CN103897853A - Preparation method of improved detergent - Google Patents
Preparation method of improved detergent Download PDFInfo
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- CN103897853A CN103897853A CN201210578268.4A CN201210578268A CN103897853A CN 103897853 A CN103897853 A CN 103897853A CN 201210578268 A CN201210578268 A CN 201210578268A CN 103897853 A CN103897853 A CN 103897853A
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Abstract
The invention discloses a preparation method of an improved detergent. The method comprises the following steps: adding while stirring the following materials into a reactor: 2-8 parts of a mixture of carbolic acid, citric acid and tartaric acid, 11-13 parts of sucrose fatty acid ester and 10 parts of glycerol, wherein the stirring speed is 15-25 rpm, and the adding speed is 1-6 L/min; and heating the stirred mixture with heating temperature of 50 DEG C at a speed lower than 4 DEG C / min. The detergent produced by the method of the invention has strong detergency and delicate appearance, is convenient for carrying and household usage, and can be widely used in washing food cooker, cooking bench, heavy oil on cooking fume exhauster, and heavy oil on hard surfaces such as toilet tiles and porcelain ware.
Description
Technical field
The present invention relates to a kind of preparation method of improved washing composition, belong to industrial chemical field.
Background technology
Although the heavy cleaning agent in traditional kitchen is to the greasy dirt strong detergency on smoke exhaust ventilator, but because of alkalescence stronger, and contain a large amount of glycol ethers, propylene glycol equal solvent, and can not be used for cleaning tableware, when use, accidentally suck or contact skin all harmful.In present life staying idle at home, people generally clean the greasy dirt on ceramic tile or the Ceramic vessel in kitchen with scrubbing powder, but in scrubbing powder, surfactant content is lower, more difficult the removing of heavy oil dirt on ceramic tile.Therefore, if there is a kind of decontamination effect strong, safety non-toxic, and can must bring convenience to daily life for the washing composition that cleans the lip-deep heavy oil dirts such as kitchen Chinese dinner service, the kitchen range top, smoke exhaust ventilator, ceramic tile, Ceramic vessel, lavatory ceramic tile.
Summary of the invention
The deficiency existing for prior art, technical problem to be solved by this invention is, a kind of preparation method of improved washing composition is provided, decontamination effect is strong, safety non-toxic, and with low cost, operational safety.
For solving the problems of the technologies described above, the technical scheme that the present invention takes is that a kind of preparation method of improved washing composition, comprises the following steps:
(1) by weight following material is added in reactor: 10 parts of phenylic acid, citric acid and tartaric mixture 2-8 part, sucrose fatty ester 11-13 part, glycerine, in adition process, stir, stirring velocity 15-25 rev/min, adds speed 1-6 liter/min;
(2) the above-mentioned mixture being stirred is heated, 50 degrees Celsius of heating top temperatures, heating temperature rise is lower than 4 degrees celsius/minute;
(3) mixture heating is left standstill, leave standstill and carry out in process coolingly, cooling temperature is lower than 5 degrees Celsius, and time of repose was higher than 50 minutes;
(4) by weight the mixture after leaving standstill is added to following material: ethanol 10-15 part, 6 parts of Sunmorl N 60Ss, 10 parts of thioglycolic acids, in filling process, stir, stirring velocity is 10-15 rev/min;
(5) mixture after stirring leaves standstill, and time of repose was more than 1 hour;
(6) mixture after leaving standstill is filtered, filter and use thick eye mesh screen;
(7) mixture after filtering is carried out to heated and stirred, after heated and stirred, leave standstill 1-1.5 hour.
Optimize, the preparation method of above-mentioned improved washing composition, in its step (6), the mesh diameter of thick eye mesh screen is higher than 0.3 millimeter.
Washing composition strong detergency, outward appearance exquisiteness that method of the present invention is produced, carry with family easy to usely, can be widely used in the washing of heavy oil dirt on the crust such as washing, washing, lavatory ceramic tile and the Ceramic vessel of smoke exhaust ventilator heavy oil dirt of cooker and the kitchen range top etc.; When use, dip in after water and washing composition with wiper, then clean surface has cooker, the kitchen range top, Ceramic vessel or the smoke exhaust ventilator etc. of greasy dirt, or water-soluble washing composition rear washing surface is had to cooker, the kitchen range top, Ceramic vessel or the smoke exhaust ventilator of greasy dirt; Washing composition has weakly alkaline, harmless, and other liquid washing agents and powdered detergent relatively, has advantages of low-consuming.
Embodiment
embodiment 1
The present invention is a kind of preparation method of improved washing composition, comprises the following steps:
(1) by weight following material is added in reactor: phenylic acid, citric acid and 2 parts, tartaric mixture, 11 parts of sucrose fatty esters, 10 parts of glycerine, in adition process, stir, 15 revs/min of stirring velocitys, add 1 liter/min of speed;
(2) the above-mentioned mixture being stirred is heated, 50 degrees Celsius of heating top temperatures, heating temperature rise is lower than 4 degrees celsius/minute;
(3) mixture heating is left standstill, leave standstill and carry out in process coolingly, cooling temperature is lower than 5 degrees Celsius, and time of repose was higher than 50 minutes;
(4) by weight the mixture after leaving standstill is added to 10 parts of following material ethanol, 6 parts of Sunmorl N 60Ss, 10 parts of thioglycolic acids, in filling process, stir, stirring velocity is 10 revs/min;
(5) mixture after stirring leaves standstill, and time of repose was more than 1 hour;
(6) mixture after leaving standstill is filtered, filter and use thick eye mesh screen;
(7) mixture after filtering is carried out to heated and stirred, after heated and stirred, leave standstill 1 hour, in its step (6), the mesh diameter of thick eye mesh screen is higher than 0.3 millimeter.
