CN103788899B - Fireproof elastic sealing gum - Google Patents
Fireproof elastic sealing gum Download PDFInfo
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- CN103788899B CN103788899B CN201410057020.2A CN201410057020A CN103788899B CN 103788899 B CN103788899 B CN 103788899B CN 201410057020 A CN201410057020 A CN 201410057020A CN 103788899 B CN103788899 B CN 103788899B
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- China
- Prior art keywords
- parts
- attapulgite
- calcium carbonate
- silicon
- fireproof elastic
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 238000007789 sealing Methods 0.000 title abstract 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 51
- DOIRQSBPFJWKBE-UHFFFAOYSA-N dibutyl phthalate Chemical compound CCCCOC(=O)C1=CC=CC=C1C(=O)OCCCC DOIRQSBPFJWKBE-UHFFFAOYSA-N 0.000 claims abstract description 26
- 239000000377 silicon dioxide Substances 0.000 claims abstract description 25
- 239000000843 powder Substances 0.000 claims abstract description 15
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims abstract description 14
- 229960000892 attapulgite Drugs 0.000 claims abstract description 14
- 239000000835 fiber Substances 0.000 claims abstract description 14
- 239000010438 granite Substances 0.000 claims abstract description 14
- 229910052625 palygorskite Inorganic materials 0.000 claims abstract description 14
- 239000005662 Paraffin oil Substances 0.000 claims abstract description 13
- ISKQADXMHQSTHK-UHFFFAOYSA-N [4-(aminomethyl)phenyl]methanamine Chemical compound NCC1=CC=C(CN)C=C1 ISKQADXMHQSTHK-UHFFFAOYSA-N 0.000 claims abstract description 13
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 claims abstract description 13
- 229910000019 calcium carbonate Inorganic materials 0.000 claims abstract description 13
- 239000000839 emulsion Substances 0.000 claims abstract description 13
- 239000011521 glass Substances 0.000 claims abstract description 13
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 claims abstract description 13
- BIKXLKXABVUSMH-UHFFFAOYSA-N trizinc;diborate Chemical compound [Zn+2].[Zn+2].[Zn+2].[O-]B([O-])[O-].[O-]B([O-])[O-] BIKXLKXABVUSMH-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000002994 raw material Substances 0.000 claims abstract description 9
- 239000000565 sealant Substances 0.000 claims description 17
- 229910052799 carbon Inorganic materials 0.000 claims description 13
- 235000013312 flour Nutrition 0.000 claims description 13
- 239000003921 oil Substances 0.000 claims description 13
- 238000003756 stirring Methods 0.000 claims description 13
- 239000004575 stone Substances 0.000 claims description 13
- DMYOHQBLOZMDLP-UHFFFAOYSA-N 1-[2-(2-hydroxy-3-piperidin-1-ylpropoxy)phenyl]-3-phenylpropan-1-one Chemical compound C1CCCCN1CC(O)COC1=CC=CC=C1C(=O)CCC1=CC=CC=C1 DMYOHQBLOZMDLP-UHFFFAOYSA-N 0.000 claims description 12
- 229920013649 Paracril Polymers 0.000 claims description 12
- -1 acrylic ester Chemical class 0.000 claims description 12
- 229910021502 aluminium hydroxide Inorganic materials 0.000 claims description 12
- XLXGCFTYXICXJF-UHFFFAOYSA-N ethylsilicon Chemical compound CC[Si] XLXGCFTYXICXJF-UHFFFAOYSA-N 0.000 claims description 12
- 229940059574 pentaerithrityl Drugs 0.000 claims description 12
- 229960001866 silicon dioxide Drugs 0.000 claims description 12
- 235000012239 silicon dioxide Nutrition 0.000 claims description 12
- 238000002360 preparation method Methods 0.000 claims description 5
- 238000010792 warming Methods 0.000 claims description 5
- 230000005855 radiation Effects 0.000 abstract description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 3
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 abstract 1
- 235000017166 Bambusa arundinacea Nutrition 0.000 abstract 1
- 235000017491 Bambusa tulda Nutrition 0.000 abstract 1
