CN103923670A - Industrial treatment method and industrial treatment device for oil field waste - Google Patents
Industrial treatment method and industrial treatment device for oil field waste Download PDFInfo
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- 239000002699 waste material Substances 0.000 title claims abstract description 58
- 238000000034 method Methods 0.000 title claims abstract description 47
- 238000010438 heat treatment Methods 0.000 claims abstract description 163
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 86
- 238000000926 separation method Methods 0.000 claims abstract description 35
- 238000009833 condensation Methods 0.000 claims abstract description 32
- 230000005494 condensation Effects 0.000 claims abstract description 32
- 239000007787 solid Substances 0.000 claims abstract description 16
- 238000000746 purification Methods 0.000 claims abstract description 12
- 238000005070 sampling Methods 0.000 claims abstract description 5
- 239000007789 gas Substances 0.000 claims description 114
- 238000001035 drying Methods 0.000 claims description 70
- 239000012265 solid product Substances 0.000 claims description 32
- 238000012545 processing Methods 0.000 claims description 31
- 238000007599 discharging Methods 0.000 claims description 29
- 230000008569 process Effects 0.000 claims description 29
- 238000002203 pretreatment Methods 0.000 claims description 24
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 23
- 229910052760 oxygen Inorganic materials 0.000 claims description 23
- 239000001301 oxygen Substances 0.000 claims description 23
- 239000010881 fly ash Substances 0.000 claims description 22
- 238000011084 recovery Methods 0.000 claims description 15
- 239000007788 liquid Substances 0.000 claims description 14
- 238000007670 refining Methods 0.000 claims description 13
- 229930195733 hydrocarbon Natural products 0.000 claims description 12
- 150000002430 hydrocarbons Chemical class 0.000 claims description 12
- 239000000446 fuel Substances 0.000 claims description 11
- 230000008676 import Effects 0.000 claims description 9
- 239000002912 waste gas Substances 0.000 claims description 9
- 229910052756 noble gas Inorganic materials 0.000 claims description 8
- 239000003208 petroleum Substances 0.000 claims description 7
- 238000007711 solidification Methods 0.000 claims description 5
- 230000008023 solidification Effects 0.000 claims description 5
- 238000000197 pyrolysis Methods 0.000 abstract description 8
- 230000000694 effects Effects 0.000 abstract description 3
- 238000004064 recycling Methods 0.000 abstract description 3
- 239000000126 substance Substances 0.000 abstract description 2
- 239000003921 oil Substances 0.000 description 134
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- 238000005516 engineering process Methods 0.000 description 6
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- 238000012546 transfer Methods 0.000 description 6
- 239000000428 dust Substances 0.000 description 5
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 4
- 238000010521 absorption reaction Methods 0.000 description 4
- 235000011089 carbon dioxide Nutrition 0.000 description 4
- 238000005553 drilling Methods 0.000 description 4
- 238000005259 measurement Methods 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
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- MWPLVEDNUUSJAV-UHFFFAOYSA-N anthracene Chemical compound C1=CC=CC2=CC3=CC=CC=C3C=C21 MWPLVEDNUUSJAV-UHFFFAOYSA-N 0.000 description 2
- 230000005540 biological transmission Effects 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
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- 238000011161 development Methods 0.000 description 2
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- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 239000003570 air Substances 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 229910052804 chromium Inorganic materials 0.000 description 1
- 239000011651 chromium Substances 0.000 description 1
- 239000000567 combustion gas Substances 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 230000005672 electromagnetic field Effects 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- GVEPBJHOBDJJJI-UHFFFAOYSA-N fluoranthrene Natural products C1=CC(C2=CC=CC=C22)=C3C2=CC=CC3=C1 GVEPBJHOBDJJJI-UHFFFAOYSA-N 0.000 description 1
- 239000000295 fuel oil Substances 0.000 description 1
- 238000002309 gasification Methods 0.000 description 1
- 239000003673 groundwater Substances 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 230000013011 mating Effects 0.000 description 1
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
- 229910052753 mercury Inorganic materials 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000003129 oil well Substances 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
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- 238000005406 washing Methods 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
Classifications
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10B—DESTRUCTIVE DISTILLATION OF CARBONACEOUS MATERIALS FOR PRODUCTION OF GAS, COKE, TAR, OR SIMILAR MATERIALS
- C10B53/00—Destructive distillation, specially adapted for particular solid raw materials or solid raw materials in special form
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10B—DESTRUCTIVE DISTILLATION OF CARBONACEOUS MATERIALS FOR PRODUCTION OF GAS, COKE, TAR, OR SIMILAR MATERIALS
- C10B19/00—Heating of coke ovens by electrical means
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G1/00—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal
- C10G1/02—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal by distillation
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G1/00—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal
- C10G1/10—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal from rubber or rubber waste
-
- E—FIXED CONSTRUCTIONS
- E21—EARTH OR ROCK DRILLING; MINING
- E21B—EARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
- E21B21/00—Methods or apparatus for flushing boreholes, e.g. by use of exhaust air from motor
- E21B21/06—Arrangements for treating drilling fluids outside the borehole
- E21B21/063—Arrangements for treating drilling fluids outside the borehole by separating components
- E21B21/065—Separating solids from drilling fluids
- E21B21/066—Separating solids from drilling fluids with further treatment of the solids, e.g. for disposal
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Life Sciences & Earth Sciences (AREA)
- Organic Chemistry (AREA)
- Geology (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Wood Science & Technology (AREA)
- Mining & Mineral Resources (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Physics & Mathematics (AREA)
- Environmental & Geological Engineering (AREA)
- Fluid Mechanics (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Processing Of Solid Wastes (AREA)
Abstract
The invention provides an industrial treatment method for oil field waste. The industrial treatment method for oil field waste comprises the following steps: carrying out sampling analysis on the oil field waste, preheating to 80-300 DEG C by using high-temperature steam or conduction oil, then carrying out microwave pyrolysis treatment, controlling pressure at minus 5000 to minus 100 Pa, thus obtaining solid treatment substances and gas, condensing, separating and purifying the gas, and finally recycling so as to obtain water, oil and non-condensable gas. An industrial treatment device for oil field waste comprises a feed hopper, a dryer, a microwave heating cavity, a microwave generator, a heating device and a condensation separation purification device, wherein the feed hopper is connected to the dryer which is connected to the microwave heating cavity, a steam or conduction oil outlet of the heating device is connected to a steam or conduction oil outlet of the dryer; gas outlets of the dryer and the microwave heating cavity are connected to the condensation separation purification device; the microwave generator is connected to the microwave heating cavity. The industrial treatment method and the industrial treatment device have good treatment effects, high utilization rate of energy sources and good economical efficiency.