embodiment 2
The present invention is a kind of preparation method of improved washing composition, comprises the following steps:
(1) by weight following material is added in reactor: phenylic acid, citric acid and 8 parts, tartaric mixture, 13 parts of sucrose fatty esters, 10 parts of glycerine, in adition process, stir, 25 revs/min of stirring velocitys, add 6 liters/min of speed;
(2) the above-mentioned mixture being stirred is heated, 50 degrees Celsius of heating top temperatures, heating temperature rise is lower than 4 degrees celsius/minute;
(3) mixture heating is left standstill, leave standstill and carry out in process coolingly, cooling temperature is lower than 5 degrees Celsius, and time of repose was higher than 50 minutes;
(4) by weight the mixture after leaving standstill is added to 15 parts of following material ethanol, 6 parts of Sunmorl N 60Ss, 10 parts of thioglycolic acids, in filling process, stir, stirring velocity is 15 revs/min;
(5) mixture after stirring leaves standstill, and time of repose was more than 1 hour;
(6) mixture after leaving standstill is filtered, filter and use thick eye mesh screen;
(7) mixture after filtering is carried out to heated and stirred, after heated and stirred, leave standstill 1.5 hours, in its step (6), the mesh diameter of thick eye mesh screen is higher than 0.3 millimeter.
Washing composition strong detergency, outward appearance exquisiteness that method of the present invention is produced, carry with family easy to usely, can be widely used in the washing of heavy oil dirt on the crust such as washing, washing, lavatory ceramic tile and the Ceramic vessel of smoke exhaust ventilator heavy oil dirt of cooker and the kitchen range top etc.; When use, dip in after water and washing composition with wiper, then clean surface has cooker, the kitchen range top, Ceramic vessel or the smoke exhaust ventilator etc. of greasy dirt, or water-soluble washing composition rear washing surface is had to cooker, the kitchen range top, Ceramic vessel or the smoke exhaust ventilator of greasy dirt; Washing composition has weakly alkaline, harmless, and other liquid washing agents and powdered detergent relatively, has advantages of low-consuming.
Certainly, above-mentioned explanation is not limitation of the present invention, and the present invention is also not limited to above-mentioned giving an example; those skilled in the art; in essential scope of the present invention, variation, remodeling, interpolation or the replacement made, all should belong to protection scope of the present invention.
Claims (2)
1. a preparation method for improved washing composition, comprises the following steps:
(1) by weight following material is added in reactor: 10 parts of phenylic acid, citric acid and tartaric mixture 2-8 part, sucrose fatty ester 11-13 part, glycerine, in adition process, stir, stirring velocity 15-25 rev/min, adds speed 1-6 liter/min;
(2) the above-mentioned mixture being stirred is heated, 50 degrees Celsius of heating top temperatures, heating temperature rise is lower than 4 degrees celsius/minute;
(3) mixture heating is left standstill, leave standstill and carry out in process coolingly, cooling temperature is lower than 5 degrees Celsius, and time of repose was higher than 50 minutes;
(4) by weight the mixture after leaving standstill is added to following material: ethanol 10-15 part, 6 parts of Sunmorl N 60Ss, 10 parts of thioglycolic acids, in filling process, stir, stirring velocity is 10-15 rev/min;
(5) mixture after stirring leaves standstill, and time of repose was more than 1 hour;
(6) mixture after leaving standstill is filtered, filter and use thick eye mesh screen;
(7) mixture after filtering is carried out to heated and stirred, after heated and stirred, leave standstill 1-1.5 hour.
2. the preparation method of improved washing composition according to claim 1, is characterized in that: in described step (6), the mesh diameter of thick eye mesh screen is higher than 0.3 millimeter.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210578268.4A CN103897853A (en) | 2012-12-28 | 2012-12-28 | Preparation method of improved detergent |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210578268.4A CN103897853A (en) | 2012-12-28 | 2012-12-28 | Preparation method of improved detergent |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103897853A true CN103897853A (en) | 2014-07-02 |
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ID=50989431
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201210578268.4A Pending CN103897853A (en) | 2012-12-28 | 2012-12-28 | Preparation method of improved detergent |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103897853A (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2001057174A1 (en) * | 2000-02-01 | 2001-08-09 | Reckitt Benckiser Inc. | Hard surface cleaning composition |
| CN102690727A (en) * | 2012-06-19 | 2012-09-26 | 海安县国力化工有限公司 | Disinfectant washing agent |
| CN102703917A (en) * | 2012-06-04 | 2012-10-03 | 李东日 | Rust removing detergent |
-
2012
- 2012-12-28 CN CN201210578268.4A patent/CN103897853A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2001057174A1 (en) * | 2000-02-01 | 2001-08-09 | Reckitt Benckiser Inc. | Hard surface cleaning composition |
| CN102703917A (en) * | 2012-06-04 | 2012-10-03 | 李东日 | Rust removing detergent |
| CN102690727A (en) * | 2012-06-19 | 2012-09-26 | 海安县国力化工有限公司 | Disinfectant washing agent |
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| Date | Code | Title | Description |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20140702 |