CN103757974B - A kind of pure careless type rice paper, pure careless type rice paper slurry and pulping process thereof - Google Patents
A kind of pure careless type rice paper, pure careless type rice paper slurry and pulping process thereof Download PDFInfo
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- CN103757974B CN103757974B CN201310752081.6A CN201310752081A CN103757974B CN 103757974 B CN103757974 B CN 103757974B CN 201310752081 A CN201310752081 A CN 201310752081A CN 103757974 B CN103757974 B CN 103757974B
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Abstract
The invention discloses a kind of pure careless type rice paper slurry, comprise by weight percentage the pure straw pulp of following component: 70-80%, the slurry of pure straw pulp is dense is 72-78%; The active powder of 15-25% calcium agent; 0.5-2% cationic starch; The agent of 0.5-2% vegetalitas anti-photooxidation; 1-4% paper making additive. The pulping process that the invention also discloses a kind of pure careless type rice paper slurry, comprises the steps: to get Shatian straw, puts into water and soaks, and draining, is placed in milk of lime and floods; Code heap retting; Water proof boiling, stand, the air-dry forage that obtains are shone in cooling, rinsing afterwards; Forage is pulverized, washes material, add water and obtain starching the dense pure straw pulp for 72-78%; Take pure straw pulp, the active powder of calcium agent, cationic starch, the agent of vegetalitas anti-photooxidation and paper making additive by proportioning, after mixing, obtain above-mentioned pure careless type rice paper slurry. The invention also discloses a kind of pure careless type rice paper that adopts above-mentioned pure careless type rice paper slurry to make.
Description
Technical field
The present invention relates to rice paper technical field, particularly a kind of pure careless type rice paper slurry and pulping process thereof,And the pure careless type rice paper that adopts described pure careless type rice paper slurry to make.
Background technology
China's rice paper is called for short rice paper, is the treasure of the men of literature and writing, painting and calligraphy famous expert favourite. Protect through national heritageDepartment's definition rice paper is by being produced Jingxian County, Anhui Province. It is representative that Jingxian County produces rice paper Yi little ridge, in its period of great prosperity,There is the meaning in " 13 holes, nine ridges, rice paper is made in hole, hole ". So far the nine ridge 13 former rice paper canopies in hole are as far as the something lost of the Ming DynastyMark is still faintly visible. Rice paper is produced taking Barks of Pteroceltis Tatarinowii and Shatian straw as raw material and is made by hand traditionally. At presentRice paper has become one of important pillar industry of local economy, except producing rice paper, ancient rice paper, also a large amount of rawProduce the china picture-character paper comparatively low-grade towards masses, also have in addition rice paper inferior, this causes wingceltis raw material supply tenDivide nervous. For this reason, local government has raised money wingceltis woods bases newly-built, but applicant thinks, opens up newRaw material sources have far-reaching realistic meaning to the production of ancient rice paper.
Summary of the invention
The present invention proposes a kind of pure careless type rice paper, pure careless type rice paper slurry and pulping process thereof, adopt ShatianStraw replaces Barks of Pteroceltis Tatarinowii, has saved cost, and its pulping process is simple, and effects on slurry making is good.
The pure careless type rice paper slurry of one that the present invention proposes, comprises following component: 70-80% by weight percentagePure straw pulp, the slurry of pure straw pulp is dense is 72-78%; The active powder of 15-25% calcium agent; 0.5-2% cation forms sedimentPowder; The agent of 0.5-2% vegetalitas anti-photooxidation; 1-4% paper making additive.
In detailed description of the invention, the percentage by weight of pure straw pulp can be 70%, 72%, 73%, 75%,76%, 78%, 79%, 80%, the percentage by weight of the active powder of calcium agent can be 15%, 16%, 18%, 20%,21%, 22%, 23%, 24%, 25%, the percentage by weight of cationic starch is 0.5%, 0.7%, 0.8%, 1%,1.1%, 1.2%, 1.5%, 1.7%, 1.9%, 2%, the percentage by weight of vegetalitas anti-photooxidation agent is 0.5%,0.6%, 0.8%, 1%, 1.2%, 1.3%, 1.5%, 1.7%, 1.9%, 2%, the weight percent of paper making additiveThan can be 1%, 1.5%, 1.9%, 2%, 2.2%, 2.5%, 2.9%, 3.4%, 3.7%, 4%.
