CN103961520A - Amur Corktree Bark and Fructus Gardeniae dampness eliminating agent production technology - Google Patents
Amur Corktree Bark and Fructus Gardeniae dampness eliminating agent production technology Download PDFInfo
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- CN103961520A CN103961520A CN201310042219.3A CN201310042219A CN103961520A CN 103961520 A CN103961520 A CN 103961520A CN 201310042219 A CN201310042219 A CN 201310042219A CN 103961520 A CN103961520 A CN 103961520A
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Abstract
The invention discloses an Amur Corktree Bark and Fructus Gardeniae dampness eliminating agent production technology, and belongs to the medicine production field. The technology comprises the following steps: washing twenty medicines comprising Amur Corktree Bark, Radix Scutellariae, Rheum officinale, Fructus Gardeniae, Barbed Skullcap Herb, Hedyotis diffusa, honeysuckle flower, Rehmannia glutinosa Libosch, Herba Houttuyniae, Capillary Wormwood Herb, radix bupleuri, isatis root, root of Lithospermum erythrorhizon, scorpion, Weeping Forsythia, Ricepaperplant Pith, Fructus Kochiae, talcum, Rhizoma Anemarrhenae and licorice root, drying, cutting Rehmannia glutinosa Libosch to form slices, respectively crushing the nineteen medicines to form crude powders, adding all the medicinal materials into an ultrasonic extraction tank, adding ethanol, carrying out normal temperature dipping, adjusting the temperature to 40-60DEG C, starting ultrasonic extraction and stirring, carrying out micro-porous filtration, adding ethanol to medicine residues, adjusting the temperature to 40-60DEG C, carrying out ultrasonic extraction while stirring, carrying out micro-porous filtration, mixing the above obtained filtrates, adding a proper amount of ethanol to a quantitative amount, uniformly stirring, and filling to obtain an Amur Corktree Bark and Fructus Gardeniae dampness eliminating agent. The technology has the characteristics of simple operation, production cost saving, improvement of the curative effects of the medicines, energy consumption reduction and environment pollution reduction.
Description
Technical field
The present invention relates to technical field of medicament, is a kind of Baizhi dehumidizer made from gloden cyllress and cape jasmine etc. Chinese herbal medicines production technology specifically.
Background technology
Traditional drug is produced and is mainly taked to decoct, effective ingredient in concentration extraction medical material, medical material decocts through high temperature, this process need be carried out high temperature heating with pressure (pressure: 0.02-0.05MPa, temperature: 85-110 degree Celsius), if the time, temperature control is bad, yield and the quality of medicine will directly be affected, generally at least to decoct 2 times, each 1-3 hour, and then concentrated or alcohol stain reconcentration, these method leaching process are comparatively complicated, operation is loaded down with trivial details, wayward, many (as: the hot reflux tanks of equipment configuration, single (two) concentrator, Alcohol-settling tank, percolate pot, firing equipment, cooling device etc.), there is investment large, power consumption is large, pollute the features such as larger, be unfavorable for environmental conservation, simultaneously because extracting excess Temperature, most of effective ingredient in medical material are destroyed, directly affect the health giving quality of medicine.
Summary of the invention
The present invention seeks to for provide a kind of simple to operate, save production cost, improve pharmaceutical effectiveness, reduce energy resource consumption, reduce the Baizhi dehumidizer made from gloden cyllress and cape jasmine etc. Chinese herbal medicines production technology of environmental pollution.
