CN103947908A - Preparation method of anti-oxidation and anti-pollution multi-nutrient block for dairy cows - Google Patents
Preparation method of anti-oxidation and anti-pollution multi-nutrient block for dairy cows Download PDFInfo
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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Abstract
The invention discloses a preparation method of an anti-oxidation and anti-pollution multi-nutrient block for dairy cows, belonging to the technical field of a block for the dairy cows. The method takes molasses, urea, vitamins and mineral elements as main raw materials; the anti-oxidation and anti-pollution multi-nutrient block is prepared by scientifically compounding natural antioxidant substances, Chinese herb extracts and seasoning extracts; the prepared multi-nutrient block for the dairy cows is moderate in hardness, dampproof, breakage-proof and high in weather fastness; the lapping surface of the block is low in bacterial content which is 1.5 per ten thousand of a comparison group; after the multi-nutrient block is used, the milk yield of the lactating dairy cows can be remarkably increased by 19.02%, the first estrus time is shortened by 13 days after parturition of the dairy cows, the conception rate of the dairy cows at the first estrus period is increased by 16.5% after parturition of the dairy cows, the oestrus proportion of the postpartum dairy cow group is increased by 18.4%, the feed intake and the immunity of the organism of the dairy cows can be effectively improved, the occurrence rates of nutritional diseases such as abnormal addiction disease, foot rot, white muscle disease, postpartum paralysis, rickets, mastitis, coarse fur and the like of the dairy cows can be remarkably reduced, and the occurrence rates are averagely reduced by 3.3-16.7%.
Description
Technical field
The present invention relates to milk cow and lick brick, particularly a kind of preparation method of anti-oxidant, anti-pollution milk cow composite nutrient licking brick.
Background technology
Licking brick (MMUB) is that " molasses-mineral element-urea is licked brick " (molasses-mineral-urealblock) is called for short, being the novel product that a kind of needs simple, effectively supplement salt, minerals and vitamins etc. for meeting domestic animal form above nutritional labeling mixed preparing according to a certain percentage, is to be placed on the place at water source or the cubed feed that crib limit is licked for cattle and sheep.The object that brick is licked in application is, herd with drylot feeding process in, to cattle and sheep, supplement the nutrients such as mineral matter, nonprotein nitrogen, vitamin, improve cattle and sheep feed intake and efficiency of feed utilization, promotion growth, increase economic efficiency.Particularly, in Winter-Spring withered grass season, in the situation of the feed feeds such as green hay, agricultural crop straw and ensilage to cattle and sheep, supplementary feeding is licked brick and is seemed particularly important.Research shows; the composite nutrient licking brick of feeding can improve rumenic acid soda balance; supplement milk cow itself and required various vitamin and the trace element of rumen microorganism; for rumen microorganism provides more favourable living environment; be milk cow body more nutriment is provided, thereby improve the output of milk and improve milk quality.
Milk cow is due to the difference of health status and physiological status, between its individuality to nutrient and salt need to be also different, milk cow can independently lick brick by self-demand.Therefore, even Japan and the U.S. in strict accordance with the cattle farm of TMR feeding and management, also take to lick this technology of brick and supplement mineral matter element and vitamin.In animal husbandry developed countries such as the U.S., Britain, Holland, Australia, the supplementary feeding technical measures of herding with drylot feeding necessity have been become.FAO has been generalized to the practical technique of this small investment, instant effect more than 70 countries such as Asia and Africa, and Bing third world countries have obtained very ten-strike in promoting, and peasant calls " cattle and sheep are chocolate " favorably licking brick.
The research of licking brick for cattle and sheep is started late in China, and late 1980s has just just started development at northern area.In recent years, China herding worker has carried out some research and application about nutrition lap brick production technology, equipment research and development and the aspects such as cattle and sheep of feeding, obtained certain achievement, but the research and production level of China's licking brick for cattle and sheep lags significantly behind animal husbandry developed country, in China, because the production of licking brick is in the starting stage, technology is relatively backward, there is no unified standard, the kind of licking brick is a lot, and call is different, general according to lick brick ingredient account for its ratio number name.For example, the mineral matter element of take is licked brick as the main complex mineral that cries, and the urea of take is the main urea nutrition lap brick that cries, the molasses of take be lead be molasses nutrition lap brick.The existing nutrition lap brick of China contains urea, molasses, mineral matter element, vitamin etc. mostly, is therefore composite nutrient licking brick.Still the interpolation probiotics having, Chinese herbal medicine, fungal cultures etc., raw material is different in a word, Various Functions.
As can be seen here, how the raw material of no matter licking brick changes; No matter herd or drylot feeding; No matter be cattle and sheep or other domestic animal; Licking brick as a kind of feed, there is following common ground in its feed: 1. selective autonomous feed; Imperfect, be exposed in air for a long time; 3. in environment, pernicious bacteria content is high; 4. the process of feeding is licked the control of brick difficult quality.Due to above feed feature, lick brick quality and in the process of feeding, have larger hidden danger of quality: easily moisture absorption, frangible; Nutriment especially vitamin (as vitamin E), mineral element (as selenium), amino acid etc. is oxidizable; The pollution of harmful microorganism to nutritional labeling (as molasses); Temperature is on licking impact of brick quality etc.For above-mentioned situation, herding scientific research personnel has researched and developed corresponding milk cow and has licked brick, such as: Chinese patent CN102524595B discloses a kind of protection against the tide that has, breakage-proof, efficient licking brick for cattle and sheep, by iron oxide red 0.6-1.0 part, zinc oxide 0.4-0.8 part, basic copper chloride 0.2-0.6 part, manganese oxide 0.02-0.06 part, magnesia 1-2 part, calcium monohydrogen phosphate 15-18 part, sodium selenite, calcium iodate, mixture 2.5-3.0 part of cobalt chloride and medical stone, B B-complex 0.5-0.8 part, rare earth 3.48-3.8 part, the raw material preparation of salt 69.94-76.3 part (weight), can be moistureproof, breakage-proof, accurately control the cattle and sheep amount of licking, nutritious, strong health-care function, short long effective, improve the output of milk obvious, hair matter gross weight improves fast feature.Chinese patent CN102113637B discloses the short breeding of a kind of weatherability type ox and has licked brick, by coated retinol1 .0～2.800, coated vitamin D 0.50～1.00, coated vitamin E 5.00～10.00, yeast selenium 5-10, glucoheptonic acid cobalt 5-10, dihydropyridine 15, stone flour 160, calcium monohydrogen phosphate 120, salt 433.8-443.8, urea 80, the raw material preparation of molasses 160 (weight portion), in formula, use coated vitamin, strengthened the stability of vitamin, but once licking, dressing can dissolve very soon, vitamin can still can be exposed in air and is oxidized, and mineral element also can be oxidized, antioxidant effect is still poor, utilization of nutrients is low.Above-mentioned two patents do not solve milk cow and lick that brick is oxidizable, the problem of easy pollution.
In nature and animal body, there is a kind of chemical substance that is called free radical, as ultra-oxygen anion free radical, organic peroxy base, hydroxy radical.These free radicals are very unstable, can cause oxidative damage to cell, and more seriously, free radical can cause radical reaction, and radical reaction is circulating chain reaction, and every circulation primary all can produce peroxide, as hydrogen peroxide and unsaturated hydroperoxides.These peroxide are very unstable, have very strong oxidation, can cause peroxide injury to DNA, RNA, mitochondrial membrane, endoplasm sarcolemma, cell membrane.The peroxide injury that the peroxide that free radical and radical reaction produce causes is the fundamental cause that causes Animal Aging and produce various diseases.Free radical is extensively present in nature, as contaminated and through air, the smoke from cigarette of ultraviolet ray (solar radiation), smoke in video, omnipresent in various organisms.In animal body, have the reaction that stops free radical, eliminate the material of free radical and peroxide, just make animal health grow up, antioxidant has: selenium, flavonoids, vitamin E, vitamin A, vitamin C, ubiquinone, glutathione, half peptide propylhomoserin.Antioxidase has: glutathione peroxidase (GSH-Px is containing selenium), glutathione reductase (GSSG-R), superoxide dismutase (SOD) (cupric, zinc or manganese), peroxidase (CAT, iron content) etc.These materials form the anti-oxidative defense mechanism in animal body, avoid peroxide injury.Trace element also synthesizes, participates in enzymatic synthesis, participates in organism metabolism, improves enzymatic activity etc. with vitamin (vitamin E) synergy, participation protein in animal body except eliminating free radical, very extremely important to animal in a word.
