CN103906755B - 纯化方法 - Google Patents
纯化方法 Download PDFInfo
- Publication number
- CN103906755B CN103906755B CN201280044051.3A CN201280044051A CN103906755B CN 103906755 B CN103906755 B CN 103906755B CN 201280044051 A CN201280044051 A CN 201280044051A CN 103906755 B CN103906755 B CN 103906755B
- Authority
- CN
- China
- Prior art keywords
- acid
- solvent
- ligand
- complexing agent
- phenanthroline
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/547—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
- C07F9/6564—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms
- C07F9/6571—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms having phosphorus and oxygen atoms as the only ring hetero atoms
- C07F9/6574—Esters of oxyacids of phosphorus
- C07F9/65746—Esters of oxyacids of phosphorus the molecule containing more than one cyclic phosphorus atom
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2231/00—Catalytic reactions performed with catalysts classified in B01J31/00
- B01J2231/30—Addition reactions at carbon centres, i.e. to either C-C or C-X multiple bonds
- B01J2231/32—Addition reactions to C=C or C-C triple bonds
- B01J2231/321—Hydroformylation, metalformylation, carbonylation or hydroaminomethylation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
- B01J31/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
- B01J31/18—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes containing nitrogen, phosphorus, arsenic or antimony as complexing atoms, e.g. in pyridine ligands, or in resonance therewith, e.g. in isocyanide ligands C=N-R or as complexed central atoms
- B01J31/1845—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes containing nitrogen, phosphorus, arsenic or antimony as complexing atoms, e.g. in pyridine ligands, or in resonance therewith, e.g. in isocyanide ligands C=N-R or as complexed central atoms the ligands containing phosphorus
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
- Treating Waste Gases (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201161541291P | 2011-09-30 | 2011-09-30 | |
| US61/541,291 | 2011-09-30 | ||
| PCT/US2012/054197 WO2013048701A1 (en) | 2011-09-30 | 2012-09-07 | Purification process |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103906755A CN103906755A (zh) | 2014-07-02 |
| CN103906755B true CN103906755B (zh) | 2018-02-27 |
Family
ID=46940590
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201280044051.3A Active CN103906755B (zh) | 2011-09-30 | 2012-09-07 | 纯化方法 |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US9428529B2 (enExample) |
| EP (1) | EP2751122B1 (enExample) |
| JP (1) | JP6068482B2 (enExample) |
| KR (1) | KR101987513B1 (enExample) |
| CN (1) | CN103906755B (enExample) |
| IN (1) | IN2014CN02246A (enExample) |
| TW (1) | TWI628001B (enExample) |
| WO (1) | WO2013048701A1 (enExample) |
| ZA (1) | ZA201401261B (enExample) |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3706822A (en) * | 1969-10-02 | 1972-12-19 | James E Caldwell | Method of refining esters of organophosphorus |
| US4143075A (en) * | 1976-08-12 | 1979-03-06 | Union Carbide Corporation | Control of condensation products in hydroformylation process |
| US4276235A (en) * | 1980-04-24 | 1981-06-30 | The United States Of America As Represented By The United States Department Of Energy | Method for purifying bidentate organophosphorous compounds |
| CN101307072A (zh) * | 2001-02-08 | 2008-11-19 | 旭瑞达有限公司 | 提纯磷酸酯的方法 |
| CN101981041A (zh) * | 2008-03-28 | 2011-02-23 | 陶氏环球技术公司 | 用于单次氯酸化膦合成的等温方法 |
Family Cites Families (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3527809A (en) * | 1967-08-03 | 1970-09-08 | Union Carbide Corp | Hydroformylation process |
