CN103897834A - Preparation method of household detergent - Google Patents
Preparation method of household detergent Download PDFInfo
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- CN103897834A CN103897834A CN201210582598.0A CN201210582598A CN103897834A CN 103897834 A CN103897834 A CN 103897834A CN 201210582598 A CN201210582598 A CN 201210582598A CN 103897834 A CN103897834 A CN 103897834A
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Abstract
The invention discloses a preparation method of a household detergent. The preparation method comprises the following steps: (1) adding the following raw materials (in parts by weight) of 25-30 parts of saccharose oleate, 30-35 parts of glycerinum and 1-3 parts of sodium chloride in a reaction kettle, mixing in an adding process at a mixing speed of 15-25 turns/min, heating in a mixing process at a mixing temperature of 45-65 DEG C; and standing a mixture after heating, and naturally cooling to a room temperature in a standing process for 35-45 min. The household detergent produced by adopting the preparation method disclosed by the invention is good in foaming property, capable of deeply cleaning tableware, high in activity of a surfactant, strong in deep detergency, less in residues, harmless to a human body, and suitable for being widely applied.
Description
Technical field
The preparation method who the present invention relates to a kind of household detergent, belongs to filed of daily-use chemical industry.
Background technology
Dish washing detergent is divided into detergent for washing dishware with hand and Dishwashing detergent for machine washing, the grease that can be used on clean tableware, the residues such as protein, till now, as detergent builder, an alkali metal salt of the known multipolymer that has polyacrylic acid, poly-methylene-succinic acid, vinylformic acid and toxilic acid etc., in general, mainly contain tensio-active agent, for example alkyl benzene sulphonate (ABS), alkyl-sulphate, fatty acid amide for the washing composition of tableware at home.But, although an alkali metal salt of poly-hydroxy acid can improve detersive power,, the problem poor with surfactant compatibility is not resolved always, so need now a kind of new preparation method, carry out production surfactant activity high, the household detergent that detersive power is good.
Summary of the invention
The deficiency existing for prior art, technical problem to be solved by this invention is, a kind of preparation method of household detergent is provided, surfactant activity is high, detersive power good, and with low cost.
For solving the problems of the technologies described above, the technical scheme that the present invention takes is that a kind of preparation method of household detergent, comprises the following steps:
(1) following material (calculating by weight) is added in reactor: Sugar Ester O 1570 25-30 part, glycerine 30-35 part, sodium-chlor 1-3 part, in adition process, stir, stirring velocity is 15-25 rev/min, in whipping process, heat, Heating temperature is 45-65 degree Celsius;
(2) after heating, mixture is left standstill, leave standstill in process, make mixture naturally be down to room temperature, time of repose is 35-45 minute;
(3) mixture after leaving standstill is filtered, after filtration, mixture is heated to Heating temperature 45-65 degree Celsius;
(4) after heating, mixture is left standstill, leave standstill in process, make mixture naturally be down to room temperature, time of repose is 35-45 minute;
(5) be cycled to repeat step (2)-step (4) 2-4 time;
(6) after step (5) completes, in mixture, add polyacrylic acid 0.5-2 weight part, alpha-methyl styrene 0.1-0.5 weight part and deionized water 20-25 weight part, in adition process, stir;
(7) mixture after step (6) is completed leaves standstill.
Optimize, the preparation method of above-mentioned household detergent, the use mesh screen in its step (3) filters, and the size of mesh of mesh screen is 60-100 order.
The washing composition that method of the present invention is produced: foaminess is good, can be profound clean to tableware, and surfactant activity is high, deep-pollution-removing power chamber, and residue is few, harmless to the person, is applicable to being widely used.
Embodiment
embodiment 1
The present invention is a kind of preparation method of household detergent, comprises the following steps:
(1) following material (calculating by weight) is added in reactor: 25 parts of Sugar Ester O 1570s, 30 parts of glycerine, 1 part, sodium-chlor, in adition process, stir, stirring velocity is 15 revs/min, in whipping process, heats, and Heating temperature is 45-65 degree Celsius;
(2) after heating, mixture is left standstill, leave standstill in process, make mixture naturally be down to room temperature, time of repose is 35 minutes;
(3) mixture after leaving standstill is filtered, after filtration, mixture is heated to 45 degrees Celsius of Heating temperatures;
(4) after heating, mixture is left standstill, leave standstill in process, make mixture naturally be down to room temperature, time of repose is 35 minutes;
(5) be cycled to repeat step (2)-step (4) 2 times;
(6) after step (5) completes, in mixture, add polyacrylic acid 0.5 weight part, alpha-methyl styrene 0.1 weight part and deionized water 20 weight parts, in adition process, stir;
(7) mixture after step (6) is completed leaves standstill.Use mesh screen in step (3) filters, and the size of mesh of mesh screen is 60 orders.
