CN103976489A - Method for making butyronitrile anti-skid fully-impregnated safety port glove - Google Patents

Method for making butyronitrile anti-skid fully-impregnated safety port glove Download PDF

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Publication number
CN103976489A
CN103976489A CN201410146137.8A CN201410146137A CN103976489A CN 103976489 A CN103976489 A CN 103976489A CN 201410146137 A CN201410146137 A CN 201410146137A CN 103976489 A CN103976489 A CN 103976489A
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China
Prior art keywords
gloves
steeping
skidding
preparation
butyronitrile
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CN201410146137.8A
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Chinese (zh)
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CN103976489B (en
Inventor
周星余
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SHANDONG XINGYU GLOVES CO Ltd
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SHANDONG XINGYU GLOVES CO Ltd
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Abstract

The invention discloses a method for making a butyronitrile anti-skid fully-impregnated safety port glove. The method comprises the steps of material preparation, glue mixing, soaking and drying. The surface of the glove produced by adopting the method in the technical scheme is frosted, so that the defects of slippage of the butyronitrile glove due to water and oil are effectively overcome, the application field of the butyronitrile glove is better expanded, and the working safety of a user is better protected.

Description

The anti-skidding preparation method who entirely soaks safety mouthful gloves of a kind of butyronitrile
Technical field
The present invention relates to the manufacture method of rubber gloves, relate to specifically a kind of butyronitrile anti-skidding entirely soak safe mouthful
The preparation method of gloves.
Background technology
Existing butyronitrile safety mouthful gloves are widely used in the industries such as petrochemical industry, paint printing, agriculture and animal husbandry, automobile mechanical maintenance; There is lightly sensitive, soft comfortable wear-resisting heat-insulation warm keeping, oil stain preventing function, acid and alkali-resistance, the performance such as anticorrosive.After impregnation, be divided into and partly soak and entirely soak two kinds, but be all smooth with regard to surperficial surface smoothness, therefore existing common butyronitrile gloves easily skids running into after water or oil, causes a lot of inconvenience to people's work.
Summary of the invention
The technical problem to be solved in the present invention is for the deficiencies in the prior art, and a kind of water or oil of meeting is provided
The anti-skidding preparation method who entirely soaks safety mouthful gloves of rear non-slip butyronitrile.
For addressing the above problem, the present invention by the following technical solutions: a kind of butyronitrile is anti-skidding soaks the preparation method of safety mouthful gloves entirely, it is characterized in that: comprise the following steps:
(1), get the raw materials ready, get NBR latex, blowing agent, thickener and water-based PU resin for subsequent use;
(2), impregnation, NBR latex and thickener are joined in liquid mixing agitator and carry out an impregnation, obtain single-steeping glue; NBR latex, blowing agent and water-based PU are joined in liquid mixing agitator and carry out secondary impregnation, obtain double-steeping glue;
(3), dipping, first gloves embryo is immersed in single-steeping glue and carries out single-steeping, then immerse and in double-steeping glue, carry out double-steeping;
(4), dry, gloves complete double-steeping are entered to drying baker and dry and obtain product.
Below further improvement of the present invention:
NBR latex in step (1): blowing agent: thickener: the mass ratio=100:2:1:5 of water-based PU resin.
Further improve:
When an impregnation, control liquid mixing agitator rotating speed 30 rad/min, mixing time is half an hour.
Further improve:
The rotating speed of controlling liquid mixing agitator when secondary impregnation is 30 rad/min, and mixing time is half an hour.
Further improve:
First prebake conditions gloves embryo before single-steeping, prebake conditions temperature is controlled at 22-26 DEG C, after preliminary drying completes, gloves embryo is enclosed within on fingerprint, and baking, makes gloves embryo temperature reach 40 DEG C, is then immersed in single-steeping glue, enters into preliminary drying district preliminary drying after whirl coating, even glue.
Further improve:
Gloves embryo after double-steeping is carried out to whirl coating, the operation of even glue.
Further improve:
Described baking step comprises dries for the first time and dries for the second time, first dries for the first time, after then drying for the second time, obtains product.
Further improve:
While oven dry for the first time, controlling temperature is 60 DEG C, and baking time is 30 minutes.
Further improve:
While oven dry for the second time, controlling temperature is 120 DEG C, and baking time is 60-80 minute.
Further improve:
Described blowing agent is the mixed solution of sodium acid carbonate and water, and wherein the mass ratio of sodium acid carbonate and water is 1:10; Described thickener is casein.
The glove surface that the present invention adopts the preparation method of technique scheme to produce is frosted shape, has effectively improved the shortcoming that butyronitrile gloves and water and oil skid, and has better opened up the application of butyronitrile gloves, and has better protected user's work safety.
Detailed description of the invention
Embodiment, the anti-skidding preparation method who entirely soaks safety mouthful gloves of a kind of butyronitrile, comprises the following steps:
1, get the raw materials ready: NBR latex, blowing agent, thickener and water-based PU resin, wherein NBR latex: blowing agent: thickener: the mass ratio=100:2:1:5 of water-based PU resin.
Described NBR latex is southern Supreme Being's NBR latex of import, canned, and mass concentration is 44%.
Described blowing agent is the mixed solution of sodium acid carbonate and water, and wherein the mass ratio of sodium acid carbonate and water is 1:10.
Described thickener is casein.
Described water-based PU resin is import Korea S water-based PU resin, 100Kg/ bucket, and mass concentration is 50%.
2, impregnation:
An impregnation: NBR latex and thickener are joined in liquid mixing agitator by the consumption of step 1, control rotating speed 30 rad/min, stir half an hour, obtain single-steeping glue;
Secondary impregnation: NBR latex, blowing agent and water-based PU are joined in liquid mixing agitator by the consumption of step 1, control rotating speed 30 rad/min, stir half an hour, obtain double-steeping glue.
3, dipping:
Single-steeping: first prebake conditions gloves embryo, prebake conditions temperature is controlled at 22-26 DEG C, after having toasted, gloves embryo is enclosed within on fingerprint, baking, makes gloves embryo temperature reach 40 DEG C, then be immersed in the single-steeping glue in step 2, whirl coating gets rid of unnecessary glue 10 times, evener glue is uniformly distributed glue 3 times, avoids occurring glue beans, enter afterwards preliminary drying district and dry 20 minutes, preliminary drying district temperature is controlled at 80 DEG C;
Double-steeping: the gloves that single-steeping is completed are immersed in the double-steeping glue obtaining in step 2 again, and whirl coating gets rid of unnecessary glue 5 times, and even glue is uniformly distributed glue 3 times, avoids occurring glue beans.
4, dry:
Gloves complete double-steeping in step 3 are entered to drying baker, dry for the first time, temperature 60 C, time 30 minutes, and then dry for the second time, 120 DEG C of temperature, time 60-80 minute, obtain product.
The gloves that the present invention adopts above-mentioned steps to make, meet or exceed national standard, wherein sizing material adhesive force (peel strength) is 40N, glue face thickness is 2mm, glue face tearing strength meets and exceeds level Four (>=75N), glue face is wear-resistant power >=8000rad, reaches level Four level, and glue face ageing resistace reaches 1 grade of product requirement.

