CN103757974A - Pure grass-type rice paper, pure grass-type rice paper pulp and pulping technology thereof - Google Patents
Pure grass-type rice paper, pure grass-type rice paper pulp and pulping technology thereof Download PDFInfo
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Abstract
The invention discloses pure grass-type rice paper pulp, comprising the following components by weight percent: 70-80% of pure straw pulp of which the concentration is 72-78%, 15-25% of calcium active powder, 0.5-2% of cationic starch, 0.5-2% of plant-resistance light oxidant, and 1-4% of papermaking additive. The invention also discloses a pulping technology of pure grass-type rice paper pulp. The technology comprises the following steps: taking straws of a sandy land and putting into water to soak and drain; putting into lime milk to dip; stacking and retting; stewing in a manner of isolating from water; cooling, tedding after rinsing, and air drying, so as to obtain a fodder; pulverizing and washing the fodder; adding water to obtain the pure grass-type paper pulp of which the concentration is 72-78%; weighing the pure grass-type paper pulp, the calcium active powder, the cationic starch, the plant-resistance light oxidant and the papermaking additive according to the proportion; evenly mixing, thus obtaining the pure grass-type rice paper pulp. A pure grass-type rice paper prepared from the pure grass-type rice paper pulp is also disclosed by the invention.
Description
Technical field
The present invention relates to rice paper technical field, particularly a kind of pure careless type rice paper slurry and pulping process thereof, and the pure careless type rice paper that adopts described pure careless type rice paper slurry to make.
Background technology
China's rice paper is called for short rice paper, is the treasure of the men of literature and writing, painting and calligraphy famous expert favourite.Through national heritage protection department, definition rice paper is produced by Jingxian County, Anhui Province.It is representative that Jingxian County produces rice paper Yi little ridge, in its period of great prosperity, has the meaning in " 13 holes, nine ridges, rice paper is made in hole, hole ".So far the nine ridge 13 former rice paper canopies in hole are still faintly visible as far as the traces of the Ming Dynasty.Rice paper is produced and be take Barks of Pteroceltis Tatarinowii and Shatian straw and make by hand as raw material traditionally.Rice paper has become one of important pillar industry of local economy at present, and except producing rice paper, ancient rice paper, also a large amount of production, towards the comparatively low-grade china picture-character paper of masses, also has rice paper inferior in addition, and this causes wingceltis raw material supply very nervous.For this reason, local government has raised money wingceltis woods bases newly-built, but applicant thinks, opens up new raw material sources the production of ancient rice paper is had to far-reaching realistic meaning.
Summary of the invention
The present invention proposes a kind of pure careless type rice paper, pure careless type rice paper slurry and pulping process thereof, adopt Shatian straw to replace Barks of Pteroceltis Tatarinowii, saved cost, its pulping process is simple, and effects on slurry making is good.
A kind of pure careless type rice paper slurry that the present invention proposes, comprises the pure straw pulp of following component: 70-80% by weight percentage, and the slurry of pure straw pulp is dense is 72-78%; The active powder of 15-25% calcium agent; 0.5-2% cationic starch; The agent of 0.5-2% vegetalitas anti-photooxidation; 1-4% paper making additive.
In the specific embodiment, the percentage by weight of pure straw pulp can be 70%, 72%, 73%, 75%, 76%, 78%, 79%, 80%, the percentage by weight of the active powder of calcium agent can be 15%, 16%, 18%, 20%, 21%, 22%, 23%, 24%, 25%, the percentage by weight of cationic starch is 0.5%, 0.7%, 0.8%, 1%, 1.1%, 1.2%, 1.5%, 1.7%, 1.9%, 2%, the percentage by weight of vegetalitas anti-photooxidation agent is 0.5%, 0.6%, 0.8%, 1%, 1.2%, 1.3%, 1.5%, 1.7%, 1.9%, 2%, the percentage by weight of paper making additive can be 1%, 1.5%, 1.9%, 2%, 2.2%, 2.5%, 2.9%, 3.4%, 3.7%, 4%.
In the specific embodiment, the slurry of pure straw pulp is dense can be 72%, 73%, 75%, 76%, 77%, 78%.
Preferably, the active powder of described calcium agent is that powdered whiting is through the active powder of the stearic acid modified calcium carbonate obtaining.