- 241001330002 Bambuseae Species 0.000 abstract 1
- 229920000459 Nitrile rubber Polymers 0.000 abstract 1
- 235000015334 Phyllostachys viridis Nutrition 0.000 abstract 1
- 239000011425 bamboo Substances 0.000 abstract 1
- 239000011324 bead Substances 0.000 abstract 1
- 239000003610 charcoal Substances 0.000 abstract 1
- 229920001971 elastomer Polymers 0.000 abstract 1
- XWRLQRLQUKZEEU-UHFFFAOYSA-N ethyl(hydroxy)silicon Chemical compound CC[Si]O XWRLQRLQUKZEEU-UHFFFAOYSA-N 0.000 abstract 1
- 239000012530 fluid Substances 0.000 abstract 1
- 229910021485 fumed silica Inorganic materials 0.000 abstract 1
- 229910052900 illite Inorganic materials 0.000 abstract 1
- 239000004005 microsphere Substances 0.000 abstract 1
- VGIBGUSAECPPNB-UHFFFAOYSA-L nonaaluminum;magnesium;tripotassium;1,3-dioxido-2,4,5-trioxa-1,3-disilabicyclo[1.1.1]pentane;iron(2+);oxygen(2-);fluoride;hydroxide Chemical compound [OH-].[O-2].[O-2].[O-2].[O-2].[O-2].[F-].[Mg+2].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[K+].[K+].[K+].[Fe+2].O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2 VGIBGUSAECPPNB-UHFFFAOYSA-L 0.000 abstract 1
- 229920001021 polysulfide Polymers 0.000 abstract 1
- 239000005077 polysulfide Substances 0.000 abstract 1
- 150000008117 polysulfides Polymers 0.000 abstract 1
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 239000003063 flame retardant Substances 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 description 2
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 description 1
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 1
- 229930040373 Paraformaldehyde Natural products 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 229920002866 paraformaldehyde Polymers 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
Landscapes
- Compositions Of Macromolecular Compounds (AREA)
- Sealing Material Composition (AREA)
Abstract
The invention discloses fireproof elastic sealing gum which is prepared from the following raw materials in parts by weight: 50-80 parts of acrylate emulsion, 5-6 parts of polysulfide rubber, 5-10 parts of nitrile rubber, 3-5 parts of granite powder, 2-3 parts of illite powder, 2-3 parts of attapulgite, 3-5 parts of bamboo charcoal fiber, 2-3 parts of hollow microspheres, 1-3 parts of glass beads, 5-6 parts of fumed silica, 5-8 parts of nanometer calcium carbonate, 10-12 parts of ethyl siloxane fluid, 3-4 parts of aluminum hydroxide, 0.5-1.5 parts of dibutyl tin diacetate, 3-5 parts of dibutyl phthalate, 5-10 parts of zinc borate, 2-3 parts of pentaerythritol, 2-3 parts of silica and 5-8 parts of paraffin oil. The fireproof elastic sealing gum disclosed by the invention has excellent water resistance and radiation resistance, and also has cold resistance, high temperature resistance and good flame resistance.
Description
Technical field
The present invention relates to fireproof material technology field, particularly relate to a kind of fireproof elastic sealant.
Background technology
Fireproof elastic sealant is mainly used in cable, airduct, oil pipe, tracheae etc. isolates through the fire prevention of the various opening formed when wall, floor and cable testing bridge.Because of the requirement of particular surroundings, fireproof seal gum must have resistance to ray, resistance to ozone, cold-resistant, ageing-resistant, high temperature resistant, fire-retardant contour performance.Existing seal gum can not possess fire-retardant, radiation hardness, resistance to ozone, the property such as water-fast simultaneously.
Summary of the invention
The object of the invention is to overcome the deficiencies in the prior art, provide a kind of and there is excellent water tolerance and radiation resistance, and there is fireproof elastic sealant that is cold-resistant, high temperature resistant, good flame resistance simultaneously.
