CN103770195A - Fiber ceramic powder compression forming process - Google Patents

Fiber ceramic powder compression forming process Download PDF

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Publication number
CN103770195A
CN103770195A CN201210396191.9A CN201210396191A CN103770195A CN 103770195 A CN103770195 A CN 103770195A CN 201210396191 A CN201210396191 A CN 201210396191A CN 103770195 A CN103770195 A CN 103770195A
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Prior art keywords
fiber
fiber ceramics
composite
ceramics powder
forming technique
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CN201210396191.9A
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CN103770195B (en
Inventor
樊强
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Zhejiang Jiahong Automobile Technology Co ltd
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Shanghai Jiu Qian Industrial Co Ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B28WORKING CEMENT, CLAY, OR STONE
    • B28BSHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
    • B28B1/00Producing shaped prefabricated articles from the material
    • B28B1/52Producing shaped prefabricated articles from the material specially adapted for producing articles from mixtures containing fibres, e.g. asbestos cement
    • B28B1/521Producing shaped prefabricated articles from the material specially adapted for producing articles from mixtures containing fibres, e.g. asbestos cement from dry mixtures to which a setting agent is applied after forming
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B28WORKING CEMENT, CLAY, OR STONE
    • B28BSHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
    • B28B1/00Producing shaped prefabricated articles from the material
    • B28B1/52Producing shaped prefabricated articles from the material specially adapted for producing articles from mixtures containing fibres, e.g. asbestos cement
    • B28B1/522Producing shaped prefabricated articles from the material specially adapted for producing articles from mixtures containing fibres, e.g. asbestos cement for producing multi-layered articles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B28WORKING CEMENT, CLAY, OR STONE
    • B28BSHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
    • B28B3/00Producing shaped articles from the material by using presses; Presses specially adapted therefor

Abstract

The invention relates to a composite material, in particular to a fiber ceramic powder compression forming process. The fiber ceramic powder compression forming process is characterized by comprising the steps of 1 mixing fiber powder and ceramic powder and adding a cutting agent into the mixture to prepare a fiber and ceramic powder mixture; 2 performing compression forming on the fiber and ceramic powder mixture to form a fiber ceramic powder blank; 3 enabling the curing agent to react to enable the fiber ceramic powder blank to be cured so as to obtain a fiber ceramic composite material. The fiber ceramic composite material is manufactured by means of a compression curing method, and the fiber ceramic powder compression forming process has the advantages of being simple and high in efficiency.

