CN103911889A - Compound level dyeing assistant for textile, and preparation method thereof - Google Patents
Compound level dyeing assistant for textile, and preparation method thereof Download PDFInfo
- Publication number
- CN103911889A CN103911889A CN201310680931.6A CN201310680931A CN103911889A CN 103911889 A CN103911889 A CN 103911889A CN 201310680931 A CN201310680931 A CN 201310680931A CN 103911889 A CN103911889 A CN 103911889A
- Authority
- CN
- China
- Prior art keywords
- level dyeing
- compound level
- dyeing assistant
- polyvinylpyrrolidone
- auxiliary agent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000004043 dyeing Methods 0.000 title claims abstract description 40
- 150000001875 compounds Chemical class 0.000 title claims abstract description 28
- 238000002360 preparation method Methods 0.000 title claims abstract description 7
- 239000004753 textile Substances 0.000 title abstract description 5
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims abstract description 44
- 229920002717 polyvinylpyridine Polymers 0.000 claims abstract description 15
- 229920000036 polyvinylpyrrolidone Polymers 0.000 claims abstract description 15
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 claims abstract description 15
- 239000001267 polyvinylpyrrolidone Substances 0.000 claims abstract description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 15
- 239000012752 auxiliary agent Substances 0.000 claims description 19
- 238000009941 weaving Methods 0.000 claims description 18
- OZCXMZAXJKGAIW-UHFFFAOYSA-N 1-ethylperoxybutane Chemical compound CCCCOOCC OZCXMZAXJKGAIW-UHFFFAOYSA-N 0.000 claims description 14
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims description 14
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 14
- VAKMIIPDYZXBEV-DPMBMXLASA-M potassium;(z,12r)-12-hydroxyoctadec-9-enoate Chemical compound [K+].CCCCCC[C@@H](O)C\C=C/CCCCCCCC([O-])=O VAKMIIPDYZXBEV-DPMBMXLASA-M 0.000 claims description 14
- 229910052708 sodium Inorganic materials 0.000 claims description 14
- 239000011734 sodium Substances 0.000 claims description 14
- 239000000047 product Substances 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 6
- 239000012467 final product Substances 0.000 claims description 3
- 239000000975 dye Substances 0.000 abstract description 13
- 238000013508 migration Methods 0.000 abstract description 3
- 230000005012 migration Effects 0.000 abstract description 3
- 230000009286 beneficial effect Effects 0.000 abstract description 2
- 239000003792 electrolyte Substances 0.000 abstract description 2
- POAOYUHQDCAZBD-UHFFFAOYSA-N 2-butoxyethanol Chemical compound CCCCOCCO POAOYUHQDCAZBD-UHFFFAOYSA-N 0.000 abstract 1
- PLUHAVSIMCXBEX-UHFFFAOYSA-N azane;dodecyl benzenesulfonate Chemical compound N.CCCCCCCCCCCCOS(=O)(=O)C1=CC=CC=C1 PLUHAVSIMCXBEX-UHFFFAOYSA-N 0.000 abstract 1
- 238000005354 coacervation Methods 0.000 abstract 1
- LCRMGUFGEDUSOG-UHFFFAOYSA-N naphthalen-1-ylsulfonyloxymethyl naphthalene-1-sulfonate;sodium Chemical compound [Na].C1=CC=C2C(S(=O)(OCOS(=O)(=O)C=3C4=CC=CC=C4C=CC=3)=O)=CC=CC2=C1 LCRMGUFGEDUSOG-UHFFFAOYSA-N 0.000 abstract 1
- SJXYCCRUTIHMCE-GOXDOWKOSA-K tripotassium;(z)-12-hydroxyoctadec-9-enoate;propane-1,2,3-triol Chemical compound [K+].[K+].[K+].OCC(O)CO.CCCCCCC(O)C\C=C/CCCCCCCC([O-])=O.CCCCCCC(O)C\C=C/CCCCCCCC([O-])=O.CCCCCCC(O)C\C=C/CCCCCCCC([O-])=O SJXYCCRUTIHMCE-GOXDOWKOSA-K 0.000 abstract 1
- 230000000694 effects Effects 0.000 description 5
- 239000000835 fiber Substances 0.000 description 5
- 238000000034 method Methods 0.000 description 4
- 239000003795 chemical substances by application Substances 0.000 description 3
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 239000000986 disperse dye Substances 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 229920002635 polyurethane Polymers 0.000 description 1
- 239000004814 polyurethane Substances 0.000 description 1
- 238000002203 pretreatment Methods 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 238000010186 staining Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
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- Coloring (AREA)
Abstract
