CN103952276B - A kind of brewing method of preserved egg cordyceps militaris liquor - Google Patents
A kind of brewing method of preserved egg cordyceps militaris liquor Download PDFInfo
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Abstract
The present invention relates to a kind of brewing method of preserved egg cordyceps militaris liquor, using Pollen Pini, Cordyceps militaris (L.) Link., Poria cocos and sealwort as raw material, by treatment process such as the ultrasonic lixiviate of white wine, freezing treatment and ceramic filters, prepared that a cost is low, mouthfeel good and there is delaying senility, the health promoting wine of effect of promoting longevity, health promoting wine making method of the present invention is by advanced filtering technique, make prepared wine clarity and good stability, easy to operate.
Description
Technical field
The present invention relates to a kind of alcoholic drink mixed with fruit juice, particularly relate to a kind of brewing method of preserved egg cordyceps militaris liquor, belong to field of food health care.
Background technology
There are three aspects in the direction of white wine technical development: 1.: traditional potability white wine, high-end white wine; 2.: modern blending technique and the fragrance to white wine are familiar with, the white spirit of the solid-liquid combination brewageed; 3.: on the basis of traditional liquor, increase a part have pharmaceutical cpd that is functional, trophicity, some that compensate in white wine is not enough, but maintains the base style of white wine.
The ancient Chinese medical science of uphold nature spirit, is considered as the important channel nourished the body by diet, passed in the health wisdom do not put out in thousand, emphasizes " integration of drinking and medicinal herbs, residence is mended in drink ".This had also both maintained nutrition and effect of raw material, had again conditioning healthy nutritive value, was the daily nutrient excellent product drinking and adjust health.But China's health promoting wine mainly with normally used tonic Chinese medicinal materials for raw material, become according to proved recipe of traditional Chinese medicine infuse, there is specific color (as yellow, brown) and special odor, the similar medicinal liquor of this product, consume this alcohol product on a public occasion, to the sensation of people's one " in poor nick ", a lot of people has certain scruples, and this constrains the social consumption amount of this health promoting wine to a certain extent.Therefore, in the exploitation of alcohol product, the raw material of the integration of drinking and medicinal herbs of some gentle nourishings should be selected, make every effort to reach medicine cordiale perfume and coordinate, meet the mouthfeel of human consumer and the demand of nourishing.
Ultrasonic-leaching ratio juris utilizes hyperacoustic cavatition, the enormous pressure that cavitation produces causes breaking of the thing cell that is broken, and whole rupture process completes instantaneously, increasing frequency and the speed of molecular motion of material, adding the penetration power of solvent; The oscillating action that simultaneously ultrasonic wave produces strengthens the release of intracellular matter, diffusion and dissolving, accelerates the stripping of effective constituent.Except cavitation and oscillating action, hyperacoustic many second-order effects, as emulsification, pulverizing, chemical effect etc. are also all conducive to the transfer of effective components in plants, and abundant and solvent, promote the carrying out of extracting, early stage ultrasonic extraction process is adopted to raw material by technique, obtain more effective ingredient in raw material, improve the nourishing ability of product.
Ceramic membrane is filtering system comparatively conventional at present, is the porous asymmetric film be prepared from material through special technology such as aluminum oxide, titanium oxide, zirconium whites.Ceramic membrane filter is a kind of fluid sepn process of " cross flow filter " form: under the driving of pressure effect, stock liquid is at film Bottomhole pressure, small-molecule substance is through film, and the concentrated solution tunicle containing macromolecular components retains, thus makes fluid reach the object of separation, concentrated, purifying.It has numerous advantages such as separation efficiency is high, effect stability, chemical stability are good, acid and alkali-resistance, organic solvent-resistant, resistance to bacterium, high temperature resistant, antipollution, physical strength are high, film regenerability is good, sepn process is simple, energy consumption is low, simple and convenient operation and maintenance, film long service life.Ceramic membrane equipment has been successfully applied to food, beverage, has planted the various fields such as the processing of (medicine) object depth, biological medicine, fermentation, fine chemistry industry, can be used for the separation in technological process, clarification, purifying, concentrated, degerming, desalination etc.Ceramic membrane equipment can replace traditional solid-liquid separating equipment such as whizzer, sheet frame, and the quality of feed liquid is traditional method can not compare, and the yield of product is also high than traditional method.
