CN104233880B - A kind of acrylic polyester blend fabric One Bath Dyeing Process - Google Patents
A kind of acrylic polyester blend fabric One Bath Dyeing Process Download PDFInfo
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- CN104233880B CN104233880B CN201410461407.4A CN201410461407A CN104233880B CN 104233880 B CN104233880 B CN 104233880B CN 201410461407 A CN201410461407 A CN 201410461407A CN 104233880 B CN104233880 B CN 104233880B
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Abstract
The invention discloses the dyeing of a kind of energy-saving and emission-reduction;Especially a kind of acrylic polyester blend fabric One Bath Dyeing Process;It is an object of the invention to provide a kind of production efficiency height, reduce production cost and a kind of acrylic polyester blend fabric One Bath Dyeing Process of energy-saving and emission-reduction;After being processed by pre-treatment degreaser and nonionic leveler, adjust the surface nature of fabric difference fiber, after adding the dispersant of nonionic, isolate the interaction of the anionic dispersing agent in the dye of positive ion and disperse dyes and emulsifying agent, realize one-bath dyeing method in such a situa-tion, therefore the effect of different stock-dye same hue, energy-saving and emission-reduction and raising production efficiency are reached.
Description
Technical field
The present invention relates to the dyeing of a kind of energy-saving and emission-reduction;Especially a kind of acrylic polyester blend fabric one
Bath method dyeing.
Background technology
The dyeing of multi-component fiber fabric, dyestuff distribution on each fiber and the phase interaction of staining and dyestuff
With all a lot of practical problem can be brought to dyeing, as higher to dyestuff selection requirements, the control of dyeing
Being more difficult to than Single Fiber, dyefastness reduces, color matching difficulty, it is difficult to contaminating homochromy, heterochromatic form and aspect are restricted,
Colour brightness reduces, and fibre property deteriorates.Therefore, not every multi-component fiber fabric can be carried out
One-bath dyeing.Such as the blend fabric of acrylon Yu terylene, owing to acrylon need with cationic dyeing, and
Terylene needs to use disperse dyeing, but containing anionic dispersing agent, emulsifying in general merchandise disperse dyes
Agent etc., can occur considerably complicated between same dye bath cationic dyestuff and anionic dispersing agents and emulsifying agent
Interaction, so the at present commonly used two-bath process of acrylic polyester blend fabric, but this dyer
The shortcoming such as skill exists water, electricity, vapour consumption is big, production efficiency is low and discharge of wastewater is big.
For problem above, it is badly in need of us and solves.
Summary of the invention
It is an object of the invention to overcome the deficiencies in the prior art, it is provided that a kind of production efficiency is high, reduce production
Cost and a kind of acrylic polyester blend fabric One Bath Dyeing Process of energy-saving and emission-reduction.
In order to achieve the above object, a kind of acrylic polyester blend fabric one-bath dyeing work designed by the present invention
Skill, step is as follows: the first step, pre-treatment: immerse acrylic polyester blend fabric containing 0.5~2g/L oil removing
In the aqueous solution of agent and 0.5~2g/L nonionic surfactant, and proportioning between the two is 1:1;And
Room temperature is to slowly warm up to 70~90 DEG C with 1~2.5 DEG C/min, is incubated 10~30 minutes, then room temperature with 1~
2.5 DEG C/min is slowly dropped to less than 70 DEG C, then discharges water;Second step, dyeing: (1), injection are containing 1~5g/L
The aqueous solution of non-ionic dispersing agent, impregnates the operating of acrylic polyester blend fabric 1~5 minute;(2), add
Enter 0.5~2g/L anion levelling agent and 0.5~2g/L glacial acetic acid, and proportioning between the two be 1:1,
The operating of acrylic polyester blend fabric is impregnated 1~5 minute;(3), disperse dyeing 1~5 minutes are added, so
After be to slowly warm up to 60~80 DEG C from room temperature with 1~2.5 DEG C/min, dye 5~20 minutes;(4), add 0.5~
5g/L cationic levelling agent, impregnates the operating of acrylic polyester blend fabric 5~15 minutes;(5), add sun from
Sub-dyestuff, dyes 2~10 minutes, and room temperature is to slowly warm up to 120~130 DEG C with 1~2.5 DEG C/min,
Being incubated 30~60 minutes, then room temperature discharges water to less than 70 DEG C with 1~2.5 DEG C/min slow cooling, more clearly
Water washs;3rd step, soaps: add 1~5g/L soaping agent aqueous solution, and room temperature is delayed with 1~2.5 DEG C/min
Slowly it is warming up to 60~80 DEG C, is incubated 20~30 minutes, discharges water, add 1 the most again~5g/L fatty acid amide sulphur
Acid sodium, room temperature is to slowly warm up to 60~80 DEG C with 1~2.5 DEG C/min, is incubated 20~30 minutes, discharges water,
Wash with clear water again;4th step, soft finish: add water, room temperature with 1~2.5 DEG C/min be warming up to 45~
60 DEG C, add 1~5g/L amino-silicone oil softening agent, be incubated 20~30 minutes, go out cylinder open-width removing the work, and
With 120~130 DEG C of sizings.
