CN103894123A - 一种洁净气体灭火剂的中试合成装置 - Google Patents
一种洁净气体灭火剂的中试合成装置 Download PDFInfo
- Publication number
- CN103894123A CN103894123A CN201210517746.0A CN201210517746A CN103894123A CN 103894123 A CN103894123 A CN 103894123A CN 201210517746 A CN201210517746 A CN 201210517746A CN 103894123 A CN103894123 A CN 103894123A
- Authority
- CN
- China
- Prior art keywords
- reactor
- reaction
- synthesizer
- bromo
- trifluoro propene
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000006243 chemical reaction Methods 0.000 claims abstract description 19
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Chemical compound BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000011521 glass Substances 0.000 claims abstract description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000007788 liquid Substances 0.000 claims abstract description 9
- 238000005286 illumination Methods 0.000 claims abstract description 8
- 238000011020 pilot scale process Methods 0.000 claims description 12
- 239000003513 alkali Substances 0.000 claims description 11
- 238000007599 discharging Methods 0.000 claims description 10
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 claims description 9
- 229910052794 bromium Inorganic materials 0.000 claims description 9
- 239000000126 substance Substances 0.000 claims description 9
- FFTOUVYEKNGDCM-OWOJBTEDSA-N (e)-1,3,3-trifluoroprop-1-ene Chemical compound F\C=C\C(F)F FFTOUVYEKNGDCM-OWOJBTEDSA-N 0.000 claims description 8
- FDMFUZHCIRHGRG-UHFFFAOYSA-N 3,3,3-trifluoroprop-1-ene Chemical compound FC(F)(F)C=C FDMFUZHCIRHGRG-UHFFFAOYSA-N 0.000 claims description 6
- 239000000463 material Substances 0.000 claims description 6
- 244000025254 Cannabis sativa Species 0.000 claims description 5
- WYTGDNHDOZPMIW-RCBQFDQVSA-N alstonine Natural products C1=CC2=C3C=CC=CC3=NC2=C2N1C[C@H]1[C@H](C)OC=C(C(=O)OC)[C@H]1C2 WYTGDNHDOZPMIW-RCBQFDQVSA-N 0.000 claims description 5
- 238000003860 storage Methods 0.000 claims description 5
- 238000010521 absorption reaction Methods 0.000 claims description 3
- 230000006698 induction Effects 0.000 claims description 3
- 238000005859 coupling reaction Methods 0.000 claims description 2
- 238000000034 method Methods 0.000 claims description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims 1
- 238000007259 addition reaction Methods 0.000 claims 1
- 125000005843 halogen group Chemical group 0.000 claims 1
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 claims 1
- 229910052753 mercury Inorganic materials 0.000 claims 1
- 229910052751 metal Inorganic materials 0.000 claims 1
- 239000002184 metal Substances 0.000 claims 1
- 239000000203 mixture Substances 0.000 claims 1
- 229910052708 sodium Inorganic materials 0.000 claims 1
- 239000011734 sodium Substances 0.000 claims 1
- 239000003795 chemical substances by application Substances 0.000 abstract description 3
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 238000001816 cooling Methods 0.000 abstract description 2
- QKBKGNDTLQFSEU-UHFFFAOYSA-N 2-bromo-3,3,3-trifluoroprop-1-ene Chemical compound FC(F)(F)C(Br)=C QKBKGNDTLQFSEU-UHFFFAOYSA-N 0.000 abstract 1
- 238000007789 sealing Methods 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- 239000000498 cooling water Substances 0.000 description 2
- 239000012452 mother liquor Substances 0.000 description 2
- 238000010924 continuous production Methods 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000003379 elimination reaction Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000013067 intermediate product Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 238000009423 ventilation Methods 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/141—Feedstock
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- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
Description