The above-mentioned mechanism of action is also that milk cow licks the final purpose that brick adds vitamin and mineral element, trace element, but, because milk cow licks the imperfect long term exposure of brick in the air that contains free radical, can cause on the one hand the oxidation of vitamin and mineral element, trace element, reduce its utilization rate, weaken its antioxidation to milk cow machine interior free yl, have a strong impact on the Growth and reproduction of milk cow, bring out the generation of various diseases, reduce milk cow production performance, increase milk cattle cultivating cost; Also can cause on the other hand the microbial contamination of high sugared nutriment-molasses.
Grape seed extract (former blue and white plain OPC) is the effective active nutrition of extracting from grape pip, is often equipped with the refining supplementary antioxidant nutraceutical forming of the primary raw materials such as vitamin E.Grape seed extract is new and effective natural material essential in a kind of human body extracting from grape pip.It is anti-oxidant, the strongest material of removing free radical ability that current occurring in nature is found, its antioxidation activity is 50 times, ascorbic 20 times of the plain E of dimension, it can effectively remove unnecessary free radical in human body, has the superpower effect that delays senility and strengthen immunity.
Ginkgo biloba p.e has prevention and cure of cardiovascular disease, anti-ageing, the effect of anti-cancer.Remove too much free radical in body; the lipid generation peroxidization that suppresses cell membrane; thereby Cell protection film; prevent a series of injuries that radical pair body causes; by stimulating the release of catecholamine and suppressing degraded; and by stimulating the generation of prostacyclin and endothelium relaxing factor to produce auterial diastole effect, jointly keep the tension force of artery and vein blood vessel.There is the whole blood of reduction viscosity, promote red blood cell and leukocytic target, improve sanguimotor effect.Increase the supply of ischemic tissue to oxygen and glucose, increase the quantity of some neurotransmitter receptor, as muscarinic, norepinephrine and Serotonin receptor.Grape pip procyanidin (Earthquake of Anyang station in Henan Jing Sen bio tech ltd is on sale), ginkgo biloba p.e (production of Xuzhou Heng Kai ginkgo Products Co., Ltd) market all have finished product to sell.
Rosemary, Xue MingRosma rinus officinalis (Rosmarinus officinalis L) is Labiatae Rosmarinus plant, is the Plants compared with high anti-oxidation effect that has of generally acknowledging at present.(Wuhan Yuancheng Technology Development Co., Ltd. is on sale)
At present, lick composite, the moistureproof breakage-proof Research Literature of brick nutrition more about milk cow, Effect of Anti oxidation, antipollution few, does not even have, and adds natural to milk cow and licks in brick and be expected to address the above problem.
Summary of the invention
Technical problem solved by the invention is for existing milk cow, to lick the defect of brick, with molasses, urea, vitamin and mineral element are primary raw material, composite Chinese herbal medicine extract and the flavoring extract that there is the Natural Antioxidants of strong anti-oxidation and there is bacteria resistance function and fragrance of science, prepare a kind of anti-oxidant, anti-pollution milk cow composite nutrient licking brick, existing milk cow, lick under the environment and mode of brick feed, can effectively prevent that milk cow from adding the nutriment loss of brick and polluting, effectively improve the growth of milk cow, breeding and production performance, the generation of prevention various diseases, also can promote milk cow appetite, increase feed intake, to reduce milk cattle cultivating cost, increase economic benefit.
In order to achieve the above object, the present invention is by the following technical solutions:
A preparation method for anti-oxidant, anti-pollution milk cow composite nutrient licking brick, comprises the steps:
Described composite nutrient licking brick is prepared by the raw material of following parts by weight:
Salt 55-75 part, molasses 30-50 part, glutinous rice 25-45 part, urea 25-35 part, medical stone 30-35 part, dicalcium powder 25-35 part, alumino-silicate 20-35 part, natural 20-35 part, Chinese herbal medicine extract 5-10 part, flavoring extract 5-10 part, rare earth 6-8 part, yeast selenium 3-5 part, calcium iodate 2-4 part, magnesia 2-4 part, B B-complex 1-3 part, iron oxide red 1-1.5 part, zinc oxide 1-1.5 part, basic copper chloride 0.8-1.2 part, cobalt chloride 0.5-0.8 part, manganese oxide 0.1-0.3 part, urease inhibitor 0.1-0.3 part;
Preferred described milk cow composite nutrient licking brick is prepared by the raw material of following parts by weight:
Salt 60-70 part, molasses 35-45 part, glutinous rice 30-40 part, urea 27-32 part, medical stone 31-33 part, dicalcium powder 28-32 part, alumino-silicate 25-30 part, natural 25-30 part, Chinese herbal medicine extract 6-8 part, flavoring extract 6-8 part, rare earth 6.5-7.5 part, yeast selenium 3.5-4.5 part, calcium iodate 2.5-3.5 part, magnesia 3-3.5 part, B B-complex 1.5-2.5 part, iron oxide red 1.2-1.4 part, zinc oxide 1.2-1.4 part, basic copper chloride 0.9-1.1 part, cobalt chloride 0.6-0.7 part, manganese oxide 0.15-0.25 part, urease inhibitor 0.15-0.25 part,
First salt, medical stone, alumino-silicate and rare earth are pulverized, made its granularity reach 100 orders; Then get by weight proportion molasses and be heated to 160-170 ℃, according to part by weight, adding urea, mix and blend 10 minutes; When being reduced to 60 ℃, question response thing temperature successively adds by weight proportion salt, medical stone, dicalcium powder, alumino-silicate, rare earth and glutinous rice, mix and blend 15 minutes; Then successively add by weight proportion yeast selenium, calcium iodate, magnesia, iron oxide red, zinc oxide, basic copper chloride, cobalt chloride, manganese oxide, urease inhibitor, mix and blend 15 minutes; Finally successively add by weight proportion Chinese herbal medicine extract, B B-complex, natural and flavoring extract, stir 10-15 minute; Finally compound is put in mould, utilize hydraulic press on pressing mold every square centimeter with 540-640kg pressure pressing 25-35, be pressed into 2-10kg bulk second and lick brick, then carry out the demoulding, detection, packing and obtain anti-oxidant, anti-pollution milk cow composite nutrient licking brick.
The preparation method of described glutinous rice is: first glutinous rice soaks 24-48h through impurity elimination, after cleaning in 18 ℃-25 ℃ of water temperatures, and moisture reaches 25%-30% (immersion standard is complete with the grain of rice, finger alunite rice be broken); Then normal pressure steam a rice 15min-25min (steam rice reach ripe and not thoroughly, rotten, outer soft, loosely in hard be evenly advisable thoroughly and not, the final grain of rice should be without the white heart) obtain there is high viscosity, miscible glutinous rice.
Described natural is any or several combinations in grape pip procyanidin, Rosmarinus officinalis extract and apricot leaf extract; The mass ratio that described grape pip procyanidin, Rosmarinus officinalis extract and apricot leaf extract mix is 2-3:1-2:0.5-1.5;
Described grape pip procyanidin is bought in Earthquake of Anyang station in Henan Jing Sen bio tech ltd, and ginkgo biloba p.e is bought in Xuzhou Heng Kai ginkgo Products Co., Ltd, and Rosmarinus officinalis extract is bought in Wuhan Yuancheng Technology Development Co., Ltd., is pressed powder.