In detailed description of the invention, the slurry of pure straw pulp is dense can be 72%, 73%, 75%, 76%, 77%, 78%.
Preferably, the active powder of described calcium agent is that powdered whiting is through the stearic acid modified calcium carbonate activity obtainingPowder.
Preferably, the whiteness of described powdered whiting is more than 96, and particle diameter is between 1000-1200 order, excellentSelect the powdered whiting of particle diameter more than 1250 orders.
Preferably, described vegetalitas antioxygen photo etching is four [β-(3,5-di-tert-butyl-hydroxy phenyl) propionic acid]Pentaerythritol ester, its molecular formula is C73H108O12。
Preferably, described pure careless type rice paper slurry comprises the pure toilet paper of following component: 75-78% by weight percentageSlurry, the slurry of pure straw pulp is dense is 74-76%; The active powder of 18-22% calcium agent; 0.8-1.2% cationic starch;The agent of 0.8-1.2% vegetalitas anti-photooxidation; 1.5-2.5% paper making additive.
Preferably, described pure careless type rice paper slurry comprises following component by weight percentage: 76% pure straw pulp,The slurry of pure straw pulp is dense is 75%; The active powder of 20% calcium agent; 1% cationic starch; 1% vegetalitas anti-photooxidationAgent; 2% paper making additive.
The pulping process that the invention allows for a kind of pure careless type rice paper slurry, comprises the steps:
S1, get Shatian straw, remove rice leaf spike of rice, after lashing, put into water and soak 13-17 days, after pulling outDraining 0.8-2h, is then placed in milk of lime and floods 5-10 days;
S2, by S1, tear open after 27-32 days through the straw code heap retting of dipping pile stand-by;
S3, by the straw water proof boiling 20-40h through retting in S2, after cooling, rinsing, shine stand 20-40 days;1-5 carries out air-dryly after taking second place so repeatedly, obtains forage;
S4, the forage in S3 is pulverized, washes material after, add suitable quantity of water, obtaining starching dense is 72-78%Pure straw pulp;
S5, take the pure straw pulp that obtains in S4, the active powder of calcium agent, cation according to percentage by weight and form sedimentPowder, the agent of vegetalitas anti-photooxidation and paper making additive, obtain above-mentioned pure careless type rice paper slurry after mixing.
Preferably, so repeatedly 1-5 time until straw carries out after being white in color air-dry.
Preferably, in S1, soak 15 days in water, draining 1h floods 7 days in milk of lime; ?In S2, code heap retting 30 days; In S3, water proof boiling 30h, shine stand 30 days, repeatedly 1-5 time untilStraw is white in color.
The invention allows for a kind of pure careless type rice paper, adopt above-mentioned pure careless type rice paper slurry to make.
In the present invention, adopt Shatian straw to replace Barks of Pteroceltis Tatarinowii to carry out slurrying, because Barks of Pteroceltis Tatarinowii lignin containsMeasure lower, easily slurrying, calcium carbonate content is high, is conducive to improve the profit mill performance of rice paper, fiber finer cell wallThick, microfibril is many, makes the ink absorption of rice paper good, and the pure careless type rice paper slurry of making has Barks of Pteroceltis TatarinowiiThe advantage of slurry, the raw material sources of Shatian straw are wide, and cost is lower; In pure straw pulp, add vegetalitas anti-Photooxidant, has ensured the ageing resistace of the pure careless type rice paper of preparation to have significantly improved service life; MakeWith the active powder of calcium agent, make the pure careless type rice paper of preparation there is very superior profit China ink and writing quality; DescribedThe pulping process of pure careless type rice paper is simple, and effects on slurry making is good, is applicable to extensive rice paper and produces.