embodiment 2
The present invention is a kind of preparation method of household detergent, comprises the following steps:
(1) following material (calculating by weight) is added in reactor: 30 parts of Sugar Ester O 1570s, 35 parts of glycerine, 3 parts, sodium-chlor, in adition process, stir, stirring velocity is 25 revs/min, in whipping process, heats, and Heating temperature is 65 degrees Celsius;
(2) after heating, mixture is left standstill, leave standstill in process, make mixture naturally be down to room temperature, time of repose is 45 minutes;
(3) mixture after leaving standstill is filtered, after filtration, mixture is heated to 65 degrees Celsius of Heating temperatures;
(4) after heating, mixture is left standstill, leave standstill in process, make mixture naturally be down to room temperature, time of repose is 45 minutes;
(5) be cycled to repeat step (2)-step (4) 4 times;
(6) after step (5) completes, in mixture, add polyacrylic acid 2 weight parts, alpha-methyl styrene 0.5 weight part and deionized water 25 weight parts, in adition process, stir;
(7) mixture after step (6) is completed leaves standstill.Use mesh screen in step (3) filters, and the size of mesh of mesh screen is 100 orders.
The washing composition that method of the present invention is produced: foaminess is good, can be profound clean to tableware, and surfactant activity is high, deep-pollution-removing power chamber, and residue is few, harmless to the person, is applicable to being widely used.
Certainly, above-mentioned explanation is not limitation of the present invention, and the present invention is also not limited to above-mentioned giving an example; those skilled in the art; in essential scope of the present invention, variation, remodeling, interpolation or the replacement made, all should belong to protection scope of the present invention.
Claims (2)
1. a preparation method for household detergent, comprises the following steps:
(1) following material (calculating by weight) is added in reactor: Sugar Ester O 1570 25-30 part, glycerine 30-35 part, sodium-chlor 1-3 part, in adition process, stir, stirring velocity is 15-25 rev/min, in whipping process, heat, Heating temperature is 45-65 degree Celsius;
(2) after heating, mixture is left standstill, leave standstill in process, make mixture naturally be down to room temperature, time of repose is 35-45 minute;
(3) mixture after leaving standstill is filtered, after filtration, mixture is heated to Heating temperature 45-65 degree Celsius;
(4) after heating, mixture is left standstill, leave standstill in process, make mixture naturally be down to room temperature, time of repose is 35-45 minute;
(5) be cycled to repeat step (2)-step (4) 2-4 time;
(6) after step (5) completes, in mixture, add polyacrylic acid 0.5-2 weight part, alpha-methyl styrene 0.1-0.5 weight part and deionized water 20-25 weight part, in adition process, stir;
(7) mixture after step (6) is completed leaves standstill.
2. the preparation method of household detergent according to claim 1, is characterized in that: being filtered in described step (3) used mesh screen to filter, and the size of mesh of mesh screen is 60-100 order.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210582598.0A CN103897834A (en) | 2012-12-28 | 2012-12-28 | Preparation method of household detergent |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210582598.0A CN103897834A (en) | 2012-12-28 | 2012-12-28 | Preparation method of household detergent |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103897834A true CN103897834A (en) | 2014-07-02 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201210582598.0A Pending CN103897834A (en) | 2012-12-28 | 2012-12-28 | Preparation method of household detergent |
Country Status (1)
| Country | Link |
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| CN (1) | CN103897834A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105220478A (en) * | 2015-10-20 | 2016-01-06 | 湖州国信物资有限公司 | Easy degreasing finishing agent of a kind of new type natural and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102071111A (en) * | 2011-01-12 | 2011-05-25 | 广州立白企业集团有限公司 | Laundry liquid and preparation method thereof |
| CN102703245A (en) * | 2012-06-18 | 2012-10-03 | 桑达化工（南通）有限公司 | Detergent for tableware |
-
2012
- 2012-12-28 CN CN201210582598.0A patent/CN103897834A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102071111A (en) * | 2011-01-12 | 2011-05-25 | 广州立白企业集团有限公司 | Laundry liquid and preparation method thereof |
| CN102703245A (en) * | 2012-06-18 | 2012-10-03 | 桑达化工（南通）有限公司 | Detergent for tableware |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105220478A (en) * | 2015-10-20 | 2016-01-06 | 湖州国信物资有限公司 | Easy degreasing finishing agent of a kind of new type natural and preparation method thereof |
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| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20140702 |
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| WD01 | Invention patent application deemed withdrawn after publication |