Description

Fiber ceramics powder pressing forming technique
Technical field
The present invention relates to material, be specifically related to composite.
Background technology
In composite production process, the preparation method of composite mainly contains sintering process, fusion casting, meltblown method etc.Wherein sintering process is the most common.Sintering process is by part material pre-fired grog, and broken and screening, then mixes with raw material according to a certain ratio, through overmolding, be dried and burn till.Technique is comparatively complicated.
Summary of the invention
The object of the invention is to, provide a kind of fiber ceramics powder pressing forming technique, to solve the problems of the technologies described above.
Technical problem solved by the invention can realize by the following technical solutions:
Fiber ceramics powder pressing forming technique, is characterized in that,
Step 1, composite fibre powder, ceramic powders, and sneak into curing agent, prepare fiber ceramics powder mixture;
Step 2, gets fiber ceramics powder mixture, compressing, forms fiber ceramics idiosome;
Step 3, lures curing agent reaction into, makes fiber ceramics idiosome be solidified into fiber ceramics composite.The present invention prepares fiber ceramics composite by the method for press curing, has the advantages that technique is simple, efficiency is high.
Fiber dust preferred glass fibers powder in step 1.Can be long glass fibres powder, can be also the short glass powder of cutting.Glass fibre is to have good insulating, heat resistance is strong, corrosion resistance good, mechanical strength is high feature.And it manufactures through high temperature melting, wire drawing, doff, the technique such as weave cotton cloth take glass marble or discarded glass as raw material, have the advantages that cost is low.In step 1, fiber dust can also be ceramic fibre, and ceramic fibre is a kind of lightweight refracrory, has lightweight, high temperature resistant, Heat stability is good, thermal conductivity is low, specific heat is little and the advantage such as resistance to mechanical shock.
And, in fiber ceramics powder mixture, can also sneak into bonding agent, further to improve bonding strength everywhere.
Curing agent in step 1 can be thermal curing agents, light curing agent.When adopting thermal curing agents, step 3 can be lured curing agent reaction into by the mode of heating.When adopting light curing agent, step 3 can be lured curing agent reaction into by the mode of ultra violet lamp.Certainly also allow two kinds of curing agent to coexist.While adopting thermal curing agents, preferably high temperature thermal curing agents.Step 3 is lured the reaction of high temperature thermal curing agents into by the mode of high-temperature firing.
In step 2, first layering compacting, then by each layer of stacking moulding, then suppresses, and forms fiber ceramics idiosome.Also can first suppress one deck, then on the layer suppressing, feed in raw material and suppress again, then repeat the reinforced process of compacting again, until moulding forms fiber ceramics idiosome.
In step 2, can not adding between the layers any is not the material of fiber ceramics powder mixture.Intensity is consistent everywhere for the fiber ceramics composite solidifying to form with assurance.Also can add between the layers adhesive, increase the intensity of junction by adhesive.
Above-mentioned two methods have effectively improved the tight ness rating of piling up, and can, by above-mentioned two methods, obtain fine and close fiber ceramics idiosome.
The present invention can also adopt following technique, first by fiber ceramics powder mixture compacting stratification, form Fiber Laminated pottery idiosome, then lure curing agent reaction into, make Fiber Laminated pottery idiosome be solidified into Fiber Laminated ceramic composite, then by the stacking moulding of a plurality of stratiform fiber ceramics composite, and each adjacent two-layer Fiber Laminated ceramic composite is connected, forms fiber ceramics composite.
Can two-layer Fiber Laminated ceramic composite be connected by adhesive.Also can between two-layer Fiber Laminated ceramic composite, add fiber ceramics powder mixture, then lure the curing agent reaction in fiber ceramics powder mixture into, two-layer Fiber Laminated ceramic composite is connected.For example, lure its reaction into by the mode of calcining.
Accompanying drawing explanation
Fig. 1 is process flow diagram of the present invention.
The specific embodiment
For technological means, creation characteristic that the present invention is realized, reach object and effect is easy to understand, further set forth the present invention below in conjunction with concrete diagram.
With reference to Fig. 1, fiber ceramics powder pressing forming technique, mainly comprises:
Step 1, composite fibre powder, ceramic powders, and sneak into curing agent, prepare fiber ceramics powder mixture;
