CN103923736A - Method for extracting antioxidant crocodile grease - Google Patents
Method for extracting antioxidant crocodile grease Download PDFInfo
- Publication number
- CN103923736A CN103923736A CN201410172599.7A CN201410172599A CN103923736A CN 103923736 A CN103923736 A CN 103923736A CN 201410172599 A CN201410172599 A CN 201410172599A CN 103923736 A CN103923736 A CN 103923736A
- Authority
- CN
- China
- Prior art keywords
- crocodile
- grease
- oxidant
- extracting method
- herbal medicine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Medicines Containing Plant Substances (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention provides a method for extracting antioxidant crocodile grease. Compared with the prior art, not only is the problem that the grease is easily oxidized solved, but also a potential safety hazard caused by adding of a synthetic antioxidant to the grease is avoided, and green, healthy and environment-friendly ideas are accorded. IC50 is the concentration of the required antioxidant when the removal rate is 50%, and frequently applied to comparison of the ability for removing DPPH.free radical, and the half maximal inhibitory concentration (IC50) is determined by drawing a curve according to the removal rate of different concentrations of antioxidants. The IC50 is smaller in value, which indicates that the oxidation resistance is stronger and the ability of removing free radical is stronger. The crocodile grease extracted by the traditional method (control group) is detected by adopting the DPPH method and compared with the grease product obtained in the embodiments 1,4 (experimental group) disclosed by the invention in the antioxidant activity; the determination result displays the crocodile grease IC50=24.920mg/mL extracted by the traditional method, a final grease product IC50=14.138mg/mL obtained by the embodiment 1, and the final grease product IC50=14.545mg/mL obtained by the embodiment 4. The antioxidant activity of the final crocodile grease product extracted by the Chinese herbal medicine soup is obviously improved.
Description
Technical field
The present invention relates to a kind of anti-oxidant crocodile grease extracting method.
Background technology
1. Chinese alligator and grease thereof
In China, about the record history of existing more than 3000 year of Chinese alligator, the medicinal history of Chinese alligator is of long standing and well established.Compendium of Material Medica is recorded Chinese alligator (being Chinese alligator), and " first cures mainly trusted subordinate Zheng Disorder lump in the abdomen; Fu Jian gathers; Fever and chills; The blood five colors and the dead muscle of sore scabies under coupling pain, metrorrhagia in woman's underbelly the moon; Cure mainly weak breath and inhale, foot is not on the spot; Do not record moisture perverse trend, all legendary venomous insects, Fu Nei Disorder lump in the abdomen, evil sore; Its fat cures mainly and rubs wind and dislike sore; Its meat can be controlled Fu Nei Disorder lump in the abdomen, dislikes sore ".
2. the oxidation of grease
The effect of water and enzyme etc. in light, heat, airborne oxygen and grease often makes grease deterioration corruption.The animal-plant oil that ordinary method is extracted easily generates the intermediate products such as oxide compound, hydroperoxide and decomposes and produces volatility and non-volatile fatty acid, aldehyde, ketone and alcohol etc. in storage, even produces toxic substance.Lipid-antioxidant activity, for ensureing that oil quality is extremely important, adds antioxidant to prevent grease oxidation rancid conventionally at grease with containing people in the course of processing of fatty foods.Traditional antioxidant is mainly the chemosynthesis antioxidants such as BHA, BHT, PG, TBHQ, but the toxic side effect that these antioxidants have allows many countries stop using or strictly limits its use.
3. natural antioxidants
Although traditional synthetic antioxidant action effect is remarkable, is restricted because existing safety issue.The antioxidant that safety, nontoxic natural antioxidants replace synthetic will be a kind of inexorable trend.A lot of to the research of herbal medicine oxidation-resistance both at home and abroad at present, from multiple herbal medicine, extract Natural Antioxidants.
4. existing patented technology and prior art scheme
Chinese patent (application number 2010142451.0) discloses a kind of crocodile grease and preparation method thereof and purposes.
Chinese patent (application number 2010142451.0) " a kind of crocodile grease and preparation method thereof and purposes ", wherein crocodile grease is by supercritical CO
2extracting process is prepared from, taking fresh alligator oil en as raw material, after frozen drying is processed, after grinding powder, be placed in the reactor of overcritical equipment, heating, pass in supercritical carbon dioxide fluid and extract, carry out second depressurized parsing separation to being rich in the carbonic acid gas of target extracting substance again, the carbonic acid gas after separation continues to participate in supercritical extraction circulation, isolated active substance crocodile grease.