Detailed description of the invention
Embodiment 1
A kind of pure careless type rice paper slurry, comprises following component: 77% pure straw pulp, pure toilet paper by weight percentageSlurry slurry dense be 78%; The active powder of 16% calcium agent; 1.6% cationic starch; 2% vegetalitas anti-photooxidation agent and3.4% paper making additive; Wherein, the active powder of described calcium agent be whiteness more than 96, particle diameter is 1025 objectsPowdered whiting is through the active powder of the stearic acid modified calcium carbonate obtaining; Described vegetalitas antioxygen photo etching is four [β-(3,5-di-tert-butyl-hydroxy phenyl) propionic acid] pentaerythritol ester, its molecular formula is C73H108O12。
Embodiment 2
A kind of pure careless type rice paper slurry, comprises following component: 74.5% pure straw pulp, pure grass by weight percentageThe slurry of paper pulp is dense is 73%; The active powder of 20% calcium agent; 0.8% cationic starch; 1.2% vegetalitas anti-photooxidationAgent and 3.5% paper making additive; Wherein, the active powder of described calcium agent be whiteness more than 96, particle diameter is 1100Object powdered whiting is through the active powder of the stearic acid modified calcium carbonate obtaining; Described vegetalitas antioxygen photo etching isFour [β-(3,5-di-tert-butyl-hydroxy phenyl) propionic acid] pentaerythritol ester, its molecular formula is C73H108O12。
Embodiment 3
A kind of pure careless type rice paper slurry, comprises following component: 71.6% pure straw pulp, pure grass by weight percentageThe slurry of paper pulp is dense is the active powder of 72%, 24% calcium agent, 1.5% cationic starch, 1.5% vegetalitas anti-photooxidationAgent and 1.4% paper making additive; Wherein, the active powder of described calcium agent be whiteness more than 96, particle diameter is 1200Object powdered whiting is through the active powder of the stearic acid modified calcium carbonate obtaining; Described vegetalitas antioxygen photo etching isFour [β-(3,5-di-tert-butyl-hydroxy phenyl) propionic acid] pentaerythritol ester, its molecular formula is C73H108O12。
Embodiment 4
A kind of pure careless type rice paper slurry, comprises following component: 76% pure straw pulp, pure toilet paper by weight percentageThe slurry of slurry is dense is the active powder of 75%, 20% calcium agent, 1% cationic starch, 1% vegetalitas anti-photooxidation agent and 2%Paper making additive; Wherein, the active powder of described calcium agent be whiteness more than 96, particle diameter is 1150 object heavysCalcium carbonate is through the active powder of the stearic acid modified calcium carbonate obtaining; Described vegetalitas antioxygen photo etching is four [β-(3,5-di-tert-butyl-hydroxy phenyl) propionic acid] pentaerythritol ester, its molecular formula is C73H108O12。
The present invention proposes a kind of pure careless type rice paper, adopt the pure careless type rice paper described in above-described embodiment 1-4Slurry is made.
In embodiment 1-4, the pulping process of above-mentioned pure careless type rice paper slurry, comprises the steps:
S1, get Shatian straw, remove rice leaf spike of rice, after lashing, put into water and soak 13-17 days, as 13 days,14 days, 15 days, 16 days, 17 days, pull rear draining 0.8-2h out, as 0.8h, 1h, 1.5h, 2h, soBe placed in milk of lime and flood 5-10 days, as 5 days, 6 days, 7 days, 8 days, 9 days, 10 days;
S2, by S1, tear open after 27-32 days through the straw code heap retting of dipping pile stand-by, as 27 days, 28My god, 30 days, 31 days, 32 days;
S3, by the straw water proof boiling 20-40h through retting in S2, as 20h, 22h, 25h, 30h, 33h,35h, 39h, 40h, shine stand 20-40 days after cooling, rinsing, as 20 days, 25 days, 30 days, 35 days,40 days; 1-5 time so repeatedly, as 1 time, 2 times, 3 times, 4 times, 5 times until after straw is white in colorCarry out air-dryly, obtain forage;
S4, the forage in S3 is pulverized, washes material after, add suitable quantity of water, obtaining starching dense is 72-78%Pure straw pulp, densely can be 72%, 73%, 75%, 76%, 77%, 78% as starched;
S5, take the pure straw pulp 70-80% that obtains in S4, the active powder of calcium agent according to percentage by weight15-25%, cationic starch 0.5-2%, vegetalitas anti-photooxidation agent 0.5-2% and paper making additive 1-4%, mixedAfter closing evenly, obtain above-mentioned pure careless type rice paper slurry.
