CN103815061B - Blend edible oil of peony seed oil and sesame oil and preparation method of blend edible oil - Google Patents

Blend edible oil of peony seed oil and sesame oil and preparation method of blend edible oil Download PDF

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Publication number
CN103815061B
CN103815061B CN201410080181.3A CN201410080181A CN103815061B CN 103815061 B CN103815061 B CN 103815061B CN 201410080181 A CN201410080181 A CN 201410080181A CN 103815061 B CN103815061 B CN 103815061B
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oil
peony
seed
powder
peony seeds
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CN201410080181.3A
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Chinese (zh)
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CN103815061A (en
Inventor
杨永庆
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洛阳春魁农业开发有限公司
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Abstract

The invention provides a blend edible oil of peony seed oil and sesame oil, and a preparation method of the blend edible oil. The preparation method comprises the following steps: taking sesame seeds and shelled peony seeds respectively, conducting physical squeezing to prepare crude sesame oil and crude peony seed oil after the sesame seeds and shelled peony seeds are processed; respectively refining the two crude oils, so that refined peony seed oil and refined sesame oil are obtained; blending the refined peony seed oil and the refined sesame oil according to the weight ratio of 1: (0.5-2), so that the blend edible oil is obtained. According to the invention, after the sesame seeds and the shelled peony seeds are subjected to series of processing, the cell structure is destroyed, and the water content of the cells is reduced, so that grease in the cells can be separated from the cells in the process of squeezing, thereby improving the oil yield.