The invention discloses a compound level dyeing assistant for textile, and a preparation method thereof. The compound level dyeing assistant for the textile is composed of the following components by weight: 1-3 parts of polyvinyl pyridine, 2-6 parts of polyvinylpyrrolidone, 1-3 parts of hydroxyethyl butyl ether, 0.4-0.8 part of ammonium dodecylbenzene sulfonate, 0.3-0.6 part of potassium castorate, 0.1-0.3 part of sodium methylene dinaphthalene sulfonate, 10-20 parts of isopropanol and 12-18 parts of water. Compared with a conventional level dyeing assistant, the compound level dyeing assistant provided by the invention has the following beneficial effects that (1) the compound level dyeing assistant has excellent dispersibility for dispersing dyes; (2) the compound level dyeing assistant makes the dyes not occur coacervation; (3) the compound level dyeing assistant has small foamability; (4) the compound level dyeing assistant has excellent migration performance; (5) the compound level dyeing assistant has no achromatic property; and (6) the compound level dyeing assistant has relatively good electrolyte resistance.
Description
Technical field
The invention belongs to textile auxiliary technical field, more specifically relate to the compound level dyeing auxiliary agent of a kind of weaving.
Background technology
In textile dyeing, there will be barriness and specking, quality frequent and fiber itself has close relationship, is because physics, the chemical constitution of fiber are inhomogeneous on the one hand; Be on the other hand due to dyeing pre-treatment and dyeing condition improper due to.
The method of level dyeing is a lot, and their object is: 1, make dye molecule be evenly distributed on fiber surface; 2, the dyestuff that makes to be distributed on fiber surface spreads to fibrous inside.Can be by controlling dyeing kinetics, control the concentration of dye bath and temperature evenly, with the good dyestuff of migration property, realize above-mentioned purpose with moving the measure such as stain and carrier, high-temp dyeing for a long time.
Although rely on superb staining technique, strict careful operation, sometimes can obtain uniform Color, be not often that very safe, the most simple and easy to do method still adds levelling agent.
Condition as levelling agent is: 1, can make dyestuff lentamente by fibers adsorption (having the slow effect of dying); If 2 dye inhomogeneously, can make the dyestuff of dark part move (thering is the effect of dying that moves) to light-colored part; 3, do not reduce dyefastness.So every have the slow auxiliary agent dying and move the effect of dying and be called levelling agent.
Chinese patent CN201110338076.1 discloses a kind of organic silicon modified polyurethane level dyeing softener, this level dyeing softener has certain even dyeing effect, but owing to trying to achieve merely even dyeing effect, thereby the dyestuff pulling down from fabric is remained in dye bath in a large number, cause the colourity that dyeing is uneconomical and increase was dyeed in residual night.
Summary of the invention
The object of the invention is to overcome the deficiency that prior art exists, provide a kind of weaving compound level dyeing auxiliary agent.
Another object of the present invention is to provide the preparation method of this weaving with compound level dyeing auxiliary agent.
For achieving the above object, the present invention has taked following technical scheme:
A kind of compound level dyeing auxiliary agent for weaving, in weight portion, composed of the following components:
Polyvinyl pyridine: 1～3, polyvinylpyrrolidone: 2～6,
Ethoxy butyl ether: 1～3, DBSA ammonium: 0.4～0.8,
Potassium ricinoleate: 0.3～0.6, sodium metnylene bis-naphthalene sulfonate: 0.1～0.3,
Isopropyl alcohol: 10～20, water: 12～18.
As preferably, described one compound level dyeing auxiliary agent for weaving, in weight portion, composed of the following components:
Polyvinyl pyridine: 1, polyvinylpyrrolidone: 2, ethoxy butyl ether: 1,
DBSA ammonium: 0.4, potassium ricinoleate: 0.3,
Sodium metnylene bis-naphthalene sulfonate: 0.1, isopropyl alcohol: 10, water: 12.