Description
Technical field
The present invention relates to oil field waste process field, particularly industrial treatment method and the device thereof of oil field waste.
Background technology
Oil field waste is often referred to the oily sludge and silt, the soil of crude oil pollution, the crude oil that in landwaste, water-based mud and oil-base mud, oil recovery and the oil well operation process producing in drilling process, produce and lets slip bottom settlings thing in journey etc. at storage tank internal memory.Oil field waste, except containing certain petroleum substance, also contains the toxic substances such as a large amount of benzene homologues, phenols, anthracene, pyrene, the heavy metals such as salt and copper, zinc, chromium, mercury.These oil field wastes are difficult for processing, and under natural condition, completely decompose and need the years up to a hundred, and not only directly land occupation and space, and severe contamination air, soil and groundwater, restricted the prodution and development of petroleum industry to a certain extent.
Along with the requirement of national environmental protection statutory standard improves constantly, law enforcement for environmental protection dynamics continues to increase, and the pollution control of oil field waste and recycling become the focus that the industry keeps sustainable development to face.For innoxious, the recycling treatment of oil field waste, mainly comprise now modified, separation and extraction treatment technology, solidification technology, incineration treatment technology, biologic treating technique, re-injection and blending technology, pyrolysis processing technology etc.
Conventionally the electrically heated of pyrolysis processing utilization or combustion gas, fuel oil, coal-fired heating method, its heat transmission is mainly by thermal conduction, convection current, three kinds of approach of radiation.These traditional heating method for pyrolysis heating efficiency are low, make product after treatment be up to state standards, and the energy often expending is more, and economy is lower.
Summary of the invention
The technical problem that the present invention solves is to provide a kind of industrial treatment method and device thereof of oil field waste, and treatment effect is good, and energy utilization rate is high, good economy performance.
The industrial treatment method that the invention discloses oil field waste, comprises the following steps:
(A) oil field waste is carried out after sampling analysis, use steam heating or heat-conducting oil heating that oil field waste is preheated to 80～300 DEG C, obtain pre-treatment solid product and gas, described gas is through condensation separation and purifying treatment, recovery obtains water, oil and noncondensable gas, and the oil of described recovery and noncondensable gas are for the fuel of steam heating or heat-conducting oil heating;
(B) described pre-treatment solid product is carried out to microwave-heating processing, control pressure is-5000～-100Pa, obtains total petroleum hydrocarbons content lower than 3% solids treatment thing and gas;
Described gas, through condensation separation and purifying treatment, reclaims and obtains water and oil, and the oil of described recovery is for the fuel of steam heating or heat-conducting oil heating.
Preferably, described steps A) in, when described thermal pretreatment, control oxygen level lower than 7%.
Preferably, described step B) in, when processing, described microwave-heating controls oxygen level lower than 7%.
Preferably, described step B) also comprise described solids treatment thing is sprayed to rewetting or solidification treatment.
The industrial treatment device that the invention discloses oil field waste, comprising:
Hopper, drying machine, microwave heating chamber, microwave generator, heating unit and condensation separation refining plant;
Described hopper is connected with the feed end of drying machine;
The discharge end of described drying machine is connected with the feed end of described microwave heating chamber;
Described heating unit is steam boiler or heat conducting oil boiler, and the vapour outlet of described heating unit or thermal oil outlet are connected with steam inlet or the heat conductive oil inlet of drying machine;
The pneumatic outlet of described drying machine and the pneumatic outlet of microwave heating chamber are all connected with condensation separation refining plant;
Described microwave generator is connected with microwave heating chamber.
Preferably, also comprise gas lock or feeding device; Described feeding device is feed auger and the rotary unloading device connecting successively, is connected or feeding device connects between the feed end of described hopper and drying machine by gas lock.
Preferably, also comprise discharging spiral, described discharging spiral is connected with microwave heating chamber discharge end.
Preferably, described discharging shaped spiral housing is outside equipped with the first recirculated water chuck, and described feed auger housing is outside equipped with the second recirculated water chuck, and described the first recirculated water chuck is connected with the second recirculated water chuck by hot water or cold water's pipeline.
Preferably, described condensation separation refining plant comprises fly-ash separator, condenser, blower fan, waste gas purification apparatus, gravitational settler, water-and-oil separator.
Connecting order is that fly-ash separator is connected with condenser, and the pneumatic outlet of condenser is connected with waste gas purification apparatus by blower fan; The liquid exit of condenser is connected with gravitational settler; The water outlet of gravitational settler is connected with water-and-oil separator.