Description

A kind of peony seed oil and sesame oil blending edible oil and preparation method thereof
Technical field
The present invention relates to edible oil field, specifically a kind of peony seed oil and sesame oil blending edible oil and preparation method thereof.
Background technology
Sesame oil is again sesame oil, sesame oil, has common sesame oil, ground sesameseed oil and machine to squeeze sesame oil three productions technique.They are all take sesame as the oil product that raw material is produced.No matter the grease extracted from sesame is sesame oil or ground sesameseed oil, and its aliphatic acid is substantially containing oleic acid 35.0-49.4%, linoleic acid 37.7-48.4%, arachidic acid 0.4-1.2%.The digestibility of sesame oil reaches 98%.Not containing harmful composition in sesame oil, and containing vitamin E abundant especially with than more rich linoleic acid.
Peony seed oil is edible oil that is emerging, that have edible health double effects, take from peony seed, wherein be rich in the elements such as protein, fat, potassium, calcium, magnesium, phosphorus, selenium and vitamin B1, B2, carrotene etc., and contain the very strong odd-carbon fatty acid of active anticancer as C15, C17 etc., aliphatic acid in addition containing a small amount of circulus is as sad in 2-hexyl cyclopropane, is widely used in medicine, health care, food, superior cosmetics, lubrication wet goods industry.
In prior art, the extraction of vegetable oil generally has two kinds of techniques:
1) extract technology: the biscuit after squeezing, uses chemical solvent leaching grease.Advantage: oil yield is high, output is large, saves cost.Shortcoming: nutritional labeling reduces, belongs to chemical industry.
2) squeezing process: adopt the squeezing of the method for machinery pressure to extract grease.Advantage: all original nutritional labelings can be retained, physical squeezing.Shortcoming: oil yield is low, cost is high.
Summary of the invention
The object of the invention is to overcome the problem that the oil yield of conventional press method is low, and then a kind of peony seed oil and sesame oil blending edible oil and preparation method thereof are provided, the ready-mixed oil prepared by the method is nutritious, overcome the problem that conventional press technique oil yield is low, make the squeezing oil yield of peony seeds and sesame exceed about 12% than the oil yield of conventional press method.
The technical scheme that the present invention takes for achieving the above object is: a kind of peony seed oil and sesame oil blending edible oil, to be in harmonious proportion to form by the peony seed oil of refining and sesame oil by weight the ratio of 1:0.5-2.
The method preparing above-mentioned peony seed oil and sesame oil blending edible oil is: get til seed respectively and the peony seeds that shells carries out physical squeezing after treatment and obtains sesame oil crude oil and peony seeds crude oil, again namely the refined sesame oil obtained after two kinds of crude oils respectively refining and refining peony seed oil are obtained product in the mediation of above-mentioned ratio, wherein, the process of described til seed and the peony seeds that shells comprises the following steps:
1) drain after respectively til seed and the peony seeds after shelling being added to the water immersion 2-5h, and put into the freezing 15-20h of environment that temperature is less than-45 DEG C immediately, then in sub-zero low temperature environment, respectively til seed and peony seeds are ground into the peony seeds powder that the til seed powder that particle diameter is 0.5-1mm and particle diameter are 1-2mm, for subsequent use;
2) the til seed powder of step 1) and peony seeds powder being taken out and under the environment temperature of 20-25 DEG C, join mass concentration is respectively in the salt solution of 15-18%, leaves standstill 17-24h after then passing into supersonic oscillations 3-5min wherein, for subsequent use;
3) adopt centrifugation make step 2) in til seed powder be separated with salt solution with peony seeds powder, be then dry under the condition of 65-70 DEG C to be less than 5% to moisture content in temperature, respectively til seed powder and peony seeds powder squeezed afterwards.
Described step 2) condition of supersonic oscillations is: the ultrasonic wave of the corresponding 120-150W of salt solution of every kilogram, hyperacoustic frequency is 80-110KHz.
The rotating speed of centrifugation in described step 3) is 2500-4000r/min.
Isolate the salt solution after til seed powder and peony seeds powder in described step 3) and isolate sesame oil crude oil and peony seeds crude oil by distillation procedure.
In the present invention, first til seed and peony seeds being soaked in water is to make the cell of til seed and peony seeds fully absorb water, then in the freezing environment below-45 DEG C freezing after and under the environment temperature of 20-25 DEG C, put into salt solution, destroy eucaryotic cell structure like this, be convenient to squeeze time fuel-displaced;
Meanwhile, til seed powder and peony seeds powder are placed in the salt solution that mass concentration is 15-18%, the cell dehydration of til seed and peony seeds can be made, cell volume reduces, not only be convenient to follow-up oven dry, and eliminate moisture unnecessary in cell, improve squeezing oil yield; Introduce supersonic oscillations in the process, not only play stirring action, and the cyto-architectural effect of destruction can be played; In follow-up centrifugation, the grease outer layers of cell interior also can be made to move, be convenient to be extracted in expressing process.
In the present invention, by til seed and the freezing rear pulverizing of peony seeds, granularity is less, is more conducive to post-processed and improves oil yield, but, in crushing process, have amount of grease and be extracted, the particle of pulverizing is less, the grease of crushing process loss is more, consider above factor, after pulverizing, the particle diameter of peony seeds powder is that 1-2mm is advisable, and the particle diameter of til seed powder to be 0.5-1mm be advisable; And, be compared to and directly pulverize, pulverize in sub-zero low temperature environment immediately after freezing in the freezing environment below-45 DEG C, the loss of grease in crushing process can be effectively reduced.