Wherein, the degreaser described in the first step is the mixture of fatty alcohol and polyoxyethylene ether.
Wherein, the nonionic surfactant described in the first step is the condensation substance of oxirane and alkylphenol.
Wherein, the aqueous solution of the non-ionic dispersing agent described in second step is sodium methylene bis-naphthalene sulfonate.
Wherein, the anion levelling agent described in second step is alkyl or aryl sulfonate.
Wherein, the cationic levelling agent described in second step is quaternary ammonium salt.
Wherein, the soaping agent aqueous solution described in the 3rd step is polyester polyethers cage construction high polymer.
A kind of acrylic polyester blend fabric One Bath Dyeing Process of gained of the present invention, by pre-treatment degreaser and
After nonionic leveler processes, adjust the surface nature of fabric difference fiber, add the dispersion of nonionic
After agent, isolate the interaction of the anionic dispersing agent in the dye of positive ion and disperse dyes and emulsifying agent,
Realize one-bath dyeing method in such a situa-tion, therefore reach the effect of different stock-dye same hue,
Energy-saving and emission-reduction and raising production efficiency.
A kind of acrylic polyester blend fabric One Bath Dyeing Process of gained of the present invention and current acrylic polyester blending
The Performance comparision of the commonly used two-bath process of fabric is as follows:
Type | One-bath dyeing | Two-bath process |
With quantity of steam (ton) | 20 | 40 |
Water consumption (ton) | 20 | 40 |
Power consumption (kilowatt) | 300 | 600 |
Dyeing time (hour) | 6 | 12 |
Detailed description of the invention
Embodiment 1:
A kind of acrylic polyester blend fabric One Bath Dyeing Process that the present embodiment describes, step is as follows:
The first step, pre-treatment: acrylic polyester blend fabric is immersed containing 1g/L fatty alcohol and polyoxyethylene ether
Mixture and 1g/L oxirane are with the aqueous solution of the condensation substance of alkylphenol, and room temperature is with 1.5 DEG C/min
Being to slowly warm up to 85 DEG C, be incubated 20 minutes, then room temperature is down to 70 DEG C with 1.5 DEG C/min, discharges water;The
Two steps, dyeing: (1), the injection aqueous solution containing 2g/L sodium methylene bis-naphthalene sulfonate, by acrylic polyester blending
Fabric operating dipping 3 minutes, (2), addition 1.5g/L sodium alkyl sulfonate and 0.5g/L glacial acetic acid, by acrylon
Polyester blended fabric operating dipping 5 minutes, (3), add disperse dyeing 5 minutes, then room temperature is with 1.5 DEG C
/ minute it is warming up to 65 DEG C, dye 10 minutes, (4), then adding that 1g/L Shanghai Ya Yun company is refined can even AR
Cationic levelling agent, by acrylic polyester blend fabric operating dipping 5 minutes, (5), add the dye of positive ion, dye
Color 5 minutes, room temperature is warming up to 128 DEG C with 1.5 DEG C/min, is incubated 30 minutes, then room temperature with 1 DEG C/
Minute it is cooled to less than 70 DEG C, discharges water, then clear water washing;3rd step, soaps: refined with 1.5g/L Shanghai
Company's T CW is refined matches soaping agent solution for fortune, and room temperature is warming up to 80 DEG C with 2 DEG C/min, is incubated 20 minutes,
Discharging water, add 2g/L fatty acid amide sodium sulfonate the most again, room temperature is warming up to 60 DEG C with 2 DEG C/min, is incubated 20
Minute, discharging water, then wash with clear water, the 4th step, soft finish: after adding water, room temperature is with 1.5 DEG C/min
It is warming up to 50 DEG C, adds 2g/L amino-silicone oil softening agent, be incubated 20 minutes, go out cylinder open-width removing the work, and with