The present invention adopts following technical scheme to achieve these goals:
A kind of fireproof elastic sealant, comprise the raw material of following weight part: acrylic ester emulsion 50-80 part, thiorubber 5-6 part, paracril 5-10 part, granite powder 3-5 part, Erie stone flour 2-3 part, attapulgite 2-3 part, bamboo-carbon fibre 3-5 part, cenosphere 2-3 part, granulated glass sphere 1-3 part, gas-phase silica 5-6 part, nano-calcium carbonate 5-8 part, ethyl silicon oil 10-12 part, aluminium hydroxide 3-4 part, dibutyltin diacetate 0.5-1.5 part, dibutyl phthalate 3-5 part, zinc borate 5-10 part, tetramethylolmethane 2-3 part, silicon-dioxide 2-3 part, paraffin oil 5-8 part.
Preferably, fireproof elastic sealant, comprises the raw material of following weight part: acrylic ester emulsion 60 parts, thiorubber 5 parts, paracril 10 parts, granite powder 5 parts, Erie's stone flour 3 parts, attapulgite 2 parts, bamboo-carbon fibre 4 parts, cenosphere 2 parts, granulated glass sphere 2 parts, gas-phase silica 5 parts, nano-calcium carbonate 6 parts, ethyl silicon oil 10 parts, 3 parts, aluminium hydroxide, dibutyltin diacetate 1.2 parts, dibutyl phthalate 4 parts, zinc borate 6 parts, tetramethylolmethane 2 parts, silicon-dioxide 2 parts, paraffin oil 6 parts.
Described fireproof elastic sealant, preparation method is: first add in kneader by said ratio by acrylic ester emulsion, thiorubber, paracril, dibutyltin diacetate, dibutyl phthalate, zinc borate, tetramethylolmethane, paraffin oil, at 30-50 DEG C, stir 20-30 minute; Add granite powder, Erie's stone flour, attapulgite, bamboo-carbon fibre, cenosphere, granulated glass sphere again, 2-3 hour is stirred at 50-80 DEG C, then gas-phase silica, nano-calcium carbonate, ethyl silicon oil, aluminium hydroxide, silicon-dioxide stirring 1-2 hour is added, vacuumize and heat and be slowly warming up to 50-60 DEG C, keep vacuum tightness-0.065 ± 0.002Mpa, insulated and stirred 1-2 hour.
Compared with the prior art, beneficial effect of the present invention is as follows:
The present invention is by adding water-fast, radiation hardness, the high thermal resistance compositions such as granite powder, Erie's stone flour, attapulgite, cenosphere, in addition, the objectionable impurities such as bamboo-carbon fibre PARA FORMALDEHYDE PRILLS(91,95), benzene, toluene, ammonia and dust can play absorption, decompose the effect of peculiar smell and smelly eliminating.Fireproof elastic sealant of the present invention has excellent water tolerance and radiation resistance, and has cold-resistant, high temperature resistant and good flame retardant properties simultaneously.
Embodiment
Below in conjunction with embodiment, the invention will be further described.
Embodiment 1:
A kind of fireproof elastic sealant, comprises the raw material of following weight part: the raw material comprising following weight part: acrylic ester emulsion 60 parts, thiorubber 5 parts, paracril 10 parts, granite powder 5 parts, Erie's stone flour 3 parts, attapulgite 2 parts, bamboo-carbon fibre 4 parts, cenosphere 2 parts, granulated glass sphere 2 parts, gas-phase silica 5 parts, nano-calcium carbonate 6 parts, ethyl silicon oil 10 parts, 3 parts, aluminium hydroxide, dibutyltin diacetate 1.2 parts, dibutyl phthalate 4 parts, zinc borate 6 parts, tetramethylolmethane 2 parts, silicon-dioxide 2 parts, paraffin oil 6 parts.