Described Chinese herbal medicine extract is prepared by the raw material of following parts by weight: Radix Angelicae Sinensis 55-65 part, Ligusticum wallichii 55-65 part, fructus amomi 50-60 part, radix paeoniae rubrathe 50-60 part, Divine Comedy 45-55 part, Fructus Hordei Germinatus 45-55 part, motherwort 45-55 part, costus root 40-45 part, Radix Codonopsis 40-45 part, Radix Astragali 40-45 part, honeysuckle 40-45 part, cordate houttuynia 35-45 part, Poria cocos 35-45 part, fushen 35-45 part, polygala root 30-40 part, fry fennel 30-40 part, bighead atractylodes rhizome 30-40 part, bark of official magnolia 30-40 part, Radix Glycyrrhizae 25-35 part, hawthorn 25-35 part, dried orange peel 25-35 part;
The preparation method of described Chinese herbal medicine extract is: respectively said herbal medicine being crushed to particle diameter is below 2 millimeters, then in container, evenly mix and add the water of 3-6 times of weight, control temperature 70 C-90 ℃ and keep 2-4h, then be cooled to 45-60 ℃, add the mixing enzyme preparation of mixed material gross weight 5-10% to carry out enzymolysis, with newborn acid for adjusting pH value, be 5.5-6.8, enzymolysis 2-4h, finally add the mixture of mixed material 0.5-3 times of weight ethanol and propyl alcohol, control temperature to 60 ℃-78 ℃ of maintenance 3-4h, filter; It is more than 20% that filtrate decompression is concentrated into solid content, and then freeze drying, 40 ℃ of low-temperature grinding obtain Chinese herbal medicine extract, grinding particle size 0.1-0.2mm;
The parts by weight of described mixed enzyme consist of: endo-beta-glucanase 10-20 part, outer 1,4 beta-glucanase 10-20 part, beta-glucosidase 10-15 part, zytase 15-20 part, pentosanase 15-20 part, Pullulanase 20-30 part, beta amylase 10-15 part, neutral proteinase 10-15 part, acid protease 10-15 part, superoxide dismutase 5-10 part, glucose oxidase 5-10 part, acid phosphatase 5-10 part;
The mass ratio that described ethanol and propyl alcohol mix is 1:1-2, described concentration of alcohol >=75%.
The preparation method of described flavoring extract is: flavoring is cleaned, drain, add its quality 0.1-1 water-wet 3-8h doubly, after-18--22 ℃ of freezing 1-2h, pulverize immediately, freezing thickness of feed layer 3-5cm, grinding particle size 0.5-3mm, then add acetic acid, regulating pH value is 3.0-3.5, at power 150-300W, under frequency 2000Hz condition, carry out Microwave Extraction, wherein, each microwave irradiation total time 60-80s, carry out compartment irradiation: irradiation 10s, interval 10s, control temperature 20-35 ℃, so irradiation is 10 times, simultaneously at power 200-300W, under frequency 30-40KHz condition, carry out ultrasonic wave assisted extraction, insulation 1-3h, then, under power 200-400W, frequency 2000Hz condition, carry out Microwave Extraction, wherein, each microwave irradiation total time 90-105s, carry out compartment irradiation: irradiation 15s, interval 10s, controls temperature 40-60 ℃, and so irradiation is 10 times, simultaneously at power 300-500W, under frequency 40-50KHz condition, carry out ultrasonic wave assisted extraction, be finally naturally cooled to room temperature, in electric-field intensity 25-35kV/cm, burst length 400-600 μ s, carries out high-pressure pulse electric (PEF) and extracts 15-20min under pulse frequency 200-300Hz condition, fully stir extract, sealing, spontaneous fermentation 3-5d, filters, it is more than 20% that filtrate decompression is concentrated into solid content, and then freeze drying, 40 ℃ of low-temperature grinding obtain and obtain flavoring extract, grinding particle size 0.1-0.2mm,
Described flavoring is complete dry product flavoring; Described dry product flavoring is: at least one or several flavoring mixing with arbitrary proportion in Chinese prickly ash, Chinese anise, cloves, spiceleaf, Chinese cassia tree, fennel seeds, lemonlike citrus leaf, vanilla, cardamom, thyme; Described dry product flavoring moisture < 10%.
Described alumino-silicate is for having selective strong adsorbing alumino-silicate or alumino-silicate derivatives, composite with Chinese herbal medicine extract science, the multiple toxin such as energy adsorption of aflatoxin, vomitoxin, zearalenone, T-2 toxin, also tool strengthens immunity, protects the effects such as the strong kidney of liver, and the nutrition such as amino acid, vitamin, trace element in can adsorption feed;
Preferably, described alumino-silicate is the de-mycin (Novasil Plus) that du pont company produces, it is a kind of alumino-silicate derivatives that is different from ordinary silicon aluminate, it is synthetics, have latticed multilayer or chain structure, divalence or Tricationic and oxygen or hydroxyl are split into octahedral covalent structure; Silica forms tetrahedral covalent structure with oxygen or hydroxyl.De-mycin have three types binding site interlayer passage, top layer and side with mould, once after de-mycin and moldin combination, not easily separated in animal body, only having 10% can be with strong organic solvent dissolution out.
Described medical stone contains cattle and sheep needs the trace elements such as K, Ca, Mg and Si, Fe, Zn, Cu, Mo, Se, Mn, Sr, Ni, V, Li, Co, Cr, I, Ge, Ti to reach kind more than 40, also contains cattle and sheep essential amino acid.Have the toxin such as the harmful heavy metal of stronger absorption, bacterium, have diuresis, stomach invigorating, protect the liver, relax the muscles and stimulate the blood circulation, strengthen the function of cardiopulmonary vigor, bactericidal antiphlogistic, significantly improving gives milk produces meat and wool production.
Described dicalcium powder is 100-200 order, and whiteness requires 95%, calcium carbonate content 99%, pure free from admixture.
Described rare earth is exactly lanthanide series in the periodic table of chemical element---lanthanum (La), cerium (Ce), praseodymium (Pr), neodymium (Nd), promethium (Pm), samarium (Sm), europium (Eu), gadolinium (Gd), terbium (Tb), dysprosium (Dy), holmium (Ho), erbium (Er), thulium (Tm), ytterbium (Yb), lutetium (Lu), and with group of the lanthanides closely-related two elements of 15 elements---scandium (Sc) and yttrium (Y) totally 17 kinds of elements, be called rare earth element (Rare Earth).Be called for short rare earth (RE or R), the high viscosity hydrophobic type rare earth that contains 17 kinds of rare elements, to the formation of organism internal hormone or enzyme or activated efficient catalytic effect, obviously improve cattle and sheep weightening finish, improve cattle and sheep immunity, improve meat, improve meat grade, it is the adhesive that licking brick for cattle and sheep is special good, in licking brick for cattle and sheep formula, add rare earth, can alleviate the cracked property of licking brick for cattle and sheep, and can make goods present certain gloss.
Described per kilogram B B-complex comprises vitamin E 9600mg, dehydroretinol 800mg, orotic acid 000mg, Catergen 000mg, riboflavin 1600mg, pantothenic acid 1900mg, pyridoxamine 1800mg, cobalamin 1200mg, inositol 5000mg, neo dohyfral D3 5500mg, prokayvit 4000mg; Its surplus is carrier, and described carrier is 30 order rice brans.
Described iron oxide red contains the essential ferro element of cattle and sheep, and humidity resistance is stronger than ferrous sulfate, iron oxide red formal name used at school iron oxide red, another name di-iron trioxide, molecular formula Fe
2o
3.
Described urease inhibitors is phenyl dihydro based phosphates.
Beneficial effect:
1. the milk cow composite nutrient licking brick that prepared by the present invention is with molasses, urea, vitamin and mineral element are primary raw material, composite Chinese herbal medicine extract and the flavoring extract that there is the Natural Antioxidants of strong anti-oxidation and there is bacteria resistance function and fragrance of science, that prepares is anti-oxidant, anti-pollution milk cow composite nutrient licking brick, existing milk cow, lick under the environment and mode of brick feed, can effectively prevent that milk cow from adding the nutriment loss of brick and polluting, effectively improve the growth of milk cow, breeding and production performance, the generation of prevention various diseases, also can promote milk cow appetite, increase feed intake, to reduce milk cattle cultivating cost, increase economic benefit.Through feeding experiment, show: compare with existing commercially available composite nutrient licking brick, hardness is moderate, and the amount of licking is stablized about 60-80g/ day/head, moistureproof breakage-proof, without phenomenons such as decortication, loose, fragments, weatherability is strong; Can effectively improve cow feeding amount and milk cow immunity of organisms, milk cow physical health; Licking brick, to lick surperficial miscellaneous bacteria content low, is 1.5/10000ths of control group, and anti-environmental pollution effect is strong, can prevent from licking the loss of the nutriment such as molasses in brick; Can significantly improve the milk yield of lactating cow, head day increases by 5.45 kilograms of the outputs of milk, improves 19.02%; Can greatly shorten the 13 days time of milk cow postpartum heat, improve the conception rate 16.5% of the first feelings phase of postpartum milk cow, increase the ratio of oestrusing 18.4% of Postpartum Cows colony, effectively improve the reproductive performance of milk cow; The incidence that can significantly reduce the nutritive diseases such as the different addiction of milk cow is sick, hoof is rotten, white muscle disease, cow postpartum paralysis, rickets, mammitis, tertia hair, on average reduces 3.3-16.7%, has greatly improved the health status of milk cow.