Claims (10)

1. the anti-skidding preparation method who entirely soaks safety mouthful gloves of butyronitrile, is characterized in that: comprise the following steps:
(1), get the raw materials ready, get NBR latex, blowing agent, thickener and water-based PU resin for subsequent use;
(2), impregnation, NBR latex and thickener are joined in liquid mixing agitator and carry out an impregnation, obtain single-steeping glue; NBR latex, blowing agent and water-based PU are joined in liquid mixing agitator and carry out secondary impregnation, obtain double-steeping glue;
(3), dipping, first gloves embryo is immersed in single-steeping glue and carries out single-steeping, then immerse and in double-steeping glue, carry out double-steeping;
(4), dry, gloves complete double-steeping are entered to drying baker and dry and obtain product.
2. the anti-skidding preparation method who entirely soaks safety mouthful gloves of a kind of butyronitrile according to claim 1, is characterized in that: NBR latex in step (1): blowing agent: thickener: the mass ratio=100:2:1:5 of water-based PU resin.
3. the anti-skidding preparation method who entirely soaks safety mouthful gloves of a kind of butyronitrile according to claim 1, is characterized in that: when an impregnation, control liquid mixing agitator rotating speed 30 rad/min, mixing time is half an hour.
4. the anti-skidding preparation method who entirely soaks safety mouthful gloves of a kind of butyronitrile according to claim 3, is characterized in that: the rotating speed of controlling liquid mixing agitator when secondary impregnation is 30 rad/min, and mixing time is half an hour.
5. the anti-skidding preparation method who entirely soaks safety mouthful gloves of a kind of butyronitrile according to claim 1, it is characterized in that: first prebake conditions gloves embryo before single-steeping, prebake conditions temperature is controlled at 22-26 DEG C, after preliminary drying completes, gloves embryo is enclosed within on fingerprint, baking, make gloves embryo temperature reach 40 DEG C, be then immersed in single-steeping glue, after whirl coating, even glue, enter into preliminary drying district preliminary drying.
6. the anti-skidding preparation method who entirely soaks safety mouthful gloves of a kind of butyronitrile according to claim 5, is characterized in that: the gloves embryo after double-steeping carries out whirl coating, the operation of even glue.
7. the anti-skidding preparation method who entirely soaks safety mouthful gloves of a kind of butyronitrile according to claim 1, is characterized in that: described baking step comprises dries for the first time and dry for the second time, first dries for the first time, after then drying for the second time, obtains product.
8. the anti-skidding preparation method who entirely soaks safety mouthful gloves of a kind of butyronitrile according to claim 7, is characterized in that: while oven dry for the first time, controlling temperature is 60 DEG C, and baking time is 30 minutes.
9. the anti-skidding preparation method who entirely soaks safety mouthful gloves of a kind of butyronitrile according to claim 8, is characterized in that: while oven dry for the second time, controlling temperature is 120 DEG C, and baking time is 60-80 minute.
10. the anti-skidding preparation method who entirely soaks safety mouthful gloves of a kind of butyronitrile according to claim 1, is characterized in that: described blowing agent is the mixed solution of sodium acid carbonate and water, and wherein the mass ratio of sodium acid carbonate and water is 1:10; Described thickener is casein.
CN201410146137.8A 2014-04-14 2014-04-14 The preparation method of the safe mouth gloves of the anti-skidding full leaching of a kind of butyronitrile Active CN103976489B (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107841001A (en) * 2017-12-01 2018-03-27 北京瑞京乳胶制品有限公司 A kind of emulsion foaming insulation material and its application in emgloves field
CN108638407A (en) * 2018-05-18 2018-10-12 山东星宇手套有限公司 A kind of preparation method of two times butyronitrile foam gloves of a time butyronitrile smooth surface