Preferably, the whiteness of described powdered whiting is more than 96, particle diameter between 1000-1200 order, the powdered whiting of preferable particle size more than 1250 orders.
Preferably, described vegetalitas antioxygen photo etching is four [β-(3,5-di-tert-butyl-hydroxy phenyl) propionic acid] pentaerythritol ester, and its molecular formula is C
73h
108o
12.
Preferably, described pure careless type rice paper slurry comprises the pure straw pulp of following component: 75-78% by weight percentage, and the slurry of pure straw pulp is dense is 74-76%; The active powder of 18-22% calcium agent; 0.8-1.2% cationic starch; The agent of 0.8-1.2% vegetalitas anti-photooxidation; 1.5-2.5% paper making additive.
Preferably, described pure careless type rice paper slurry comprises following component by weight percentage: 76% pure straw pulp, and the slurry of pure straw pulp is dense is 75%; The active powder of 20% calcium agent; 1% cationic starch; 1% vegetalitas anti-photooxidation agent; 2% paper making additive.
The pulping process that the invention allows for a kind of pure careless type rice paper slurry, comprises the steps:
S1, get Shatian straw, remove rice leaf spike of rice, after lashing, put into water and soak 13-17 days, pull rear draining 0.8-2h out, be then placed in milk of lime and flood 5-10 days;
S2, by S1, through the straw code heap retting of dipping, tear open after 27-32 days pile stand-by;
S3, by S2 through the straw water proof boiling 20-40h of retting, after cooling, rinsing, shine stand 20-40 days; 1-5 carries out air-dryly after taking second place so repeatedly, obtains forage;
S4, the forage in S3 is pulverized, washes material after, add suitable quantity of water, obtaining starching dense is the pure straw pulp of 72-78%;
S5, according to percentage by weight, take the pure straw pulp that obtains in S4, the active powder of calcium agent, cationic starch, the agent of vegetalitas anti-photooxidation and paper making additive, after mixing, obtain above-mentioned pure careless type rice paper slurry.
Preferably, so repeatedly 1-5 time until straw carries out after being white in color air-dry.
Preferably, in S1, soak 15 days in water, draining 1h floods 7 days in milk of lime; In S2, code heap retting 30 days; In S3, water proof boiling 30h, shines stand 30 days, repeatedly 1-5 time until straw be white in color.
The invention allows for a kind of pure careless type rice paper, adopt above-mentioned pure careless type rice paper slurry to make.
In the present invention, adopt Shatian straw to replace Barks of Pteroceltis Tatarinowii to carry out slurrying, because Barks of Pteroceltis Tatarinowii content of lignin is lower, easily slurrying, calcium carbonate content is high, be conducive to improve the profit mill performance of rice paper, fibrocyte wall thickness, microfibril is many, make the ink absorption of rice paper good, the pure careless type rice paper slurry of making has advantages of Barks of Pteroceltis Tatarinowii slurry, and the raw material sources of Shatian straw are wide, and cost is lower; In pure straw pulp, add the agent of vegetalitas anti-photooxidation, guaranteed the ageing resistace of the pure careless type rice paper of preparation, significantly improved service life; Use the active powder of calcium agent, make the pure careless type rice paper of preparation there is very superior profit China ink and writing quality; The pulping process of described pure careless type rice paper is simple, and effects on slurry making is good, is applicable to extensive rice paper and produces.
The specific embodiment
Embodiment 1
A pure careless type rice paper slurry, comprises following component by weight percentage: 77% pure straw pulp, and the slurry of pure straw pulp is dense is 78%; The active powder of 16% calcium agent; 1.6% cationic starch; 2% vegetalitas anti-photooxidation agent and 3.4% paper making additive; Wherein, the active powder of described calcium agent be whiteness more than 96, particle diameter is that 1025 object powdered whitings are through the active powder of the stearic acid modified calcium carbonate obtaining; Described vegetalitas antioxygen photo etching is four [β-(3,5-di-tert-butyl-hydroxy phenyl) propionic acid] pentaerythritol ester, and its molecular formula is C
73h
108o
12.