2. the milk cow composite nutrient licking brick science that prepared by the present invention composite nontoxic, have no side effect, natural that non-oxidizability is strong; herd with drylot feeding environment under; in the selective autonomous feed process of milk cow; be exposed to air imperfect lick natural in brick first with airborne radical reaction; thereby protected the nutritional labeling of licking brick; especially vitamin and mineral element exempt from oxidation, have avoided the loss of composite nutrient licking brick nutriment.
3. the milk cow composite nutrient licking brick science that prepared by the present invention is composite has bacteria resistance function and the Chinese herbal medicine extract of the flavoring extract of the fragrance that improves a poor appetite and prevent disease, raising immunity, the microorganism that can suppress in environment is licking brick superficial growth breeding, effectively prevent from licking brick on the feed in process other nutriment such as molasses by the microorganism in environment, utilized, prevent from licking the pollution that brick is subject to environmental microorganism in the process of feeding.
4. the milk cow composite nutrient licking brick that prepared by the present invention adds glutinous rice as adhesive and filler; inorganic alkaline adhesive and coagulating agent consumption (such as cement, quick lime etc.) have effectively been reduced; reduced the generation of the interior alkaline matter of cow rumen and urea reaction volatilization ammonia; protected environment; prevent milk cow apocleisis; return milk cow simultaneously and supplemented starch based nutriment, preparation lick brick densification, solid, smooth in appearance.
5. the composite alumino-silicate of milk cow composite nutrient licking brick science and the Chinese herbal medicine extract that prepared by the present invention, not only can be used as filler and curing agent that milk cow licks brick, the multiple toxin such as the alternative adsorption of aflatoxin of what is more important, vomitoxin, zearalenone, T-2 toxin, also tool strengthens immunity, protects the effects such as the strong kidney of liver, and the nutrition such as amino acid, vitamin, trace element in can adsorption feed.
6. the preparation method of Chinese herbal medicine extract of the present invention and flavoring extract can extract Chinese herbal medicine and the contained active ingredient of flavoring to greatest extent, has effectively improved raw material availability, has reduced production cost.
7. preparation method's technique of milk cow composite nutrient licking brick of the present invention is simple, easy to operate, and equipment and environmental requirement are low, are produced on a large scale.
The specific embodiment
Below by specific embodiment narration the present invention.Unless stated otherwise, in the present invention, technological means used is method known in those skilled in the art.In addition, embodiment is interpreted as illustrative, but not limits the scope of the invention, and the spirit and scope of the invention are only limited by claims.To those skilled in the art, do not deviating under the prerequisite of essence of the present invention and scope various changes that the material component in these embodiments and consumption are carried out or change and also belong to protection scope of the present invention.
The preparation of embodiment 1 flavoring extract
The preparation method of flavoring extract is: flavoring is cleaned, drained, the water-wet 5h that adds 0.5 times of its quality, after-20 ℃ of freezing 1.5h, pulverize immediately, freezing thickness of feed layer 4cm, grinding particle size 2mm, then add acetic acid, regulating pH value is 3.2, under power 250, frequency 2000Hz condition, carries out Microwave Extraction, wherein, each microwave irradiation total time 70s, carries out compartment irradiation: irradiation 10s, interval 10s, control 30 ℃ of temperature, so irradiation is 10 times, simultaneously at power 250W, carries out ultrasonic wave assisted extraction under frequency 35KHz condition; Insulation 2h then, carries out Microwave Extraction under power 300W, frequency 2000Hz condition, wherein, each microwave irradiation total time 90s, carries out compartment irradiation: irradiation 15s, interval 10s, controls temperature 50 C, and so irradiation is 10 times, simultaneously at power 400W, under frequency 45KHz condition, carry out ultrasonic wave assisted extraction, be finally naturally cooled to room temperature, in electric-field intensity 30kV/cm, burst lengths 500 μ s, carries out high-pressure pulse electric (PEF) and extracts 18min under pulse frequency 250Hz condition; Fully stir extract, sealing, spontaneous fermentation 4d, filters; It is more than 20% that filtrate decompression is concentrated into solid content, and then freeze drying, 40 ℃ of low-temperature grinding obtain the flavoring extract of grinding particle size 0.1mm;
Described flavoring is complete dry product flavoring, and moisture < 10%;
Described dry product flavoring is: the flavoring that Chinese prickly ash, Chinese anise, cloves, spiceleaf, Chinese cassia tree, fennel seeds, lemonlike citrus leaf, vanilla, cardamom, thyme mix with arbitrary proportion.
The preparation of embodiment 2 Chinese herbal medicine extracts
Chinese herbal medicine extract is prepared by the raw material of following parts by weight: 60 parts of Radix Angelicae Sinensis, 60 parts of Ligusticum wallichiis, 55 parts of fructus amomis, 55 parts of the radix paeoniae rubrathe, 50 parts of Divine Comedy, 50 parts, Fructus Hordei Germinatus, 50 parts of motherworts, 42 parts of costus root, 42 parts of Radix Codonopsis, 42 parts of the Radixs Astragali, 42 parts of honeysuckles, 40 parts of cordate houttuynias, 40 parts, Poria cocos, 40 parts of fushens, 35 parts of polygala roots, fry 35 parts, fennel, 35 parts of the bighead atractylodes rhizomes, 35 parts of the barks of official magnolia, 30 parts, Radix Glycyrrhizae, 30 parts of hawthorn, 30 parts of dried orange peels;
The preparation method of described Chinese herbal medicine extract is: respectively said herbal medicine being crushed to particle diameter is below 2 millimeters, then in container, evenly mix and add the water of 5 times of weight, control 80 ℃ of temperature and keep 3h, then being cooled to 50 ℃, adding the mixing enzyme preparation of mixed material gross weight 8% to carry out enzymolysis, is 6.0 with newborn acid for adjusting pH value, enzymolysis 3h, finally add the mixture of 2 times of weight ethanol of mixed material and propyl alcohol, control temperature to 72 ℃ and keep 4h, filter; It is more than 20% that filtrate decompression is concentrated into solid content, and then freeze drying, 40 ℃ of low-temperature grinding obtain the Chinese herbal medicine extract of grinding particle size 0.1mm;
The parts by weight of described mixed enzyme consist of: 15 parts of endo-beta-glucanases, 15 parts of outer 1,4 beta-glucanases, 12 parts of beta-glucosidases, 18 parts of zytases, 18 parts of pentosanases, 25 parts of Pullulanases, 12 parts of beta amylases, 12 parts of neutral proteinases, 12 parts of acid proteases, 8 parts of superoxide dismutases, 8 parts of glucose oxidases, 8 parts of acid phosphatases;
The mass ratio that described ethanol and propyl alcohol mix is 1:1, described concentration of alcohol 75%.