As preferably, described one compound level dyeing auxiliary agent for weaving, in weight portion, composed of the following components:
Polyvinyl pyridine: 3, polyvinylpyrrolidone: 6, ethoxy butyl ether: 3,
DBSA ammonium: 0.8, potassium ricinoleate: 0.6,
Sodium metnylene bis-naphthalene sulfonate: 0.3, isopropyl alcohol: 20, water: 18.
As preferably, described one compound level dyeing auxiliary agent for weaving, in weight portion, composed of the following components:
Polyvinyl pyridine: 2, polyvinylpyrrolidone: 4, ethoxy butyl ether: 2,
DBSA ammonium: 0.6, potassium ricinoleate: 0.5,
Sodium metnylene bis-naphthalene sulfonate: 0.2, isopropyl alcohol: 16, water: 15.
In technique scheme, described a kind of weaving by the preparation method of compound level dyeing auxiliary agent, comprises following technical step:
(1) by proportioning, polyvinyl pyridine, polyvinylpyrrolidone, ethoxy butyl ether and isopropyl alcohol are mixed, be heated to 30～50 ℃, dispersed with stirring is even;
(2) by soluble in water to DBSA ammonium, potassium ricinoleate and sodium metnylene bis-naphthalene sulfonate, be uniformly dispersed;
(3) product of step (1) and step (2) is mixed, stir, be down to room temperature and get final product to obtain finished product.
Compared with prior art, the present invention has following beneficial effect:
(1) DISPERSE DYES is had to good dispersiveness;
(2) in dye bath, do not make dyestuff generation cohesion;
(3) foaming characteristic is little;
(4) there is good migration property energy;
(5) do not sell look;
(6) there is good electrolyte-resistant performance.
The specific embodiment
Below in conjunction with specific embodiment, the invention will be further described, but the present invention's scope required for protection is not limited to the scope cited with embodiment.
Embodiment 1
A kind of compound level dyeing auxiliary agent for weaving, in weight portion, composed of the following components:
Polyvinyl pyridine: 1, polyvinylpyrrolidone: 2, ethoxy butyl ether: 1,
DBSA ammonium: 0.4, potassium ricinoleate: 0.3,
Sodium metnylene bis-naphthalene sulfonate: 0.1, isopropyl alcohol: 10, water: 12.
Embodiment 2
A kind of compound level dyeing auxiliary agent for weaving, in weight portion, composed of the following components:
Polyvinyl pyridine: 3, polyvinylpyrrolidone: 6, ethoxy butyl ether: 3,
DBSA ammonium: 0.8, potassium ricinoleate: 0.6,
Sodium metnylene bis-naphthalene sulfonate: 0.3, isopropyl alcohol: 20, water: 18.
Embodiment 3
A kind of compound level dyeing auxiliary agent for weaving, in weight portion, composed of the following components:
Polyvinyl pyridine: 2, polyvinylpyrrolidone: 4, ethoxy butyl ether: 2,
DBSA ammonium: 0.6, potassium ricinoleate: 0.5,
Sodium metnylene bis-naphthalene sulfonate: 0.2, isopropyl alcohol: 16, water: 15.
In above-described embodiment, described a kind of weaving by the preparation method of compound level dyeing auxiliary agent, comprises following technical step:
(1) by proportioning, polyvinyl pyridine, polyvinylpyrrolidone, ethoxy butyl ether and isopropyl alcohol are mixed, be heated to 30～50 ℃, dispersed with stirring is even;
(2) by soluble in water to DBSA ammonium, potassium ricinoleate and sodium metnylene bis-naphthalene sulfonate, be uniformly dispersed;
(3) product of step (1) and step (2) is mixed, stir, be down to room temperature and get final product to obtain finished product.
Claims (5)
1. a compound level dyeing auxiliary agent for weaving, is characterized in that, in weight portion, composed of the following components:
Polyvinyl pyridine: 1～3, polyvinylpyrrolidone: 2～6,
Ethoxy butyl ether: 1～3, DBSA ammonium: 0.4～0.8,
Potassium ricinoleate: 0.3～0.6, sodium metnylene bis-naphthalene sulfonate: 0.1～0.3,
Isopropyl alcohol: 10～20, water: 12～18.