Embodiment 2
A pure careless type rice paper slurry, comprises following component by weight percentage: 74.5% pure straw pulp, and the slurry of pure straw pulp is dense is 73%; The active powder of 20% calcium agent; 0.8% cationic starch; 1.2% vegetalitas anti-photooxidation agent and 3.5% paper making additive; Wherein, the active powder of described calcium agent be whiteness more than 96, particle diameter is that 1100 object powdered whitings are through the active powder of the stearic acid modified calcium carbonate obtaining; Described vegetalitas antioxygen photo etching is four [β-(3,5-di-tert-butyl-hydroxy phenyl) propionic acid] pentaerythritol ester, and its molecular formula is C
73h
108o
12.
Embodiment 3
A pure careless type rice paper slurry, comprises following component by weight percentage: 71.6% pure straw pulp, and the slurry of pure straw pulp is dense is the active powder of 72%, 24% calcium agent, 1.5% cationic starch, 1.5% vegetalitas anti-photooxidation agent and 1.4% paper making additive; Wherein, the active powder of described calcium agent be whiteness more than 96, particle diameter is that 1200 object powdered whitings are through the active powder of the stearic acid modified calcium carbonate obtaining; Described vegetalitas antioxygen photo etching is four [β-(3,5-di-tert-butyl-hydroxy phenyl) propionic acid] pentaerythritol ester, and its molecular formula is C
73h
108o
12.
Embodiment 4
A pure careless type rice paper slurry, comprises following component by weight percentage: 76% pure straw pulp, and the slurry of pure straw pulp is dense is the active powder of 75%, 20% calcium agent, 1% cationic starch, 1% vegetalitas anti-photooxidation agent and 2% paper making additive; Wherein, the active powder of described calcium agent be whiteness more than 96, particle diameter is that 1150 object powdered whitings are through the active powder of the stearic acid modified calcium carbonate obtaining; Described vegetalitas antioxygen photo etching is four [β-(3,5-di-tert-butyl-hydroxy phenyl) propionic acid] pentaerythritol ester, and its molecular formula is C
73h
108o
12.
The present invention proposes a kind of pure careless type rice paper, adopt the pure careless type rice paper slurry described in above-described embodiment 1-4 to make.
In embodiment 1-4, the pulping process of above-mentioned pure careless type rice paper slurry, comprises the steps:
S1, get Shatian straw, remove rice leaf spike of rice, after lashing, put into water and soak 13-17 days, as 13 days, 14 days, 15 days, 16 days, 17 days, pull rear draining 0.8-2h out, as 0.8h, 1h, 1.5h, 2h, be then placed in milk of lime and flood 5-10 days, as 5 days, 6 days, 7 days, 8 days, 9 days, 10 days;
S2, by S1, through the straw code heap retting of dipping, tear open after 27-32 days pile stand-by, as 27 days, 28 days, 30 days, 31 days, 32 days;
S3, by S2 through the straw water proof boiling 20-40h of retting, as 20h, 22h, 25h, 30h, 33h, 35h, 39h, 40h, after cooling, rinsing, shine stand 20-40 days, as 20 days, 25 days, 30 days, 35 days, 40 days; 1-5 time so repeatedly, as 1 time, 2 times, 3 times, 4 times, 5 times, until straw carries out after being white in color air-dryly, obtain forage;
S4, the forage in S3 is pulverized, washes material after, add suitable quantity of water, obtaining starching dense is the pure straw pulp of 72-78%, as starched, densely can be 72%, 73%, 75%, 76%, 77%, 78%;
S5, according to percentage by weight, take the pure straw pulp 70-80% that obtains in S4, the active powder 15-25% of calcium agent, cationic starch 0.5-2%, vegetalitas anti-photooxidation agent 0.5-2% and paper making additive 1-4%, after mixing, obtain above-mentioned pure careless type rice paper slurry.
In the embodiment of the present invention, adopt Shatian straw to replace Barks of Pteroceltis Tatarinowii to carry out slurrying, because Barks of Pteroceltis Tatarinowii content of lignin is lower, easily slurrying, calcium carbonate content is high, be conducive to improve the profit mill performance of rice paper, fibrocyte wall thickness, microfibril is many, make the ink absorption of rice paper good, the pure careless type rice paper slurry of making has advantages of Barks of Pteroceltis Tatarinowii slurry, and the raw material sources of Shatian straw are wide, and cost is lower; In pure straw pulp, add the agent of vegetalitas anti-photooxidation, guaranteed the ageing resistace of the pure careless type rice paper of preparation, significantly improved service life; Use the active powder of calcium agent, make the pure careless type rice paper of preparation there is very superior profit China ink and writing quality; The pulping process of described pure careless type rice paper is simple, and effects on slurry making is good, is applicable to extensive rice paper and produces.
