CN103774489B - A kind of preparation method of rice paper straw pulp - Google Patents
A kind of preparation method of rice paper straw pulp Download PDFInfo
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- CN103774489B CN103774489B CN201310646528.1A CN201310646528A CN103774489B CN 103774489 B CN103774489 B CN 103774489B CN 201310646528 A CN201310646528 A CN 201310646528A CN 103774489 B CN103774489 B CN 103774489B
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Abstract
The preparation method that the invention discloses a kind of rice paper straw pulp, (1), Shatian Caulis et Folium Oryzae defoliation, fringe are lashed, soak at clear water reserviors, dewatering, impregnate lime cream;(2), dipping pull out after terminating, code heap on Polypropylence Sheet, tear the upper rice steamer pot of heap, Steam by water bath after retting open, after cooling, discharging rinsing, shine beach;(3), receive Steam by water bath, clear water rinsing again behind beach, shine beach, so repeat to material white after added air-dry warehouse-in deposit, obtain forage；(4), take after forage pulverizes, removes sand and wash material, add suitable quantity of water, vegetalitas antioxygen photo etching, cationic starch, high whiteness calcium preparation active powder, self-control auxiliary agent are made into slip, to obtain final product.
Description
Technical field
The present invention relates to papermaking process field, be exactly the preparation method of a kind of rice paper straw pulp.
Background technology
China's rice paper is called for short rice paper, is the treasure of the men of literature and writing, painting and calligraphy famous expert's favourite.Department's definition rice paper is protected to be produced by Jingxian County, Anhui Province through national heritage.Jingxian County produces rice paper with little ridge for representative, in its period of great prosperity, has the meaning in " nine holes, ridge 13, rice paper is made in hole, hole ".So far the nine former rice paper canopies in hole, ridges 13 are still faintly visible as far as the traces of the Ming Dynasty.Rice paper produces and makes by hand for raw material with Barks of Pteroceltis Tatarinowii and Shatian Caulis et Folium Oryzae traditionally.Current rice paper has become one of important pillar industry of local economy, and except production rice paper, ancient rice paper, also a large amount of china picture-character papers produced towards masses' comparatively low grade, in addition with rice paper inferior.This causes that wingceltis raw material supply is very nervous.For this, local government has raised money wingceltis woods base newly-built.But it is applicant's understanding that open up the production to ancient rice paper of the new raw material sources there is far-reaching realistic meaning.
Summary of the invention
The preparation method that it is an object of the invention to provide a kind of high-quality rice paper straw pulp.
Above-mentioned purpose is realized by below scheme:
A kind of preparation method of rice paper straw pulp, it is characterised in that:
Comprise the following steps:
(1), Shatian Caulis et Folium Oryzae defoliation, fringe are lashed, pull out after clear water reserviors soak 14-16 days, after dewatering about 1h, dipping lime cream 6-8 days;
(2), dipping pull out after terminating, code heap on Polypropylence Sheet, tear the upper rice steamer pot of heap, Steam by water bath 20-40h after retting 28-32 days open, after cooling, discharging rinsing, shine beach 30 50 days;
(3), receive Steam by water bath 30-40h, clear water rinsing again behind beach, shine beach 30 50 days, so repeat to material white after added air-dry warehouse-in deposit, obtain forage；
(4), take after forage pulverizes, removes sand and wash material, add suitable quantity of water, vegetalitas antioxygen photo etching, cationic starch, high whiteness calcium preparation active powder, self-control auxiliary agent are made into slip, to obtain final product.
The preparation method of described a kind of rice paper straw pulp, it is characterised in that:
Described forage, high whiteness calcium preparation active powder, cationic starch, vegetalitas antioxygen photo etching, self-control auxiliary agent part by weight be: 75-77:18-22:1-1.2:1.9-2.1:1-1.2:.
The preparation method of described a kind of rice paper straw pulp, it is characterised in that: described forage, high whiteness calcium preparation active powder, cationic starch, vegetalitas antioxygen photo etching, self-control auxiliary agent part by weight be: 76:20:1:2:1.
The preparation method of described a kind of rice paper straw pulp, it is characterised in that: described high whiteness calcium preparation active powder be particle diameter 1000-1200 order, whiteness more than 96 through stearic acid modified calcium carbonate active powder.
The preparation method of described a kind of rice paper straw pulp, it is characterised in that:
Described vegetalitas antioxygen photo etching refers to four [β-(3,5-di-tert-butyl-hydroxy phenyl) propanoic acid] pentaerythritol ester.
The preparation method of described a kind of rice paper straw pulp, it is characterized in that: the preparation method of self-control auxiliary agent is: take straw ash, add suitable quantity of water to stir, add the Silane coupling agent KH550 being equivalent to the epoxy soybean oil of straw ash weight 1-2%, 1-2%, the irgasfos 168 of 0.2-0.5% and appropriate water, after stirring 20-30 minute, take out at 33-36 DEG C, dry, to obtain final product.