Preferably, the tail gas outlet of described heating unit and the noble gas import of drying machine or microwave heating chamber are connected.
Compared with prior art, the invention provides a kind of industrial treatment method of oil field waste.First, the application, according to the proximate analysis data of the oil field waste obtaining, carries out preheating and microwave-heating processing to it; The heating rate of microwave is fast, and penetrance is high, and processing efficiency and heating uniformity are all better than traditional pyrolytic technique, and economic feasibility is high.Secondly, carry out the microwave-heating under-5000～-100Pa pressure after thermal pretreatment again, can reduce the boiling point of oil content in material, improve the gasification rate of oil content, reduced the energy expenditure in microwave-heating stage, processing efficiency is high.Again, pre-treatment and microwave-heating are processed the gas producing through condensation separation and purifying treatment and recovery, and the oil obtaining and noncondensable gas, for the fuel of steam heating or heat-conducting oil heating, are realized fuel self-sufficiency, have higher energy utilization rate and economy.Finally, pre-heating stage can be removed the moisture in oil field waste in a large number, reduces the vapour quantity that the microwave-heating stage produces, and reduces " sparking " probability.
The present invention completes thermal pretreatment in drying machine, then pre-treatment solid product is delivered in microwave heating chamber and completes microwave-heating processing, the gas producing the treatment stage of pretreatment stage and microwave-heating utilizes condensation separation refining plant to complete vapor-liquid separation and purify and reclaims.
Brief description of the drawings
The structural representation of the industrial treatment device of the oil field waste that Fig. 1 provides for embodiment 1;
The structural representation of the industrial treatment device of the oil field waste that Fig. 2 provides for embodiment 2;
The structural representation of the industrial treatment device of the oil field waste that Fig. 3 provides for embodiment 3;
The structural representation of the industrial treatment device of the oil field waste that Fig. 4 provides for embodiment 4.
Embodiment
In order further to understand the present invention, below in conjunction with embodiment, the preferred embodiment of the invention is described, but should be appreciated that these are described is for further illustrating the features and advantages of the present invention, instead of limiting to the claimed invention.
The industrial treatment method that the embodiment of the invention discloses oil field waste, comprises the following steps:
(A) oil field waste is carried out to sampling analysis, use steam heating or heat-conducting oil heating that oil field waste is preheated to 80～300 DEG C, obtain pre-treatment solid product and gas, described gas, through condensation separation and purifying treatment, reclaims and obtains water, oil and noncondensable gas; The oil of described recovery and noncondensable gas are for the fuel of steam heating or heat-conducting oil heating;
(B) described pre-treatment solid product is carried out to microwave-heating processing, control pressure is-5000～-100Pa, obtains total petroleum hydrocarbons content lower than 3% solids treatment thing and gas;
Described gas, through condensation separation and purifying treatment, reclaims and obtains water and oil, and the oil of described recovery is for the fuel of steam heating or heat-conducting oil heating; Described solids treatment thing, through spray rewetting or solidification treatment, is discharged and is carried out accumulating.
In the present invention, oil field waste is carried out to sampling analysis, determine the essentially consist of oil field waste, can calculate the final pyrolysis temperature needing according to processing requirements, the present invention is not particularly limited for the method for described calculating.In pretreatment stage, use steam heating or heat-conducting oil heating that material is preheated to 80～300 DEG C, be preferably 85～95 DEG C, obtain pre-treatment solid product and gas.Described gas is the mixture of the hydro carbons of water vapor and C1～C7.Described gas, through condensation separation and purifying treatment, obtains water, oil and non-condensable gas, and the oil of described recovery and noncondensable gas are for the fuel of steam heating or heat-conducting oil heating, thereby save energy improves energy utilization rate.When described pre-treatment, preferably control oxygen level lower than 7%, catch fire or explode to prevent oil generation of waste materials flammable explosive gas.The mode of described control oxygen level be preferably the tail gas that steam boiler or heat conducting oil boiler are produced as rare gas element for pre-treatment.
Obtain, after described pre-treatment solid product, it being carried out to microwave-heating processing, control pressure is-5000～-100Pa, and described pressure is preferably-1000～-200Pa, obtains total petroleum hydrocarbons content lower than 3% solids treatment thing and gas.Because the one-tenth of oil field waste is grouped into complexity, the application can be grouped into according to its one-tenth, can suitably adjust the output rating of microwave-heating stage microwave generator for certain treatment capacity and processing requirements, realize mating of operating parameters and processing demands, and save the energy.According to different cleanup standards, the total petroleum hydrocarbons content of the solids treatment thing preferably finally obtaining is lower than 1%.When low-carbon (LC) hydrocarbon content is higher in oil field waste, can adopt the microwave-heating processing of lower-wattage and short period, when higher hydrocarbons content is higher, adopt the microwave-heating processing of higher-wattage and long period.When described microwave-heating is processed, preferably control oxygen level lower than 7%, catch fire or explode to prevent oil generation of waste materials flammable explosive gas.The mode of described control oxygen level is preferably to be processed as rare gas element the tail gas of steam boiler or heat conducting oil boiler generation for microwave-heating.
Obtain, after described solids treatment thing, preferably also comprising described solids treatment thing being sprayed to rewetting or solidification treatment, to reduce drop temperature, prevent from scalding and dust pollution, simplify subsequent processes.
The gas that described microwave-heating processing obtains, through condensation separation and purifying treatment, reclaims and obtains water and oil; The oil of described recovery is for the fuel of steam heating or heat-conducting oil heating.