Claims (4)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201210517746.0A CN103894123B (zh) | 2012-12-06 | 2012-12-06 | 一种洁净气体灭火剂的中试合成装置 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201210517746.0A CN103894123B (zh) | 2012-12-06 | 2012-12-06 | 一种洁净气体灭火剂的中试合成装置 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN103894123A true CN103894123A (zh) | 2014-07-02 |
CN103894123B CN103894123B (zh) | 2016-04-06 |
Family
ID=50985881
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201210517746.0A Active CN103894123B (zh) | 2012-12-06 | 2012-12-06 | 一种洁净气体灭火剂的中试合成装置 |
Country Status (1)
Country | Link |
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CN (1) | CN103894123B (zh) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111470939A (zh) * | 2020-04-17 | 2020-07-31 | 威海新元化工有限公司 | 一种连续生产2-溴-3,3,3-三氟丙烯的生产装置及方法 |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH08247554A (ja) * | 1995-03-13 | 1996-09-27 | Matsushita Electric Ind Co Ltd | 電気湯沸器 |
CN202516542U (zh) * | 2012-03-06 | 2012-11-07 | 美药星(南京)制药有限公司 | 反应釜pH及温度自动控制系统 |
CN102964207A (zh) * | 2012-12-22 | 2013-03-13 | 威海新元化工有限公司 | 一种2-溴-3,3,3-三氟丙烯的制备方法 |
CN202909714U (zh) * | 2012-10-17 | 2013-05-01 | 联化科技股份有限公司 | 一种用于光催化溴化反应的装置 |
-
2012
- 2012-12-06 CN CN201210517746.0A patent/CN103894123B/zh active Active
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH08247554A (ja) * | 1995-03-13 | 1996-09-27 | Matsushita Electric Ind Co Ltd | 電気湯沸器 |
CN202516542U (zh) * | 2012-03-06 | 2012-11-07 | 美药星(南京)制药有限公司 | 反应釜pH及温度自动控制系统 |
CN202909714U (zh) * | 2012-10-17 | 2013-05-01 | 联化科技股份有限公司 | 一种用于光催化溴化反应的装置 |
CN102964207A (zh) * | 2012-12-22 | 2013-03-13 | 威海新元化工有限公司 | 一种2-溴-3,3,3-三氟丙烯的制备方法 |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111470939A (zh) * | 2020-04-17 | 2020-07-31 | 威海新元化工有限公司 | 一种连续生产2-溴-3,3,3-三氟丙烯的生产装置及方法 |
CN111470939B (zh) * | 2020-04-17 | 2022-12-09 | 新元化学(山东)股份有限公司 | 一种连续生产2-溴-3,3,3-三氟丙烯的生产装置及方法 |
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Publication number | Publication date |
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CN103894123B (zh) | 2016-04-06 |
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Legal Events
Date | Code | Title | Description |
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C06 | Publication | ||
PB01 | Publication | ||
ASS | Succession or assignment of patent right |
Owner name: NANTONG BOAI FINE CHEMICAL INDUSTRY CO., LTD. Free format text: FORMER OWNER: JIANGSU HIGHSTAR POWER CO., LTD.;JIANGSU PROVINCE NEW POWER BATTERY + MATERIALS ENGINEERING TECHNOLO Effective date: 20140616 Free format text: FORMER OWNER: NANTONG LICHI ENERGY TECHNOLOGY CO., LTD. Effective date: 20140616 |
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C41 | Transfer of patent application or patent right or utility model | ||
TA01 | Transfer of patent application right |
Effective date of registration: 20140616 Address after: 226200 fine chemical industry park, Qidong, Jiangsu Applicant after: Nantong Boai Fine Chemical Engineering Co.,Ltd. Address before: 226200 No. 306 Heping South Road, Huilong Town, Jiangsu, Qidong Applicant before: JIANGSU HIGHSTAR BATTERY MANUFACTURING Co.,Ltd. Applicant before: NANTONG LICHI ENERGY TECHNOLOGY Co.,Ltd. |
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C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
TR01 | Transfer of patent right |
Effective date of registration: 20170907 Address after: 226200 No. 306 Heping South Road, Huilong Town, Jiangsu, Qidong Patentee after: JIANGSU HIGHSTAR BATTERY MANUFACTURING Co.,Ltd. Address before: 226200 fine chemical industry park, Qidong, Jiangsu Patentee before: Nantong Boai Fine Chemical Engineering Co.,Ltd. |
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TR01 | Transfer of patent right | ||
CP03 | Change of name, title or address | ||
CP03 | Change of name, title or address |
Address after: 226200 No.306 Heping South Road, Huilong Town, Qidong City, Nantong City, Jiangsu Province Patentee after: Jiangsu haisida power supply Co.,Ltd. Address before: 226200 No. 306 Heping South Road, Huilong Town, Jiangsu, Qidong Patentee before: JIANGSU HIGHSTAR BATTERY MANUFACTURING Co.,Ltd. |