CN103882724A - Method for processing fabric by utilizing silver-loaded chitosan antibacterial agent - Google Patents
Method for processing fabric by utilizing silver-loaded chitosan antibacterial agent Download PDFInfo
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- CN103882724A CN103882724A CN201210557556.1A CN201210557556A CN103882724A CN 103882724 A CN103882724 A CN 103882724A CN 201210557556 A CN201210557556 A CN 201210557556A CN 103882724 A CN103882724 A CN 103882724A
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- chitosan
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- loaded silver
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Abstract
The invention discloses a method for processing a fabric by utilizing a silver-loaded chitosan antibacterial agent. The method comprises the following steps: putting powdery chitosan in water, adding distilled water, immersing the powdery chitosan in water for 55-65min to fully wet the powdery chitosan, adding industrial glacial acetic acid, stirring by a stirrer to make the industrial glacial acetic acid fully dissolved, allowing the obtained solution to stand for 30min, and filtering the solution to obtain a chitosan solution; reacting the prepared chitosan solution with a silver nitrate solution to prepare the silver-loaded chitosan antibacterial agent; putting the fabric in the silver-loaded chitosan antibacterial agent, immersing at room temperature for 30min, and padding the fabric on a vertical electric rolling dolly with a solution padding rate of 80-90%; and washing, and drying. The method has the advantages of simplicity, good antibacterial property, and no color change of the finished fabric, is suitable for the antibacterial finishing of fabrics.
Description
Technical field
The invention belongs to fabric technical field, be specifically related to a kind of method of utilizing chitosan-loaded silver antibacterial agent to process fabric.
Background technology
Along with social development, people more and more favor antibacterial function clothes, also more and more higher to its requirement, antiseptic is not only wanted efficient, safety, but also environmentally friendly, pollution-free, non-stimulated, developmental research is a kind of not to be arranged for clothes, easy to change, heat-resistant stability is high, bactericidal effect good, and efficient, durable and safe antiseptic comes into one's own day by day.
Summary of the invention
The above-mentioned technical problem existing in order to overcome prior art field, the object of the invention is to, and a kind of method of utilizing chitosan-loaded silver antibacterial agent to process fabric is provided, and method is simple, and anti-microbial property is good.
The method of utilizing chitosan-loaded silver antibacterial agent to process fabric provided by the invention, comprises the following steps:
One, Powdered shitosan is put into water, adding distil water soaks 55-65min, makes it fully moistening, adds afterwards industrial glacial acetic acid, with mixer stirring, it is fully dissolved, and leaves standstill after 30min, and solution is filtered, and obtains chitosan solution;
Two, the chitosan solution configuring is reacted with liquor argenti nitratis ophthalmicus, prepare chitosan-loaded silver antibacterial agent;
Three, gained chitosan-loaded silver antibacterial agent is added distilled water place 3h, stir afterwards, obtain concentration and be 4% chitosan-loaded silver antibiotic finishing solution;
Four, fabric is put into chitosan-loaded silver antibacterial agent, under room temperature, soaked 30min, be placed on afterwards vertical electric and roll pad dyeing on dolly, pick-up rate is 80-90%;
Five, fabric is put into constant temperature oven dries under the temperature conditions of 100 DEG C;
Six, dry after fabric to put into temperature be the water of 40 DEG C, adopt neutral cleaning solution to wash 30min, after washing, dry.
Described chitosan solution, the concentration of shitosan is 1%, the concentration of industrial glacial acetic acid is 1%.
The method of utilizing chitosan-loaded silver antibacterial agent to process fabric provided by the invention, its beneficial effect is, chitosan solution is improved, and makes composite silver carrying antiseptic, is more suitable for fabric to arrange, anti-microbial property is good; Belong to natural antibacterial agent, non-stimulated to human body, non-environmental-pollution problem, finish fabric nondiscolouring.
Detailed description of the invention
Below in conjunction with an embodiment, the method for utilizing chitosan-loaded silver antibacterial agent to process fabric provided by the invention is described in detail.
Embodiment
The method of utilizing chitosan-loaded silver antibacterial agent to process fabric of the present embodiment, comprises following production stage:
One, Powdered shitosan is put into water, adding distil water soaks 60min, make it fully moistening, add afterwards industrial glacial acetic acid, stir with mixer, it is fully dissolved, leave standstill after 30min, solution is filtered, obtain chitosan solution, the concentration of shitosan is 1%, and the concentration of industrial glacial acetic acid is 1%;
Two, the chitosan solution configuring is reacted with liquor argenti nitratis ophthalmicus, prepare chitosan-loaded silver antibacterial agent;
Three, gained chitosan-loaded silver antibacterial agent is added distilled water place 3h, stir afterwards, obtain concentration and be 4% chitosan-loaded silver antibiotic finishing solution;
Four, fabric is put into chitosan-loaded silver antibacterial agent, under room temperature, soaked 30min, be placed on afterwards vertical electric and roll pad dyeing on dolly, pick-up rate is 82%;
Five, fabric is put into constant temperature oven dries under the temperature conditions of 100 DEG C;
Six, dry after fabric to put into temperature be the water of 40 DEG C, adopt neutral cleaning solution to wash 30min, after washing, dry.