The industrial treatment device that the invention also discloses oil field waste, comprising:
Hopper, drying machine, microwave heating chamber, microwave generator, heating unit and condensation separation refining plant;
Described hopper is connected with the feed end of drying machine;
The discharge end of described drying machine is connected with the feed end of described microwave heating chamber;
Described heating unit is steam boiler or heat conducting oil boiler, and the vapour outlet of described heating unit or thermal oil outlet are connected with steam inlet or the heat conductive oil inlet of drying machine;
The pneumatic outlet of described drying machine is all connected with condensation separation refining plant with the pneumatic outlet of microwave heating chamber;
Described microwave generator is connected with microwave heating chamber.
In the present invention, described drying machine is oil field waste obtains pre-treatment solid product and gas device through preheating.The present invention is not particularly limited for the kind of described drying machine, is preferably paddle-dryer.
Described hopper is the import of oil field waste, and described hopper is connected with the feed end of drying machine.Described hopper is preferably connected by gas lock with the feed end of drying machine or feeding device connects, and described feeding device is feed auger and the rotary unloading device connecting successively.
Described heating unit is steam boiler or heat conducting oil boiler, for drying machine provides high temperature thermal medium.The vapour outlet of described heating unit or thermal oil outlet are connected with steam inlet or the heat conductive oil inlet of drying machine.Described heating unit produces high-temperature steam or thermal oil, is input to steam inlet or the heat conductive oil inlet in described drying machine by vapour outlet or thermal oil outlet, and oil field waste is carried out to preheating.Described heating unit produces tail gas simultaneously, i.e. the gas such as carbonic acid gas.Preferably, the tail gas outlet of described heating unit is connected with the noble gas import of drying machine, the tail gas of generation is input in drying machine, to control the oxygen level in drying machine.Preferably, the tail gas outlet of described heating unit is connected with the noble gas import of microwave heating chamber, the tail gas of generation is input in microwave heating chamber, to control the oxygen level in microwave heating chamber.
Described microwave heating chamber is the device that pre-treatment solid product is carried out to microwave-heating processing.In described microwave heating chamber, preferably by transport unit, pre-treatment solid product is carried, described transport unit is preferably travelling belt, blade transfer roller, worm conveyor or scraper conveyor.Described microwave generator is the device that produces microwave, its energy that is electromagnetic field by electric energy conversion.Described microwave generator can be one or more.Described microwave generator is connected with microwave heating chamber by Bragg Transducer for Waveguide Devices, and electromagnetic transmission, in microwave heating chamber, is carried out to microwave-heating processing to pre-treatment solid product, and making residue water and the hydrocarbon conversion is wherein gas, remaining solids treatment thing.The discharge end of described drying machine is preferably connected with described microwave heating chamber feed end by gas lock or rotary unloading device.The discharge end of described microwave heating chamber is preferably connected with discharging spiral by gas lock or rotary unloading device.
In order to improve energy utilization rate, preferably be outside equipped with the first recirculated water chuck at described discharging shaped spiral housing, described feed auger housing is outside equipped with the second recirculated water chuck, and described the first recirculated water chuck is connected with the second recirculated water chuck with hot water line by cold water pipeline.Water in described the first recirculated water chuck absorbs the heat of the solids treatment thing of microwave heating chamber discharge, and temperature raises, and is delivered to the second recirculated water chuck by hot water line, for the auxiliary preheating of oil field waste.In the second recirculated water chuck, the water of releases heat is transmitted back to the first recirculated water chuck by cold water pipeline again, completes the recycle of heat.
The effect of described condensation separation refining plant is that gas is carried out to condensation, vapor-liquid separation and purification.The pneumatic outlet of described drying machine and the pneumatic outlet of microwave heating chamber are all connected with condensation separation refining plant.Described condensation separation refining plant preferably comprises fly-ash separator, condenser, blower fan, waste gas purification apparatus, gravitational settler, water-and-oil separator;
Connecting order is that fly-ash separator is connected with condenser, and the pneumatic outlet of condenser is connected with waste gas purification apparatus by blower fan; The liquid exit of condenser is connected with gravitational settler, and the water outlet of gravitational settler is connected with water-and-oil separator.
Or the position of described blower fan can suitably regulate according to those skilled in the art's general knowledge.Described condensation separation refining plant also preferably comprises fly-ash separator, blower fan, condenser, waste gas purification apparatus, gravitational settler, water-and-oil separator;
Connecting order is that fly-ash separator outlet is connected with condenser by blower fan, and the pneumatic outlet of condenser is connected with waste gas purification apparatus; The liquid exit of condenser is connected with gravitational settler, and the water outlet of gravitational settler is connected with water-and-oil separator.
The present invention is not particularly limited for the kind of described fly-ash separator, is preferably sack cleaner or cyclone dust.Described condenser is preferably one or more.Described water-and-oil separator is preferably one or more.Described waste gas purification apparatus is preferably water washing device, activated charcoal filter or UV high-efficient gas purifier.
In order further to understand the present invention, below in conjunction with embodiment, industrial treatment method and the device of oil field waste provided by the invention are described, protection scope of the present invention is not limited by the following examples.
Embodiment 1
Industrial treatment device and the technical process of the oil field waste that embodiment 1 provides, as shown in Figure 1.
In Fig. 1, hopper (1) is connected with drying machine (3) by gas lock (2), and the vapour outlet of steam boiler (6) is connected with the steam inlet of drying machine (3).
The discharge end of drying machine (3) is connected with the feed end of microwave heating chamber (4) by gas lock (2-1), and microwave generator (7) is connected with microwave heating chamber (4) by Bragg Transducer for Waveguide Devices.In microwave heating chamber (4), be provided with blade transfer roller (5).