The preparation method of described a kind of rice paper straw pulp, it is characterized in that: the preparation method of described high whiteness calcium preparation active powder is: take ground calcium carbonate, add suitable quantity of water to stir, add the stearic acid being equivalent to straw ash weight 2-4%, after stirring 20-30 minute at 35-38 DEG C, take out, dry, to obtain final product.
The invention have the benefit that
1, this rice paper slip does not use wingceltis, and main raw material(s) is Shatian Caulis et Folium Oryzae.
2, process with slurry employs vegetalitas antioxygen photo etching, it is ensured that the ageing resistance of rice paper.
3, the calcium carbonate employed in process with slurry in high whiteness calcium preparation active powder refers to the ground calcium carbonate (more than 1025 orders) that Jingxian County is local.
Detailed description of the invention
Embodiment 1:
The preparation method of a kind of rice paper straw pulp, comprises the following steps:
(1), Shatian Caulis et Folium Oryzae defoliation, fringe are lashed, pull out after clear water reserviors soak 1:5 days, after dewatering 1h, dipping lime cream 7 days;
(2), dipping pull out after terminating, code heap on Polypropylence Sheet, retting tears the upper rice steamer pot of heap, Steam by water bath 30h open after 30 days, shine beach 40 days after cooling, discharging rinsing;
(3), receive Steam by water bath 40h, clear water rinsing again behind beach, shine beach 40 days, so repeat to material white after added air-dry warehouse-in deposit, obtain forage；
(4), take after forage pulverizes, removes sand and wash material, add suitable quantity of water, vegetalitas antioxygen photo etching, cationic starch, high whiteness calcium preparation active powder, self-control auxiliary agent are made into slip, to obtain final product.
Described forage, high whiteness calcium preparation active powder, cationic starch, vegetalitas antioxygen photo etching, self-control auxiliary agent part by weight be: 76:20:1:2:1.
Described high whiteness calcium preparation active powder be particle diameter 1200 order, whiteness more than 96 through stearic acid modified ground calcium carbonate active powder.
The preparation method of described a kind of rice paper straw pulp,
Described vegetalitas antioxygen photo etching refers to four [β-(3,5-di-tert-butyl-hydroxy phenyl) propanoic acid] pentaerythritol ester.
The preparation method of self-control auxiliary agent is: take straw ash, adds suitable quantity of water and stirs, add be equivalent to the epoxy soybean oil of straw ash weight 2%, 1% Silane coupling agent KH550, the irgasfos 168 of 0.5% and appropriate water, after stirring 30 minutes, take out at 36 DEG C, dry, to obtain final product.
Embodiment 1 technique routinely being made rice paper detect, experimental result is shown in following table:
Embodiment 2,
A kind of preparation method of rice paper straw pulp,
Comprise the following steps:
(1), Shatian Caulis et Folium Oryzae defoliation, fringe are lashed, pull out after clear water reserviors soak 15 days, after dewatering about 1h, dipping lime cream 8 days;
(2), dipping pull out after terminating, code heap on Polypropylence Sheet, retting tears the upper rice steamer pot of heap, Steam by water bath 40h open after 28 days, shine beach 50 days after cooling, discharging rinsing;
(3), receive Steam by water bath 40h, clear water rinsing again behind beach, shine beach 50 days, so repeat to material white after added air-dry warehouse-in deposit, obtain forage；
(4), take after forage pulverizes, removes sand and wash material, add suitable quantity of water, vegetalitas antioxygen photo etching, cationic starch, high whiteness calcium preparation active powder, self-control auxiliary agent are made into slip, to obtain final product.
The preparation method of described a kind of rice paper straw pulp, it is characterised in that: described forage, high whiteness calcium preparation active powder, cationic starch, vegetalitas antioxygen photo etching, self-control auxiliary agent part by weight be: 76:20:1:2:1.
Described vegetalitas antioxygen photo etching refers to four [β-(3,5-di-tert-butyl-hydroxy phenyl) propanoic acid] pentaerythritol ester.
The preparation method of self-control auxiliary agent is: take straw ash, adds suitable quantity of water and stirs, add be equivalent to the epoxy soybean oil of straw ash weight 2%, 2% Silane coupling agent KH550, the irgasfos 168 of 0.2% and appropriate water, after stirring 20 minutes, take out at 33 DEG C, dry, to obtain final product.
The preparation method of described high whiteness calcium preparation active powder is: take the ground calcium carbonate of 1025 orders, adds suitable quantity of water and stirs, adds the stearic acid being equivalent to straw ash weight 2%, after stirring 30 minutes, takes out, dry, to obtain final product at 38 DEG C.