Described fireproof elastic sealant, preparation method is: first add in kneader by said ratio by acrylic ester emulsion, thiorubber, paracril, dibutyltin diacetate, dibutyl phthalate, zinc borate, tetramethylolmethane, paraffin oil, stirs 30 minutes at 40 DEG C; Add granite powder, Erie's stone flour, attapulgite, bamboo-carbon fibre, cenosphere, granulated glass sphere again, stir 3 hours at 60 DEG C, then add gas-phase silica, nano-calcium carbonate, ethyl silicon oil, aluminium hydroxide, silicon-dioxide stirs 2 hours, vacuumize and heat and be slowly warming up to 60 DEG C, keep vacuum tightness-0.065Mpa, insulated and stirred 2 hours.
Embodiment 2:
A kind of fireproof elastic sealant, comprises the raw material of following weight part: acrylic ester emulsion 50 parts, thiorubber 5 parts, paracril 7 parts, granite powder 3, part, Erie's stone flour 2 parts, attapulgite 2 parts, bamboo-carbon fibre 3 parts, cenosphere 2 parts, granulated glass sphere 1 part, gas-phase silica 5 parts, nano-calcium carbonate 5 parts, ethyl silicon oil 10 parts, 3 parts, aluminium hydroxide, dibutyltin diacetate 0.7 part, dibutyl phthalate 3 parts, zinc borate 8 parts, tetramethylolmethane 2 parts, silicon-dioxide 2 parts, paraffin oil 5 parts.
Described fireproof elastic sealant, preparation method is: first add in kneader by said ratio by acrylic ester emulsion, thiorubber, paracril, dibutyltin diacetate, dibutyl phthalate, zinc borate, tetramethylolmethane, paraffin oil, stirs 30 minutes at 30 DEG C; Add granite powder, Erie's stone flour, attapulgite, bamboo-carbon fibre, cenosphere, granulated glass sphere again, stir 3 hours at 50 DEG C, then add gas-phase silica, nano-calcium carbonate, ethyl silicon oil, aluminium hydroxide, silicon-dioxide stirs 2 hours, vacuumize and heat and be slowly warming up to 50 DEG C, keep vacuum tightness-0.063Mpa, insulated and stirred 1 hour.
Embodiment 3:
A kind of fireproof elastic sealant, comprises the raw material of following weight part: acrylic ester emulsion 80 parts, thiorubber 6 parts, paracril 10 parts, granite powder 5 parts, Erie's stone flour 3 parts, attapulgite 3 parts, bamboo-carbon fibre 5 parts, cenosphere 3 parts, granulated glass sphere 3 parts, gas-phase silica 6 parts, nano-calcium carbonate 8 parts, ethyl silicon oil 12 parts, 4 parts, aluminium hydroxide, dibutyltin diacetate 1.5 parts, dibutyl phthalate 5 parts, zinc borate 10 parts, tetramethylolmethane 3 parts, silicon-dioxide 3 parts, paraffin oil 8 parts.
Described fireproof elastic sealant, preparation method is: first add in kneader by said ratio by acrylic ester emulsion, thiorubber, paracril, dibutyltin diacetate, dibutyl phthalate, zinc borate, tetramethylolmethane, paraffin oil, stirs 20 minutes at 50 DEG C; Add granite powder, Erie's stone flour, attapulgite, bamboo-carbon fibre, cenosphere, granulated glass sphere again, stir 2 hours at 80 DEG C, then add gas-phase silica, nano-calcium carbonate, ethyl silicon oil, aluminium hydroxide, silicon-dioxide stirs 2 hours, vacuumize and heat and be slowly warming up to 60 DEG C, keep vacuum tightness-0.067Mpa, insulated and stirred 2 hours.
Claims (3)
1. a fireproof elastic sealant, it is characterized in that: the raw material comprising following weight part: acrylic ester emulsion 50-80 part, thiorubber 5-6 part, paracril 5-10 part, granite powder 3-5 part, Erie stone flour 2-3 part, attapulgite 2-3 part, bamboo-carbon fibre 3-5 part, cenosphere 2-3 part, granulated glass sphere 1-3 part, gas-phase silica 5-6 part, nano-calcium carbonate 5-8 part, ethyl silicon oil 10-12 part, aluminium hydroxide 3-4 part, dibutyltin diacetate 0.5-1.5 part, dibutyl phthalate 3-5 part, zinc borate 5-10 part, tetramethylolmethane 2-3 part, silicon-dioxide 2-3 part, paraffin oil 5-8 part.