Step 2, gets fiber ceramics powder mixture, compressing, forms fiber ceramics idiosome;
Step 3, lures curing agent reaction into, makes fiber ceramics idiosome be solidified into fiber ceramics composite.The present invention prepares fiber ceramics composite by the method for press curing, has the advantages that technique is simple, efficiency is high.
Specific embodiment 1
Step 1, composite fibre powder, ceramic powders, and sneak into curing agent, prepare fiber ceramics powder mixture;
Step 2, first layering compacting, then by each layer of stacking moulding, then suppresses, and forms fiber ceramics idiosome.
Step 3, lures curing agent reaction into, makes fiber ceramics idiosome be solidified into fiber ceramics composite.The present invention prepares fiber ceramics composite by the method for press curing, has the advantages that technique is simple, efficiency is high.
Specific embodiment 2
Step 1, composite fibre powder, ceramic powders, and sneak into curing agent, prepare fiber ceramics powder mixture;
Step 2, first suppresses one deck, then on the layer suppressing, feeds in raw material and suppresses, then repeats the reinforced process of compacting again, until moulding forms fiber ceramics idiosome.
Step 3, lures curing agent reaction into, makes fiber ceramics idiosome be solidified into fiber ceramics composite.The present invention prepares fiber ceramics composite by the method for press curing, has the advantages that technique is simple, efficiency is high.
In specific embodiment 1, example 2, can not adding between the layers any is not the material of fiber ceramics powder mixture.Intensity is consistent everywhere for the fiber ceramics composite solidifying to form with assurance.Also can add between the layers adhesive, increase the intensity of junction by adhesive.
Specific embodiment 3
Step 1, composite fibre powder, ceramic powders, and sneak into curing agent, prepare fiber ceramics powder mixture;
Step 2, first by fiber ceramics powder mixture compacting stratification, form Fiber Laminated pottery idiosome, then lure curing agent reaction into, make Fiber Laminated pottery idiosome be solidified into Fiber Laminated ceramic composite, then by the stacking moulding of a plurality of stratiform fiber ceramics composite, and each adjacent two-layer Fiber Laminated ceramic composite is connected, forms fiber ceramics composite.
Can two-layer Fiber Laminated ceramic composite be connected by adhesive.Also can between two-layer Fiber Laminated ceramic composite, add fiber ceramics powder mixture, then lure the curing agent reaction in fiber ceramics powder mixture into, two-layer Fiber Laminated ceramic composite is connected.For example, lure its reaction into by the mode of calcining.
In above-mentioned three embodiment, fiber dust preferred glass fibers powder in step 1.Can be long glass fibres powder, can be also the short glass powder of cutting.Glass fibre is to have good insulating, heat resistance is strong, corrosion resistance good, mechanical strength is high feature.And it manufactures through high temperature melting, wire drawing, doff, the technique such as weave cotton cloth take glass marble or discarded glass as raw material, have the advantages that cost is low.In step 1, fiber dust can also be ceramic fibre, and ceramic fibre is a kind of lightweight refracrory, has lightweight, high temperature resistant, Heat stability is good, thermal conductivity is low, specific heat is little and the advantage such as resistance to mechanical shock.
And, in fiber ceramics powder mixture, can also sneak into bonding agent, further to improve bonding strength everywhere.
Curing agent in step 1 can be thermal curing agents, light curing agent.When adopting thermal curing agents, step 3 can be lured curing agent reaction into by the mode of heating.When adopting light curing agent, step 3 can be lured curing agent reaction into by the mode of ultra violet lamp.Certainly also allow two kinds of curing agent to coexist.While adopting thermal curing agents, preferably high temperature thermal curing agents.Step 3 is lured the reaction of high temperature thermal curing agents into by the mode of high-temperature firing.
The various embodiments described above all can be prepared fiber ceramics composite.In described fiber ceramics composite, contain glass fibre.Experiment shows, the high temperature resistant temperature of this material can reach 1000 ~ 1200 degrees Celsius.
More than show and described basic principle of the present invention and principal character and advantage of the present invention.The technical staff of the industry should understand; the present invention is not restricted to the described embodiments; that in above-described embodiment and description, describes just illustrates principle of the present invention; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications, and these changes and improvements all fall in the claimed scope of the invention.The claimed scope of the present invention is defined by appending claims and equivalent thereof.

