CN103760019A - Horizontal material stretch compression tester assorted with atomic force microscope - Google Patents

Horizontal material stretch compression tester assorted with atomic force microscope Download PDF

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Publication number
CN103760019A
CN103760019A CN201310751692.9A CN201310751692A CN103760019A CN 103760019 A CN103760019 A CN 103760019A CN 201310751692 A CN201310751692 A CN 201310751692A CN 103760019 A CN103760019 A CN 103760019A
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Prior art keywords
atomic force
force microscope
horizontal material
sample
fixed
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CN201310751692.9A
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CN103760019B (en
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钟建
魏岱旭
周涓
何丹农
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Shanghai National Engineering Research Center for Nanotechnology Co Ltd
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Shanghai National Engineering Research Center for Nanotechnology Co Ltd
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Abstract

The invention relates to a horizontal material stretch compression tester assorted with an atomic force microscope. A transmission mechanism comprises a plurality of screw rods, a moving beam, a reducer, a left clamp and a right clamp, wherein a hollow structure is adopted as the tabletop of a frame; a servo motor and a power supply are arranged in the left beam of the frame; screw rods are arranged in the front side beam and the rear side beam of the frame, respectively; two ends of the moving beam are in transmission connection with two screw rods, respectively; the rotating shafts of one end of the two screw rods are fixedly connected with two driven wheels, respectively; the driven wheels are in transmission connection with the reducer via arc synchronous toothed belts; the reducer and the servo motor are in transmission connection; the left clamp is fixed on the inner side of the left beam; the right clamp is fixed on a force sensor; the force sensor is fixed on a movable beam. The tester is simple in structure and convenient to use; due to the adoption of the tester, the worktable space of the atomic force microscope can be satisfied, the surface appearance of a sample can be measured by using the atomic force microscope after the sample is stretched or compressed to a certain degree, so as to analyze out the affect on the sample structure caused by stretching or compressing.

Description

The horizontal material extending compression test of the supporting use of atomic force microscope
Technical field
The present invention relates to analysis classes instrument field, be specifically related to a kind of improvement of material extending compression test structure of and atomic force microscope coupling.
Background technology
Scientific research be unable to do without the exploitation of science and technology and instrument, in order will the detection of the measurement of nano material and Mechanical Properties of Products and microscopic appearance to be organically combined, academia and engineering technological are being developed some mechanics test devices and are being come and scanning electron microscope (SEM), transmission electron microscope (TEM), the micro-nano optical viewers such as atomic force microscope (AFM) are used in conjunction with, thereby can in depth explore microscopic damage fracture behaviour and the mechanism of all kinds of nano materials and goods, and and load, material structure and performance between correlativity rule.
There is now a kind of horizontal dynamic and static electrohydraulic-servo microexamination testing machine, mainly by main frame, hydraulic power source, composition of the control system.Wherein, main frame is provided with adjusts oil cylinder subsystem, and servo-cylinder is from system, and optical microscope and three-dimensional Mobile Slide, for sample provides experiment porch; And by computer control.But this machine construction is comparatively complicated, structure is special, can not meet the space that atomic force microscope can be worked, thereby also cannot support the use with atomic force microscope, thereby cannot when sample being carried out to Compression and Expansion operation, utilize atomic force microscope observation sample urn Topography to change.Therefore be necessary to manufacture and the matched horizontal material extending compression test of atomic force microscope.
Summary of the invention
For limitation of the prior art, the object of the invention is, a kind of and matched material extending compression test of atomic force microscope is provided.
The present invention adopts following technical scheme:
The horizontal material extending compression test of the supporting use of atomic force microscope, includes gear train, servomotor and power supply; It is characterized in that, gear train comprises leading screw, moving beam, speed reduction unit, left fixture, right fixture;
The table top of framework is hollow structure, in its left crossbeam, is provided with servomotor, power supply; In framework all side beam, rear curb girder, be respectively arranged with leading screw, moving beam two ends two leading screws that are in transmission connection respectively; The rotation axis of two leading screw one end is affixed with two engaged wheels respectively, and engaged wheel is in transmission connection by circular arc synchronous toothed belt and speed reduction unit; Speed reduction unit is connected with servo motor transmission;
Left fixture is fixed on left crossbeam inner side above, and right fixture is fixed on power sensor, and power sensor is fixed on movable beam.
After the present invention and atomic force microscope are supporting, can sample is stretched and the Mechanics Performance Testing such as compression in sample is carried out to atomic force microscope test.The present invention can be for the measurement to samples such as organic and inorganic, compound substances.
When the present invention applies, forward and backward curb girder, moving beam and left crossbeam are work space, make the present invention and atomic force microscope supporting.The two ends of test sample are separately fixed on left fixture and right fixture, have screw screw on fixture, can make fixture tightly clamp sample after tighten the screws; By left fixture and right clamp clamps sample two ends, make test specimens product be positioned at the below of atomic force microscope probe 15, in work space.By the use of combining of the present invention and atomic force microscope, thus the macro-mechanical property of analytical sample and the microscopic damage fracture behaviour under stretching/compressing condition, and and load, material structure and performance between correlativity rule.
The present invention adopts horizontal type structure, simple in structure, easy to use, can meet the space that atomic force microscope can be worked, can to sample, stretch or be compressed to the surface topography that to a certain degree utilizes afterwards atomic force microscope measurement sample, thereby analyze, stretch or the impact of compression on sample structure.The present invention simultaneously also can measure the macro-mechanical property of sample.Thereby the advantage of the advantage of atomic force microscope and omnipotent mechanical test machine can be combined, and result of use is good.
Accompanying drawing explanation
Accompanying drawing 1 is perspective view of the present invention.
Accompanying drawing 2 is left crossbeam inner structure schematic diagram.
Accompanying drawing 3 is leading screw, circular arc synchronous toothed belt and speed reduction unit syndeton schematic diagram
1 framework, 2 left crossbeams, 3 leading screws, 31 rotation axiss, 4 moving beams, 5 all side beams, 6 rear curb girders, 7 speed reduction units, 71 followers, 8 circular arc synchronous toothed belts, 9 power sensors, 10 left fixtures, 11 right fixtures, 12 controllers, 13 brace summers, 14 power supplys, 15 atomic force microscope probes, 16 protection rubber, 17 servomotors.
Embodiment
The preferred embodiments of the present invention accompanying drawings is as follows:
The horizontal material extending compression test of the supporting use of atomic force microscope, includes gear train, servomotor 17 and power supply 14; Gear train comprises leading screw 3, moving beam 4, speed reduction unit 7, left fixture 10, right fixture 11;
The table top of framework 1 is hollow structure, in its left crossbeam 2, is provided with servomotor 17, power supply 14; In framework all side beam 5, rear curb girder 6, be respectively arranged with leading screw 3, one moving beam 4 two ends two leading screws that are in transmission connection respectively; The rotation axis 31 of two leading screw one end is affixed with two engaged wheels 71 respectively, and engaged wheel is in transmission connection by circular arc synchronous toothed belt 8 and speed reduction unit 7; Speed reduction unit and servomotor 8 are in transmission connection;
Left fixture 10 is fixed on left crossbeam 2 inner sides, and right fixture 11 is fixed on power sensor 9, and power sensor 9 is fixed on movable beam 4.
Arranged outside at all side beam, rear curb girder internal thread thick stick has protection rubber 16, and the inner side of leading screw is provided with brace summer 13.Brace summer can play to whole horizontal material extending compression test machine frame the effect of bracing reinforcement.The effect of protection rubber is protection leading screw.
On framework before measurement beam, be provided with controller 12; Controller connects respectively power supply, power sensor, computing machine, servomotor.
Described left fixture and right fixture keep level, and the adjustable range of distance is 200-1100mm.
Principle of work of the present invention is: utilize the two ends of left fixture and right clamp clamps sample, thereby and the screw screw of tightening on fixture make fixture tightly clamp sample; Start power switch, utilize subsequently computer software to control, driven by servomotor speed reduction unit, utilizes circular arc synchronous toothed belt to drive guide screw movement, and rotatablely moving of leading screw drives movable beam to move left and right, thereby sample is stretched or compressed; The mechanical signal that controller collection power sensor is collected and the signal of servomotor, thereby the distance that can Quality control is stretched or compresses, and then the macro-mechanical property of analytic sample, and stop stretching or compression by stretching or being compressed to after certain distance, now utilize atomic force microscope to carry out nano level imaging to sample surfaces, just can analyze the structural change of the rear sample of tractive compression.