Claims (2)
1. a method of utilizing chitosan-loaded silver antibacterial agent to process fabric, is characterized in that: comprise the following steps:
One, Powdered shitosan is put into water, adding distil water soaks 55-65min, makes it fully moistening, adds afterwards industrial glacial acetic acid, with mixer stirring, it is fully dissolved, and leaves standstill after 30min, and solution is filtered, and obtains chitosan solution;
Two, the chitosan solution configuring is reacted with liquor argenti nitratis ophthalmicus, prepare chitosan-loaded silver antibacterial agent;
Three, gained chitosan-loaded silver antibacterial agent is added distilled water place 3h, stir afterwards, obtain concentration and be 4% chitosan-loaded silver antibiotic finishing solution;
Four, fabric is put into chitosan-loaded silver antibacterial agent, under room temperature, soaked 30min, be placed on afterwards vertical electric and roll pad dyeing on dolly, pick-up rate is 80-90%;
Five, fabric is put into constant temperature oven dries under the temperature conditions of 100 DEG C;
Six, dry after fabric to put into temperature be the water of 40 DEG C, adopt neutral cleaning solution to wash 30min, after washing, dry.
2. the method for utilizing chitosan-loaded silver antibacterial agent to process fabric according to claim 1, is characterized in that: described chitosan solution, and the concentration of shitosan is 1%, the concentration of industrial glacial acetic acid is 1%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210557556.1A CN103882724A (en) | 2012-12-20 | 2012-12-20 | Method for processing fabric by utilizing silver-loaded chitosan antibacterial agent |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210557556.1A CN103882724A (en) | 2012-12-20 | 2012-12-20 | Method for processing fabric by utilizing silver-loaded chitosan antibacterial agent |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103882724A true CN103882724A (en) | 2014-06-25 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201210557556.1A Pending CN103882724A (en) | 2012-12-20 | 2012-12-20 | Method for processing fabric by utilizing silver-loaded chitosan antibacterial agent |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104611938A (en) * | 2014-12-31 | 2015-05-13 | 芜湖恒杰膨润土科技有限公司 | Antibacterial fiber and preparation method thereof |
| CN105088774A (en) * | 2015-09-06 | 2015-11-25 | 泉州市品诚电子科技有限公司 | Preparation method of long-acting antibacterial fabric |
| CN105200773A (en) * | 2015-10-15 | 2015-12-30 | 武汉纺织大学 | Preparation method of nano-silver coating of chitosan modified fabric |
| CN106106522A (en) * | 2016-06-23 | 2016-11-16 | 中国人民解放军军事医学科学院卫生学环境医学研究所 | A kind of nano zine oxide carries silver chitosan compound anti-bacteria agent and preparation method thereof |
| CN106174723A (en) * | 2016-08-31 | 2016-12-07 | 浙江棉田针织有限公司 | A kind of intelligent antibacterial motion bra |
| CN106667357A (en) * | 2016-12-06 | 2017-05-17 | 太仓大唐化纤厂 | Antibacterial fiber closestool seat cushion |
| CN108560180A (en) * | 2018-02-07 | 2018-09-21 | 海宁市美元达经编有限公司 | A kind of production technology of antibacterial underwear fabric |
| CN109162095A (en) * | 2018-07-25 | 2019-01-08 | 苏州联畅特种纤维有限公司 | A kind of antibacterial dacron yarn and preparation method thereof |
| CN113981563A (en) * | 2021-11-12 | 2022-01-28 | 杭州港华纺织有限公司 | Antibacterial polyester high stretch yarn and preparation method thereof |
-
2012
- 2012-12-20 CN CN201210557556.1A patent/CN103882724A/en active Pending
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104611938A (en) * | 2014-12-31 | 2015-05-13 | 芜湖恒杰膨润土科技有限公司 | Antibacterial fiber and preparation method thereof |
| CN104611938B (en) * | 2014-12-31 | 2016-08-24 | 芜湖恒杰膨润土科技有限公司 | Anti-bacterial fibre and preparation method thereof |
| CN105088774A (en) * | 2015-09-06 | 2015-11-25 | 泉州市品诚电子科技有限公司 | Preparation method of long-acting antibacterial fabric |
| CN105200773A (en) * | 2015-10-15 | 2015-12-30 | 武汉纺织大学 | Preparation method of nano-silver coating of chitosan modified fabric |
| CN105200773B (en) * | 2015-10-15 | 2017-10-27 | 武汉纺织大学 | The Nano Silver coating production of chitin modified fabric |
| CN106106522A (en) * | 2016-06-23 | 2016-11-16 | 中国人民解放军军事医学科学院卫生学环境医学研究所 | A kind of nano zine oxide carries silver chitosan compound anti-bacteria agent and preparation method thereof |
| CN106106522B (en) * | 2016-06-23 | 2019-05-14 | 中国人民解放军军事医学科学院卫生学环境医学研究所 | A kind of nano zine oxide-load silver chitosan compound anti-bacteria agent and preparation method thereof |
| CN106174723A (en) * | 2016-08-31 | 2016-12-07 | 浙江棉田针织有限公司 | A kind of intelligent antibacterial motion bra |
| CN106667357A (en) * | 2016-12-06 | 2017-05-17 | 太仓大唐化纤厂 | Antibacterial fiber closestool seat cushion |
| CN108560180A (en) * | 2018-02-07 | 2018-09-21 | 海宁市美元达经编有限公司 | A kind of production technology of antibacterial underwear fabric |
| CN109162095A (en) * | 2018-07-25 | 2019-01-08 | 苏州联畅特种纤维有限公司 | A kind of antibacterial dacron yarn and preparation method thereof |
| CN113981563A (en) * | 2021-11-12 | 2022-01-28 | 杭州港华纺织有限公司 | Antibacterial polyester high stretch yarn and preparation method thereof |
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Application publication date: 20140625 |