2. fireproof elastic sealant according to claim 1, is characterized in that: the raw material comprising following weight part: acrylic ester emulsion 60 parts, thiorubber 5 parts, paracril 10 parts, granite powder 5 parts, Erie's stone flour 3 parts, attapulgite 2 parts, bamboo-carbon fibre 4 parts, cenosphere 2 parts, granulated glass sphere 2 parts, gas-phase silica 5 parts, nano-calcium carbonate 6 parts, ethyl silicon oil 10 parts, 3 parts, aluminium hydroxide, dibutyltin diacetate 1.2 parts, dibutyl phthalate 4 parts, zinc borate 6 parts, tetramethylolmethane 2 parts, silicon-dioxide 2 parts, paraffin oil 6 parts.
3. fireproof elastic sealant according to claim 1, it is characterized in that: its preparation method is: first by said ratio, acrylic ester emulsion, thiorubber, paracril, dibutyltin diacetate, dibutyl phthalate, zinc borate, tetramethylolmethane, paraffin oil are added in kneader, at 30-50 DEG C, stir 20-30 minute; Add granite powder, Erie's stone flour, attapulgite, bamboo-carbon fibre, cenosphere, granulated glass sphere again, 2-3 hour is stirred at 50-80 DEG C, then gas-phase silica, nano-calcium carbonate, ethyl silicon oil, aluminium hydroxide, silicon-dioxide stirring 1-2 hour is added, vacuumize and heat and be slowly warming up to 50-60 DEG C, keep vacuum tightness-0.065 ± 0.002Mpa, insulated and stirred 1-2 hour.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410057020.2A CN103788899B (en) | 2014-02-20 | 2014-02-20 | Fireproof elastic sealing gum |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410057020.2A CN103788899B (en) | 2014-02-20 | 2014-02-20 | Fireproof elastic sealing gum |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103788899A CN103788899A (en) | 2014-05-14 |
| CN103788899B true CN103788899B (en) | 2015-07-08 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410057020.2A Expired - Fee Related CN103788899B (en) | 2014-02-20 | 2014-02-20 | Fireproof elastic sealing gum |
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Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105652397A (en) * | 2016-01-27 | 2016-06-08 | 苏州权素船舶电子有限公司 | Wear-resisting optical cable |
| CN106147097A (en) * | 2016-08-26 | 2016-11-23 | 安庆市金鹰新型建材科技股份有限公司 | A kind of wood plastic decorative construction material |
| CN109575845A (en) * | 2018-11-26 | 2019-04-05 | 天长市永泰密封材料有限公司 | A kind of fire-type sealant and preparation method thereof |
| CN111100584A (en) * | 2019-12-18 | 2020-05-05 | 湖南省和祥润新材料有限公司 | Building decoration adhesive and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1370809A (en) * | 2002-02-26 | 2002-09-25 | 李绍弟 | Multifunctional high-viscosity polyphenyl glue |
| EP2343339A1 (en) * | 2008-10-08 | 2011-07-13 | Denki Kagaku Kogyo Kabushiki Kaisha | Adhesive composition and adhesion method |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7524563B2 (en) * | 2005-04-13 | 2009-04-28 | Shin-Etsu Chemical Co., Ltd. | Flame retardant adhesive composition, and adhesive sheet, coverlay film and flexible copper-clad laminate using same |
-
2014
- 2014-02-20 CN CN201410057020.2A patent/CN103788899B/en not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1370809A (en) * | 2002-02-26 | 2002-09-25 | 李绍弟 | Multifunctional high-viscosity polyphenyl glue |
| EP2343339A1 (en) * | 2008-10-08 | 2011-07-13 | Denki Kagaku Kogyo Kabushiki Kaisha | Adhesive composition and adhesion method |
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| CN103788899A (en) | 2014-05-14 |
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