Embodiment 3
A preparation method for anti-oxidant, anti-pollution milk cow composite nutrient licking brick, comprises the steps:
Described milk cow composite nutrient licking brick is prepared by the raw material of following parts by weight:
65 parts of salt, 40 parts, molasses, 35 parts of glutinous rices, 30 parts, urea, 32 parts of medical stones, 30 parts of dicalcium powders, 28 parts of de-mycins, 28 parts of naturals, 7 parts of Chinese herbal medicine extracts, 7 parts of flavoring extracts, 7 parts of rare earths, 4 parts of yeast seleniums, 3 parts of calcium iodates, 3.2 parts, magnesia, 2 parts of B B-complexes, 1.3 parts of iron oxide reds, 1.3 parts, zinc oxide, 1.0 parts of basic copper chlorides, 0.65 part of cobalt chloride, 0.2 part of manganese oxide, 0.2 part of urease inhibitor;
The preparation method of described glutinous rice is: first glutinous rice soaks 36h in 22 ℃ of water temperatures after impurity elimination, cleaning, and moisture reaches 28%; Then normal pressure steam a rice 20min obtain there is high viscosity, miscible glutinous rice;
Described de-mycin is the de-mycin (Novasil Plus) that du pont company produces;
Described natural is the mixture of grape pip procyanidin, Rosmarinus officinalis extract and apricot leaf extract, and the mass ratio of mixing is 2.5:1.5:1; Described grape pip procyanidin is bought in Earthquake of Anyang station in Henan Jing Sen bio tech ltd, and ginkgo biloba p.e is bought in Xuzhou Heng Kai ginkgo Products Co., Ltd, and Rosmarinus officinalis extract is bought in Wuhan Yuancheng Technology Development Co., Ltd., is pressed powder;
Described flavoring extract is embodiment 1 preparation, and described Chinese herbal medicine extract is embodiment 2 preparations;
Described per kilogram B B-complex comprises vitamin E 9600mg, dehydroretinol 800mg, orotic acid 000mg, Catergen 000mg, riboflavin 1600mg, pantothenic acid 1900mg, pyridoxamine 1800mg, cobalamin 1200mg, inositol 5000mg, neo dohyfral D3 5500mg, prokayvit 4000mg; Its surplus is carrier, and carrier is 30 order rice brans.
First salt, medical stone, de-mycin and rare earth are pulverized, made its granularity reach 100 orders; Then get by weight proportion molasses and be heated to 165 ℃, according to part by weight, adding urea, mix and blend 10 minutes; When being reduced to 60 ℃, question response thing temperature successively adds by weight proportion salt, medical stone, dicalcium powder, de-mycin, rare earth and glutinous rice, mix and blend 15 minutes; Then successively add by weight proportion yeast selenium, calcium iodate, magnesia, iron oxide red, zinc oxide, basic copper chloride, cobalt chloride, manganese oxide, urease inhibitor, mix and blend 15 minutes; Finally successively add Chinese herbal medicine extract, B B-complex, natural and flavoring extract by weight proportion, stir 10 minutes; Finally compound is put in mould, utilize hydraulic press on pressing mold every square centimeter with 540-640kg pressure pressing 25-35, be pressed into 2-10kg bulk second and lick brick, then carry out the demoulding, detection, packing and obtain anti-oxidant, anti-pollution milk cow composite nutrient licking brick.
Embodiment 4
A preparation method for anti-oxidant, anti-pollution milk cow composite nutrient licking brick, comprises the steps:
Described milk cow composite nutrient licking brick is prepared by the raw material of following parts by weight:
55 parts of salt, 30 parts, molasses, 25 parts of glutinous rices, 25 parts, urea, 30 parts of medical stones, 25 parts of dicalcium powders, 20 parts of de-mycins, 20 parts of grape pip procyanidins, 5 parts of Chinese herbal medicine extracts, 5 parts of flavoring extracts, 6 parts of rare earths, 3 parts of yeast seleniums, 2 parts of calcium iodates, 2 parts, magnesia, 1 part of B B-complex, 1 part of iron oxide red, 1 part, zinc oxide, 0.8 part of basic copper chloride, 0.5 part of cobalt chloride, 0.1 part of manganese oxide, 0.1 part of urease inhibitor;
Described glutinous rice, de-mycin, grape pip procyanidin, flavoring extract, Chinese herbal medicine extract, B B-complex are identical with embodiment 3;
The preparation method of described anti-oxidant, anti-pollution milk cow composite nutrient licking brick is with embodiment 3.
Embodiment 5
A preparation method for anti-oxidant, anti-pollution milk cow composite nutrient licking brick, comprises the steps:
Described milk cow composite nutrient licking brick is prepared by the raw material of following parts by weight:
60 parts of salt, 35 parts, molasses, 30 parts of glutinous rices, 27 parts, urea, 31 parts of medical stones, 28 parts of dicalcium powders, 25 parts of de-mycins, 25 parts of naturals, 6 parts of Chinese herbal medicine extracts, 6 parts of flavoring extracts, 6.5 parts of rare earths, 3.5 parts of yeast seleniums, 2.5 parts of calcium iodates, 3 parts, magnesia, 1.5 parts of B B-complexes, 1.2 parts of iron oxide reds, 1.2 parts, zinc oxide, 0.9 part of basic copper chloride, 0.6 part of cobalt chloride, 0.15 part of manganese oxide, 0.15 part of urease inhibitor;
Described natural is the mixture that grape pip procyanidin and Rosmarinus officinalis extract mix with mass ratio 3:2;
Described glutinous rice, de-mycin, flavoring extract, Chinese herbal medicine extract, B B-complex, grape pip procyanidin are identical with embodiment 3 with Rosmarinus officinalis extract;
The preparation method of described anti-oxidant, anti-pollution milk cow composite nutrient licking brick is with embodiment 3.
Embodiment 6
A preparation method for anti-oxidant, anti-pollution milk cow composite nutrient licking brick, comprises the steps:
Described milk cow composite nutrient licking brick is prepared by the raw material of following parts by weight:
70 parts of salt, 45 parts, molasses, 40 parts of glutinous rices, 32 parts, urea, 33 parts of medical stones, 32 parts of dicalcium powders, 30 parts of de-mycins, 30 parts of naturals, 8 parts of Chinese herbal medicine extracts, 8 parts of flavoring extracts, 7.5 parts of rare earths, 4.5 parts of yeast seleniums, 3.5 parts of calcium iodates, 3.5 parts, magnesia, 2.5 parts of B B-complexes, 1.4 parts of iron oxide reds, 1.4 parts, zinc oxide, 1.1 parts of basic copper chlorides, 0.7 part of cobalt chloride, 0.25 part of manganese oxide, 0.25 part of urease inhibitor;
Described natural is the mixture that grape pip procyanidin, Rosmarinus officinalis extract and apricot leaf extract mix with mass ratio 2:1:0.5;
Described glutinous rice, de-mycin, flavoring extract, Chinese herbal medicine extract, B B-complex, grape pip procyanidin, Rosmarinus officinalis extract are identical with embodiment 3 with apricot leaf extract;
The preparation method of described anti-oxidant, anti-pollution milk cow composite nutrient licking brick is with embodiment 3.
Embodiment 7
A preparation method for anti-oxidant, anti-pollution milk cow composite nutrient licking brick, comprises the steps:
Described milk cow composite nutrient licking brick is prepared by the raw material of following parts by weight:
75 parts of salt, 50 parts, molasses, 45 parts of glutinous rices, 35 parts, urea, 35 parts of medical stones, 35 parts of dicalcium powders, 35 parts of de-mycins, 35 parts of grape pip procyanidins, 10 parts of Chinese herbal medicine extracts, 10 parts of flavoring extracts, 8 parts of rare earths, 5 parts of yeast seleniums, 4 parts of calcium iodates, 4 parts, magnesia, 3 parts of B B-complexes, 1.5 parts of iron oxide reds, 1.5 parts, zinc oxide, 1.2 parts of basic copper chlorides, 0.8 part of cobalt chloride, 0.3 part of manganese oxide, 0.3 part of urease inhibitor;
Described glutinous rice, de-mycin, grape pip procyanidin, flavoring extract, Chinese herbal medicine extract, B B-complex are identical with embodiment 3;
The preparation method of described anti-oxidant, anti-pollution milk cow composite nutrient licking brick is with embodiment 3.
The feeding effect test of anti-oxidant, the anti-pollution milk cow composite nutrient licking brick of embodiment 8
1 materials and methods
1.1 test material
1.1.1 anti-oxidant, anti-pollution milk cow composite nutrient licking brick, the commercially available high yield cow composite nutrient licking brick (production of Linyi, Shandong Province many Variety Salts of Qian Yuan Co., Ltd) of the embodiment of the present invention 3 preparations, be 10Kg/ piece, and the date of manufacture is close.
1.1.2 test milk cow: test is carried out a certain cattle farm in Miyun Region of Beijing, and kind is the above milk cow of china holstein cows 2 tire, be 300 days average lactation period, and totally 60, wherein 2 tire is 24,3 14, tires, 4 13, tires, 59, tires.Test ox is age-based, parity, lactation period, the identical or close pair principle of the output of milk in early stage, testing ox, is only divided into experimental group and control group, 30 every group.A upper parity milk cow annual output of milk experimental group 8274kg, control group 8353kg.