Claims (4)

1. the horizontal material extending compression test of the supporting use of atomic force microscope, includes gear train, servomotor and power supply; It is characterized in that, gear train comprises leading screw, moving beam, speed reduction unit, left fixture, right fixture;
The table top of framework is hollow structure, in its left crossbeam, is provided with servomotor, power supply; In framework all side beam, rear curb girder, be respectively arranged with leading screw, moving beam two ends two leading screws that are in transmission connection respectively; The rotation axis of two leading screw one end is affixed with two engaged wheels respectively, and engaged wheel is in transmission connection by circular arc synchronous toothed belt and speed reduction unit; Speed reduction unit is connected with servo motor transmission;
Left fixture is fixed on left crossbeam inner side above, and right fixture is fixed on power sensor, and power sensor is fixed on movable beam.
2. according to the horizontal material extending compression test of the supporting use of atomic force microscope claimed in claim 1, it is characterized in that there is protection rubber in the arranged outside of all side beam, rear curb girder internal thread thick stick, the inner side of leading screw is provided with brace summer.
3. according to the horizontal material extending compression test of the supporting use of the atomic force microscope described in claim 1 or 2, it is characterized in that, on framework before measurement beam, be provided with controller; Controller connects respectively power supply, power sensor, computing machine and servomotor.
4. the horizontal material extending compression test of the supporting use of atomic force microscope according to claim 3, is characterized in that, described left fixture and right fixture keep level, and the adjustable range of distance is 200-1100mm.
CN201310751692.9A 2013-12-31 2013-12-31 Atomic force microscope is supporting with horizontal material extending compression test Expired - Fee Related CN103760019B (en)

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CN103760019B CN103760019B (en) 2016-04-27

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104316399A (en) * 2014-10-16 2015-01-28 上海纳米技术及应用国家工程研究中心有限公司 Lever-type tensile fixture for horizontal type material stretch compression tester for atomic force microscope
CN106596260A (en) * 2016-11-09 2017-04-26 深圳烯湾科技有限公司 Tensile testing method based on atomic force microscope probe
CN107192604A (en) * 2017-04-14 2017-09-22 上海海洋大学 The horizontal material Compression and Expansion testing machine gear driving sample holder of AFM
CN107290207A (en) * 2017-06-06 2017-10-24 华南理工大学 A kind of material testing apparatus based on AFM and electrodynamics stretching-machine
CN107764640A (en) * 2017-09-13 2018-03-06 上海海洋大学 The supporting Universal micro mechanics machine of AFM
CN112748099A (en) * 2020-12-21 2021-05-04 湘潭大学 Material micro-stretching device used with atomic force microscope and using method thereof

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JP2003207432A (en) * 2002-01-15 2003-07-25 Kansai Tlo Kk Apparatus for testing micromaterial and method for evaluating dynamic characteristics by the same
CN103105510A (en) * 2013-01-31 2013-05-15 上海纳米技术及应用国家工程研究中心有限公司 Film sample stretching device used for being matched with atomic force microscope (AFM)
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JP2003207432A (en) * 2002-01-15 2003-07-25 Kansai Tlo Kk Apparatus for testing micromaterial and method for evaluating dynamic characteristics by the same
CN103105510A (en) * 2013-01-31 2013-05-15 上海纳米技术及应用国家工程研究中心有限公司 Film sample stretching device used for being matched with atomic force microscope (AFM)
CN103344494A (en) * 2013-07-16 2013-10-09 中国农业大学 Straw stretching property test device

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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104316399A (en) * 2014-10-16 2015-01-28 上海纳米技术及应用国家工程研究中心有限公司 Lever-type tensile fixture for horizontal type material stretch compression tester for atomic force microscope
CN104316399B (en) * 2014-10-16 2017-01-11 上海纳米技术及应用国家工程研究中心有限公司 Lever-type tensile fixture for horizontal type material stretch compression tester for atomic force microscope
CN106596260A (en) * 2016-11-09 2017-04-26 深圳烯湾科技有限公司 Tensile testing method based on atomic force microscope probe
CN107192604A (en) * 2017-04-14 2017-09-22 上海海洋大学 The horizontal material Compression and Expansion testing machine gear driving sample holder of AFM
CN107290207A (en) * 2017-06-06 2017-10-24 华南理工大学 A kind of material testing apparatus based on AFM and electrodynamics stretching-machine
CN107764640A (en) * 2017-09-13 2018-03-06 上海海洋大学 The supporting Universal micro mechanics machine of AFM
CN112748099A (en) * 2020-12-21 2021-05-04 湘潭大学 Material micro-stretching device used with atomic force microscope and using method thereof

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