For achieving the above object, the technical solution used in the present invention is: Baizhi dehumidizer made from gloden cyllress and cape jasmine etc. Chinese herbal medicines production technology, comprises the steps:
(1), Cortex Phellodendri, Radix Scutellariae, Radix Et Rhizoma Rhei, Fructus Gardeniae, Herba Scutellariae Barbatae, Herba Hedyotidis Diffusae, Flos Lonicerae, Radix Rehmanniae, Herba Houttuyniae, Herba Artemisiae Scopariae, Radix Bupleuri, Radix Isatidis, Radix Arnebiae (Radix Lithospermi), Scorpio, Fructus Forsythiae, Medulla Tetrapanacis, the Fructus Kochiae, Talcum, the Rhizoma Anemarrhenae, Radix Glycyrrhizae are amounted to 20 taste medical materials, clean post-drying, except Radix Rehmanniae is cut into slices, all the other medical materials are pulverized respectively;
(2), all medical materials in step (1) are dropped into supersound extraction tank, add the ethanol that medical material 2.2-2.7 times quality, concentration are 40%-60%, after normal temperature dipping 11-13 hour, adjust the temperature to 40-60 DEG C of supersound extraction 1-1.5 hour, stirred once every 8-12 minute during this time, then carry out microporous filter, obtain first-time filtrate and medicinal residues;
(3), the medicinal residues of gained in step (2) are added to the ethanol that medical material 2.2-2.7 times quality, concentration are 40%-60%, adjust the temperature to 40-60 DEG C and carry out again supersound extraction 25-35 minute, stirred once every 8-12 minute during this time, again carry out microporous filter, obtain secondary filtrate, the filtrate that obtains for twice merges, then to add concentration be that the ethanol of 40%-60% complements to the front 90%-91% that adds ethanol volume summation for twice, and the fill that stirs obtains Baizhi dehumidizer made from gloden cyllress and cape jasmine etc. Chinese herbal medicines.
Further: in described step (1), the each composition weight umber of 20 taste medical material is: Cortex Phellodendri 13-21 part, Radix Scutellariae 9-17 part, Radix Et Rhizoma Rhei 8-16 part, Fructus Gardeniae 6-14 part, Herba Scutellariae Barbatae 9-17 part, Herba Hedyotidis Diffusae 13-21 part, Flos Lonicerae 9-17 part, Radix Rehmanniae 13-21 part, Herba Houttuyniae 9-17 part, Herba Artemisiae Scopariae 9-17 part, Radix Bupleuri 4-12 part, Radix Isatidis 2-6 part, Radix Arnebiae (Radix Lithospermi) 4-12 part, Scorpio 2-6 part, Fructus Forsythiae 6-14 part, Medulla Tetrapanacis 2-8 part, Fructus Kochiae 4-12 part, Talcum 6-14 part, Rhizoma Anemarrhenae 9-17 part, Radix Glycyrrhizae 4-12 part.
Further: described step (1) Chinese crude drug grinding particle size is 10 orders.
Further: in described step (2), dip time is 12 hours, and the described supersound extraction time is 1 hour, described stirring is to stir once every 10 minutes.
Further: in described step (3), the supersound extraction time is 30 minutes, described stirring is to stir once every 10 minutes.
Further: described step (2) and (3) supersound extraction temperature are 50 DEG C.
Further: described step (2) and (3) supersound extraction frequency are 15-30Hz.
Further: described step (2) and (3) supersound extraction frequency are 20Hz.
Useful technique effect of the present invention is compared with traditional handicraft:
1. the present invention adopts current domestic advanced person's ultrasonic wave extraction, more easier than traditional extraction technique, easy to control, medical material effective component extraction rate exceeds traditional extraction technique, recovery rate, far away higher than traditional extraction technique, improves the utilization rate of medical material simultaneously, saves the cost of crude drug, be more suitable for the modern production of medicine, greatly improve prouctiveness.
2. the pharmaceutical production technique that the present invention is relatively traditional is comparatively simple, has reduced a large amount of production links, is convenient to quality control; Reduce human resources's configuration simultaneously, reduce personnel cost.
3. main production equipments of the present invention: only need supersound extraction device, microfilter and automatic filling machine, relatively traditional process equipment drops into upper obviously minimizing.
4. at normal temperatures, medical material is pulverized, soaks, is softened by modern crafts; Adopt again advanced ultrasonic technology to extract, ensured that medical material effective ingredient fully extracts, effectively reduce the loss of effective ingredient in medical material, guarantee quality and the curative effect of medicine.
5. leaching process of the present invention is temperature required low, reduces energy resource consumption, has reduced waste gas, waste discharge amount simultaneously; Become industry energy conservation and reduce discharging new way, for the sustainable development of enterprise lays the foundation.