The research of probing in recent years the antioxygenation of natural anti-reflecting oxide to grease is more and more.The people's such as Zhu Zhenbao (2008) research shows that the alcohol extract of Japanese Honeysuckle and water extract all have the snperoxiaized ability of certain oil-control.The people such as Zhang Lei (2009) find in test in soya-bean oil matrix, and the lotus flavone extracting solution that massfraction is 0.12% oxidation occurs has good effect suppressing soya-bean oil; In lard matrix, the lotus flavone extracting solution that massfraction is 0.1% can effectively suppress lard and be oxidized.The people such as Deng Ping Nan (2000) utilize the Pericarpium Citri junoris extract that ethyl acetate is extracted to have obvious anti-oxidant activity to lard, and slightly stronger than the resistance of oxidation of synthetized oxidation preventive agent.The people's such as Li Yingqiu (2004) test card open-birth Rhizoma Zingiberis Recens extract can suppress the oxidative rancidity of food oils effectively.
In sum, in prior art, there is following technical problem: in existing patented technology, the extraction of grease will be passed through multiple working procedure, whole treatment process complexity, can not solve the problem of oxidation that grease meets with in preservation process, and still needs to add other antioxidant while being applied to research and development of products.
Summary of the invention
The object of the present invention is to provide a kind of anti-oxidant crocodile grease extracting method, directly in extraction process, solve the oxidizable problem of grease based on traditional technology, be by crocodile fat with the preservation of herbal medicine mixed freezing and directly obtain and extract anti-oxidant crocodile grease, the crocodile oil obtaining through technique of the present invention can be directly need to add the antioxidant of synthetic as the starting material of daily chemical products etc.
Concrete technical scheme is as follows:
A kind of anti-oxidant crocodile grease extracting method, comprises the steps:
(1) gather crocodile fat and pulverize;
(2) prepare Chinese herbal medicine fluid;
(3) the crocodile fat of pulverizing is mixed to stir evenly with the Chinese herbal medicine fluid making obtain mixture;
(4) by described mixture freezing;
(5) mixture is thawed reheat and be warming up to grease and separate out completely;
(6) filter to obtain target product.
Further, further comprise step (7): the grease filtrate obtaining is put into whizzer more centrifugal, obtain target product.
Further, in step (1), be specially and gather fresh crocodile fat, remove impurity, clean, pulverize.
Further, step (2) specifically comprises the steps:
(2-1) by following weight part take herbal raw material respectively water soak: dried orange peel 1.0-20.0 part; Ginger 0.1-20.0 part; Root bark of tree peony 0.1-15.0 part; Pomegranate rind 0.1-10.0 part; Radix Glycyrrhizae 0.1-10.0 part; Chrysanthemum 0.1-15.0 part; Japanese Honeysuckle 0.1-20.0 part;
(2-2) respectively by dried orange peel, ginger, the root bark of tree peony, pomegranate rind, Radix Glycyrrhizae, chrysanthemum, Japanese Honeysuckle boiling, decocting liquid is poured out to preservation;
(2-3) by being concentrated into 5～10 times amounts of water content to crude drug gross weight after decocting liquid merging, make Chinese herbal medicine fluid.
Further, be specially and put into subzero 20～80 DEG C of freezings of refrigerator in step (4), wherein fat is 1～10g/mL with the ratio of herb liquid.
Further, in step (5), mixture placement room temperature is thawed half an hour to 4 hour, is heated to 50～110 DEG C.
Further, centrifugal 1～10 minute of whizzer (1000～3000r/min) in step (7).
Further, in step (2-1), soak time is 6～12 hours.
Further, in step (2-2), amount of water is respectively 8～20 times of crude drug weight, and decocting time is respectively 20～40 minutes.
Further, in step (2-2), need the decocting adding again with amount to boil the same time, decoct altogether three times.
Compared with prior art, the present invention has not only solved the easily problem of oxidation of grease, and the potential safety hazard of having avoided the antioxidant that adds synthetic in grease to bring, meets green, health, environmental protection concept.