1.2 test daily rations form: test group and control group adopt same feeding and management method.Daily ration consists of fine fodder (corn 52.7%, wheat bran 8%, dregs of beans 7%, cotton dregs 9%, peanut meal 9%, corn DDGS 8%, premix 7115A6%), and coarse fodder is corn silage, sheep's hay, the beans stalks of rice, wheat, etc., clover etc.
1.3 test methods: test group is placed the brick of licking of the embodiment of the present invention 3 preparations in cowshed sports ground, control group is placed commercially available high yield cow composite nutrient licking brick in cowshed sports ground, milk cow independently licks, test group and control group adopt identical feeding manner and way to manage, all fine fodder 4-8kg of giving milk for autogamy in examination Cow-feeding field, adjust corn silage quantitative feeding 20kg/ days, roughage (sheep's hay, the beans stalks of rice, wheat, etc., clover) free choice feeding according to raising stage and the output of milk.
1.4 pilot projects and scheme:
1.4.1 licking brick protection against the tide, breakage-proof performance observes: brick moisture absorption situation is licked in experimental period observations, has or not the phenomenons such as decortication, loose, fragment, records the amount of licking and whether stablizes (whether hardness is suitable);
1.4.2 licking brick pollution-proof performance detects: to licking surperficial smelling through licking the brick of licking of 20 days summer, then with aseptic water washing, lick surface, get 100 times of the aseptic dilutions of flushing liquor, dilution is placed in (NA culture medium) 37 ℃ in aseptic flat board and cultivates 36h, calculates the total number of bacteria that every ml flushing liquor contains;
1.4.3 licking brick antioxygenic property detects: that by pocket knife scraping, licks that brick licks surperficial equal in quality adds brick powder, join respectively in lard, mix, be placed in the constant temperature oven of 60 ± 0.5 ℃, stir once at regular intervals, and exchange its position in baking oven.Every sampling in 5 days, detect its peroxide value (peroxide value, POV), measure altogether 25d, the mensuration of peroxide value is carried out according to GB/T5009.37-2003;
1.4.4 milk cow body condition is evaluated: the physique of milk cow is carried out to marking system overall merit, evaluate per February 1 time, and totally 6 times, record result, milk cow body condition can reflect cow feeding amount size;
1.4.5 milk cow production performance detects: the output of milk of measuring and record every cow head within lactation period;
1.4.6 immunity of cow detects: whole experimental period monitoring cow serum immunoglobulin (Ig) average content, and monitor once per February, and record, evaluates immunity of cow level;
1.4.7 cow reproduction Performance Detection: detect and the participate in the experiment rutting situation of cow in perinatal period of record, whether gestation is as the criterion with the examination per rectum in latter 60 days of breeding;
1.4.8 disease surveillance and record: adopt conventional means to monitor nutritive disease incidence the records such as different addiction is sick, hoof is rotten, white muscle disease, cow postpartum paralysis, rickets, mammitis, tertia hair;
1.5 statistical analyses are processed initial data with EXCEL software, then use SAS[11] method carries out variance analysis.
1.6 test period experimental periods,, from end of day in January 10 in-2013 on January 10th, 2012, lasted 1 year.
2. result of the test
2.1 lick brick protection against the tide, breakage-proof result
Test group: initial average every every the amount of licking of milk cow is 90-120g, is stabilized in 60-80g/ day/head after 20 days.Whole experimental period, rain in spring and summer and do not cause that to lick piece soft, lick piece and remain initial hardness, without decortication, loose, fall slag situation, and the amount of licking remains at 60-80g/ day/head;
Control group: initial average every every the amount of licking of milk cow is 70-90g, increases to 100-110g/ day/head after 30 days, increases to 110-120g/ day/head after 60 days, after 90 days, increase to 120-125g/ day/head, after 120 days, be down to 80-100g/ day/head, after 150 days, have 3 cow heads to stop licking, after 20 days, start to lick, average 50-60g/ day/head, increase gradually, the amount of licking is unstable, cannot add up, whole experimental period, loose 2,5 of decortications after rain, fall 12 of slags;
Above result shows: it is more moderate than control group hardness that test group is licked brick, and moistureproof, breakage-proof effective, weatherability is strong.
2.2 lick brick antipollution result as table 1
Table 1 is licked brick surface sterile aqueous rinse solution miscellaneous bacteria cultivation results
| Project | Smell | Miscellaneous bacteria content |
| Test group | Slight peculiar smell | 1.13x10 2(CFU/ml) |
| Control group | Heavier peculiar smell | 7.68x10 4(CFU/ml) |
| Cowshed sports ground | —— | 3.48x10 3(CFU/m 3) |
Above result shows: test group is licked the brick miscellaneous bacteria in environment that can effectively suppress to feed, to licking the pollution of brick, has stronger antibacterial effect than control group, is 1.5/10000ths of control group, can prevent from licking the loss of the nutriment such as molasses in brick.
2.3 lick the anti-oxidant result of brick as table 2
Table 2 is licked brick the non-oxidizability of lard (peroxide value) is detected after licking
Above result shows: compare with control group; test group is licked brick very strong non-oxidizability; antioxidant effect is nearly 12 times of contrast; the oxidational losses that can effectively prevent from licking the nutriments such as vitamin in brick, mineral element, trace element, can be milk cow body more Antioxidative Factors is provided.
2.4 lick the impact of brick on milk cow body condition
Table 3 milk cow 5 part Body Condition Score standards
| Score value | Vertebra portion | Flank | Buttocks both sides | Root of the tail both sides | Hipbone, ischium joint |
| 1 | Very outstanding | Root root is visible | Excessive settlement | Crypts is very dark | Very outstanding |
| 2 | Obviously outstanding | Most visible | Obviously sink | Crypts is obvious | Obviously outstanding |
| 3 | Outstanding a little | Minority is visible | Sagging a little | Crypts is slightly aobvious | Outstanding a little |
| 4 | Straight | Lose completely | Straight | Crypts is not aobvious | Do not show outstanding |
| 5 | Plentiful | Plentiful | Plentiful | Plentiful | Plentiful |
Table 4 milk cow body condition visual examination appraisal result
Above result shows: test group is licked brick and compared with control group, the trend that milk cow Body Condition Score is significantly improved, can improve milk cow to the digestion of nutriment, absorption and metabolism, improve feed intake, be conducive to promote and improve the synthetic of the framework materials such as the interior albumen of body, fat, obviously can improve the body condition of milk cow.
2.5 lick the impact of brick on milk production of cow
The table 5 milk cow in lactation period output of milk
| ? | Number (head) | Give milk number of days (my god) | Total output of milk (kg) | The average output of milk (kg/ days. head) |
| Control group | 30 | 300 | 8598 | 28.66±5.16 |
| Test group | 30 | 300 | 10232 | 34.11±5.92 |
| Process difference b | ? | ? | ? | 6.45 |
Above result shows: test group is compared with control group, and head day increases by 5.45 kilograms of the outputs of milk, improves 19.02%, t check significant difference (P < 0.05), licks the milk yield that brick can significantly improve lactating cow.
2.6 lick the impact of brick on immunity of cow
Table 6 cow serum immunoglobulin content testing result
In cow serum, the content of Immunoglobulin IgA, IgM, IgG is the important indicator of judgement milk cow humoral immunity level.As seen from the experiment, cow birth stress cause serum immune globulin IgA, IgM, IgG content sharply to decline, and humoral immune function is suppressed.Above result shows: test group is licked brick can be increased the content of cow birth phase serum IgA, IgM, IgG and maintain higher level, and relatively stable, can effectively strengthen milk cow humoral immune function.
2.7 lick the impact of brick on Diseases of Cow reproductive performance
Table 7 Diseases of Cow reproductive performance testing result
Result of the test shows, compare with control group, test group Diseases of Cow can shorten the 13 days time of milk cow postpartum heat greatly, improves the conception rate 16.5% of the first feelings phase of postpartum milk cow, the ratio of oestrusing 18.4% that increases Postpartum Cows colony, effectively improves the reproductive performance of milk cow.
2.8 lick brick to the pathogenetic impact of dairy cow nutrition disease
Table 8 dairy cow nutrition disease detection result
Above result shows: test group is compared with control group, aspect prevention dairy cow nutrition disease, can significantly reduce the incidence of disease of various diseases, the average 3.3-16.7% that reduces, t checks significant difference (P < 0.05), the present invention licks the incidence that brick can significantly reduce the nutritive diseases such as the different addiction of milk cow is sick, hoof is rotten, white muscle disease, cow postpartum paralysis, rickets, mammitis, tertia hair, improves the health status of milk cow.
Claims (10)
- One kind anti-oxidant, the preparation method of anti-pollution milk cow composite nutrient licking brick, it is characterized in that, comprise the steps: accurately to take salt 55-75 part, molasses 30-50 part, glutinous rice 25-45 part, urea 25-35 part, medical stone 30-35 part, dicalcium powder 25-35 part, alumino-silicate 20-35 part, natural 20-35 part, Chinese herbal medicine extract 5-10 part, flavoring extract 5-10 part, rare earth 6-8 part, yeast selenium 3-5 part, calcium iodate 2-4 part, magnesia 2-4 part, B B-complex 1-3 part, iron oxide red 1-1.5 part, zinc oxide 1-1.5 part, basic copper chloride 0.8-1.2 part, cobalt chloride 0.5-0.8 part, manganese oxide 0.1-0.3 part, urease inhibitor 0.1-0.3 part, first salt, medical stone, alumino-silicate and rare earth are pulverized, made its granularity reach 100 orders, then get by weight proportion molasses and be heated to 160-170 ℃, according to part by weight, adding urea, mix and blend 10 minutes, when being reduced to 60 ℃, question response thing temperature successively adds by weight proportion salt, medical stone, dicalcium powder, alumino-silicate, rare earth and glutinous rice, mix and blend 15 minutes, then successively add by weight proportion yeast selenium, calcium iodate, magnesia, iron oxide red, zinc oxide, basic copper chloride, cobalt chloride, manganese oxide, urease inhibitor, mix and blend 15 minutes, finally successively add by weight proportion Chinese herbal medicine extract, B B-complex, natural and flavoring extract, stir 10-15 minute, finally compound is put in mould, utilize hydraulic press on pressing mold every square centimeter with 540-640kg pressure pressing 25-35, be pressed into 2-10kg bulk second and lick brick, then carry out the demoulding, detection, packing and obtain anti-oxidant, anti-pollution milk cow composite nutrient licking brick.
- 2. as claimed in claim 1 anti-oxidant, the preparation method of anti-pollution milk cow composite nutrient licking brick, it is characterized in that, described milk cow composite nutrient licking brick is prepared by the raw material of following parts by weight: salt 60-70 part, molasses 35-45 part, glutinous rice 30-40 part, urea 27-32 part, medical stone 31-33 part, dicalcium powder 28-32 part, alumino-silicate 25-30 part, natural 25-30 part, Chinese herbal medicine extract 6-8 part, flavoring extract 6-8 part, rare earth 6.5-7.5 part, yeast selenium 3.5-4.5 part, calcium iodate 2.5-3.5 part, magnesia 3-3.5 part, B B-complex 1.5-2.5 part, iron oxide red 1.2-1.4 part, zinc oxide 1.2-1.4 part, basic copper chloride 0.9-1.1 part, cobalt chloride 0.6-0.7 part, manganese oxide 0.15-0.25 part, urease inhibitor 0.15-0.25 part.
- 3. the preparation method of anti-oxidant, anti-pollution milk cow composite nutrient licking brick as claimed in claim 1, is characterized in that, described natural is any or several combinations in grape pip procyanidin, Rosmarinus officinalis extract and apricot leaf extract.
- 4. the preparation method of anti-oxidant, anti-pollution milk cow composite nutrient licking brick as claimed in claim 1, it is characterized in that, the preparation method of described glutinous rice is: first glutinous rice soaks 24-48h in 18 ℃-25 ℃ of water temperatures after impurity elimination, cleaning, and moisture reaches 25%-30%; Then normal pressure steam a rice 15min-25min obtain there is high viscosity, miscible glutinous rice.
- 5. the preparation method of anti-oxidant, anti-pollution milk cow composite nutrient licking brick as claimed in claim 1, is characterized in that, the mass ratio that described grape pip procyanidin, Rosmarinus officinalis extract and apricot leaf extract mix is 2-3:1-2:0.5-1.5.
- 6. as claimed in claim 1 anti-oxidant, the preparation method of anti-pollution milk cow composite nutrient licking brick, it is characterized in that, described Chinese herbal medicine extract is prepared by the raw material of following parts by weight: Radix Angelicae Sinensis 55-65 part, Ligusticum wallichii 55-65 part, fructus amomi 50-60 part, radix paeoniae rubrathe 50-60 part, Divine Comedy 45-55 part, Fructus Hordei Germinatus 45-55 part, motherwort 45-55 part, costus root 40-45 part, Radix Codonopsis 40-45 part, Radix Astragali 40-45 part, honeysuckle 40-45 part, cordate houttuynia 35-45 part, Poria cocos 35-45 part, fushen 35-45 part, polygala root 30-40 part, fry fennel 30-40 part, bighead atractylodes rhizome 30-40 part, bark of official magnolia 30-40 part, Radix Glycyrrhizae 25-35 part, hawthorn 25-35 part, dried orange peel 25-35 part, respectively said herbal medicine being crushed to particle diameter is below 2 millimeters, then in container, evenly mix and add the water of 3-6 times of weight, control temperature 70 C-90 ℃ and keep 2-4h, then be cooled to 45-60 ℃, add the mixing enzyme preparation of mixed material gross weight 5-10% to carry out enzymolysis, with newborn acid for adjusting pH value, be 5.5-6.8, enzymolysis 2-4h, finally add the mixture of mixed material 0.5-3 times of weight ethanol and propyl alcohol, control temperature to 60 ℃-78 ℃ of maintenance 3-4h, filter, it is more than 20% that filtrate decompression is concentrated into solid content, and then freeze drying, 40 ℃ of low-temperature grinding obtain the Chinese herbal medicine extract that grinding particle size is 0.1-0.2mm,The parts by weight of described mixed enzyme consist of: endo-beta-glucanase 10-20 part, outer 1,4 beta-glucanase 10-20 part, beta-glucosidase 10-15 part, zytase 15-20 part, pentosanase 15-20 part, Pullulanase 20-30 part, beta amylase 10-15 part, neutral proteinase 10-15 part, acid protease 10-15 part, superoxide dismutase 5-10 part, glucose oxidase 5-10 part, acid phosphatase 5-10 part;The mass ratio that described ethanol and propyl alcohol mix is 1:1-2, described concentration of alcohol >=75%.
- 7. as claimed in claim 1 anti-oxidant, the preparation method of anti-pollution milk cow composite nutrient licking brick, it is characterized in that, the preparation method of described flavoring extract is: flavoring is cleaned, drain, add its quality 0.1-1 water-wet 3-8h doubly, after-18--22 ℃ of freezing 1-2h, pulverize immediately, freezing thickness of feed layer 3-5cm, grinding particle size 0.5-3mm, then add acetic acid, regulating pH value is 3.0-3.5, at power 150-300W, under frequency 2000Hz condition, carry out Microwave Extraction, wherein, each microwave irradiation total time 60-80s, carry out compartment irradiation: irradiation 10s, interval 10s, control temperature 20-35 ℃, so irradiation is 10 times, simultaneously at power 200-300W, under frequency 30-40KHz condition, carry out ultrasonic wave assisted extraction, insulation 1-3h, then, under power 200-400W, frequency 2000Hz condition, carry out Microwave Extraction, wherein, each microwave irradiation total time 90-105s, carry out compartment irradiation: irradiation 15s, interval 10s, controls temperature 40-60 ℃, and so irradiation is 10 times, simultaneously at power 300-500W, under frequency 40-50KHz condition, carry out ultrasonic wave assisted extraction, be finally naturally cooled to room temperature, in electric-field intensity 25-35kV/cm, burst length 400-600 μ s, carries out high-pressure pulse electric (PEF) and extracts 15-20min under pulse frequency 200-300Hz condition, fully stir extract, sealing, spontaneous fermentation 3-5d, filters, it is more than 20% that filtrate decompression is concentrated into solid content, and then freeze drying, 40 ℃ of low-temperature grinding obtain and obtain flavoring extract, grinding particle size 0.1-0.2mm,Described flavoring is complete dry product flavoring, and moisture < 10%;Described dry product flavoring is: at least one or several flavoring mixing with arbitrary proportion in Chinese prickly ash, Chinese anise, cloves, spiceleaf, Chinese cassia tree, fennel seeds, lemonlike citrus leaf, vanilla, cardamom, thyme.
