CN103966025A - Extraction method for Miao medicines gaultheria yunnanensis essential oil and gaultheria yunnanensis hydrolat - Google Patents
Extraction method for Miao medicines gaultheria yunnanensis essential oil and gaultheria yunnanensis hydrolat Download PDFInfo
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- CN103966025A CN103966025A CN201310074642.1A CN201310074642A CN103966025A CN 103966025 A CN103966025 A CN 103966025A CN 201310074642 A CN201310074642 A CN 201310074642A CN 103966025 A CN103966025 A CN 103966025A
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Abstract
The invention discloses an extraction method for Miao medicines gaultheria yunnanensis essential oil and gaultheria yunnanensis hydrolat, and the method fills the blank of the background technology, in other words, there is no method for extracting gaultheria yunnanensis essential oil and gaultheria yunnanensis hydrolat from a Miao medicine. The method is divided into distillation extraction of dry and fresh gaultheria yunnanensis. The method is characterized in that the method for dipping, percolating and distillation extraction of dry gaultheria yunnanensis comprises: adding crude gaultheria yunnanensis powder into a solvent, and performing sealing immersing at a normal temperature; putting the dipping solution in a percolating barrel, pressurizing for 5-15 days and performing percolating; and putting the percolated solution into a distiller, so as to obtain gaultheria yunnanensis essential oil. The method for distillation extraction of fresh gaultheria yunnanensis comprises: segmenting roots, stems, leaves and flowers of fresh gaultheria yunnanensis, putting in a distiller, adding water; heating, performing condensation on steam containing fragrant essential oil, so as to obtain an oil-water mixture; and performing separation to obtain gaultheria yunnanensis essential oil and gaultheria yunnanensis hydrolat. The gaultheria yunnanensis essential oil and the gaultheria yunnanensis hydrolat have the effects of refreshing and restoring consciousness, relaxing muscle, generating fragrance and preventing odor, mitigating fatigue and improving dizzy state. The gaultheria yunnanensis essential oil and the gaultheria yunnanensis hydrolat are easy to use, can be used for direct smearing, massaging along channels, acupoint massaging, spraying at affected parts or drop injection into bath.
Description
Technical field
The present invention is a kind of extracting process of effective ingredient, particularly the extracting process of a seedling medicine Stem and leaf of Yunnan Wintergreen essential oil and Stem and leaf of Yunnan Wintergreen hydrosol.
Background technology
In prior art, use the method extracting to extract certain medicine customary, the medicine extracting is people's treating disease, alleviates and even eliminates slight illness and brought into play great effect.But, in prior art, there is no from the method that extracts Stem and leaf of Yunnan Wintergreen essential oil and Stem and leaf of Yunnan Wintergreen hydrosol in seedling medicine.
Summary of the invention
In order to fill up the blank part in above-mentioned background technology, the object of this invention is to provide the extracting process of a seedling medicine Stem and leaf of Yunnan Wintergreen essential oil and Stem and leaf of Yunnan Wintergreen hydrosol.Technical solution of the present invention is: from being grown in the Stem and leaf of Yunnan Wintergreen that is named as the Miao Ling mountain of Guizhou, also claim to extract seedling medicine Stem and leaf of Yunnan Wintergreen essential oil and Stem and leaf of Yunnan Wintergreen hydrosol in the plant of coal fruit, Radix seu Folium Gaultheriae Forrestii or MANSHANXIANG.The present invention is divided into from dry product Stem and leaf of Yunnan Wintergreen dipping → diacolation → distillation extraction with from two kinds of methods of fresh goods Stem and leaf of Yunnan Wintergreen distillation extraction.It is characterized in that:
One, dry product Stem and leaf of Yunnan Wintergreen dipping → diacolation → distillation extraction method
(1). Stem and leaf of Yunnan Wintergreen is ground into slightly last, adds solvent, then airtight dipping 15 days～20 days at normal temperatures, needs often it to be carried out to jolting and stirring during this time;
(2). flood after 15 days～20 days, steeping fluid is inserted in diacolation bucket, and on steeping fluid, place heavier filter plate, so that steeping fluid is pressurizeed; 5 days～the piston of later opening exit for 15 days carries out diacolation.
(3). the above-mentioned percolate of collecting is inserted in distiller, to reclaim molten coal wherein, obtain comparatively pure plants essential oil, namely Stem and leaf of Yunnan Wintergreen essential oil of the present invention.
Two, fresh goods Stem and leaf of Yunnan Wintergreen distillation extraction method
After the root of fresh Stem and leaf of Yunnan Wintergreen, stem, leaf and flower are cut to joint, insert in distiller and add water; Then at the bottom-heated of distiller; In the time being full of steam in distiller, endophytic volatile oil is also along with water vapour evaporation, and the prolong by top enters condenser together with water vapour; The water vapour that contains volatile oil is converted into oil-water mixture after condensation; This oil-water mixture is collected in container and after tripping device is processed and obtains oil plant (essential oil) and water material (hydrosol) two portions, separated airtight depositing and obtain Stem and leaf of Yunnan Wintergreen essential oil and Stem and leaf of Yunnan Wintergreen hydrosol.
Traditional effect of Stem and leaf of Yunnan Wintergreen, for dispelling rheumatism, is relaxed the muscles and stimulate the blood circulation, and removes obstruction in channels to relieve pain, and is used for treating rheumatic arthritis, wound, oedema, acute filthy disease, strain, skin sufferings.The Stem and leaf of Yunnan Wintergreen essential oil extracting according to the present invention and Stem and leaf of Yunnan Wintergreen hydrosol, except possessing above-mentioned effect, also have and produce refreshing effect to the mind, the muscle of releiving, and fragrance is kept away dirty, lessens fatigue, and improves the effect of giddy state.Its use is simple, convenient, can directly apply, and massage channel, acupoint massage, sparges affected part or instillation balneation, has extremely strong practicality, in the Huimin application of large health industry, will bring into play larger conduct.