IC
50refer to the concentration of required antioxidant when clearance rate is 50%, be usually used in the size of comparison scavenging ability of DPPH free radical.Obtain half inhibiting rate (IC according to the clearance rate of different concns antioxidant as curve
50).IC
50be worth littlely, show that its resistance of oxidation is stronger, it is stronger to remove free radical ability.Adopt DPPH method detect traditional method (control group) extract crocodile oil and with the present invention in the oil and fat product that obtains of embodiment Isosorbide-5-Nitrae (experimental group) carry out anti-oxidant activity comparison, measurement result shows the crocodile oil IC that adopts traditional method for extracting
50=24.920mg/mL, the grease finished product IC that embodiment 1 obtains
50=14.138mg/mL, the grease finished product IC that embodiment 4 obtains
50=14.545mg/mL.Employing Chinese herbal medicine fluid extracts the crocodile oil finished product anti-oxidant activity obtaining and obviously improves.
Embodiment
Below in conjunction with embodiment, the present invention is described further.
The present embodiment utilizes the oxidation-resistance of herbal medicine to prepare anti-oxidant crocodile grease:
1), gather fresh crocodile fat, removal impurity, clean, pulverizing.
2), adopt and prepare with the following method Chinese herbal medicine fluid:
2.1, by following weight part take herbal raw material respectively water soak, soak time is 6～12 hours: dried orange peel 1.0-20.0 part; Ginger 0.1-20.0 part; Root bark of tree peony 0.1-15.0 part; Pomegranate rind 0.1-10.0 part; Radix Glycyrrhizae 0.1-10.0 part; Chrysanthemum 0.1-15.0 part; Japanese Honeysuckle 0.1-20.0 part; 2.2, respectively by dried orange peel, ginger, the root bark of tree peony, pomegranate rind, Radix Glycyrrhizae, chrysanthemum, Japanese Honeysuckle boiling, amount of water is respectively 8～20 times of crude drug weight, and decocting time is respectively 20～40 minutes, and decocting liquid is poured out to preservation; Add again with the decocting of amount and boil the same time, decoct altogether three times;
2.3, by being concentrated into 5～10 times amounts of water content to crude drug gross weight after three decocting liquids merging, make Chinese herbal medicine fluid.
3), the crocodile fat of pulverizing is mixed with the Chinese herbal medicine fluid making after stirring evenly and puts into subzero 20～80 DEG C of freezings of refrigerator, wherein ratio fatty and herb liquid is 1～10g/mL.
4), freezing crocodile fat and the mixture of herbal medicine are placed to room temperature thaw to reheat half an hour to 4 hour and be warming up to 50～110 DEG C filter to obtain target product after grease is separated out completely, or continue step 5).
5), the grease filtrate obtaining is put into centrifugal 1～10 minute of whizzer (1000～3000r/min) again, obtain target product.
Above-mentioned steps 2) in the formula of described Chinese herbal medicine fluid, dried orange peel (Citri reticulatae pericarpium) is the dry mature skin of Rutaceae tangerine and cultivated variety thereof, and the flavonoid that contains in dried orange peel, phenols, essential oil, pigment, obacalactone etc. are the antibacterial and oxidation resistant chemical compositions with potentiality to be exploited; Ginger (the rhizome of Zingiberis Rhizoma Recens) Wei Zingiberaceae perennial root herbaceous plant ginger, contain the special composition such as volatile ginger oil and gingerol, modern medicine study confirms the effects such as ginger has anti-oxidant, anti-inflammatory, hepatic cholagogic, stomach invigorating antiemetic, stimulates circulation, regulates nervus centralis, antibacterial, desinsection; Pomegranate rind (Granati Pericarpium) is the dry pericarp of Punicaceae Punica plant pomegranate, have antibacterial, anticancer, antiviral significantly, effect such as anti-oxidant grade, and as natural antioxidants, pomegranate rind wide material sources, extraction yield is high, anti-oxidant activity is strong, with body avidity strong and safe, there is the incomparable advantage of synthetized oxidation preventive agent; The root bark of tree peony (Moutan Cortex) is the dry root skin of Ranunculaceae Paeonia plant tree peony, containing paeonolide, paeonol, paeoniflorin, Oxypaeoniflorin, Benzoylpaeoniflorin