Detailed description of the invention
In the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described, obviously, described embodiment is only the present invention's part embodiment, instead of whole embodiment.Based on the embodiment in the present invention, those of ordinary skill in the art, not making the every other embodiment obtaining under creative work prerequisite, belong to the scope of protection of the invention.
Embodiment 1
Baizhi dehumidizer made from gloden cyllress and cape jasmine etc. Chinese herbal medicines production technology;
(1), Cortex Phellodendri 13g, Radix Scutellariae 9g, Radix Et Rhizoma Rhei 8g, Fructus Gardeniae 6g, Herba Scutellariae Barbatae 9g, Herba Hedyotidis Diffusae 13g, Flos Lonicerae 9g, Radix Rehmanniae 13g, Herba Houttuyniae 9g, Herba Artemisiae Scopariae 9g, Radix Bupleuri 4g, Radix Isatidis 2g, Radix Arnebiae (Radix Lithospermi) (root) 4g, Scorpio 3g, Fructus Forsythiae 6g, Medulla Tetrapanacis 3g, Fructus Kochiae 4g, Talcum 6g, Rhizoma Anemarrhenae 9g, Radix Glycyrrhizae 6g are amounted to 20 taste medical materials, clean post-drying, except Radix Rehmanniae is cut into slices, all the other medical materials are ground into respectively coarse powder;
(2), medical material is dropped into the supersound extraction tank that frequency is 15Hz, adding concentration is 50% ethanol 600ml, and normal temperature dipping, after 11 hours, adjusts the temperature to 40 DEG C of supersound extraction 1 hour, stirs once during this time every 8 minutes, and micropore filters, and obtains first-time filtrate and medicinal residues;
(3), the medicinal residues of gained in step (2) being added to concentration is 40% ethanol 500ml again, adjusting the temperature to 40 DEG C ultrasonic (frequency 15Hz) extracts 25 minutes, stirred once at interval of 8 minutes, micropore filters to obtain secondary filtrate, twice filtrate is merged, adding concentration is that 40% ethanol 15ml complements to the 1000ml fill that stirs again, and obtains Baizhi dehumidizer made from gloden cyllress and cape jasmine etc. Chinese herbal medicines.
Embodiment 2
Baizhi dehumidizer made from gloden cyllress and cape jasmine etc. Chinese herbal medicines production technology;
(1), Cortex Phellodendri 17g, Radix Scutellariae 13g, Radix Et Rhizoma Rhei 12g, Fructus Gardeniae 10g, Herba Scutellariae Barbatae 13g, Herba Hedyotidis Diffusae 17g, Flos Lonicerae 13g, Radix Rehmanniae 17g, Herba Houttuyniae 13g, Herba Artemisiae Scopariae 13g, Radix Bupleuri 8g, Radix Isatidis 4g, Radix Arnebiae (Radix Lithospermi) (root) 8g, Scorpio 4g, Fructus Forsythiae 10g, Medulla Tetrapanacis 6g, Fructus Kochiae 8g, Talcum 10g, Rhizoma Anemarrhenae 14g, Radix Glycyrrhizae 8g are amounted to 20 taste medical materials, clean post-drying, except Radix Rehmanniae is thinly sliced, all the other medical materials are ground into respectively coarse powder;
(2), gained medical material in step (1) is dropped into the supersound extraction tank that frequency is 20Hz, adding concentration is 50% ethanol 600ml, and normal temperature dipping is after 12 hours, adjust the temperature to 50 DEG C of supersound extraction 1.3 hours, stirred once every 10 minutes, micropore filters, and obtains first-time filtrate and medicinal residues;
(3), gained medicinal residues in step (2) being added to concentration is 60% ethanol 550ml again, adjusting the temperature to 50 DEG C ultrasonic (frequency 20Hz) extracts 25 minutes, stirred once every 10 minutes, micropore filters to obtain secondary filtrate, twice filtrate is merged, adding concentration is that 50% ethanol 20ml complements to the 1000ml fill that stirs again, and obtains Baizhi dehumidizer made from gloden cyllress and cape jasmine etc. Chinese herbal medicines.