The pneumatic outlet of drying machine (3) and microwave heating chamber (4) is all connected with fly-ash separator (12), fly-ash separator (12) is connected with condenser (13) and condenser (13-1) successively, and the pneumatic outlet of condenser (13-1) is connected with UV high-efficient gas purifier (15) by blower fan (14).The liquid exit of condenser (13) and condenser (13-1) is connected with gravitational settler (16), and the water outlet of gravitational settler (16) is connected with water-and-oil separator (17).
The discharge end of microwave heating chamber (4) is connected with discharging spiral (8) by gas lock (2-2), is provided with spray equipment (9) in discharging spiral (8).The end below of discharging spiral (8) is provided with discharge bin (10).
The tail gas outlet of steam boiler (6) is connected with the noble gas import of drying machine (3) and microwave heating chamber (4) respectively.
Measurement of oxygen content device (12) is connected with drying machine (3) and microwave heating chamber (4) respectively.
Oil field waste enters drying machine (3) through hopper (1) through gas lock (2), and the high-temperature steam that utilizes steam boiler (6) to produce carries out preheating to oil field waste, obtains water vapor, oil gas and pre-treatment solid product.Pre-treatment solid product enters in microwave heating chamber (4) and carries out microwave-heating processing through gas lock (2-1), obtains water vapor, oil gas and microwave-heating solid product.The water vapor and the oil gas that in drying machine and microwave heating chamber, produce are extracted out by blower fan (14), through fly-ash separator (12) dedusting, locate to be condensed at condenser (13), condenser (13-1), the noncondensable gas obtaining, by blower fan (14) and UV high-efficient gas purifier (15), is discharged in atmosphere; The liquid that condensation obtains carries out oily water separation by gravitational settler (16) and water-and-oil separator (17).
The solid product that completes microwave-heating processing arrives the discharging spiral (8) in downstream by gas lock (2-2), carry out gradually discharge.Use spray equipment (9) to spray wet treatment again to solid product, final handled thing falls into discharge bin (10), carries out accumulating simultaneously.
Embodiment 2
Industrial treatment device and the technical process of the oil field waste that embodiment 2 provides, as shown in Figure 2.
In Fig. 2, hopper (1) is connected with drying machine (4) with rotary unloading device (3) by feed auger (2), and the vapour outlet of steam boiler (7) is connected with the steam inlet of drying machine (4).The discharge end of drying machine (4) is connected with the feed end of microwave heating chamber (5) by rotary unloading device (3-1), and microwave generator (8) is connected with microwave heating chamber (5) by Bragg Transducer for Waveguide Devices.In microwave heating chamber (5), be provided with conveying travelling belt (6).
The pneumatic outlet of drying machine (4) and microwave heating chamber (5) is connected with fly-ash separator (13), blower fan (14) and condenser (15) and condenser (15-1) respectively successively, and the pneumatic outlet of condenser (15-1) is connected with UV high-efficient gas purifier (16).The liquid exit of condenser (15) and condenser (15-1) is connected with gravitational settler (17), and the water outlet of gravitational settler (17) is connected with water-and-oil separator (18).The discharge end of microwave heating chamber (5) is connected with discharging spiral (9) by rotary unloading device (3-2).In discharging spiral (9), be provided with spray equipment (10), the end below of discharging spiral (9) is provided with discharge bin (11).
The tail gas outlet of steam boiler (7) is connected with the noble gas import of drying machine (4) and microwave heating chamber (5) respectively.
Measurement of oxygen content device (12) is connected with drying machine (4) and microwave heating chamber (5) respectively.
Oil field waste enters in drying machine (4) through hopper (1), feed auger (2) and rotary unloading device (3), and the high-temperature steam that utilizes steam boiler (7) to produce carries out preheating, obtains water vapor, oil gas and pre-treatment solid product.Pre-treatment solid product enters in microwave heating chamber (5) and carries out microwave-heating processing through rotary unloading device (3-1), obtains water vapor, oil gas and microwave-heating solid product.The water vapor and the oil gas that in drying machine and microwave heating chamber, produce are extracted out by blower fan (14), through fly-ash separator (13) dedusting, arrive condenser (15) and condenser (15-1) and locate to be condensed, the noncondensable gas obtaining, by UV high-efficient gas purifier (16), is discharged in atmosphere; The liquid that condensation obtains carries out oily water separation by gravitational settler (17) and water-and-oil separator (18).
The solid product that completes microwave-heating processing arrives the discharging spiral (9) in downstream by rotary unloading device (3-2), carry out gradually discharge.Use spray equipment (10) to spray wet treatment again to solid product, final handled thing falls into discharge bin (11), carries out accumulating simultaneously.
Embodiment 3
Industrial treatment device and the technical process of the oil field waste that embodiment 3 provides, as shown in Figure 3.
In Fig. 3, hopper (1) is connected with drying machine (3) by gas lock (2), and the thermal oil outlet of heat conducting oil boiler (6) is connected with the heat conductive oil inlet of drying machine (3).
The discharge end of drying machine (3) is connected with the feed end of microwave heating chamber (4) by gas lock (2-1), and microwave generator (7) is connected with microwave heating chamber (4) by Bragg Transducer for Waveguide Devices.In microwave heating chamber (4), be provided with scraper conveyor (5).
The pneumatic outlet of drying machine (3) and microwave heating chamber (4) is connected with fly-ash separator (12), condenser (13) and condenser (13-1) respectively successively, and the pneumatic outlet of condenser (13-1) is connected with activated charcoal filter (15) by blower fan (14).The liquid exit of condenser (13) and condenser (13-1) is connected with gravitational settler (16), and the water outlet of gravitational settler (16) is connected with water-and-oil separator (17).