| US4283562A (en) | 1979-10-26 | 1981-08-11 | Union Carbide Corporation | Hydroformylation process using stable rhodium catalyst |
| US4400548A (en) | 1981-08-17 | 1983-08-23 | Union Carbide Corporation | Hydroformylation process using bisphosphine monooxide ligands |
| US4789753A (en) | 1984-02-17 | 1988-12-06 | Union Carbide Corporation | Phosphite ligands |
| US4599206A (en) | 1984-02-17 | 1986-07-08 | Union Carbide Corporation | Transition metal complex catalyzed reactions |
| US4668651A (en) | 1985-09-05 | 1987-05-26 | Union Carbide Corporation | Transition metal complex catalyzed processes |
| US4748261A (en) * | 1985-09-05 | 1988-05-31 | Union Carbide Corporation | Bis-phosphite compounds |
| US4716250A (en) * | 1986-07-10 | 1987-12-29 | Union Carbide Corporation | Hydroformylation using low volatile/organic soluble phosphine ligands |
| US4845306A (en) * | 1987-04-24 | 1989-07-04 | Eastman Kodak Company | Catalyst material recovery or concentration process |
| TW213465B (enExample) | 1991-06-11 | 1993-09-21 | Mitsubishi Chemicals Co Ltd | |
| KR960007736B1 (ko) * | 1993-07-27 | 1996-06-11 | 한국과학기술연구원 | 원료 가스 중에 함유된 철 카르보닐 화합물의 제거 방법 |
| US5710344A (en) | 1996-11-08 | 1998-01-20 | E. I. Du Pont De Nemours And Company | Process to prepare a linear aldehyde |
| US6265620B1 (en) | 1997-03-27 | 2001-07-24 | Mitsubishi Chemical Corporation | Process for producing aldehydes |
| US6548708B1 (en) * | 1998-08-05 | 2003-04-15 | Sri International | Preparation of biphosphine ligands for incorporation into catalytic complexes |
| DE10005084C1 (de) * | 2000-02-04 | 2001-09-13 | Celanese Chem Europe Gmbh | Verfahren zur Wiedergewinnung von Rhodium aus Reaktionsprodukten der Oxosynthese |
| US7872156B2 (en) | 2007-12-26 | 2011-01-18 | Eastman Chemical Company | Fluorophosphite containing catalysts for hydroformylation processes |
| CN102177171B (zh) * | 2008-10-08 | 2014-02-12 | 陶氏技术投资有限公司 | 合成二亚磷酸酯的淤浆方法 |
-
2012
- 2012-09-07 CN CN201280044051.3A patent/CN103906755B/zh active Active
- 2012-09-07 EP EP12766510.7A patent/EP2751122B1/en active Active
- 2012-09-07 IN IN2246CHN2014 patent/IN2014CN02246A/en unknown
- 2012-09-07 US US14/345,489 patent/US9428529B2/en active Active
- 2012-09-07 KR KR1020147011515A patent/KR101987513B1/ko active Active
- 2012-09-07 WO PCT/US2012/054197 patent/WO2013048701A1/en not_active Ceased
- 2012-09-07 JP JP2014533557A patent/JP6068482B2/ja active Active
- 2012-09-28 TW TW101135701A patent/TWI628001B/zh active
-
2014
- 2014-02-19 ZA ZA2014/01261A patent/ZA201401261B/en unknown
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3706822A (en) * | 1969-10-02 | 1972-12-19 | James E Caldwell | Method of refining esters of organophosphorus |
| US4143075A (en) * | 1976-08-12 | 1979-03-06 | Union Carbide Corporation | Control of condensation products in hydroformylation process |
| US4276235A (en) * | 1980-04-24 | 1981-06-30 | The United States Of America As Represented By The United States Department Of Energy | Method for purifying bidentate organophosphorous compounds |
| CN101307072A (zh) * | 2001-02-08 | 2008-11-19 | 旭瑞达有限公司 | 提纯磷酸酯的方法 |
| CN101981041A (zh) * | 2008-03-28 | 2011-02-23 | 陶氏环球技术公司 | 用于单次氯酸化膦合成的等温方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| KR20140090169A (ko) | 2014-07-16 |
| IN2014CN02246A (enExample) | 2015-06-12 |
| EP2751122B1 (en) | 2018-10-24 |
| JP6068482B2 (ja) | 2017-01-25 |
| US9428529B2 (en) | 2016-08-30 |
| TWI628001B (zh) | 2018-07-01 |
| KR101987513B1 (ko) | 2019-06-10 |
| ZA201401261B (en) | 2015-05-27 |
| EP2751122A1 (en) | 2014-07-09 |
| JP2014534179A (ja) | 2014-12-18 |
| WO2013048701A1 (en) | 2013-04-04 |
| TW201317053A (zh) | 2013-05-01 |
| US20150073169A1 (en) | 2015-03-12 |
| CN103906755A (zh) | 2014-07-02 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |