CN103800246A - 一种义齿清洁液的制备方法 - Google Patents

一种义齿清洁液的制备方法 Download PDF

Info

Publication number
CN103800246A
CN103800246A CN201410067811.3A CN201410067811A CN103800246A CN 103800246 A CN103800246 A CN 103800246A CN 201410067811 A CN201410067811 A CN 201410067811A CN 103800246 A CN103800246 A CN 103800246A
Authority
CN
China
Prior art keywords
grams
cleaning liquid
tooth cleaning
preparation
false tooth
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201410067811.3A
Other languages
English (en)
Other versions
CN103800246B (zh
Inventor
英敏霞
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Qingdao Wilhelm Denture Technology Co ltd
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Publication of CN103800246A publication Critical patent/CN103800246A/zh
Application granted granted Critical
Publication of CN103800246B publication Critical patent/CN103800246B/zh
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Cosmetics (AREA)

Abstract

本发明涉及一种义齿清洁液的制备方法，该方法包括下列步骤：称取防风40克、紫花地丁80克、干姜30克、五味子60克、佩兰20克、甘草60克、马齿苋90克、甘遂40克、独活60克、黄柏90克、升麻20克、白芷50克、益母草20克，加入水2000毫升，置于密封的烧瓶内，在70℃的水浴下加热3小时，冷却至室温，过滤，收集滤液，浓缩至800毫升，即为所述的义齿清洁液。本发明所述的义齿清洁液具有优良去垢杀菌效果，能广泛应用于临床。

Description

一种义齿清洁液的制备方法
本发明是申请日为2012年12月31日、申请号为201210595535.9、发明名称为“义齿清洁液”的专利的分案申请
技术领域
本发明涉及口腔修复领域，具体来说涉及一种义齿清洁液的制备方法。
背景技术
义齿比真牙更易附着细菌，沉积污垢，色素，形成结石，严重影响配戴义齿患者的口腔卫生。据报道戴全口或半口义齿的病人约有65%患义齿性口炎，这是由于义齿不清洁对口腔粘膜造成的创伤，特别是白色念珠菌所致。
发明内容
本发明的目的是提供一种义齿清洁液的制备方法。
为了实现本发明的目的，本发明提供一种义齿清洁液的制备方法，该方法包括下列步骤：称取防风40克、紫花地丁80克、干姜30克、五味子60克、佩兰20克、甘草60克、马齿苋90克、甘遂40克、独活60克、黄柏90克、升麻20克、白芷50克、益母草20克，加入水2000毫升，置于密封的烧瓶内，在70℃的水浴下加热3小时，冷却至室温，过滤，收集滤液，浓缩至800毫升，即为所述的义齿清洁液。
本发明所述的义齿清洁液具有优良去垢杀菌效果，能广泛应用于临床。
具体实施方式
以下通过具体实施方式的描述对本发明作进一步说明，但这并非是对本发明的限制，本领域技术人员根据本发明的基本思想，可以做出各种修改或改进，但是只要不脱离本发明的基本思想，均在本发明的范围之内。
实施例1：本发明义齿清洁液的制备
称取防风40克、紫花地丁80克、干姜30克、五味子60克、佩兰20克、甘草60克、马齿苋90克、甘遂40克、独活60克、黄柏90克、升麻20克、白芷50克、益母草20克，加入水2000毫升，置于密封的烧瓶内。在70℃的水浴下加热3小时，冷却至室温，过滤，收集滤液，浓缩至800毫升，即为本发明所述的义齿清洁液。
实验例1 去垢试验
义齿脏度分级标准：I级，假牙某一部分可见散在的茶渍，烟渍和污垢；II级，假牙各部分均有块状的烟渍、茶渍、污垢或结石；III级，假牙各部分均有大片或整个假牙均有烟渍、茶渍，污垢或结石。
收集具有烟茶渍，污垢和结石的义齿50件，用自来水刷洗后进行脏度分级，其中I级16例，II级12例，III级22例。然后分别浸泡在实施例1中制备的义齿清洁液中，浸泡2h，取出后用棉签擦洗，观察其去垢效果。
去垢效果的评价标准：用棉签擦洗清洁液浸泡后的义齿，根据去除色渍、污垢效果分为“+++”(轻擦即可去除)，“++”(反复轻擦可去除)，“+”(用力擦洗可去除)。
经过检查，所有义齿的去垢效果均符合“+++”的标准。
实验例2 杀菌试验
收集义齿10例，浸于无菌生理盐水中1h，洗刷下义齿上的细菌，用生理盐水稀释成103/ml菌悬液。取103/ml菌悬液0.01ml接种于皿琼脂培养基内，置于37℃温箱中24h，鉴定为常见口腔正常菌，将菌悬液与实施例1中制备的义齿清洁液1:1（体积）混合30min，分别取出0.01ml于皿培养基内划线接种，发现，菌悬液与清洁液1:1混合30min内即可杀灭细菌，无菌斑形成。

Claims (1)

1.一种义齿清洁液的制备方法，其特征在于，该方法可以包括下列步骤：称取防风40克、紫花地丁80克、干姜30克、五味子60克、佩兰20克、甘草60克、马齿苋90克、甘遂40克、独活60克、黄柏90克、升麻20克、白芷50克、益母草20克，加入水2000毫升，置于密封的烧瓶内，在70℃的水浴下加热3小时，冷却至室温，过滤，收集滤液，浓缩至800毫升，即为所述的义齿清洁液。
CN201410067811.3A 2012-12-31 2012-12-31 一种义齿清洁液的制备方法 Active CN103800246B (zh)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201210595535.9A CN103040685B (zh) 2012-12-31 2012-12-31 义齿清洁液

Related Parent Applications (1)

Application Number Title Priority Date Filing Date
CN201210595535.9A Division CN103040685B (zh) 2012-12-31 2012-12-31 义齿清洁液

Publications (2)

Publication Number Publication Date
CN103800246A true CN103800246A (zh) 2014-05-21
CN103800246B CN103800246B (zh) 2015-10-14

Family

ID=48053699

Family Applications (2)

Application Number Title Priority Date Filing Date
CN201410067811.3A Active CN103800246B (zh) 2012-12-31 2012-12-31 一种义齿清洁液的制备方法
CN201210595535.9A Expired - Fee Related CN103040685B (zh) 2012-12-31 2012-12-31 义齿清洁液

Family Applications After (1)

Application Number Title Priority Date Filing Date
CN201210595535.9A Expired - Fee Related CN103040685B (zh) 2012-12-31 2012-12-31 义齿清洁液

Country Status (1)

Country Link
CN (2) CN103800246B (zh)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107281051A (zh) * 2016-04-01 2017-10-24 广州市帕菲克义齿科技有限公司 义齿消毒液

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103393587B (zh) * 2013-08-20 2015-10-07 苏成帅 一种义齿清洁剂的制备方法
CN106377487A (zh) * 2016-09-29 2017-02-08 青岛海之源智能技术有限公司 一种义齿清洁片及其制备方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102008399A (zh) * 2010-12-22 2011-04-13 韶关蓝威消毒药业有限公司 一种抗菌漱口液制备方法
CN102429854A (zh) * 2011-11-30 2012-05-02 于文和 一种用于清除牙结石、黑黄牙斑和预防龋病的中药牙齿洁白粉
CN102600051A (zh) * 2012-03-31 2012-07-25 王战芝 一种义齿清洁片

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6309622B1 (en) * 1999-03-26 2001-10-30 Protech Professional Products, Inc. Antimicrobial denture cleansing compositions
CN102499778B (zh) * 2011-10-19 2015-03-11 五河克菱保健科技有限公司 一种多功能义齿护理片

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102008399A (zh) * 2010-12-22 2011-04-13 韶关蓝威消毒药业有限公司 一种抗菌漱口液制备方法
CN102429854A (zh) * 2011-11-30 2012-05-02 于文和 一种用于清除牙结石、黑黄牙斑和预防龋病的中药牙齿洁白粉
CN102600051A (zh) * 2012-03-31 2012-07-25 王战芝 一种义齿清洁片

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107281051A (zh) * 2016-04-01 2017-10-24 广州市帕菲克义齿科技有限公司 义齿消毒液

Also Published As

Publication number Publication date
CN103800246B (zh) 2015-10-14
CN103040685A (zh) 2013-04-17
CN103040685B (zh) 2014-05-14

Similar Documents

Publication Publication Date Title
CN106176546A (zh) 基于壳聚糖衍生物深度清理、抑菌护齿漱口水及其制备方法
Bosman et al. The reversal of localized experimental gingivitis: a comparison between mechanical toothbrushing procedures and a 0.2% chlorhexidine mouthrinse
CN103800246B (zh) 一种义齿清洁液的制备方法
CN102600051B (zh) 一种义齿清洁片
CN106265087A (zh) 一种牙根管冲洗液及其制备方法
CN109453103A (zh) 一种含瓜拉纳提取物的牙膏及其制备方法
CN107982084A (zh) 一种含三七稀有皂苷的牙膏及其制备方法
CN108175737A (zh) 一种抗牙结石中药牙膏及其制备方法
RU2419437C1 (ru) Способ лечения гиперестезии зубов
CN112494349A (zh) 一种具有抗敏感、牙龈修护和抑菌功效的口腔护理组合物
CN115721594B (zh) 一种含银杏提取物的牙膏及制备方法
KR20060093907A (ko) 식물 추출물로 이루어진 인플루엔자 바이러스에 대한 항바이러스제 및 이를 함유하는 위생용품
CN107375123B (zh) 一种弱碱性中草药假牙清洁片
CN107485584B (zh) 一种口腔护理组合物
CN103393587B (zh) 一种义齿清洁剂的制备方法
CN106885881A (zh) 一种模拟口腔环境的实验方法用于该环境的材料及应用
CN105726386B (zh) 一种防治牙菌斑的牙膏
CN110448496A (zh) 一种具有抗炎、抗敏感以及止痛作用的中药牙膏组合物及其制备方法
CN102357065A (zh) 一种草本复方牙膏
CN105726390B (zh) 一种防治牙龈炎的牙膏
CN100490848C (zh) 一种中药洗液及其制备方法
CN115040465B (zh) 一种有效祛除牙斑、牙垢的增白牙膏
CN107281051A (zh) 义齿消毒液
CN105748342B (zh) 一种含有中草药的牙膏
CN105726350A (zh) 一种含有马尾松叶的牙膏

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
ASS Succession or assignment of patent right

Owner name: GU XIANGMAO

Free format text: FORMER OWNER: YING MINXIA

Effective date: 20150826

C41 Transfer of patent application or patent right or utility model
TA01 Transfer of patent application right

Effective date of registration: 20150826

Address after: 266000 Licang, Qingdao, No. nine East water road, No. 320, No.

Applicant after: Gu Xiangmao

Address before: 272000 Jining Fu Fu Bridge Branch, 44 Youth League Road, Shizhong District, Shandong, Jining

Applicant before: Ying Minxia

C14 Grant of patent or utility model
GR01 Patent grant
CB03 Change of inventor or designer information

Inventor after: Yan Xiaowen

Inventor after: Yuan Xiao

Inventor after: Yu Jiangbo

Inventor after: Li Yantao

Inventor after: Ma Lin

Inventor after: Chen Fei

Inventor before: Ying Minxia

CB03 Change of inventor or designer information
TR01 Transfer of patent right
TR01 Transfer of patent right

Effective date of registration: 20170407

Address after: 266109 Shandong Province, Qingdao city Chengyang District Chunyang Road No. 88 days of the Digital City No. 5 building 14 layer

Patentee after: Qingdao Wilhelm Denture Technology Co.,Ltd.

Address before: 266000 Licang, Qingdao, No. nine East water road, No. 320, No.

Patentee before: Gu Xiangmao

PE01 Entry into force of the registration of the contract for pledge of patent right
PE01 Entry into force of the registration of the contract for pledge of patent right

Denomination of invention: Preparation method of false tooth cleaning liquid

Effective date of registration: 20180606

Granted publication date: 20151014

Pledgee: Qingdao high technology financing Company limited by guarantee

Pledgor: Qingdao Wilhelm Denture Technology Co.,Ltd.

Registration number: 2018370010044

PC01 Cancellation of the registration of the contract for pledge of patent right
PC01 Cancellation of the registration of the contract for pledge of patent right

Date of cancellation: 20190826

Granted publication date: 20151014

Pledgee: Qingdao high technology financing Company limited by guarantee

Pledgor: Qingdao Wilhelm Denture Technology Co.,Ltd.

Registration number: 2018370010044

PE01 Entry into force of the registration of the contract for pledge of patent right
PE01 Entry into force of the registration of the contract for pledge of patent right

Denomination of invention: A preparation method for denture cleaning solution

Effective date of registration: 20230628

Granted publication date: 20151014

Pledgee: Weihai commercial bank Limited by Share Ltd. Qingdao branch

Pledgor: Qingdao Wilhelm Denture Technology Co.,Ltd.

Registration number: Y2023980046514