Claims (10)

1. fiber ceramics powder pressing forming technique, is characterized in that,
Step 1, composite fibre powder, ceramic powders, and sneak into curing agent, prepare fiber ceramics powder mixture;
Step 2, gets fiber ceramics powder mixture, compressing, forms fiber ceramics idiosome;
Step 3, lures curing agent reaction into, makes fiber ceramics idiosome be solidified into fiber ceramics composite.
2. fiber ceramics powder pressing forming technique according to claim 1, is characterized in that, in step 2, first layering compacting, then by each layer of stacking moulding, then suppresses, and forms fiber ceramics idiosome.
3. fiber ceramics powder pressing forming technique according to claim 1, is characterized in that, in step 2, first suppress one deck, then on the layer suppressing, feed in raw material and suppress again, then repeat the reinforced process of compacting again, until moulding forms fiber ceramics idiosome.
4. according to the fiber ceramics powder pressing forming technique described in claim 2 or 3, it is characterized in that, in step 2, not adding between the layers any is not the material of fiber ceramics powder mixture.
5. fiber ceramics powder pressing forming technique according to claim 1, it is characterized in that, first by fiber ceramics powder mixture compacting stratification, form Fiber Laminated pottery idiosome, then lure curing agent reaction into, make Fiber Laminated pottery idiosome be solidified into Fiber Laminated ceramic composite, then by the stacking moulding of a plurality of stratiform fiber ceramics composite, and each adjacent two-layer Fiber Laminated ceramic composite is connected, form fiber ceramics composite.
6. fiber ceramics powder pressing forming technique according to claim 5, it is characterized in that, between two-layer Fiber Laminated ceramic composite, add fiber ceramics powder mixture, then lure the curing agent reaction in fiber ceramics powder mixture into, two-layer Fiber Laminated ceramic composite is connected.
7. according to the fiber ceramics powder pressing forming technique described in claim 1,2,3,5,6, it is characterized in that, in step 1, fiber dust is glass fibre powder.
8. according to the fiber ceramics powder pressing forming technique described in claim 1,2,3,5,6, it is characterized in that, the curing agent in step 1 is thermal curing agents, and step 3 is lured curing agent reaction into by the mode of heating.
9. fiber ceramics powder pressing forming technique according to claim 8, is characterized in that, described thermal curing agents is high temperature thermal curing agents, and step 3 is lured the reaction of high temperature thermal curing agents into by the mode of high-temperature firing.
10. fiber ceramics composite, is characterized in that, the fiber ceramics powder pressing forming technique preparation in described fiber ceramics composite material by adopting claim 1,2,3,5,6 described in any one.
CN201210396191.9A 2012-10-17 2012-10-17 Fiber ceramic powder compression forming process Active CN103770195B (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104070470A (en) * 2014-06-24 2014-10-01 郑州磨料磨具磨削研究所有限公司 Abrasive block layered press forming method and forming device thereof
CN104942967A (en) * 2015-05-27 2015-09-30 吾晓于 Ceramic matrix composite material forming technology
CN107912622A (en) * 2017-12-06 2018-04-17 邹家勇 Ensilage for ruminant and preparation method thereof
CN107981042A (en) * 2017-12-06 2018-05-04 邹家勇 Rush digestion feed for livestock and preparation method thereof
CN109016078A (en) * 2017-06-10 2018-12-18 清远市美邦陶瓷实业有限公司 A kind of fiber ceramics powder pressing forming technique

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CN1251083A (en) * 1997-03-21 2000-04-19 戴姆勒-克莱斯勒股份公司 Fibre-reinforced composite ceramics and method of producing same
CN1288874A (en) * 1999-09-16 2001-03-28 Sgl技术有限公司 Fiber-reinforced ceramic substrate composite material
CN1291538A (en) * 1999-09-10 2001-04-18 精工电子有限公司 Shaping method of ceramics
CN1387984A (en) * 2002-06-25 2003-01-01 施江澜 Formation techn of fiber reinforced ceramic-base composite material
CN1446676A (en) * 2003-04-04 2003-10-08 王军 Method of fabricating cloths for imitating natural bricks and its devices
CN1586851A (en) * 2004-09-03 2005-03-02 佛山市特地陶瓷有限公司 Distributing method for ceramic tile
EP1734023A1 (en) * 2005-06-14 2006-12-20 Deutsches Zentrum für Luft- und Raumfahrt e.V. Adjustment of the fibre content by volume of oxide ceramic fibre - composite materials
CN101353259A (en) * 2007-07-27 2009-01-28 日本碍子株式会社 Ceramic moulding body, ceramic component, and manufacturing method of ceramic moulding body and ceramic component
CN101544014A (en) * 2009-04-08 2009-09-30 武汉理工大学 Preparation method for novel high temperature resisting organic fire prevention heat insulating material
CN101795856A (en) * 2007-09-06 2010-08-04 美商绩优图科技股份有限公司 Porous washcoat-bonded fiber substrate
CN101864830A (en) * 2009-04-17 2010-10-20 卢清文 Natural stone material simulated ceramic tile and manufacture method thereof
CN102335950A (en) * 2010-07-15 2012-02-01 朱胜利 Forming method of ceramic biscuit with impact resisting structure