2. a kind of weaving according to claim 1, with compound level dyeing auxiliary agent, is characterized in that, in weight portion, composed of the following components:
Polyvinyl pyridine: 1, polyvinylpyrrolidone: 2, ethoxy butyl ether: 1,
DBSA ammonium: 0.4, potassium ricinoleate: 0.3,
Sodium metnylene bis-naphthalene sulfonate: 0.1, isopropyl alcohol: 10, water: 12.
3. a kind of weaving according to claim 1, with compound level dyeing auxiliary agent, is characterized in that, in weight portion, composed of the following components:
Polyvinyl pyridine: 3, polyvinylpyrrolidone: 6, ethoxy butyl ether: 3,
DBSA ammonium: 0.8, potassium ricinoleate: 0.6,
Sodium metnylene bis-naphthalene sulfonate: 0.3, isopropyl alcohol: 20, water: 18.
4. a kind of weaving according to claim 1, with compound level dyeing auxiliary agent, is characterized in that, in weight portion, composed of the following components:
Polyvinyl pyridine: 2, polyvinylpyrrolidone: 4, ethoxy butyl ether: 2,
DBSA ammonium: 0.6, potassium ricinoleate: 0.5,
Sodium metnylene bis-naphthalene sulfonate: 0.2, isopropyl alcohol: 16, water: 15.
5. a kind of weaving by the preparation method of compound level dyeing auxiliary agent claimed in claim 1, is characterized in that, comprises following technical step:
(1) by proportioning, polyvinyl pyridine, polyvinylpyrrolidone, ethoxy butyl ether and isopropyl alcohol are mixed, be heated to 30～50 ℃, dispersed with stirring is even;
(2) by soluble in water to DBSA ammonium, potassium ricinoleate and sodium metnylene bis-naphthalene sulfonate, be uniformly dispersed;
(3) product of step (1) and step (2) is mixed, stir, be down to room temperature and get final product to obtain finished product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310680931.6A CN103911889B (en) | 2013-12-13 | 2013-12-13 | A kind of weaving compound Levelling assistants and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310680931.6A CN103911889B (en) | 2013-12-13 | 2013-12-13 | A kind of weaving compound Levelling assistants and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103911889A true CN103911889A (en) | 2014-07-09 |
| CN103911889B CN103911889B (en) | 2016-06-22 |
Family
ID=51037863
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310680931.6A Expired - Fee Related CN103911889B (en) | 2013-12-13 | 2013-12-13 | A kind of weaving compound Levelling assistants and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103911889B (en) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104313914A (en) * | 2014-10-25 | 2015-01-28 | 合肥市安山涂层织物有限公司 | Organic silicon penetrating agent for leather |
| CN104313909A (en) * | 2014-10-20 | 2015-01-28 | 江苏金牛华尔车服饰有限公司 | Coloring agent for textile fabric |
| CN105862469A (en) * | 2016-04-20 | 2016-08-17 | 吴江福汇缘家纺有限公司 | Textile printing and dyeing auxiliary agent and preparation method thereof |
| CN106012602A (en) * | 2016-05-22 | 2016-10-12 | 南通富之岛寝具发展有限公司 | Spinning dispersing agent containing polyoxyethylene lauryl ether sodium sulfate and dicyandiamide |
| CN106223070A (en) * | 2016-07-26 | 2016-12-14 | 萧县凯奇化工科技有限公司 | A kind of vat auxiliary agent |
| CN106320020A (en) * | 2016-08-16 | 2017-01-11 | 嘉兴华晟助剂工业有限公司 | High-performance environmental-friendly dyeing guide levelling agent composition and application thereof |
| CN107476090A (en) * | 2017-09-04 | 2017-12-15 | 句容躬行创客管理咨询有限公司 | A kind of environmental type printing and dyeing assistant and preparation method thereof |
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| WO2007042379A1 (en) * | 2005-10-07 | 2007-04-19 | Clariant International Ltd | Dyeing of polyamide fibres |
| CN102965983A (en) * | 2012-11-21 | 2013-03-13 | 吴江红蔷薇纺织有限公司 | Leveling agent used for fabric and preparation method thereof |
| CN103243582A (en) * | 2013-04-16 | 2013-08-14 | 杜芳莉 | Acidic levelling agent and preparation method thereof |
| CN103290705A (en) * | 2013-07-02 | 2013-09-11 | 江苏省海安石油化工厂 | High-temperature levelling agent |
| CN103321065A (en) * | 2013-06-07 | 2013-09-25 | 张家港市德宝化工有限公司 | High-temperature leveling agent, and preparation method and application thereof |
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2013
- 2013-12-13 CN CN201310680931.6A patent/CN103911889B/en not_active Expired - Fee Related
Patent Citations (5)
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|---|---|---|---|---|
| WO2007042379A1 (en) * | 2005-10-07 | 2007-04-19 | Clariant International Ltd | Dyeing of polyamide fibres |
| CN102965983A (en) * | 2012-11-21 | 2013-03-13 | 吴江红蔷薇纺织有限公司 | Leveling agent used for fabric and preparation method thereof |
| CN103243582A (en) * | 2013-04-16 | 2013-08-14 | 杜芳莉 | Acidic levelling agent and preparation method thereof |
| CN103321065A (en) * | 2013-06-07 | 2013-09-25 | 张家港市德宝化工有限公司 | High-temperature leveling agent, and preparation method and application thereof |
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Non-Patent Citations (1)
| Title |
|---|
| 张天胜主编: "《表面活性剂应用技术》", 30 September 2001, 化学工业出版社 * |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104313909A (en) * | 2014-10-20 | 2015-01-28 | 江苏金牛华尔车服饰有限公司 | Coloring agent for textile fabric |
| CN104313909B (en) * | 2014-10-20 | 2016-08-31 | 江苏金牛华尔车服饰有限公司 | Weaving face fabric stain |
| CN104313914A (en) * | 2014-10-25 | 2015-01-28 | 合肥市安山涂层织物有限公司 | Organic silicon penetrating agent for leather |
| CN105862469A (en) * | 2016-04-20 | 2016-08-17 | 吴江福汇缘家纺有限公司 | Textile printing and dyeing auxiliary agent and preparation method thereof |
| CN106012602A (en) * | 2016-05-22 | 2016-10-12 | 南通富之岛寝具发展有限公司 | Spinning dispersing agent containing polyoxyethylene lauryl ether sodium sulfate and dicyandiamide |
| CN106223070A (en) * | 2016-07-26 | 2016-12-14 | 萧县凯奇化工科技有限公司 | A kind of vat auxiliary agent |
| CN106320020A (en) * | 2016-08-16 | 2017-01-11 | 嘉兴华晟助剂工业有限公司 | High-performance environmental-friendly dyeing guide levelling agent composition and application thereof |
| CN107476090A (en) * | 2017-09-04 | 2017-12-15 | 句容躬行创客管理咨询有限公司 | A kind of environmental type printing and dyeing assistant and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103911889B (en) | 2016-06-22 |
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Inventor after: Zeng Zhaoxiong Inventor after: Zeng Rongbao Inventor before: Ye Weiran |
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Effective date of registration: 20160420 Address after: Room 41, building 5E 362200 Fujian city of Quanzhou province Jinjiang city streets Luoshan Lanxi City Garden Applicant after: QUANZHOU XINHONG CHEMICAL TRADE Co.,Ltd. Address before: 215228, No. 5, No. eight, 05 Business District of Dongfang silk market, Shengze Town, Wujiang District, Jiangsu, Suzhou Applicant before: SUZHOU FANGRAN TEXTILE Co.,Ltd. |
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Address after: 362200, Fujian, Quanzhou, Jinjiang Qingyang street Hongshan Industrial Zone Design Park, building 2, 7 floor Patentee after: QUANZHOU XINHONG COLOR INFORMATION TECHNOLOGY CO.,LTD. Address before: Room 41, building 5E 362200 Fujian city of Quanzhou province Jinjiang city streets Luoshan Lanxi City Garden Patentee before: QUANZHOU XINHONG CHEMICAL TRADE Co.,Ltd. |
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