and benzoyl Oxypaeoniflorin, volatilization wet goods, there is the effects such as anti-oxidant, antibacterial, anti-inflammatory; Radix Glycyrrhizae (Glycyrrhizae Radix Et Rhizoma) is the dry root and rhizome of glycyrrhizic legume, glycyrrhiza inflate bat or glycyrrhiza glabra, containing triterpene compound, (glycyrrhizin also claims glycyrrhetate, glycyrrhetinic acid etc.), flavonoid compound (liquiritin, isoliquiritigenin, Liquiritigenin etc.) and licorice polysaccharide compounds etc., there is the effects such as anti-oxidant, analgesia, antibechic, anti-inflammatory, antiulcer agent, anti-allergic, can also enhancing body immunologic function, prevent and treat viral hepatitis, anticancer, anti-AIDS; Chrysanthemum (Chrysanthemi Flos) is the dry capitulum of feverfew chrysanthemum, is rich in flavonoid and phenolic compound etc., modern study show Flos Chrysanthemi extract have anti-oxidant, remove the effects such as free radical, antibacterial, antiviral, anti-inflammatory; Japanese Honeysuckle (Lonicerae Japonicae Flos) is the dry flower of caprifoliaceae plant honeysuckle, containing volatile oil, luteolin, nucite, flavonoid, inositol, saponin(e, tannin, chlorogenic acid, isochlorogenic acid etc., there is oxidation-resistance, the effect such as antibacterial, antiviral.
Preferred embodiment 1
1), gather fresh crocodile fat, removal impurity, clean, pulverizing.
2), adopt and prepare with the following method Chinese herbal medicine fluid:
2.1, by following weight part take herbal raw material respectively water soak, soak time is 6 hours: 15.0 parts of dried orange peels; All the other medicinal materials are 0.01 part;
2.2, respectively by dried orange peel, ginger, the root bark of tree peony, pomegranate rind, Radix Glycyrrhizae, chrysanthemum, Japanese Honeysuckle boiling, amount of water is respectively 10 times of crude drug weight, and decocting time is respectively 20 minutes, and decocting liquid is poured out to preservation; Add again with the decocting of amount and boil the same time, decoct altogether three times;
2.3, by being concentrated into the 5 times amounts of water content to crude drug gross weight after three decocting liquids merging, make Chinese herbal medicine fluid.
3), the crocodile fat of pulverizing is mixed with the Chinese herbal medicine fluid making after stirring evenly and puts into the subzero 20 DEG C of freezings of refrigerator, wherein ratio fatty and herb liquid is 5g/mL.
4), freezing crocodile fat and the mixture of herbal medicine being placed to room temperature thaws to reheat for 1 hour and is warming up to 70 DEG C filters to obtain target product after grease is separated out completely.
Preferred embodiment 2
1), gather fresh crocodile fat, removal impurity, clean, pulverizing.
2), adopt and prepare with the following method Chinese herbal medicine fluid:
2.1, by following weight part take herbal raw material respectively water soak, soak time is 6 hours: 10.0 parts of dried orange peels; 5.0 parts, ginger; 5.0 parts of the root barks of tree peony; 2.0 parts of pomegranate rinds; 2.0 parts, Radix Glycyrrhizae; 2.0 parts of chrysanthemums; 4.0 parts of Japanese Honeysuckles;
2.2, respectively by dried orange peel, ginger, the root bark of tree peony, pomegranate rind, Radix Glycyrrhizae, chrysanthemum, Japanese Honeysuckle boiling, amount of water is respectively 10 times of crude drug weight, and decocting time is respectively 20 minutes, and decocting liquid is poured out to preservation; Add again with the decocting of amount and boil the same time, decoct altogether three times;
2.3, by being concentrated into the 5 times amounts of water content to crude drug gross weight after three decocting liquids merging, make Chinese herbal medicine fluid.
3), the crocodile fat of pulverizing is mixed with the Chinese herbal medicine fluid making after stirring evenly and puts into the subzero 20 DEG C of freezings of refrigerator, wherein ratio fatty and herb liquid is 5g/mL.
4), freezing crocodile fat and the mixture of herbal medicine being placed to room temperature thaws to reheat for 1 hour and is warming up to 70 DEG C filters to obtain target product after grease is separated out completely.
Preferred embodiment 3
1), press the 1-4 step acquisition grease filtrate of embodiment 2.