Patent Citations (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1115974A (en) * 1993-11-04 1996-01-31 日机装株式会社 Pressure molding apparatus and pressure molding method
CN1251083A (en) * 1997-03-21 2000-04-19 戴姆勒-克莱斯勒股份公司 Fibre-reinforced composite ceramics and method of producing same
CN1291538A (en) * 1999-09-10 2001-04-18 精工电子有限公司 Shaping method of ceramics
CN1288874A (en) * 1999-09-16 2001-03-28 Sgl技术有限公司 Fiber-reinforced ceramic substrate composite material
CN1387984A (en) * 2002-06-25 2003-01-01 施江澜 Formation techn of fiber reinforced ceramic-base composite material
CN1446676A (en) * 2003-04-04 2003-10-08 王军 Method of fabricating cloths for imitating natural bricks and its devices
CN1586851A (en) * 2004-09-03 2005-03-02 佛山市特地陶瓷有限公司 Distributing method for ceramic tile
EP1734023A1 (en) * 2005-06-14 2006-12-20 Deutsches Zentrum für Luft- und Raumfahrt e.V. Adjustment of the fibre content by volume of oxide ceramic fibre - composite materials
CN101353259A (en) * 2007-07-27 2009-01-28 日本碍子株式会社 Ceramic moulding body, ceramic component, and manufacturing method of ceramic moulding body and ceramic component
CN101795856A (en) * 2007-09-06 2010-08-04 美商绩优图科技股份有限公司 Porous washcoat-bonded fiber substrate
CN101544014A (en) * 2009-04-08 2009-09-30 武汉理工大学 Preparation method for novel high temperature resisting organic fire prevention heat insulating material
CN101864830A (en) * 2009-04-17 2010-10-20 卢清文 Natural stone material simulated ceramic tile and manufacture method thereof
CN102335950A (en) * 2010-07-15 2012-02-01 朱胜利 Forming method of ceramic biscuit with impact resisting structure

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104070470A (en) * 2014-06-24 2014-10-01 郑州磨料磨具磨削研究所有限公司 Abrasive block layered press forming method and forming device thereof
CN104942967A (en) * 2015-05-27 2015-09-30 吾晓于 Ceramic matrix composite material forming technology
CN109016078A (en) * 2017-06-10 2018-12-18 清远市美邦陶瓷实业有限公司 A kind of fiber ceramics powder pressing forming technique
CN109016078B (en) * 2017-06-10 2020-11-13 清远市美邦陶瓷实业有限公司 Fiber ceramic powder compression molding process
CN107912622A (en) * 2017-12-06 2018-04-17 邹家勇 Ensilage for ruminant and preparation method thereof
CN107981042A (en) * 2017-12-06 2018-05-04 邹家勇 Rush digestion feed for livestock and preparation method thereof

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Effective date of registration: 20191211

Address after: 3 Xingye Branch Road, Yaozhuang Town, Jiashan County, Jiaxing City, Zhejiang Province

Patentee after: ZHEJIANG JIAHONG AUTOMOBILE TECHNOLOGY Co.,Ltd.

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Address after: 3 Xingye Branch Road, Yaozhuang Town, Jiashan County, Jiaxing City, Zhejiang Province

Patentee after: Zhejiang Jiahong Automobile Technology Co.,Ltd.

Address before: 3 Xingye Branch Road, Yaozhuang Town, Jiashan County, Jiaxing City, Zhejiang Province

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Denomination of invention: Pressing process of fiber ceramic powder

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