130 DEG C of sizings.
Embodiment 2:
A kind of acrylic polyester blend fabric One Bath Dyeing Process that the present embodiment describes, step is as follows:
The first step, pre-treatment: acrylic polyester blend fabric is immersed containing 1.5g/L fatty alcohol and polyoxyethylene ether
Mixture and 1.5g/L oxirane and alkylphenol condensation substance aqueous solution in, room temperature is with 2 DEG C/minute
Clock is to slowly warm up to 80 DEG C, is incubated 15 minutes, and then room temperature is down to 65 DEG C with 2 DEG C/min, discharges water;The
Two steps, dyeing: (1), the injection aqueous solution containing 3g/L sodium methylene bis-naphthalene sulfonate, by acrylic polyester blending
Fabric operating dipping 3 minutes, (2), addition 1.5g/L sodium alkyl sulfonate and 1g/L glacial acetic acid, acrylon are washed
Synthetic fibre blend fabric operating dipping 3 minutes, (3), add disperse dyeing 7 minutes, then room temperature with 2 DEG C/
Minute it is warming up to 70 DEG C, dyes 15 minutes, (4), then adding that 2g/L Shanghai Ya Yun company is refined can even AR sun
Ion levelling agent, by acrylic polyester blend fabric operating dipping 10 minutes, (5), add the dye of positive ion, dye
Color 7 minutes, room temperature is warming up to 125 DEG C with 2 DEG C/min, is incubated 40 minutes, and then room temperature is with 2 DEG C/minute
Clock is cooled to 65 DEG C, discharges water, then clear water washing;3rd step, soaps: by 2g/L Shanghai refined fortune company's T CW
Ya Kesai soaping agent solution, room temperature is warming up to 70 DEG C with 2 DEG C/min, is incubated 15 minutes, discharges water, then
Adding 3g/L fatty acid amide sodium sulfonate again, room temperature is warming up to 70 DEG C with 2 DEG C/min, is incubated 15 minutes, discharges water,
Washing with clear water, the 4th step, soft finish: after adding water, room temperature is warming up to 55 DEG C with 2 DEG C/min, adds again
Enter 3g/L amino-silicone oil softening agent, be incubated 15 minutes, go out cylinder open-width removing the work, and with 120 DEG C of sizings.
Embodiment 3:
A kind of acrylic polyester blend fabric One Bath Dyeing Process that the present embodiment describes, step is as follows:
The first step, pre-treatment: acrylic polyester blend fabric is immersed containing 2g/L fatty alcohol and polyoxyethylene ether
Mixture and 2g/L oxirane are with the aqueous solution of the condensation substance of alkylphenol, and room temperature is with 2.5 DEG C/min
Being to slowly warm up to 90 DEG C, be incubated 25 minutes, then room temperature is down to 60 DEG C with 2.5 DEG C/min, discharges water;The
Two steps, dyeing: (1), the injection aqueous solution containing 4g/L sodium methylene bis-naphthalene sulfonate, by acrylic polyester blending
Fabric operating dipping 4 minutes, (2), addition 2g/L sodium alkyl sulfonate and 2g/L glacial acetic acid, by acrylic polyester
Blend fabric operating dipping 2 minutes, (3), add disperse dyeing 7 minutes, then room temperature with 2.5 DEG C/
Minute it is warming up to 75 DEG C, dyes 15 minutes, (4), then adding that 3g/L Shanghai Ya Yun company is refined can even AR sun
Ion levelling agent, by acrylic polyester blend fabric operating dipping 15 minutes, (5), add the dye of positive ion, dye
Color 10 minutes, room temperature is warming up to 130 DEG C with 2.5 DEG C/min, is incubated 50 minutes, and then room temperature is with 2.5 DEG C
/ minute it is cooled to 60 DEG C, discharge water, then clear water washing;3rd step, soaps: with 3g/L Shanghai Ya Yun company
TCW is refined matches soaping agent solution, and room temperature is warming up to 75 DEG C with 2.5 DEG C/min, is incubated 15 minutes, discharges water,
Adding 4g/L fatty acid amide sodium sulfonate the most again, room temperature is warming up to 80 DEG C with 2.5 DEG C/min, is incubated 30 minutes,
Discharging water, then wash with clear water, the 4th step, soft finish: after adding water, room temperature is warming up to 2.5 DEG C/min
60 DEG C, add 4g/L amino-silicone oil softening agent, be incubated 30 minutes, go out cylinder open-width removing the work, and with 125 DEG C
Sizing.