2), the grease filtrate obtaining is put into centrifugal 5 minutes of whizzer (3000r/min) again, obtain target product.
Seven, alternative scheme
Preferred embodiment 4
1), gather fresh crocodile fat, removal impurity, clean, pulverizing.
2), adopt and prepare with the following method Chinese herbal medicine fluid:
2.1, by following weight part take herbal raw material respectively water soak, soak time is 9 hours: 15.0 parts, ginger; All the other are 0.01 part;
2.2, respectively by dried orange peel, ginger, the root bark of tree peony, pomegranate rind, Radix Glycyrrhizae, chrysanthemum, Japanese Honeysuckle boiling, amount of water is respectively 15 times of crude drug weight, and decocting time is respectively 30 minutes, and decocting liquid is poured out to preservation; Add again with the decocting of amount and boil the same time, decoct altogether three times;
2.3, by being concentrated into the 10 times amounts of water content to crude drug gross weight after three decocting liquids merging, make Chinese herbal medicine fluid.
3), the crocodile fat of pulverizing is mixed with the Chinese herbal medicine fluid making after stirring evenly and puts into the subzero 20 DEG C of freezings of refrigerator, wherein ratio fatty and herb liquid is 7g/mL.
4), freezing crocodile fat and the mixture of herbal medicine being placed to room temperature thaws to reheat for 2 hours and is warming up to 70 DEG C filters to obtain target product after grease is separated out completely.
Preferred embodiment 5
1), gather fresh crocodile fat, removal impurity, clean, pulverizing.
2), adopt and prepare with the following method Chinese herbal medicine fluid:
2.1, by following weight part take herbal raw material respectively water soak, soak time is 9 hours: 5.0 parts of dried orange peels; 10.0 parts, ginger; 5.0 parts of the root barks of tree peony; 3.0 parts of pomegranate rinds; 2.0 parts, Radix Glycyrrhizae; 2.0 parts of chrysanthemums; 3.0 parts of Japanese Honeysuckles;
2.2, respectively by dried orange peel, ginger, the root bark of tree peony, pomegranate rind, Radix Glycyrrhizae, chrysanthemum, Japanese Honeysuckle boiling, amount of water is respectively 15 times of crude drug weight, and decocting time is respectively 30 minutes, and decocting liquid is poured out to preservation; Add again with the decocting of amount and boil the same time, decoct altogether three times;
2.3, by being concentrated into the 10 times amounts of water content to crude drug gross weight after three decocting liquids merging, make Chinese herbal medicine fluid.
3), the crocodile fat of pulverizing is mixed with the Chinese herbal medicine fluid making after stirring evenly and puts into the subzero 20 DEG C of freezings of refrigerator, wherein ratio fatty and herb liquid is 7g/mL.
4), freezing crocodile fat and the mixture of herbal medicine being placed to room temperature thaws to reheat for 2 hours and is warming up to 70 DEG C filters to obtain target product after grease is separated out completely.
Preferred embodiment 6
1), press the 1-4 step acquisition grease filtrate of embodiment 5.
2), the grease filtrate obtaining is put into centrifugal 10 minutes of whizzer (3000r/min) again, obtain target product.
The present invention is exemplarily described above in conjunction with the embodiments; obviously specific implementation of the present invention is not subject to the restrictions described above; as long as the various improvement that adopted method design of the present invention and technical scheme to carry out; or directly apply to other occasion without improvement, all within protection scope of the present invention.
Claims (10)
1. anti-oxidant crocodile grease extracting method, is characterized in that, comprises the steps:
(1) gather crocodile fat and pulverize;
(2) prepare Chinese herbal medicine fluid;
(3) the crocodile fat of pulverizing is mixed to stir evenly with the Chinese herbal medicine fluid making obtain mixture;
(4) by described mixture freezing;
(5) mixture is thawed reheat and be warming up to grease and separate out completely;
(6) filter, obtain target product.
2. anti-oxidant crocodile grease extracting method as claimed in claim 1, is characterized in that, further comprises step (7): the grease filtrate obtaining is put into whizzer more centrifugal, obtain target product.
3. anti-oxidant crocodile grease extracting method as claimed in claim 1 or 2, is characterized in that, is specially and gathers fresh crocodile fat in step (1), removes impurity, cleans, pulverizes.