The above; it is only the preferably specific embodiment of the present invention; but protection scope of the present invention is not limited to this; anyly be familiar with those skilled in the art in the technical scope that the present invention discloses; according to technical scheme of the present invention and inventive concept thereof, be equal to replacement or changed, within all should being encompassed in protection scope of the present invention.
Claims (10)
1. a pure careless type rice paper slurry, is characterized in that, comprises by weight percentage the pure straw pulp of following component: 70-80%, and the slurry of pure straw pulp is dense is 72-78%; The active powder of 15-25% calcium agent; 0.5-2% cationic starch; The agent of 0.5-2% vegetalitas anti-photooxidation; 1-4% paper making additive.
2. pure careless type rice paper slurry according to claim 1, is characterized in that, the active powder of described calcium agent is that powdered whiting is through the active powder of the stearic acid modified calcium carbonate obtaining.
3. pure careless type rice paper slurry according to claim 2, is characterized in that, the whiteness of described powdered whiting is more than 96, and particle diameter is between 1000-1200 order.
4. pure careless type rice paper slurry according to claim 1, is characterized in that, described vegetalitas antioxygen photo etching is four [β-(3,5-di-tert-butyl-hydroxy phenyl) propionic acid] pentaerythritol ester, and its molecular formula is C
73h
108o
12.
5. according to the pure careless type rice paper slurry described in any one in claim 1-4, it is characterized in that, comprise by weight percentage the pure straw pulp of following component: 75-78%, the slurry of pure straw pulp is dense is 74-76%; The active powder of 18-22% calcium agent; 0.8-1.2% cationic starch; The agent of 0.8-1.2% vegetalitas anti-photooxidation; 1.5-2.5% paper making additive.
6. pure careless type rice paper slurry according to claim 5, is characterized in that, comprises by weight percentage following component: 76% pure straw pulp, and the slurry of pure straw pulp is dense is 75%; The active powder of 20% calcium agent; 1% cationic starch; 1% vegetalitas anti-photooxidation agent; 2% paper making additive.
7. according to a pulping process for the pure careless type rice paper slurry described in any one in claim 1-6, it is characterized in that, comprise the steps:
S1, get Shatian straw, remove rice leaf spike of rice, after lashing, put into water and soak 13-17 days, pull rear draining 0.8-2h out, be then placed in milk of lime and flood 5-10 days;
S2, by S1, through the straw code heap retting of dipping, tear open after 27-32 days pile stand-by;
S3, by S2 through the straw water proof boiling 20-40h of retting, after cooling, rinsing, shine stand 20-40 days; 1-5 carries out air-dryly after taking second place so repeatedly, obtains forage;
S4, the forage in S3 is pulverized, washes material after, add suitable quantity of water, obtaining starching dense is the pure straw pulp of 72-78%;
S5, according to percentage by weight, take the pure straw pulp that obtains in S4, the active powder of calcium agent, cationic starch, the agent of vegetalitas anti-photooxidation and paper making additive, after mixing, obtain described pure careless type rice paper slurry.
8. the pulping process of pure careless type rice paper slurry according to claim 7, is characterized in that, in S3,1-5 time until straw carries out after being white in color air-dry so repeatedly.
9. the pulping process of pure careless type rice paper slurry according to claim 7, is characterized in that, in S1, soaks 15 days in water, and draining 1h floods 7 days in milk of lime; In S2, code heap retting 30 days; In S3, water proof boiling 30h, shines stand 30 days, repeatedly 1-5 time until straw be white in color.
10. a pure careless type rice paper, is characterized in that, adopts the pure careless type rice paper slurry described in any one in claim 1-6 to make.