Embodiment 3
Baizhi dehumidizer made from gloden cyllress and cape jasmine etc. Chinese herbal medicines production technology;
(1), Cortex Phellodendri 21g, Radix Scutellariae 17g, Radix Et Rhizoma Rhei 16g, Fructus Gardeniae 14g, Herba Scutellariae Barbatae 17g, Herba Hedyotidis Diffusae 21g, Flos Lonicerae 17g, Radix Rehmanniae 21g, Herba Houttuyniae 17g, Herba Artemisiae Scopariae 17g, Radix Bupleuri 12g, Radix Isatidis 6g, Radix Arnebiae (Radix Lithospermi) (root) 12g, Scorpio 6g, Fructus Forsythiae 14g, Medulla Tetrapanacis 8g, Fructus Kochiae 12g, Talcum 14g, Rhizoma Anemarrhenae 17g, Radix Glycyrrhizae 12g are amounted to 20 taste medical materials, clean post-drying, except Radix Rehmanniae is cut into slices, all the other medical materials are ground into respectively coarse powder;
(2), gained medical material in step (1) is dropped into the supersound extraction tank that frequency is 30Hz, adding concentration is 60% ethanol 600ml, and normal temperature dipping is after 13 hours, adjust the temperature to 60 DEG C of supersound extraction 1.5 hours, stirred once every 12 minutes, micropore filters, and obtains first-time filtrate and medicinal residues;
(3), step (2) gained medicinal residues being added to concentration is 60% ethanol 600ml, adjusting the temperature to 60 DEG C ultrasonic (frequency 30Hz) extracts 35 minutes, stirred once every 12 minutes, micropore filters to obtain secondary filtrate, twice filtrate is merged, adding concentration is that 60% ethanol 25ml complements to the 1100ml fill that stirs again, and obtains Baizhi dehumidizer made from gloden cyllress and cape jasmine etc. Chinese herbal medicines.
The foregoing is only preferred embodiment of the present invention, in order to limit the present invention, within the spirit and principles in the present invention not all, any amendment of doing, be equal to replacement, improvement etc., within all should being included in protection scope of the present invention.
Claims (8)
1. Baizhi dehumidizer made from gloden cyllress and cape jasmine etc. Chinese herbal medicines production technology, is characterized in that: comprise the steps:
(1), Cortex Phellodendri, Radix Scutellariae, Radix Et Rhizoma Rhei, Fructus Gardeniae, Herba Scutellariae Barbatae, Herba Hedyotidis Diffusae, Flos Lonicerae, Radix Rehmanniae, Herba Houttuyniae, Herba Artemisiae Scopariae, Radix Bupleuri, Radix Isatidis, Radix Arnebiae (Radix Lithospermi), Scorpio, Fructus Forsythiae, Medulla Tetrapanacis, the Fructus Kochiae, Talcum, the Rhizoma Anemarrhenae, Radix Glycyrrhizae are amounted to 20 taste medical materials, clean post-drying, except Radix Rehmanniae is cut into slices, all the other medical materials are pulverized respectively;
(2), all medical materials in step (1) are dropped into supersound extraction tank, add the ethanol that medical material 2.2-2.7 times quality, concentration are 40%-60%, under room temperature, flood after 11-13 hour, adjust the temperature to 40-60 DEG C of supersound extraction 1-1.5 hour, stirred once every 8-12 minute during this time, then carry out microporous filter, obtain first-time filtrate and medicinal residues;
(3), the medicinal residues of gained in step (2) are added to the ethanol that medical material 2.2-2.7 times quality, concentration are 40%-60%, adjust the temperature to 40-60 DEG C and carry out again supersound extraction 25-35 minute, stirred once every 8-12 minute during this time, again carry out microporous filter, obtain secondary filtrate, the filtrate that obtains for twice merges, then to add concentration be that the ethanol of 40%-60% complements to the front 90%-91% that adds ethanol volume summation for twice, and the fill that stirs obtains Baizhi dehumidizer made from gloden cyllress and cape jasmine etc. Chinese herbal medicines.