The discharge end of microwave heating chamber (4) is connected with discharging spiral (8) by gas lock (2-2), is provided with spray equipment (9) in discharging spiral (8), and the end below of discharging spiral (8) is provided with discharge bin (10).
The tail gas outlet of heat conducting oil boiler (6) is connected with the noble gas import of drying machine (3) and microwave heating chamber (4) respectively.
Measurement of oxygen content device (12) is connected with drying machine (3) and microwave heating chamber (4) respectively.
Oil field waste enters drying machine (3) by hopper (1) through gas lock (2), and the high temperature heat conductive oil that utilizes heat conducting oil boiler (6) to produce heats oil field waste, obtains water vapor, oil gas and pre-treatment solid product.Pre-treatment solid product enters in microwave heating chamber (4) and carries out microwave-heating processing through gas lock (2-1).The water vapor and the oil gas that in drying machine and microwave heating chamber, produce are extracted out by blower fan (14), through fly-ash separator (12) dedusting, locate to be condensed at condenser (13) and condenser (13-1), the noncondensable gas obtaining, by activated charcoal filter (15), is discharged in atmosphere; The liquid that condensation obtains carries out oily water separation by gravitational settler (16) and water-and-oil separator (17).The oil that separation obtains can be again as the fuel of heat conducting oil boiler (6).
The solid product that completes microwave-heating processing arrives the discharging spiral (8) in downstream by gas lock (2-2), carry out gradually discharge.Use spray equipment (9) to spray wet treatment again to solid product, final handled thing falls into discharge bin (10), carries out accumulating simultaneously.
Embodiment 4
Industrial treatment device and the technical process of the oil field waste that embodiment 4 provides, as shown in Figure 4.
In Fig. 4, hopper (1) is connected with drying machine (4) with rotary unloading device (3) by feed auger (2), and the vapour outlet of steam boiler (7) is connected with the steam inlet of drying machine (4).The discharge end of drying machine (4) is connected with the feed end of microwave heating chamber (5) by rotary unloading device (3-1), and microwave generator (8) is connected with microwave heating chamber (5) by Bragg Transducer for Waveguide Devices.In microwave heating chamber (5), be provided with blade transfer roller (6).
The pneumatic outlet of drying machine (4) and microwave heating chamber (5) is connected with fly-ash separator (13) respectively, fly-ash separator (13) outlet is connected with condenser (15) and condenser (15-1) by blower fan (14), and the pneumatic outlet of condenser (15-1) is connected with activated charcoal filter (16).The liquid exit of condenser (15) and condenser (15-1) is connected with gravitational settler (17), and the water outlet of gravitational settler (17) is connected with water-and-oil separator (18).
The discharge end of microwave heating chamber (5) is connected with discharging spiral (9) by rotary unloading device (3-2), is provided with spray equipment (10) in discharging spiral (9), and the end below of discharging spiral (9) is provided with discharge bin (11).
The tail gas outlet of steam boiler (7) is connected with the noble gas import of drying machine (4) and microwave heating chamber (5) respectively.
Measurement of oxygen content device (12) is connected with drying machine (4) and microwave heating chamber (5) respectively.
The housing of discharging spiral (9) is outside equipped with the first recirculated water chuck (20a), and the housing of feed auger (2) is outside equipped with the second recirculated water chuck (20b), is connected therebetween by hot water line (19a) with cold water pipeline (19b).
Oil field waste enters drying machine (3) through hopper (1) and gas lock (2), and the high-temperature steam that utilizes steam boiler (6) to produce heats oil field waste, obtains water vapor, oil gas and pre-treatment solid product.Pre-treatment solid product enters in microwave heating chamber (4) and carries out microwave-heating processing through gas lock (2-1).The water vapor and the oil gas that in drying machine and microwave heating chamber, produce are extracted out by blower fan (14), through fly-ash separator (12) dedusting, locate to be condensed at condenser (15) and condenser (15-1), the noncondensable gas obtaining, through activated charcoal filter (16), is discharged in atmosphere; The liquid that condensation obtains carries out oily water separation by gravitational settler (17) and water-and-oil separator (18).
The solid product that completes microwave-heating processing arrives the discharging spiral (9) in downstream by gas lock (2-2), carry out gradually discharge.Use spray equipment (10) to spray wet treatment again to solid product, final handled thing falls into discharge bin (11), carries out accumulating simultaneously.
The housing of discharging spiral (9) is outside equipped with the first recirculated water chuck (20a), and the housing of feed auger (2) is outside equipped with the second recirculated water chuck (20b).Heat in the solid product that recirculated water absorption microwave heating chamber in the first recirculated water chuck (20a) is discharged, temperature raises, and is delivered to the initial material of preheating in the second recirculated water chuck (20b) via hot water line (19a).The recirculated water that releases heat, temperature reduce is got back in the first recirculated water chuck (20a) by cold water pipeline (19b), completes the recycle of heat.
Embodiment 5
Treatment unit described in employing embodiment 1 carries out the industrial treatment of oil waste.