Embodiment 2 conventionally technique being made rice paper detect, experimental result is shown in following table:
Claims (3)
1. the preparation method of a rice paper straw pulp, it is characterised in that:
Comprise the following steps:
(1) Shatian Caulis et Folium Oryzae defoliation, fringe are lashed, pull out after clear water reserviors soak 14-16 days, after dewatering 1h, dipping lime cream 6-8 days；
(2) dipping is pulled out after terminating, code heap on Polypropylence Sheet, tears the upper rice steamer pot of heap, Steam by water bath 20-40h open, shine beach 30 50 days after cooling, discharging rinsing after retting 28-32 days；
(3) behind receipts beach, Steam by water bath 30-40h, clear water rinse, shine beach 30 50 days again, so repeat to the white rear added air-dry warehouse-in of material to deposit, obtain forage；
(4) take after forage pulverizes, removes sand and wash material, add suitable quantity of water, vegetalitas antioxygen photo etching, cationic starch, high whiteness calcium preparation active powder, self-control auxiliary agent are made into slip, to obtain final product；
Described high whiteness calcium preparation active powder be particle diameter 1000-1200 order, whiteness more than 96 through stearic acid modified calcium carbonate active powder；
Described vegetalitas antioxygen photo etching refers to four [β-(3,5-di-tert-butyl-hydroxy phenyl) propanoic acid] pentaerythritol ester；
The preparation method of described self-control auxiliary agent is: take straw ash, add suitable quantity of water to stir, add the Silane coupling agent KH550 being equivalent to the epoxy soybean oil of straw ash weight 1-2%, 1-2%, the irgasfos 168 of 0.2-0.5% and appropriate water, after stirring 20-30 minute at 33-36 DEG C, take out, dry, to obtain final product；
The preparation method of described high whiteness calcium preparation active powder is: take ground calcium carbonate, adds suitable quantity of water and stirs, adds the stearic acid being equivalent to straw ash weight 2-4%, after stirring 20-30 minute, takes out, dry, to obtain final product at 35-38 DEG C.
2. the preparation method of a kind of rice paper straw pulp according to claim 1, it is characterised in that:
Described forage, high whiteness calcium preparation active powder, cationic starch, vegetalitas antioxygen photo etching, self-control auxiliary agent part by weight be: 75-77:18-22:1-1.2:1.9-2.1:1-1.2.
3. the preparation method of a kind of rice paper straw pulp according to claim 1, it is characterised in that: described forage, high whiteness calcium preparation active powder, cationic starch, vegetalitas antioxygen photo etching, self-control auxiliary agent part by weight be: 76:20:1:2:1.
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| CN103774489B true CN103774489B (en) | 2016-07-06 |
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Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108385433A (en) * | 2017-10-07 | 2018-08-10 | 谷文 | A kind of fire-retardant painting and calligraphy carrier material |
| CN108411701A (en) * | 2017-10-07 | 2018-08-17 | 谷文 | A kind of moisture-proof painting and calligraphy carrier material |
| CN108277681A (en) * | 2017-10-07 | 2018-07-13 | 霍文慧 | A kind of high tenacity rice paper material |
| CN108385431A (en) * | 2017-10-07 | 2018-08-10 | 谷文 | A kind of ageing-resistant painting and calligraphy carrier material |
| CN108411700A (en) * | 2017-10-07 | 2018-08-17 | 谷文 | A kind of painting and calligraphy carrier material |
| CN108999011B (en) * | 2018-07-02 | 2020-01-31 | 安徽泾县金星宣纸有限公司 | Processing technology for forming rice papers |
| CN111041888A (en) * | 2019-12-26 | 2020-04-21 | 同曦集团有限公司 | Antibacterial, mildew-proof and moth-proof rice paper pulp, rice paper and preparation method |
| CN112593454A (en) * | 2020-12-24 | 2021-04-02 | 胡明富 | Special semi-cooked rice paper for industrial tape writing and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1281918A (en) * | 1999-07-27 | 2001-01-31 | 杭州市化工研究所 | High-effective filter and retention aid for straw pulp for making paper |
| KR20050023824A (en) * | 2003-09-03 | 2005-03-10 | 주식회사 삼양제넥스 | Process for the production of paper using cationic starch |
| CN103171363A (en) * | 2013-03-02 | 2013-06-26 | 淄博海润丝绸发展有限公司 | Silk specially used for painting and calligraphy and manufacturing method thereof |
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- 2013-12-04 CN CN201310646528.1A patent/CN103774489B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1281918A (en) * | 1999-07-27 | 2001-01-31 | 杭州市化工研究所 | High-effective filter and retention aid for straw pulp for making paper |
| KR20050023824A (en) * | 2003-09-03 | 2005-03-10 | 주식회사 삼양제넥스 | Process for the production of paper using cationic starch |
| CN103171363A (en) * | 2013-03-02 | 2013-06-26 | 淄博海润丝绸发展有限公司 | Silk specially used for painting and calligraphy and manufacturing method thereof |
Non-Patent Citations (2)
| Title |
|---|
| 安徽泾县"千年古宣"宣纸制作工艺调查研究;方晓阳等;《北京印刷学院学报》;20081231;第16卷(第6期);第1-8页 * |
| 宣纸生产工艺与润墨;吴世新;《中华纸业》;20080415;第64-67页 * |
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