Summary of the invention
The invention provides that a cost is low, mouthfeel good and there is delaying senility, the health promoting wine of effect of promoting longevity.This health promoting wine sophistication in preparation process, makes prepared wine liquid clarity and good stability, easy to operate.
The technical scheme that the present invention solves the problems of the technologies described above is as follows: a kind of brewing method of preserved egg cordyceps militaris liquor, comprises the following steps:
1) get Pollen Pini, the white wine adding Pollen Pini quality 10 ~ 15 times carries out ultrasonic lixiviate, and after lixiviate, solid-liquid separation obtains Pollen Pini vat liquor;
2) in the mixing medicinal material of Cordyceps militaris (L.) Link., Poria cocos and sealwort composition, the white wine adding mixing medicinal material total mass 10 ~ 15 times carries out ultrasonic lixiviate first, extraction fluid; Repeat lixiviate and merge the extracting solution of extracted many times, obtaining mixing medicinal material vat liquor;
3) by aforementioned Pollen Pini vat liquor with mix medicinal material vat liquor and merge and obtain total vat liquor, add honey and blend, obtain the wine liquid after blending;
4) natural aging is carried out to the wine liquid after blending;
5) the wine liquid after natural aging carries out freezing treatment in subzero 8 to subzero 10 degrees Celsius;
6) after freezing treatment, wine liquid forms the beds of precipitation and upper strata wine liquid, and be separated upper strata wine liquid and carry out ceramic membrane filter, the product obtaining clarification is preserved egg cordyceps militaris liquor.
Further, step 1) and step 2) described in the condition of ultrasonic lixiviate be: frequency 67 ~ 73KHz, adopts circulation stirring in ultrasonic leaching process, and mixing speed is 15 ~ 40rpm, and each time of stirring is 40 ~ 60min, and mixing chamber is divided into 1 ~ 3h.
Further, step 1) the ultrasonic extraction time of Pollen Pini is 5 ~ 10 days.
Further, step 2) weight part of the composition of described mixing medicinal material and each component is as follows:
Cordyceps militaris (L.) Link. 40 ~ 50 parts;
25 ~ 35 parts, Poria cocos;
Sealwort 15 ~ 25 parts.
Preferably, step 2) to repeat the number of times of lixiviate be 1 ~ 2 time.
Further, step 2) time of mixing medicinal material ultrasonic lixiviate is first 4 ~ 6 days, the time of subsequent ultrasonic lixiviate is 3 ~ 5 days.
Further, described white wine is the white wine of 40 ~ 60%v/v.
Further, the total mass of described mixing medicinal material is 2.5 ~ 5 times of Pollen Pini quality.
Further, step 3) mass volume ratio of described honey and described total vat liquor is 0.01 ~ 0.08:1 (unit of mass volume ratio is Kg/L).
Further, step 4) condition of natural aging is: storage in room temperature 3 ~ 6 months.
Further, step 5) freezing treatment time, need in temperature-fall period to stir wine liquid.
Further, step 5) freezing treatment time, in temperature-fall period, interval stirring is carried out to wine liquid, stirred once every 30 ~ 60 minutes, the time of each stirring is 30 ~ 60 minutes, stops stirring, leave standstill 8 ~ 10 days after temperature is down to subzero 8 to subzero 10 degrees Celsius.
Further, step 6) specification of ceramic membrane is 0.05 ~ 0.15 μm.
Further, step 6) described ceramic membrane is α-Al
2o
3material, working pressure is 0.5 ~ 2mpa, and temperature range is 20 ~ 50 DEG C.
In this Production of Health Wine process, adopt membrane filtration system, effectively can remove the invalid macromolecular components of medicinal material extract, and these macromolecular components are as very unstable in polysaccharide, tannin, protein etc., not only affect the mouthfeel of wine, fragrance, color and luster, clarity, stability, and be cause the basic reason that wine body is muddy and precipitate.And integrated operation is simple, easy to clean, is convenient to production operation.
Second aspect present invention discloses a kind of preserved egg cordyceps militaris liquor, adopts aforesaid method to brewage acquisition.
Further, its raw material of preserved egg cordyceps militaris liquor of the present invention comprises Pollen Pini, Cordyceps militaris (L.) Link., Poria cocos, sealwort, white wine, and honey.