By 1000kg well drilling detritus, (water ratio is 19%, oil length is 7%) enter paddle-dryer by hopper through gas lock, high-temperature steam (vapor temperature is 160 DEG C, and pressure is 0.6MPa, and flow the is 120kg/hr) preheating material that utilizes steam boiler to produce, tentatively remove volatile constituent wherein, the gas evaporating is extracted out by high pressure positive blower, and cavity pressure is-170～-200Pa, and oxygen level is in 7% left and right, this process continues 1 hour, and material outlet temperature is 90 DEG C.Landwaste through preheating and drying enters microwave heating chamber by gas lock, arrives the feed end of blade transfer roller, and in this process, temperature is down to 60 DEG C, and regulating the rotating speed of central shaft is 1 rev/min.Two microwave generators are exported the microwave of 130kw altogether, be transferred in microwave heating chamber by Bragg Transducer for Waveguide Devices, material is heated, make its water containing and hydro carbons evaporation, depart from material, and extracted out outside cavity by high pressure positive blower in time, cavity internal pressure is-170～-200Pa, oxygen level is in 4%～7% left and right, this process continues 60 minutes, and material outlet temperature is 267 DEG C.When the solid phase residue that completes pyrolysis absorption is transported to the discharge end of heating chamber, arrive the discharging spiral in downstream by gas lock, carry out gradually discharge, final material is dropped in discharge bin, carries out accumulating.
In this process, use boiler exhaust gas (main component is carbonic acid gas) to be filled with drying machine and microwave heating chamber, to control its oxygen level.
The gas producing in dry and thermal desorption additive process is extracted out by high pressure positive blower, remove dust wherein through fly-ash separator, by a condenser, it is carried out to condensation again, the liquid phase oil water mixture obtaining flows to gravitational settler and water-and-oil separator, Separation and Recovery oil and water, noncondensable gas, through the processing of UV high-efficient gas purifier, is discharged in atmosphere.
The solid phase residue that said process is obtained is chosen 3 sample spot and is sampled respectively detection, result following (mass percent):
| Test item | Sample 1 | Sample 2 | Sample 3 |
| Solid content/% | 99.92 | 99.88 | 99.93 |
| Water ratio/% | 0 | 0 | 0 |
| Oil length/% | 0.08 | 0.12 | 0.07 |
Embodiment 6
Treatment unit described in employing embodiment 1 carries out the industrial treatment of oil waste.By 1000kg well drilling detritus, (water ratio is 19%, oil length is 7%) enter paddle-dryer by hopper through gas lock, high-temperature steam (vapor temperature is 160 DEG C, and pressure is 0.6MPa, and flow the is 120kg/hr) preheating material that utilizes steam boiler to produce, tentatively remove volatile constituent wherein, the gas evaporating is extracted out by high pressure positive blower, and cavity pressure is-170～-200Pa, and oxygen level is in 7% left and right, this process continues 1 hour, and material outlet temperature is 92 DEG C.
Landwaste through preheating and drying enters microwave heating chamber by gas lock, arrives the feed end of blade transfer roller, and in this process, temperature is down to 63 DEG C, and regulating the rotating speed of central shaft is 1 rev/min.Two microwave generators are exported the microwave of 110kw altogether, be transferred in microwave heating chamber by Bragg Transducer for Waveguide Devices, material is heated, make its water containing and hydro carbons evaporation, depart from material, and extracted out outside cavity by high pressure positive blower in time, cavity internal pressure is-170～-200Pa, oxygen level is in 7% left and right, this process continues 60 minutes, and material outlet temperature is 222 DEG C.When the solid phase residue that completes pyrolysis absorption is transported to the discharge end of heating chamber, arrive the discharging spiral in downstream by gas lock, carry out gradually discharge, final material is dropped in discharge bin, carries out accumulating.
In this process, use boiler exhaust gas (main component is carbonic acid gas) to be filled with drying machine and microwave heating chamber, to control its oxygen level.
The gas producing in dry and thermal desorption additive process is extracted out by high pressure positive blower, remove dust wherein through fly-ash separator, by a condenser, it is carried out to condensation again, the liquid phase oil water mixture obtaining flows to gravitational settler and water-and-oil separator, Separation and Recovery oil and water, noncondensable gas, through the processing of UV high-efficient gas purifier, is discharged in atmosphere.
The solid phase residue that said process is obtained is chosen 3 sample spot and is sampled respectively detection, result following (mass percent):
| Test item | Sample 1 | Sample 2 | Sample 3 |
| Solid content/% | 99.52 | 99.68 | 99.65 |
| Water ratio/% | 0 | 0 | 0 |
| Oil length/% | 0.48 | 0.32 | 0.35 |
Embodiment 7
Treatment unit described in employing embodiment 1 carries out the industrial treatment of oil waste.
By 1000kg well drilling detritus, (water ratio is 17%, oil length is 7%) enter paddle-dryer by hopper through gas lock, high-temperature steam (vapor temperature is 160 DEG C, and pressure is 0.6MPa, and flow the is 120kg/hr) preheating material that utilizes steam boiler to produce, tentatively remove volatile constituent wherein, the gas evaporating is extracted out by high pressure positive blower, and cavity pressure is-170～-200Pa, and oxygen level is in 7% left and right, this process continues 1 hour, and material outlet temperature is 90 DEG C.
Landwaste through preheating and drying enters microwave heating chamber by gas lock, arrives the feed end of blade transfer roller, and in this process, temperature is down to 62 DEG C, and regulating the rotating speed of central shaft is 1 rev/min.Two microwave generators are exported the microwave of 120kw altogether, be transferred in microwave heating chamber by Bragg Transducer for Waveguide Devices, material is heated, make its water containing and hydro carbons evaporation, depart from material, and extracted out outside cavity by high pressure positive blower in time, cavity internal pressure is-170～-200Pa, oxygen level is in 7% left and right, this process continues 60 minutes, and material outlet temperature is 245 DEG C.When the solid phase residue that completes pyrolysis absorption is transported to the discharge end of heating chamber, arrive the discharging spiral in downstream by gas lock, carry out gradually discharge, final material is dropped in discharge bin, carries out accumulating.