2. Baizhi dehumidizer made from gloden cyllress and cape jasmine etc. Chinese herbal medicines production technology according to claim 1, it is characterized in that: in described step (1), the each composition weight umber of 20 taste medical material is: Cortex Phellodendri 13-21 part, Radix Scutellariae 9-17 part, Radix Et Rhizoma Rhei 8-16 part, Fructus Gardeniae 6-14 part, Herba Scutellariae Barbatae 9-17 part, Herba Hedyotidis Diffusae 13-21 part, Flos Lonicerae 9-17 part, Radix Rehmanniae 13-21 part, Herba Houttuyniae 9-17 part, Herba Artemisiae Scopariae 9-17 part, Radix Bupleuri 4-12 part, Radix Isatidis 2-6 part, Radix Arnebiae (Radix Lithospermi) 4-12 part, Scorpio 2-6 part, Fructus Forsythiae 6-14 part, Medulla Tetrapanacis 2-8 part, Fructus Kochiae 4-12 part, Talcum 6-14 part, Rhizoma Anemarrhenae 9-17 part, Radix Glycyrrhizae 4-12 part.
3. Baizhi dehumidizer made from gloden cyllress and cape jasmine etc. Chinese herbal medicines production technology according to claim 1, is characterized in that: described step (1) Chinese crude drug grinding particle size is 10 orders.
4. Baizhi dehumidizer made from gloden cyllress and cape jasmine etc. Chinese herbal medicines production technology according to claim 1, is characterized in that: in described step (2), dip time is 12 hours, and the described supersound extraction time is 1 hour, and described stirring is to stir once every 10 minutes.
5. Baizhi dehumidizer made from gloden cyllress and cape jasmine etc. Chinese herbal medicines production technology according to claim 1, is characterized in that: in described step (3), the supersound extraction time is 30 minutes, and described stirring is to stir once every 10 minutes.
6. Baizhi dehumidizer made from gloden cyllress and cape jasmine etc. Chinese herbal medicines production technology according to claim 1, is characterized in that: described step (2) and (3) supersound extraction temperature are 50 DEG C.
7. Baizhi dehumidizer made from gloden cyllress and cape jasmine etc. Chinese herbal medicines production technology according to claim 1, is characterized in that: described step (2) and (3) supersound extraction frequency are 15-30Hz.
8. Baizhi dehumidizer made from gloden cyllress and cape jasmine etc. Chinese herbal medicines production technology according to claim 7, is characterized in that: described step (2) and (3) supersound extraction frequency are 20Hz.
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| CN201310042219.3A CN103961520A (en) | 2013-02-03 | 2013-02-03 | Amur Corktree Bark and Fructus Gardeniae dampness eliminating agent production technology |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107661435A (en) * | 2017-11-20 | 2018-02-06 | 贵州浩诚药业有限公司 | A kind of cypress Cape jasmine clearing damp spray and preparation method thereof |
| CN107837329A (en) * | 2017-11-20 | 2018-03-27 | 贵州浩诚药业有限公司 | A kind of cypress Cape jasmine clearing damp washing lotion and preparation method thereof |
| CN109362966A (en) * | 2018-11-05 | 2019-02-22 | 华中农业大学 | A kind of plant extract feed additive and application for improving sow milk performance |
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| KR101072164B1 (en) * | 2009-05-07 | 2011-10-10 | 이화여자대학교 산학협력단 | Composition comprising the extract of Anemarrhena asphodeloides Bunge for preventing and treating lipid metabolism disorder |
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Patent Citations (3)
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107661435A (en) * | 2017-11-20 | 2018-02-06 | 贵州浩诚药业有限公司 | A kind of cypress Cape jasmine clearing damp spray and preparation method thereof |
| CN107837329A (en) * | 2017-11-20 | 2018-03-27 | 贵州浩诚药业有限公司 | A kind of cypress Cape jasmine clearing damp washing lotion and preparation method thereof |
| CN109362966A (en) * | 2018-11-05 | 2019-02-22 | 华中农业大学 | A kind of plant extract feed additive and application for improving sow milk performance |
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