4. the anti-oxidant crocodile grease extracting method as described in any one in claim 1-3, is characterized in that, step (2) specifically comprises the steps:
(2-1) by following weight part take herbal raw material respectively water soak: dried orange peel 1.0-20.0 part; Ginger 0.1-20.0 part; Root bark of tree peony 0.1-15.0 part; Pomegranate rind 0.1-10.0 part; Radix Glycyrrhizae 0.1-10.0 part; Chrysanthemum 0.1-15.0 part; Japanese Honeysuckle 0.1-20.0 part;
(2-2) respectively by dried orange peel, ginger, the root bark of tree peony, pomegranate rind, Radix Glycyrrhizae, chrysanthemum, Japanese Honeysuckle boiling, decocting liquid is poured out to preservation;
(2-3) by being concentrated into 5～10 times amounts of water content to crude drug gross weight after decocting liquid merging, make Chinese herbal medicine fluid.
5. the anti-oxidant crocodile grease extracting method as described in any one in claim 1-4, is characterized in that, is specially and puts into subzero 20～80 DEG C of freezings of refrigerator in step (4), and wherein fat is 1～10g/mL with the ratio of herb liquid.
6. the anti-oxidant crocodile grease extracting method as described in any one in claim 1-5, is characterized in that, in step (5), mixture placement room temperature is thawed half an hour to 4 hour, is heated to 50～110 DEG C.
7. the anti-oxidant crocodile grease extracting method as described in any one in claim 1-6, is characterized in that, centrifugal 1～10 minute of whizzer (1000～3000r/min) in step (7).
8. anti-oxidant crocodile grease extracting method as claimed in claim 4, is characterized in that, in step (2-1), soak time is 6～12 hours.
9. the anti-oxidant crocodile grease extracting method as described in claim 4 or 8, is characterized in that, in step (2-2), amount of water is respectively 8～20 times of crude drug weight, and decocting time is respectively 20～40 minutes.
10. the anti-oxidant crocodile grease extracting method as described in claim 4,8 or 9, is characterized in that, needs the decocting adding again with amount to boil the same time in step (2-2), decocts altogether three times.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410172599.7A CN103923736B (en) | 2014-04-25 | 2014-04-25 | Anti-oxidant crocodile grease extraction |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410172599.7A CN103923736B (en) | 2014-04-25 | 2014-04-25 | Anti-oxidant crocodile grease extraction |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103923736A true CN103923736A (en) | 2014-07-16 |
| CN103923736B CN103923736B (en) | 2016-03-30 |
Family
ID=51142134
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410172599.7A Expired - Fee Related CN103923736B (en) | 2014-04-25 | 2014-04-25 | Anti-oxidant crocodile grease extraction |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103923736B (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105193916A (en) * | 2015-10-28 | 2015-12-30 | 广州善康生物科技有限公司 | Crocodile extract composition for treating rheumatoid ostealgia, and preparation method thereof |
| CN107828503A (en) * | 2017-11-30 | 2018-03-23 | 蚌埠市江淮粮油有限公司 | A kind of processing method of high-quality rapeseed oil |
| CN108707502A (en) * | 2018-04-23 | 2018-10-26 | 周华锋 | A kind of preparation method and application of alligator oil |
| CN108836896A (en) * | 2018-08-20 | 2018-11-20 | 辅必成（上海）医药科技有限公司 | A kind of stable fish oil cream for being used for skin care item and cosmetics |
| WO2021066740A1 (en) * | 2019-10-02 | 2021-04-08 | Liang Chieh Wee | Method of preparation white emulsified scented crocodile oil |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101974364A (en) * | 2009-09-27 | 2011-02-16 | 东北农业大学 | Method for extracting soybean grease from soybean emulsion |
| CN102108318A (en) * | 2010-04-07 | 2011-06-29 | 北京洪源澳达生物技术发展有限公司 | Crocodile grease and preparation method and use thereof |
| CN102304419A (en) * | 2011-08-01 | 2012-01-04 | 安徽师范大学 | Method for removing fishy smell from alligator oil |
-
2014
- 2014-04-25 CN CN201410172599.7A patent/CN103923736B/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101974364A (en) * | 2009-09-27 | 2011-02-16 | 东北农业大学 | Method for extracting soybean grease from soybean emulsion |