- 8. the preparation method of anti-oxidant, anti-pollution milk cow composite nutrient licking brick as claimed in claim 1, is characterized in that, described alumino-silicate is alumino-silicate or alumino-silicate derivatives.
- 9. the preparation method of anti-oxidant, anti-pollution milk cow composite nutrient licking brick as claimed in claim 1, is characterized in that, B B-complex comprises vitamin E 9600mg described in per kilogram, dehydroretinol 800mg, orotic acid 000mg, Catergen 000mg, riboflavin 1600mg, pantothenic acid 1900mg, pyridoxamine 1800mg, cobalamin 1200mg, inositol 5000mg, neo dohyfral D3 5500mg, prokayvit 4000mg; Its surplus is carrier, and described carrier is 30 order rice brans.
- 10. as claimed in claim 1 anti-oxidant, the preparation method of anti-pollution milk cow composite nutrient licking brick, it is characterized in that, comprise the steps: that described milk cow composite nutrient licking brick prepared by the raw material of following parts by weight: 65 parts of salt, 40 parts, molasses, 35 parts of glutinous rices, 30 parts, urea, 32 parts of medical stones, 30 parts of dicalcium powders, 28 parts of de-mycins, 28 parts of naturals, 7 parts of Chinese herbal medicine extracts, 7 parts of flavoring extracts, 7 parts of rare earths, 4 parts of yeast seleniums, 3 parts of calcium iodates, 3.2 parts, magnesia, 2 parts of B B-complexes, 1.3 parts of iron oxide reds, 1.3 parts, zinc oxide, 1.0 parts of basic copper chlorides, 0.65 part of cobalt chloride, 0.2 part of manganese oxide, 0.2 part of urease inhibitor,The preparation method of described glutinous rice is: first glutinous rice soaks 36h in 22 ℃ of water temperatures after impurity elimination, cleaning, and moisture reaches 28%; Then normal pressure steam a rice 20min obtain there is high viscosity, miscible glutinous rice;Described natural is the mixture of grape pip procyanidin, Rosmarinus officinalis extract and apricot leaf extract, and the mass ratio of mixing is 2.5:1.5:1;The preparation method of described flavoring extract is: flavoring is cleaned, drained, the water-wet 5h that adds 0.5 times of its quality, after-20 ℃ of freezing 1.5h, pulverize immediately, freezing thickness of feed layer 4cm, grinding particle size 2mm, then add acetic acid, regulating pH value is 3.2, under power 250, frequency 2000Hz condition, carries out Microwave Extraction, wherein, each microwave irradiation total time 70s, carries out compartment irradiation: irradiation 10s, interval 10s, control 30 ℃ of temperature, so irradiation is 10 times, simultaneously at power 250W, carries out ultrasonic wave assisted extraction under frequency 35KHz condition; Insulation 2h then, carries out Microwave Extraction under power 300W, frequency 2000Hz condition, wherein, each microwave irradiation total time 90s, carries out compartment irradiation: irradiation 15s, interval 10s, controls temperature 50 C, and so irradiation is 10 times, simultaneously at power 400W, under frequency 45KHz condition, carry out ultrasonic wave assisted extraction, be finally naturally cooled to room temperature, in electric-field intensity 30kV/cm, burst lengths 500 μ s, carries out high-pressure pulse electric (PEF) and extracts 18min under pulse frequency 250Hz condition; Fully stir extract, sealing, spontaneous fermentation 4d, filters; It is more than 20% that filtrate decompression is concentrated into solid content, and then freeze drying, 40 ℃ of low-temperature grinding obtain the flavoring extract of grinding particle size 0.1mm;Described dry product flavoring is: the flavoring that Chinese prickly ash, Chinese anise, cloves, spiceleaf, Chinese cassia tree, fennel seeds, lemonlike citrus leaf, vanilla, cardamom, thyme mix with arbitrary proportion;Described Chinese herbal medicine extract is prepared by the raw material of following parts by weight: 60 parts of Radix Angelicae Sinensis, 60 parts of Ligusticum wallichiis, 55 parts of fructus amomis, 55 parts of the radix paeoniae rubrathe, 50 parts of Divine Comedy, 50 parts, Fructus Hordei Germinatus, 50 parts of motherworts, 42 parts of costus root, 42 parts of Radix Codonopsis, 42 parts of the Radixs Astragali, 42 parts of honeysuckles, 40 parts of cordate houttuynias, 40 parts, Poria cocos, 40 parts of fushens, 35 parts of polygala roots, fry 35 parts, fennel, 35 parts of the bighead atractylodes rhizomes, 35 parts of the barks of official magnolia, 30 parts, Radix Glycyrrhizae, 30 parts of hawthorn, 30 parts of dried orange peels, respectively said herbal medicine being crushed to particle diameter is below 2 millimeters, then in container, evenly mix and add the water of 5 times of weight, control 80 ℃ of temperature and keep 3h, then be cooled to 50 ℃, add the mixing enzyme preparation of mixed material gross weight 8% to carry out enzymolysis, with newborn acid for adjusting pH value, be 6.0, enzymolysis 3h, finally add the mixture of 2 times of weight ethanol of mixed material and propyl alcohol, the mass ratio mixing is 1:1, control temperature to 72 ℃ and keep 4h, filter, it is more than 20% that filtrate decompression is concentrated into solid content, and then freeze drying, 40 ℃ of low-temperature grinding obtain the Chinese herbal medicine extract of grinding particle size 0.1mm,The parts by weight of described mixed enzyme consist of: 15 parts of endo-beta-glucanases, 15 parts of outer 1,4 beta-glucanases, 12 parts of beta-glucosidases, 18 parts of zytases, 18 parts of pentosanases, 25 parts of Pullulanases, 12 parts of beta amylases, 12 parts of neutral proteinases, 12 parts of acid proteases, 8 parts of superoxide dismutases, 8 parts of glucose oxidases, 8 parts of acid phosphatases;Described per kilogram B B-complex comprises vitamin E 9600mg, dehydroretinol 800mg, orotic acid 000mg, Catergen 000mg, riboflavin 1600mg, pantothenic acid 1900mg, pyridoxamine 1800mg, cobalamin 1200mg, inositol 5000mg, neo dohyfral D3 5500mg, prokayvit 4000mg, its surplus is carrier, and carrier is 30 order rice brans.First salt, medical stone, de-mycin and rare earth are pulverized, made its granularity reach 100 orders; Then get by weight proportion molasses and be heated to 165 ℃, according to part by weight, adding urea, mix and blend 10 minutes; When being reduced to 60 ℃, question response thing temperature successively adds by weight proportion salt, medical stone, dicalcium powder, de-mycin, rare earth and glutinous rice, mix and blend 15 minutes; Then successively add by weight proportion yeast selenium, calcium iodate, magnesia, iron oxide red, zinc oxide, basic copper chloride, cobalt chloride, manganese oxide, urease inhibitor, mix and blend 15 minutes; Finally successively add Chinese herbal medicine extract, B B-complex, natural and flavoring extract by weight proportion, stir 10 minutes; Finally compound is put in mould, utilize hydraulic press on pressing mold every square centimeter with 540-640kg pressure pressing 25-35, be pressed into 2-10kg bulk second and lick brick, then carry out the demoulding, detection, packing and obtain anti-oxidant, anti-pollution milk cow composite nutrient licking brick.
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| CN105028987A (en) * | 2015-06-15 | 2015-11-11 | 中国农业科学院兰州畜牧与兽药研究所 | Compound-polysacchariderace-enriched trace element licking block special for dairy cattle and preparation method for compound-polysacchariderace-enriched trace element licking block |
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| CN104770568A (en) * | 2015-04-13 | 2015-07-15 | 邵素英 | Laying chicken reproductive performance improving feed in the egg laying prophase and preparation method thereof |
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| CN114403300A (en) * | 2022-02-24 | 2022-04-29 | 广东省农业科学院动物科学研究所 | Licking brick for improving cattle feed intake and preparation process |
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