Embodiment
The present invention is described in further detail below in conjunction with embodiment: the solvent that the present invention adds in extraction is ethanol, white wine.The quantity of the water that the present invention adds in extraction exceeds 1 centimetre～2 centimetres of plants as degree taking the liquid level of water.The diacolation speed control of the present invention in extraction divided at 1ml～3ml/, oozes at a slow speed and drips.
The present invention is for extract Stem and leaf of Yunnan Wintergreen essential oil and Stem and leaf of Yunnan Wintergreen hydrosol from seedling medicine.
Claims (4)
1. the extracting process of a seedling medicine Stem and leaf of Yunnan Wintergreen essential oil and Stem and leaf of Yunnan Wintergreen hydrosol, is divided into from dry product Stem and leaf of Yunnan Wintergreen dipping → diacolation → distillation extraction with from two kinds of methods of fresh goods Stem and leaf of Yunnan Wintergreen distillation extraction, it is characterized in that:
One, dry product Stem and leaf of Yunnan Wintergreen dipping → diacolation → distillation extraction method
(1). Stem and leaf of Yunnan Wintergreen is ground into slightly last, adds solvent, then airtight dipping 15 days～20 days at normal temperatures, needs often it to be carried out to jolting and stirring during this time;
(2). flood after 15 days～20 days, steeping fluid is inserted during diacolation discloses, and on steeping fluid, place heavier filter plate, so that steeping fluid is pressurizeed; 5 days～the piston of later opening exit for 15 days carries out diacolation;
(3). the above-mentioned percolate of collecting is inserted in distiller, to reclaim molten coal wherein, obtain comparatively pure plants essential oil, namely Stem and leaf of Yunnan Wintergreen essential oil of the present invention;
Two, fresh goods Stem and leaf of Yunnan Wintergreen distillation extraction method
After the root of fresh Stem and leaf of Yunnan Wintergreen, stem, leaf and flower are cut to joint, insert in distiller and add water; Then at the bottom-heated of distiller; In the time being full of steam in distiller, endophytic volatile oil is also along with water vapour evaporation, and the prolong by top enters condenser together with water vapour; The water vapour that contains volatile oil is converted into oil-water mixture after condensation; This oil-water mixture is collected in container and after tripping device is processed and obtains oil plant (essential oil) and water material (hydrosol) two portions, it is separately deposited and obtains Stem and leaf of Yunnan Wintergreen essential oil and Stem and leaf of Yunnan Wintergreen hydrosol.
2. according to the seedling medicine Stem and leaf of Yunnan Wintergreen essential oil described in claim 1 and the extracting process of Stem and leaf of Yunnan Wintergreen hydrosol, it is characterized in that: the solvent that the present invention adds in extraction is ethanol, white wine.
3. according to the seedling medicine Stem and leaf of Yunnan Wintergreen essential oil described in claim 1 and the extracting process of Stem and leaf of Yunnan Wintergreen hydrosol, it is characterized in that: the quantity of the water that the present invention adds in extraction exceeds 1 centimetre～2 centimetres of plants as degree taking the liquid level of water.
4. according to the seedling medicine Stem and leaf of Yunnan Wintergreen essential oil described in claim 1 and the extracting process of Stem and leaf of Yunnan Wintergreen hydrosol, it is characterized in that: the diacolation speed control of the present invention in extraction divided at 1ml～3ml/.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310074642.1A CN103966025A (en) | 2013-02-06 | 2013-02-06 | Extraction method for Miao medicines gaultheria yunnanensis essential oil and gaultheria yunnanensis hydrolat |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201310074642.1A CN103966025A (en) | 2013-02-06 | 2013-02-06 | Extraction method for Miao medicines gaultheria yunnanensis essential oil and gaultheria yunnanensis hydrolat |
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| CN103966025A true CN103966025A (en) | 2014-08-06 |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105168088A (en) * | 2015-09-11 | 2015-12-23 | 司明清 | Insect-expelling refreshing mint perfume and preparation method thereof |
| CN110731916A (en) * | 2018-07-18 | 2020-01-31 | 杨易 | Tou Gu Xiang Shu |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1422646A (en) * | 2001-12-03 | 2003-06-11 | 吴永忠 | Chinese medicinal preparation for treating osteoproliferation and various rheumatalgia |
| CN1817353A (en) * | 2004-11-17 | 2006-08-16 | 贵州同济堂制药有限公司 | Use and preparing method of Dianbaizhu in treating Meniere's disease and varied vertigo |
-
2013
- 2013-02-06 CN CN201310074642.1A patent/CN103966025A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1422646A (en) * | 2001-12-03 | 2003-06-11 | 吴永忠 | Chinese medicinal preparation for treating osteoproliferation and various rheumatalgia |
| CN1817353A (en) * | 2004-11-17 | 2006-08-16 | 贵州同济堂制药有限公司 | Use and preparing method of Dianbaizhu in treating Meniere's disease and varied vertigo |
Non-Patent Citations (2)
| Title |
|---|
| 张俊巍等: "透骨香挥发油成分的研究", 《贵阳中医学院学报》 * |
| 郑林等: "化学指标结合药效学指标优选资金透骨喷雾剂提取工艺", 《中国实验方剂学杂志》 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105168088A (en) * | 2015-09-11 | 2015-12-23 | 司明清 | Insect-expelling refreshing mint perfume and preparation method thereof |
| CN110731916A (en) * | 2018-07-18 | 2020-01-31 | 杨易 | Tou Gu Xiang Shu |
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Application publication date: 20140806 |