The invention has the beneficial effects as follows: preserved egg cordyceps militaris liquor of the present invention contains the integration of drinking and medicinal herbs raw materials such as Pollen Pini, Cordyceps militaris (L.) Link., Poria cocos, sealwort, by filtering technique and the extracting method of advanced person.Prepared that a cost is low, clarity and good stability, suitable go with rice or bread drinks, mouthfeel is good and there is delaying senility, the health promoting wine acted on of promoting longevity.
Accompanying drawing explanation
Fig. 1 is preparation technology's flow process of preserved egg cordyceps militaris liquor.
Embodiment
Be described principle of the present invention and feature below in conjunction with accompanying drawing, example, only for explaining the present invention, is not intended to limit scope of the present invention.
Embodiment 1
1. material
Select Pollen Pini, Cordyceps militaris (L.) Link., Poria cocos, sealwort, four taste Chinese medicines, through Preparation process, stand-by.
2. preparation method
1) getting Pollen Pini is placed in bottom a pot for solvent extraction, add the white wine of the 40%v/v of Pollen Pini amount 10 times of quality, frequency is adopted to be the ultrasonic wave of 67KHz, ultrasonic lixiviate 10 days, stirring velocity is 15rpm, and churning time is 40min, and period distances is 3h, Pollen Pini vat liquor is obtained after vat liquor coarse filtration, for subsequent use;
2) the mixing medicinal material that gross weight is Pollen Pini 5 times is got, be put in another pot for solvent extraction, the white wine squeezing into the 40%v/v of medicinal material weight 15 times starts ultrasonic lixiviate first, frequency is adopted to be that the ultrasonic-leaching of 67KHz is after 6 days, extraction fluid after coarse filtration, the white wine again squeezing into identical amount in filter residue repeats lixiviate 1 time; The frequency of ultrasonic lixiviate is 67KHz again, and extraction time is 5 days; Merge the extracting solution of twice lixiviate, obtain mixing medicinal material vat liquor.
Mixing medicinal material, according to weight part Cordyceps militaris (L.) Link. 40 parts, 25 parts, Poria cocos, sealwort 25 parts, carries out taking, mixing; Adopt circulation stirring in twice ultrasonic-leaching process, stirring velocity is 15rpm, and churning time is 40min, and period distances is 3h.
3) by Pollen Pini vat liquor with mix medicinal material vat liquor and merge and obtain total vat liquor, squeeze into and blend in tank;
4) add honey to blending in tank, the mass volume ratio of honey and total vat liquor is: 0.01:1, stirs 2 hours, makes fully to mix, and obtains the wine liquid blent;
5) the wine liquid blent is noted storage in storage tank and carry out natural aging 4 months;
6) aging complete wine liquid is squeezed in refrigerated cylinder by Cemented filling, set freezing temp as-8 DEG C of freezing units of unlatching, and every 0.5h turn on agitator once, each churning time is 60 minutes, temperature stops after being down to design temperature stirring, leaving standstill, and freezing treatment total time is 8 days;
7) after freezing treatment, draw wine liquid from the top of the beds of precipitation and adopt ceramic membrane filter to do clarifying treatment, ceramic membrane specification is 0.15 μm, obtains clarification wine liquid and is placed in finished pot.
Embodiment 2
1. material
Select Pollen Pini, Cordyceps militaris (L.) Link., Poria cocos, sealwort, four taste Chinese medicines, through Preparation process, stand-by.
2. preparation method
1) getting Pollen Pini is placed in bottom a pot for solvent extraction, add the white wine of the 50%v/v of Pollen Pini amount 15 times of quality, frequency is adopted to be the ultrasonic wave of 70KHz, ultrasonic lixiviate 8 days, stirring velocity is 30rpm, and churning time is 60min, and period distances is 1.5h, Pollen Pini vat liquor is obtained after vat liquor coarse filtration, for subsequent use;
2) the mixing medicinal material that gross weight is Pollen Pini 2.5 times is got, be put in another pot for solvent extraction, the white wine squeezing into the 60%v/v of medicinal material weight 10 times starts ultrasonic lixiviate first, frequency is adopted to be that the ultrasonic-leaching of 70KHz is after 5 days, extraction fluid after coarse filtration, the white wine again squeezing into identical amount in filter residue repeats lixiviate 2 times; The frequency of ultrasonic lixiviate is 70KHz again, and extraction time is 4 days; Merge the extracting solution of three lixiviates, obtain mixing medicinal material vat liquor.