Beneficial effect: the present invention, by til seed and shell peony seeds after a series of process, destroys eucaryotic cell structure and decreases the water content of cell, being convenient to intracellular grease like this and separating from cell in expressing process, thus improve oil yield.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is further elaborated.
Embodiment 1
A kind of peony seed oil and sesame oil blending edible oil, formed by the ratio mediation by weight 1:0.5 of the peony seed oil of refining and sesame oil;
Its preparation method is, get til seed respectively and the peony seeds that shells carries out physical squeezing after treatment and obtains sesame oil crude oil and peony seeds crude oil, again the refining peony seed oil obtained after two kinds of crude oils respectively refining and refined sesame oil are in harmonious proportion according to the above ratio and namely obtain product, wherein, the process of described til seed and the peony seeds that shells comprises the following steps:
1) drain after respectively til seed and the peony seeds after shelling being added to the water immersion 2h, and put into the freezing 15h of environment that temperature is less than-45 DEG C immediately, then in sub-zero low temperature environment, respectively til seed and peony seeds are ground into the peony seeds powder that the til seed powder that particle diameter is 0.5-1mm and particle diameter are 1-2mm, for subsequent use;
2) the til seed powder of step 1) and peony seeds powder being taken out and under the environment temperature of 20-25 DEG C, join mass concentration is respectively in the salt solution of 15%, then 17h is left standstill after passing into supersonic oscillations 3min wherein, hyperacoustic frequency is 80KHz, the ultrasonic wave of every kilogram of corresponding 120W power of salt solution, for subsequent use;
3) adopt centrifugation make step 2) in til seed powder be separated with salt solution with peony seeds powder, the rotating speed of centrifugation is 2500r/min, then be dry under the condition of 65 DEG C to be less than 5% to moisture content in temperature, respectively til seed powder and peony seeds powder squeezed afterwards;
4) salt solution after step 3) being separated distills, and isolates the sesame oil crude oil and peony seeds crude oil that wherein contain.
Embodiment 2
A kind of peony seed oil and sesame oil blending edible oil, formed by the ratio mediation by weight 1:2 of the peony seed oil of refining and sesame oil;
Its preparation method is, get til seed respectively and the peony seeds that shells carries out physical squeezing after treatment and obtains sesame oil crude oil and peony seeds crude oil, again the refining peony seed oil obtained after two kinds of crude oils respectively refining and refined sesame oil are in harmonious proportion according to the above ratio and namely obtain product, wherein, the process of described til seed and the peony seeds that shells comprises the following steps:
1) drain after respectively til seed and the peony seeds after shelling being added to the water immersion 5h, and put into the freezing 20h of environment that temperature is less than-45 DEG C immediately, then in sub-zero low temperature environment, respectively til seed and peony seeds are ground into the peony seeds powder that the til seed powder that particle diameter is 0.5-1mm and particle diameter are 1-2mm, for subsequent use;
2) the til seed powder of step 1) and peony seeds powder being taken out and under the environment temperature of 20-25 DEG C, join mass concentration is respectively in the salt solution of 18%, then 24h is left standstill after passing into supersonic oscillations 5min wherein, hyperacoustic frequency is 110KHz, the ultrasonic wave of every kilogram of corresponding 150W power of salt solution, for subsequent use;
3) adopt centrifugation make step 2) in til seed powder be separated with salt solution with peony seeds powder, the rotating speed of centrifugation is 4000r/min, then be dry under the condition of 70 DEG C to be less than 5% to moisture content in temperature, respectively til seed powder and peony seeds powder squeezed afterwards;
4) salt solution after step 3) being separated distills, and isolates the sesame oil crude oil and peony seeds crude oil that wherein contain.
Embodiment 3
A kind of peony seed oil and sesame oil blending edible oil, formed by the ratio mediation by weight 1:1.3 of the peony seed oil of refining and sesame oil;
Its preparation method is, get til seed respectively and the peony seeds that shells carries out physical squeezing after treatment and obtains sesame oil crude oil and peony seeds crude oil, again the refining peony seed oil obtained after two kinds of crude oils respectively refining and refined sesame oil are in harmonious proportion according to the above ratio and namely obtain product, wherein, the process of described til seed and the peony seeds that shells comprises the following steps:
1) drain after respectively til seed and the peony seeds after shelling being added to the water immersion 3.5h, and put into the freezing 18h of environment that temperature is less than-45 DEG C immediately, then in sub-zero low temperature environment, respectively til seed and peony seeds are ground into the peony seeds powder that the til seed powder that particle diameter is 0.5-1mm and particle diameter are 1-2mm, for subsequent use;
2) the til seed powder of step 1) and peony seeds powder being taken out and under the environment temperature of 20-25 DEG C, join mass concentration is respectively in the salt solution of 17%, then 20h is left standstill after passing into supersonic oscillations 4min wherein, hyperacoustic frequency is 95KHz, the ultrasonic wave of every kilogram of corresponding 135W power of salt solution, for subsequent use;
3) adopt centrifugation make step 2) in til seed powder be separated with salt solution with peony seeds powder, the rotating speed of centrifugation is 3300r/min, then be dry under the condition of 68 DEG C to be less than 5% to moisture content in temperature, respectively til seed powder and peony seeds powder squeezed afterwards;
4) salt solution after step 3) being separated distills, and isolates the sesame oil crude oil and peony seeds crude oil that wherein contain.