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP3944457B2 (en) * 2003-02-06 2007-07-11 丸五産業株式会社 Anti-vibration gloves manufacturing method
CN101652235A (en) * 2007-03-30 2010-02-17 株式会社东和公司 Be formed with at random on the formation method of resin surface, the surface the different recess of size article manufacture method and by the manufacture method of the article of its manufacturing, gloves with by the gloves of its manufacturing
WO2012003641A1 (en) * 2010-07-09 2012-01-12 Lin Charles Method for making gloves with enhanced gripping power
CN203262342U (en) * 2013-05-06 2013-11-06 青岛劲手劳保用品有限公司 Reinforced leathering working glove with five gummed fingers
CN103462259A (en) * 2013-09-30 2013-12-25 山东星宇手套有限公司 Preparation process of anti-tamping gloves
CN103462258A (en) * 2013-09-30 2013-12-25 山东星宇手套有限公司 Preparation process of anti-collision gloves
CN103519439A (en) * 2013-11-04 2014-01-22 山东星宇手套有限公司 Seven-needle pure cotton white latex coated gloves and manufacturing technology thereof
CN203457850U (en) * 2013-08-05 2014-03-05 山东豪迈机械制造有限公司 Numerical-control full-automatic efficient energy-saving environment-friendly rubber coated glove production line

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP3944457B2 (en) * 2003-02-06 2007-07-11 丸五産業株式会社 Anti-vibration gloves manufacturing method
CN101652235A (en) * 2007-03-30 2010-02-17 株式会社东和公司 Be formed with at random on the formation method of resin surface, the surface the different recess of size article manufacture method and by the manufacture method of the article of its manufacturing, gloves with by the gloves of its manufacturing
WO2012003641A1 (en) * 2010-07-09 2012-01-12 Lin Charles Method for making gloves with enhanced gripping power
CN203262342U (en) * 2013-05-06 2013-11-06 青岛劲手劳保用品有限公司 Reinforced leathering working glove with five gummed fingers
CN203457850U (en) * 2013-08-05 2014-03-05 山东豪迈机械制造有限公司 Numerical-control full-automatic efficient energy-saving environment-friendly rubber coated glove production line
CN103462259A (en) * 2013-09-30 2013-12-25 山东星宇手套有限公司 Preparation process of anti-tamping gloves
CN103462258A (en) * 2013-09-30 2013-12-25 山东星宇手套有限公司 Preparation process of anti-collision gloves
CN103519439A (en) * 2013-11-04 2014-01-22 山东星宇手套有限公司 Seven-needle pure cotton white latex coated gloves and manufacturing technology thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107841001A (en) * 2017-12-01 2018-03-27 北京瑞京乳胶制品有限公司 A kind of emulsion foaming insulation material and its application in emgloves field
CN108638407A (en) * 2018-05-18 2018-10-12 山东星宇手套有限公司 A kind of preparation method of two times butyronitrile foam gloves of a time butyronitrile smooth surface

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Inventor after: Zhou Xingyu

Inventor after: Zhou Haitao

Inventor after: Gao Yonghong

Inventor before: Zhou Xingyu

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PE01 Entry into force of the registration of the contract for pledge of patent right

Denomination of invention: A preparation method of nitrile anti-skid full immersion safety mouth gloves

Effective date of registration: 20211112

Granted publication date: 20160127

Pledgee: Shandong Gaomi rural commercial bank Limited by Share Ltd.

Pledgor: SHANDONG XINGYU GLOVES Co.,Ltd.

Registration number: Y2021980012288

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Date of cancellation: 20230413

Granted publication date: 20160127

Pledgee: Shandong Gaomi rural commercial bank Limited by Share Ltd.

Pledgor: SHANDONG XINGYU GLOVES Co.,Ltd.

Registration number: Y2021980012288

PC01 Cancellation of the registration of the contract for pledge of patent right