Mixing medicinal material, according to weight part Cordyceps militaris (L.) Link. 45 parts, 35 parts, Poria cocos, sealwort 15 parts, carries out taking, mixing; Adopt circulation stirring in twice ultrasonic-leaching process, stirring velocity is 30rpm, and churning time is 50min, and period distances is 1.5h.
3) by Pollen Pini vat liquor with mix medicinal material vat liquor and merge and obtain total vat liquor, squeeze into and blend in tank;
4) add honey to blending in tank, the mass volume ratio of honey and total vat liquor is: 0.08:1, stirs 2.5 hours, makes fully to mix, and obtains the wine liquid blent;
5) the wine liquid blent is noted storage in storage tank and carry out natural aging 6 months;
6) aging complete wine liquid is squeezed in refrigerated cylinder by Cemented filling, set freezing temp as-9 DEG C of freezing units of unlatching, and every 1h turn on agitator once, each churning time is 45 minutes, temperature stops after being down to design temperature stirring, leaving standstill, and freezing treatment total time is 10 days;
7) after freezing treatment, draw wine liquid from the top of the beds of precipitation and adopt ceramic membrane filter to do clarifying treatment, ceramic membrane specification is 0.1 μm, obtains clarification wine liquid and is placed in finished pot.
Embodiment 3
1. material
Select Pollen Pini, Cordyceps militaris (L.) Link., Poria cocos, sealwort, four taste Chinese medicines, through Preparation process, stand-by.
2. preparation method
1) getting Pollen Pini is placed in bottom a pot for solvent extraction, add the white wine of the 60%v/v of Pollen Pini amount 12 times of quality, frequency is adopted to be the ultrasonic wave of 73KHz, ultrasonic lixiviate 5 days, stirring velocity is 40rpm, and churning time is 50min, and period distances is 1h, Pollen Pini vat liquor is obtained after vat liquor coarse filtration, for subsequent use;
2) the mixing medicinal material that gross weight is Pollen Pini 4 times is got, be put in another pot for solvent extraction, the white wine squeezing into the 50%v/v of medicinal material weight 10 times starts ultrasonic lixiviate first, frequency is adopted to be that the ultrasonic-leaching of 73KHz is after 4 days, extraction fluid after coarse filtration, the white wine again squeezing into identical amount in filter residue repeats lixiviate 1 time; The frequency of ultrasonic lixiviate is 73KHz again, and extraction time is 3 days; Merge the extracting solution of twice lixiviate, obtain mixing medicinal material vat liquor.
Mixing medicinal material, according to weight part Cordyceps militaris (L.) Link. 50 parts, 30 parts, Poria cocos, sealwort 20 parts, carries out taking, mixing; Adopt circulation stirring in twice ultrasonic-leaching process, stirring velocity is 40rpm, and churning time is 60min, and period distances is 1h.
3) by Pollen Pini vat liquor with mix medicinal material vat liquor and merge and obtain total vat liquor, squeeze into and blend in tank;
4) add honey to blending in tank, the mass volume ratio of honey and total vat liquor is: 0.05:1, stirs 3 hours, makes fully to mix, and obtains the wine liquid blent;
5) the wine liquid blent is noted storage in storage tank and carry out natural aging 3 months;
6) aging complete wine liquid is squeezed in refrigerated cylinder by Cemented filling, set freezing temp as-10 DEG C of freezing units of unlatching, and every 45min turn on agitator once, each churning time is 30 minutes, temperature stops after being down to design temperature stirring, leaving standstill, and freezing treatment total time is 9 days;
7) after freezing treatment, draw wine liquid from the top of the beds of precipitation and adopt ceramic membrane filter to do clarifying treatment, ceramic membrane specification is 0.05 μm, obtains clarification wine liquid and is placed in finished pot.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, within the spirit and principles in the present invention all, any amendment done, equivalent replacement, improvement etc., all should be included within protection scope of the present invention.