Claims (4)

1. the preparation method of a peony seed oil and sesame oil blending edible oil, it is characterized in that: get sesame seed respectively and the peony seeds that shells carries out physical squeezing after treatment and obtains sesame oil crude oil and peony seeds crude oil, again namely the refined sesame oil obtained after two kinds of crude oils respectively refining and refining peony seed oil are obtained product according to the weight ratio mediation of 0.5-2:1, the process of described til seed and the peony seeds that shells comprises the following steps:
1) drain after respectively til seed and the peony seeds after shelling being added to the water immersion 2-5h, and put into the freezing 15-20h of environment that temperature is less than-45 DEG C immediately, then in sub-zero low temperature environment, respectively til seed and peony seeds are ground into the peony seeds powder that the til seed powder that particle diameter is 0.5-1mm and particle diameter are 1-2mm, for subsequent use;
2) the til seed powder of step 1) and peony seeds powder being taken out and under the environment temperature of 20-25 DEG C, join mass concentration is respectively in the salt solution of 15-18%, leaves standstill 17-24h after then passing into supersonic oscillations 3-5min wherein, for subsequent use;
3) adopt centrifugation make step 2) in til seed powder be separated with salt solution with peony seeds powder, be then dry under the condition of 65-70 DEG C to be less than 5% to moisture content in temperature, respectively til seed powder and peony seeds powder squeezed afterwards.
2. the preparation method of peony seed oil according to claim 1 and sesame oil blending edible oil, is characterized in that: described step 2) condition of supersonic oscillations is: the ultrasonic wave of the corresponding 120-150W of salt solution of every kilogram, hyperacoustic frequency is 80-110KHz.
3. the preparation method of peony seed oil according to claim 1 and sesame oil blending edible oil, is characterized in that: the rotating speed of centrifugation in described step 3) is 2500-4000r/min.
4. the preparation method of peony seed oil according to claim 1 and sesame oil blending edible oil, is characterized in that: isolate the salt solution after til seed powder and peony seeds powder in described step 3) and isolate sesame oil crude oil and peony seeds crude oil by distillation procedure.
CN201410080181.3A 2014-03-06 2014-03-06 Blend edible oil of peony seed oil and sesame oil and preparation method of blend edible oil CN103815061B (en)

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CN104904872A (en) * 2015-05-14 2015-09-16 北京同仁堂安徽中药材有限公司 Paeonia suffruticosa seed oil seasoning sesame seed oil and preparation method thereof
CN104920627A (en) * 2015-06-24 2015-09-23 洛阳国花坊牡丹生物科技有限公司 Preparation method of peony seed oil and sesame oil blend edible oil
CN105969506A (en) * 2016-03-21 2016-09-28 安徽华安食品有限公司 Cold pressed sesame oil good for intestinal tract and preparation method thereof
CN105961645A (en) * 2016-03-21 2016-09-28 安徽华安食品有限公司 Ultrasonic treatment cold pressed sesame oil and preparation method thereof
CN105961644A (en) * 2016-03-21 2016-09-28 安徽华安食品有限公司 Cold pressed sesame oil with efficacy of reducing blood fat and preparation method thereof
CN106035757A (en) * 2016-06-03 2016-10-26 河南洛阳红牡丹产业研发有限公司 Preparation method of peony seed and okra seed oil
CN107177409A (en) * 2017-05-31 2017-09-19 广西北部湾珠乡橄榄食品有限公司 A kind of preparation method of olive oil
CN107881005A (en) * 2017-12-12 2018-04-06 滁州尹氏油脂有限公司 A kind of method for lifting sesame oil antioxidant content content

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CN101444239A (en) * 2008-12-26 2009-06-03 北京工商大学 Method for extracting peony seed oil
CN101653174B (en) * 2009-09-07 2012-05-02 兰州牡丹园艺开发公司 Method for preparing blend oil and cold-pressing and extracting peony seed oil
CN101649246B (en) * 2009-09-07 2012-12-19 兰州牡丹园艺开发公司 Method for extracting and refining paeonia rockii seed oil
CN102071097B (en) * 2009-11-20 2012-11-14 菏泽瑞璞牡丹产业科技发展有限公司 Cold-pressing method of peony seed oil

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Effective date of registration: 20180307

Address after: No. 4, unit 2, No. 7, courtyard No. 2, Yucai street, old city city, Henan Province, 702

Patentee after: Yang Panpan

Address before: 471003 Henan province Luoyang Xigong Mill Road Wangcheng Avenue on the west side of Mill Road 89, two floor No. 01-02001

Patentee before: Luoyang Chunkui Agricultural Development Co., Ltd.

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