10) and the little cylinder of rotary drum (18) successively coaxially isometrical connecting firmly of head and the tail.
6. cyclone-centrifuge combined liquid liquid separator according to claim 1, is characterized in that, whirl cylinder (22) inner chamber is connected with rotary drum large cylinder (8) by rotary drum horn mouth (7).
7. cyclone-centrifuge combined liquid liquid separator according to claim 1, is characterized in that, rotary drum cone cylinder (10) is conical, and cone angle is 10~20 degree.
8. cyclone-centrifuge combined liquid liquid separator according to claim 1, is characterized in that, the draw ratio of described rotary drum large cylinder (8) is 0.5~1.5.
9. cyclone-centrifuge combined liquid liquid separator according to claim 1, it is characterized in that, centrifuge left bearing (6) is arranged on the cylinder outer round surface of rotary drum neck (20), centrifuge right bearing (12) is arranged on centrifuge (9) right-hand member, on rotary drum cone cylinder (10) small end outer round surface.
CN201410231631.4A 2014-05-28 2014-05-28 Hydrocyclone-centrifuge combined liquid-liquid separator Pending CN103977917A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106669994A (en) * 2017-03-24 2017-05-17 绵阳耀邦环保科技有限公司 High-sulfur coal mine swirler provided with damping device
CN107837971A (en) * 2017-10-08 2018-03-27 大连理工大学 A kind of horizontal type structure centrifugation coagulation type seperator and its separation method
CN108514958A (en) * 2018-04-12 2018-09-11 安徽普源分离机械制造有限公司 A kind of high speed horizontal-spiral centrifuge of stability of rotation
CN108684990A (en) * 2018-05-21 2018-10-23 遵义市郎笑笑食品有限责任公司 A kind of honeysuckle beverage plant-scale equipment

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
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JPS5633053A (en) * 1979-08-28 1981-04-03 Ishikawajima Harima Heavy Ind Co Ltd Centrifuge
EP0228097A2 (en) * 1986-01-02 1987-07-08 Neyrtec Sa Rotating vortex separator for a heterogeneous liquid
US5180493A (en) * 1991-09-16 1993-01-19 Krebs Engineers Rotating hydrocyclone separator with turbulence shield
CN101049586A (en) * 2006-04-03 2007-10-10 姜大志 New type cyclone dust collector
CN101380612A (en) * 2007-07-27 2009-03-11 道达尔公司 Cyclone separator
CN202606306U (en) * 2012-06-08 2012-12-19 河北金润矿山设备集团有限公司 Integration hydrocyclone

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3648840A (en) * 1969-08-01 1972-03-14 Roy A Bobo Rotating cyclone centrifuge
JPS5633053A (en) * 1979-08-28 1981-04-03 Ishikawajima Harima Heavy Ind Co Ltd Centrifuge
EP0228097A2 (en) * 1986-01-02 1987-07-08 Neyrtec Sa Rotating vortex separator for a heterogeneous liquid
US5180493A (en) * 1991-09-16 1993-01-19 Krebs Engineers Rotating hydrocyclone separator with turbulence shield
CN101049586A (en) * 2006-04-03 2007-10-10 姜大志 New type cyclone dust collector
CN101380612A (en) * 2007-07-27 2009-03-11 道达尔公司 Cyclone separator
CN202606306U (en) * 2012-06-08 2012-12-19 河北金润矿山设备集团有限公司 Integration hydrocyclone

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Title
张頔等: "一种新型旋流萃取器的研究", 《流体机械》 *

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106669994A (en) * 2017-03-24 2017-05-17 绵阳耀邦环保科技有限公司 High-sulfur coal mine swirler provided with damping device
CN106669994B (en) * 2017-03-24 2019-01-29 威海尚品机械设备科技有限公司 It is provided with the high sulfur coal mine cyclone of damping device
CN107837971A (en) * 2017-10-08 2018-03-27 大连理工大学 A kind of horizontal type structure centrifugation coagulation type seperator and its separation method
CN107837971B (en) * 2017-10-08 2023-12-22 大连理工大学 Centrifugal coagulation type separator with horizontal structure and separation method thereof
CN108514958A (en) * 2018-04-12 2018-09-11 安徽普源分离机械制造有限公司 A kind of high speed horizontal-spiral centrifuge of stability of rotation
CN108684990A (en) * 2018-05-21 2018-10-23 遵义市郎笑笑食品有限责任公司 A kind of honeysuckle beverage plant-scale equipment

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Application publication date: 20140813