Claims (6)
1. a brewing method for preserved egg cordyceps militaris liquor, comprises the following steps:
1) get Pollen Pini, the white wine adding Pollen Pini quality 10 ~ 15 times carries out ultrasonic lixiviate, and after lixiviate, solid-liquid separation obtains Pollen Pini vat liquor, and the ultrasonic extraction time of Pollen Pini is 5 ~ 10 days;
2) in the mixing medicinal material of Cordyceps militaris (L.) Link., Poria cocos and sealwort composition, the white wine adding mixing medicinal material total mass 10 ~ 15 times carries out ultrasonic lixiviate first, extraction fluid; Repeat lixiviate and merge the extracting solution of extracted many times, obtaining mixing medicinal material vat liquor; Described mixing medicinal material is made up of Cordyceps militaris (L.) Link., Poria cocos, sealwort, and the weight part of each component is as follows: Cordyceps militaris (L.) Link. 40 parts ~ 50 parts; 25 parts ~ 35 parts, Poria cocos; Sealwort 15 parts ~ 25 parts, the total mass of described mixing medicinal material is 2.5 ~ 5 times of Pollen Pini quality;
3) by aforementioned Pollen Pini vat liquor with mix medicinal material vat liquor and merge and obtain total vat liquor, add honey and blend, obtain the wine liquid after blending;
4) natural aging is carried out to the wine liquid after blending;
5) the wine liquid after natural aging carries out freezing treatment in subzero 8 to subzero 10 degrees Celsius;
6) after freezing treatment, wine liquid forms the beds of precipitation and upper strata wine liquid, and be separated upper strata wine liquid and carry out ceramic membrane filter, the product obtaining clarification is preserved egg cordyceps militaris liquor;
The condition of described ultrasonic lixiviate is: ultrasonic frequency 67 ~ 73KHz, adopts circulation stirring in ultrasonic leaching process, and mixing speed is 15 ~ 40rpm, and each time of stirring is 40 ~ 60min, and mixing chamber is divided into 1 ~ 3h.
2. brewing method as claimed in claim 1, is characterized in that, step 2) time of mixing medicinal material ultrasonic lixiviate is first 4 ~ 6 days, the time of subsequent ultrasonic lixiviate is 3 ~ 5 days.
3. brewing method as claimed in claim 1, it is characterized in that, described white wine is the white wine of 40 ~ 60%v/v.
4. brewing method as claimed in claim 1, is characterized in that, step 3) mass volume ratio of described honey and described total vat liquor is 0.01 ~ 0.08:1.
5. brewing method as claimed in claim 1, is characterized in that, step 6) specification of ceramic membrane is 0.05 ~ 0.15 μm.
6. a preserved egg cordyceps militaris liquor, adopts method described in the arbitrary claim of claim 1-5 to brewage acquisition.
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Citations (4)
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| CN101671617A (en) * | 2009-09-28 | 2010-03-17 | 烟台新时代健康产业有限公司 | Method for brewing pine pollen health wine |
| CN101683130A (en) * | 2008-09-28 | 2010-03-31 | 王平 | Pine pollen wine and preparation method thereof |
| CN102229877A (en) * | 2011-05-16 | 2011-11-02 | 浙江亚林生物科技股份有限公司 | Brewing method for pine pollen wine |
| CN103484329A (en) * | 2013-09-26 | 2014-01-01 | 惠州市天昱酒业有限公司 | Health-care wine, and raw materials and preparation method thereof |
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2014
- 2014-04-30 CN CN201410180171.7A patent/CN103952276B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101683130A (en) * | 2008-09-28 | 2010-03-31 | 王平 | Pine pollen wine and preparation method thereof |
| CN101671617A (en) * | 2009-09-28 | 2010-03-17 | 烟台新时代健康产业有限公司 | Method for brewing pine pollen health wine |
| CN102229877A (en) * | 2011-05-16 | 2011-11-02 | 浙江亚林生物科技股份有限公司 | Brewing method for pine pollen wine |
| CN103484329A (en) * | 2013-09-26 | 2014-01-01 | 惠州市天昱酒业有限公司 | Health-care wine, and raw materials and preparation method thereof |
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Effective date of registration: 20161115 Address after: 102206 No. 1 building, No. 10, science Road, Beijing, Changping District Patentee after: New Age Health Industry(Group) Co., Ltd. Address before: 264006 No. 6, Huaihe Road, Yantai economic and Technological Development Zone, Yantai, Shandong Patentee before: Yantai new era Health Industry Co., Ltd. |
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Address after: 264006 No.15 Guiyang street, Yantai Economic and Technological Development Zone, Shandong Province Patentee after: NEW ERA HEALTH INDUSTRY (Group) Co.,Ltd. Address before: 102206 Building 1, yard 10, kekeyuan Road, Changping District, Beijing Patentee before: NEW ERA HEALTH INDUSTRY (Group) Co.,Ltd. |