In this process, use boiler exhaust gas (main component is carbonic acid gas) to be filled with drying machine and microwave heating chamber, to control its oxygen level.
The gas producing in dry and thermal desorption additive process is extracted out by high pressure positive blower, remove dust wherein through fly-ash separator, by a condenser, it is carried out to condensation again, the liquid phase oil water mixture obtaining flows to gravitational settler and water-and-oil separator, Separation and Recovery oil and water, noncondensable gas, through the processing of UV high-efficient gas purifier, is discharged in atmosphere.
The solid phase residue that said process is obtained is chosen 3 sample spot and is sampled respectively detection, result following (mass percent):
| Test item | Sample 1 | Sample 2 | Sample 3 |
| Solid content/% | 99.85 | 99.82 | 99.77 |
| Water ratio/% | 0 | 0 | 0 |
| Oil length/% | 0.15 | 0.18 | 0.23 |
The explanation of above embodiment is only for helping to understand method of the present invention and core concept thereof.It should be pointed out that for those skilled in the art, under the premise without departing from the principles of the invention, can also carry out some improvement and modification to the present invention, these improvement and modification also fall in the protection domain of the claims in the present invention.
To the above-mentioned explanation of the disclosed embodiments, make professional and technical personnel in the field can realize or use the present invention.To be apparent for those skilled in the art to the multiple amendment of these embodiment, General Principle as defined herein can, in the situation that not departing from the spirit or scope of the present invention, realize in other embodiments.Therefore, the present invention will can not be restricted to these embodiment shown in this article, but will meet the widest scope consistent with principle disclosed herein and features of novelty.
Claims (10)
1. the industrial treatment method of oil field waste, comprises the following steps:
(A) oil field waste is carried out after sampling analysis, use steam heating or heat-conducting oil heating that oil field waste is preheated to 80～300 DEG C, obtain pre-treatment solid product and gas, described gas is through condensation separation and purifying treatment, recovery obtains water, oil and noncondensable gas, and the oil of described recovery and noncondensable gas are for the fuel of steam heating or heat-conducting oil heating;
(B) described pre-treatment solid product is carried out to microwave-heating processing, control pressure is-5000～-100Pa, obtains total petroleum hydrocarbons content lower than 3% solids treatment thing and gas;
Described gas, through condensation separation and purifying treatment, reclaims and obtains water and oil, and the oil of described recovery is for the fuel of steam heating or heat-conducting oil heating.
2. treatment process according to claim 1, is characterized in that, in described step (A), controls oxygen level lower than 7% when described preheating.
3. treatment process according to claim 1, is characterized in that, described step (B) also comprises described solids treatment thing is sprayed to rewetting or solidification treatment.
4. treatment process according to claim 1, is characterized in that, in described step (B), when described microwave-heating is processed, controls oxygen level lower than 7%.
5. the industrial treatment device of oil field waste, comprising:
Hopper, drying machine, microwave heating chamber, microwave generator, heating unit and condensation separation refining plant;
Described hopper is connected with the feed end of drying machine;
The discharge end of described drying machine is connected with the feed end of described microwave heating chamber;
Described heating unit is steam boiler or heat conducting oil boiler, and the vapour outlet of described heating unit or thermal oil outlet are connected with steam inlet or the heat conductive oil inlet of drying machine;
The pneumatic outlet of described drying machine and the pneumatic outlet of microwave heating chamber are all connected with condensation separation refining plant;
Described microwave generator is connected with microwave heating chamber.
6. device according to claim 5, is characterized in that, also comprises gas lock or feeding device; Described feeding device is feed auger and the rotary unloading device connecting successively, is connected or feeding device connects between the feed end of described hopper and drying machine by gas lock.
7. device according to claim 5, is characterized in that, also comprises discharging spiral, and described discharging spiral is connected with microwave heating chamber discharge end.
8. device according to claim 6, it is characterized in that, described discharging shaped spiral housing is outside equipped with the first recirculated water chuck, and described feed auger housing is outside equipped with the second recirculated water chuck, between described the first recirculated water chuck and the second recirculated water chuck, is connected with hot water line by cold water pipeline.
9. according to the device described in claim 5～8 any one, it is characterized in that, described condensation separation refining plant comprises fly-ash separator, condenser, blower fan, waste gas purification apparatus, gravitational settler, water-and-oil separator;
Connecting order is that fly-ash separator is connected with condenser, and the pneumatic outlet of condenser is connected with waste gas purification apparatus by blower fan; The liquid exit of condenser is connected with gravitational settler; The water outlet of gravitational settler is connected with water-and-oil separator.
10. according to the device described in claim 5～8 any one, it is characterized in that, the tail gas outlet of described heating unit is connected with the noble gas import of drying machine or microwave heating chamber.
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| PCT/CN2014/076479 WO2015158016A1 (en) | 2014-04-17 | 2014-04-29 | Industrial treatment method and device for oil field wastes |
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Also Published As
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|---|---|
| CN103923670B (en) | 2016-04-20 |
| WO2015158016A1 (en) | 2015-10-22 |
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Effective date of registration: 20161101 Address after: 264000 Jerry Road, Laishan District, Shandong, Yantai, China, 9 Patentee after: RUIJIE ENVIRONMENTAL PROTECTION TECHNOLOGY CO., LTD. Address before: 264003 AUCMA Avenue, Shandong, Yantai, No. 7 Patentee before: Jereh Energy Services Co., Ltd. |