Claims (7)
1. an acrylic polyester blend fabric One Bath Dyeing Process, it is characterised in that: the first step, pre-treatment:
Acrylic polyester blend fabric is immersed containing 0.5~2g/L degreaser and 0.5~2g/L nonionic surfactant
Aqueous solution in, and proportioning between the two is 1:1;And room temperature is to slowly warm up to 1~2.5 DEG C/min
70~90 DEG C, being incubated 10~30 minutes, then room temperature is slowly dropped to less than 70 DEG C with 1~2.5 DEG C/min,
Discharge water again;Second step, dyeing: (1), the injection aqueous solution containing 1~5g/L non-ionic dispersing agent, will
Acrylic polyester blend fabric operating dipping 1~5 minute;(2), add 0.5~2g/L anion levelling agent and
0.5~2g/L glacial acetic acid, and proportioning between the two is 1:1, by acrylic polyester blend fabric operating dipping
1~5 minute;(3), add disperse dyeing 1~5 minutes, then delay with 1~2.5 DEG C/min from room temperature
Slowly it is warming up to 60~80 DEG C, dyes 5~20 minutes;(4), add 0.5~5g/L cationic levelling agent, will
Acrylic polyester blend fabric operating dipping 5~15 minutes;(5), add the dye of positive ion, dye 2~10 minutes,
And room temperature is to slowly warm up to 120~130 DEG C with 1~2.5 DEG C/min, it is incubated 30~60 minutes, then room temperature
Discharge water to less than 70 DEG C with 1~2.5 DEG C/min slow cooling, then clear water washing;3rd step, soaps: add 1~
5g/L soaping agent aqueous solution, room temperature is to slowly warm up to 60~80 DEG C with 1~2.5 DEG C/min, is incubated 20~30
Minute, discharging water, add 1 the most again~5g/L fatty acid amide sodium sulfonate, room temperature slowly rises with 1~2.5 DEG C/min
Temperature, to 60~80 DEG C, is incubated 20~30 minutes, discharges water, then wash with clear water;4th step, soft finish:
Adding water, room temperature is warming up to 45~60 DEG C with 1~2.5 DEG C/min, adds 1~5g/L amino-silicone oil softening agent,
It is incubated 20~30 minutes, goes out cylinder open-width removing the work, and with 120~130 DEG C of sizings.
A kind of acrylic polyester blend fabric One Bath Dyeing Process the most according to claim 1, its feature
It is: the degreaser described in the first step is the mixture of fatty alcohol and polyoxyethylene ether.
A kind of acrylic polyester blend fabric One Bath Dyeing Process the most according to claim 1, its feature
It is: the nonionic surfactant described in the first step is the condensation substance of oxirane and alkylphenol.
A kind of acrylic polyester blend fabric One Bath Dyeing Process the most according to claim 1, its feature
It is: the aqueous solution of the non-ionic dispersing agent described in second step is sodium methylene bis-naphthalene sulfonate.
A kind of acrylic polyester blend fabric One Bath Dyeing Process the most according to claim 1, its feature
It is: the anion levelling agent described in second step is alkyl or aryl sulfonate.
A kind of acrylic polyester blend fabric One Bath Dyeing Process the most according to claim 1, its feature
It is: the cationic levelling agent described in second step is quaternary ammonium salt.
A kind of acrylic polyester blend fabric One Bath Dyeing Process the most according to claim 1, its feature
It is: the soaping agent aqueous solution described in the 3rd step is polyester polyethers cage construction high polymer.
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CN201410461407.4A CN104233880B (en) | 2014-09-12 | 2014-09-12 | A kind of acrylic polyester blend fabric One Bath Dyeing Process |
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Cited By (1)
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DE2658063C2 (en) * | 1976-12-22 | 1978-09-07 | Hoechst Ag, 6000 Frankfurt | Process for dyeing blended fabrics made from modified polyester fibers and wool |
CN1538004A (en) * | 2003-10-23 | 2004-10-20 | 张永成 | Bath method of dyeing |
CN101845760B (en) * | 2010-05-28 | 2012-02-29 | 东莞贰发毛绒有限公司 | One-bath dyeing process for flocked fabric by hybrid flocking of nylon and acrylon |
CN101899788B (en) * | 2010-08-19 | 2012-11-21 | 中国纺织科学研究院 | One-bath dyeing method of modified polyester/wool blended fabric |
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CN107938391A (en) * | 2017-12-01 | 2018-04-20 | 山东黄河三角洲纺织科技研究院有限公司 | A kind of flax fiber colouring method |
CN107938391B (en) * | 2017-12-01 | 2020-10-30 | 山东黄河三角洲纺织科技研究院有限公司 | Flax fiber dyeing method |
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