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Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105421065A (en) * | 2015-11-27 | 2016-03-23 | 宜兴市军达浆料科技有限公司 | Method for preparing starch size capable of achieving room temperature sizing |
| CN108286205A (en) * | 2017-10-07 | 2018-07-17 | 霍文慧 | A kind of ageing-resistant rice paper material |
| CN108301250A (en) * | 2017-10-07 | 2018-07-20 | 霍文慧 | A kind of novel rice paper material |
| CN108342928A (en) * | 2017-10-07 | 2018-07-31 | 谷文 | A kind of fire prevention painting and calligraphy carrier material |
| CN108360284A (en) * | 2017-10-07 | 2018-08-03 | 霍文慧 | A kind of modified form rice paper material |
| CN108385432A (en) * | 2017-10-07 | 2018-08-10 | 霍文慧 | A kind of fire-retardant rice paper material |
| CN108411702A (en) * | 2017-10-07 | 2018-08-17 | 霍文慧 | A kind of fire-retardant rice paper material |
| CN108411699A (en) * | 2017-10-07 | 2018-08-17 | 谷文 | A kind of modified form painting and calligraphy carrier material |
| CN108411703A (en) * | 2017-10-07 | 2018-08-17 | 霍文慧 | A kind of moisture-proof rice paper material |
| CN109112870A (en) * | 2018-07-02 | 2019-01-01 | 安徽泾县金星宣纸有限公司 | A kind of preparation method of rice paper magma |
| CN112458777A (en) * | 2020-11-05 | 2021-03-09 | 江西中竹生物质科技有限公司 | Method for manufacturing rice straw pulp by ultrasonic wave |
| CN112575614A (en) * | 2020-12-24 | 2021-03-30 | 胡明富 | Special cooked rice paper for calligraphy strokes and preparation method thereof |
| CN112593455A (en) * | 2020-12-24 | 2021-04-02 | 胡明富 | Special rice paper for calligraphy and manufacturing method thereof |
| CN112593454A (en) * | 2020-12-24 | 2021-04-02 | 胡明富 | Special semi-cooked rice paper for industrial tape writing and preparation method thereof |
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| CN108360295A (en) * | 2018-04-10 | 2018-08-03 | 绩溪县上庄老胡开文墨厂 | The pure careless type rice paper of one kind, pure careless type rice paper slurry and its pulping process |
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| CN105421065A (en) * | 2015-11-27 | 2016-03-23 | 宜兴市军达浆料科技有限公司 | Method for preparing starch size capable of achieving room temperature sizing |
| CN108286205A (en) * | 2017-10-07 | 2018-07-17 | 霍文慧 | A kind of ageing-resistant rice paper material |
| CN108301250A (en) * | 2017-10-07 | 2018-07-20 | 霍文慧 | A kind of novel rice paper material |
| CN108342928A (en) * | 2017-10-07 | 2018-07-31 | 谷文 | A kind of fire prevention painting and calligraphy carrier material |
| CN108360284A (en) * | 2017-10-07 | 2018-08-03 | 霍文慧 | A kind of modified form rice paper material |
| CN108385432A (en) * | 2017-10-07 | 2018-08-10 | 霍文慧 | A kind of fire-retardant rice paper material |
| CN108411702A (en) * | 2017-10-07 | 2018-08-17 | 霍文慧 | A kind of fire-retardant rice paper material |
| CN108411699A (en) * | 2017-10-07 | 2018-08-17 | 谷文 | A kind of modified form painting and calligraphy carrier material |
| CN108411703A (en) * | 2017-10-07 | 2018-08-17 | 霍文慧 | A kind of moisture-proof rice paper material |
| CN109112870A (en) * | 2018-07-02 | 2019-01-01 | 安徽泾县金星宣纸有限公司 | A kind of preparation method of rice paper magma |
| CN109112870B (en) * | 2018-07-02 | 2020-11-03 | 安徽泾县金星宣纸有限公司 | Preparation method of rice paper raw stock |
| CN112458777A (en) * | 2020-11-05 | 2021-03-09 | 江西中竹生物质科技有限公司 | Method for manufacturing rice straw pulp by ultrasonic wave |
| CN112575614A (en) * | 2020-12-24 | 2021-03-30 | 胡明富 | Special cooked rice paper for calligraphy strokes and preparation method thereof |
| CN112593455A (en) * | 2020-12-24 | 2021-04-02 | 胡明富 | Special rice paper for calligraphy and manufacturing method thereof |
| CN112593454A (en) * | 2020-12-24 | 2021-04-02 | 胡明富 | Special semi-cooked rice paper for industrial tape writing and preparation method thereof |
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