In the embodiment of the present invention, adopt Shatian straw to replace Barks of Pteroceltis Tatarinowii to carry out slurrying, because Barks of Pteroceltis Tatarinowii woodQuality content is lower, easily slurrying, and calcium carbonate content is high, is conducive to improve the profit mill performance of rice paper, fiberCell wall thickness, microfibril is many, makes the ink absorption of rice paper good, and the pure careless type rice paper slurry of making has green grass or young cropsThe advantage of wingceltis bark slurry, the raw material sources of Shatian straw are wide, and cost is lower; In pure straw pulp, add and plantPhysical property anti-photooxidation agent, has ensured the ageing resistace of the pure careless type rice paper of preparation to have significantly improved the use longevityLife; Use the active powder of calcium agent, make the pure careless type rice paper of preparation there is very superior profit China ink and writing quality;The pulping process of described pure careless type rice paper is simple, and effects on slurry making is good, is applicable to extensive rice paper and produces.
The above, be only preferably detailed description of the invention of the present invention, but not office of protection scope of the present inventionBe limited to this, any be familiar with those skilled in the art the present invention disclose technical scope in, according to thisThe technical scheme of invention and inventive concept thereof are equal to replaces or changes, and all should be encompassed in protection of the present inventionWithin scope.
Claims (7)
1. a pure careless type rice paper slurry, is characterized in that, comprises by weight percentage following component: 70-80%Pure straw pulp, the slurry of pure straw pulp is dense is 72-78%; The active powder of 15-25% calcium agent; 0.5-2% cation forms sedimentPowder; The agent of 0.5-2% vegetalitas anti-photooxidation; 1-4% paper making additive; Described pure straw pulp is Shatian yellow pulp;
The active powder of described calcium agent is that powdered whiting is through the active powder of the stearic acid modified calcium carbonate obtaining;
The whiteness of described powdered whiting is more than 96, and particle diameter is between 1000-1200 order;
The agent of described vegetalitas anti-photooxidation is four [β-(3,5-di-tert-butyl-hydroxy phenyl) propionic acid] Ji WusiAlcohol ester, its molecular formula is C73H108O12。
2. pure careless type rice paper slurry according to claim 1, is characterized in that, by weight percentage bagDraw together the pure straw pulp of following component: 75-78%, the slurry of pure straw pulp is dense is 74-76%; The active powder of 18-22% calcium agentBody; 0.8-1.2% cationic starch; The agent of 0.8-1.2% vegetalitas anti-photooxidation; 1.5-2.5% paper making additive.
3. pure careless type rice paper slurry according to claim 2, is characterized in that, by weight percentage bagDraw together following component: 76% pure straw pulp, the slurry of pure straw pulp is dense is 75%; The active powder of 20% calcium agent; 1% sunIonic starch; 1% vegetalitas anti-photooxidation agent; 2% paper making additive.
4. according to a pulping process for the pure careless type rice paper slurry described in any one in claim 1-3, itsBe characterised in that, comprise the steps:
S1, get Shatian straw, remove rice leaf spike of rice, after lashing, put into water and soak 13-17 days, after pulling outDraining 0.8-2h, is then placed in milk of lime and floods 5-10 days;
S2, by S1, tear open after 27-32 days through the straw code heap retting of dipping pile stand-by;
S3, by the straw water proof boiling 20-40h through retting in S2, after cooling, rinsing, shine stand 20-40My god; 1-5 carries out air-dryly after taking second place so repeatedly, obtains forage;
S4, the forage in S3 is pulverized, washes material after, add suitable quantity of water, obtain starching dense for 72-78%'sPure straw pulp;
S5, take the pure straw pulp that obtains in S4, the active powder of calcium agent, cation according to percentage by weight and form sedimentPowder, the agent of vegetalitas anti-photooxidation and paper making additive, obtain described pure careless type rice paper slurry after mixing.
5. the pulping process of pure careless type rice paper slurry according to claim 4, is characterized in that,In S3,1-5 time until straw carries out after being white in color air-dry so repeatedly.
6. the pulping process of pure careless type rice paper slurry according to claim 4, is characterized in that,In S1, soak 15 days in water, draining 1h floods 7 days in milk of lime; In S2, code heap retting30 days; In S3, water proof boiling 30h, shine stand 30 days, repeatedly 1-5 time until straw be white in color.
7. a pure careless type rice paper, is characterized in that, adopts the pure grass described in any one in claim 1-6Type rice paper slurry is made.
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