| CN102108318A (en) * | 2010-04-07 | 2011-06-29 | 北京洪源澳达生物技术发展有限公司 | Crocodile grease and preparation method and use thereof |
| CN102304419A (en) * | 2011-08-01 | 2012-01-04 | 安徽师范大学 | Method for removing fishy smell from alligator oil |
Non-Patent Citations (1)
| Title |
|---|
| 张蕾等: "《荷叶黄酮对油脂抗氧化作用的研究》", 《现代食品科技》, vol. 25, no. 10, 31 December 2009 (2009-12-31) * |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105193916A (en) * | 2015-10-28 | 2015-12-30 | 广州善康生物科技有限公司 | Crocodile extract composition for treating rheumatoid ostealgia, and preparation method thereof |
| CN107828503A (en) * | 2017-11-30 | 2018-03-23 | 蚌埠市江淮粮油有限公司 | A kind of processing method of high-quality rapeseed oil |
| CN108707502A (en) * | 2018-04-23 | 2018-10-26 | 周华锋 | A kind of preparation method and application of alligator oil |
| CN108707502B (en) * | 2018-04-23 | 2021-06-18 | 湖北鳄宝生物科技研发有限公司 | Preparation method and application of alligator oil |
| CN108836896A (en) * | 2018-08-20 | 2018-11-20 | 辅必成（上海）医药科技有限公司 | A kind of stable fish oil cream for being used for skin care item and cosmetics |
| CN108836896B (en) * | 2018-08-20 | 2021-03-23 | 辅必成（上海）医药科技有限公司 | Stable fish oil emulsion for skin care products and cosmetics |
| WO2021066740A1 (en) * | 2019-10-02 | 2021-04-08 | Liang Chieh Wee | Method of preparation white emulsified scented crocodile oil |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103923736B (en) | 2016-03-30 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| Singh et al. | Cuminum cyminum–A popular spice: An updated review | |
| KR101946236B1 (en) | Cosmetical composition with antimicrobial and antioxidant using natural plant extract and cosmetics comprising thereof | |
| KR100879032B1 (en) | Natural antibacterial extracts and cosmetic composition comprising the extracts | |
| CN103923736B (en) | Anti-oxidant crocodile grease extraction | |
| CN102665674A (en) | Oral compositions containing a combination of natural extracts and related methods | |
| Sharma et al. | Comparison of anti-oxidant activity of Andrographis paniculata and Tinospora cordifolia leaves | |
| CN104306319A (en) | Ghee whitening skin cream and preparation method thereof | |
| CN104491773A (en) | Ginger granules and preparation method thereof | |
| CN112868678A (en) | Plant antibacterial mite-killing agent, preparation method thereof and daily necessities containing plant antibacterial mite-killing agent | |
| CN101569390B (en) | Pickled upturned chili and preparation method thereof | |
| CN109010173A (en) | A kind of multi-functional skin care is spraying and preparation method thereof | |
| KR101224238B1 (en) | Extract of mixed plants | |
| KR101980887B1 (en) | A cosmetic composition comprising trichosanthes kirilowii extract and metaplexis japonica extract | |
| KR101936835B1 (en) | Feminine cleanser composition comprising potato or potato pulp extract | |
| CN101361911A (en) | External skin composition with wrinkle-dispelling function and production method thereof | |
| KR101799155B1 (en) | External preparation for skin comprising extract of Traditional herb | |
| CN103284162A (en) | Aloe vera gel functional food | |
| CN106620616A (en) | Pharmaceutical composition for preventing hair loss and promoting hair growth and preparation of pharmaceutical composition | |
| KR20090047638A (en) | The functional bean curds wrapped in leaves or nonfiltered bean curds with antioxidant activity | |
| CN104068150A (en) | Tea with thick green taste and preparation method for tea | |
| WO2016117705A1 (en) | Agent for inducing production of hepatocyte growth factor | |
| CN105441230A (en) | Camellia oil cold processed soap | |
| CN108497246A (en) | A kind of plant weight losing function beverage and preparation method thereof | |
| KR20160003920A (en) | Cosmetic composition for anti-inflammation or improving skin trouble containing herb extracts | |
| Rehman et al. | Biochemical, phytochemical and antioxidant composition of Equisetum debile Roxb |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160330 Termination date: 20190425 |