CN103757638A - Solid metal rust-resisting material and preparation method thereof - Google Patents

Solid metal rust-resisting material and preparation method thereof Download PDF

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Publication number
CN103757638A
CN103757638A CN201310703510.0A CN201310703510A CN103757638A CN 103757638 A CN103757638 A CN 103757638A CN 201310703510 A CN201310703510 A CN 201310703510A CN 103757638 A CN103757638 A CN 103757638A
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China
Prior art keywords
parts
formaldehyde
rust
epoxy resin
sodium hydroxide
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Pending
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CN201310703510.0A
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Chinese (zh)
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顾评
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WUJIANG LINSU PRECISION MACHINERY Co Ltd
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WUJIANG LINSU PRECISION MACHINERY Co Ltd
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Priority to CN201310703510.0A priority Critical patent/CN103757638A/en
Publication of CN103757638A publication Critical patent/CN103757638A/en
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Abstract

The invention discloses a solid metal rust-resisting material and a preparation method thereof. The solid metal rust-resisting material consists of 10-16 parts of methylcellulose, 10-12 parts of ethylcellulose, 8-12 parts of dimethyl phthalate, 9-10 parts of methanol, 6-8 parts of sodium hydroxide of 25%, 6-8 parts of formaldehyde, 1-2 parts of sodium nitrite, 0.1-0.2 part of a rust transforming agent, 2.5-3 parts of dithioether, 2.5-3 parts of oil soluble antistatic agent, 65-70 parts of light mechanical oil and 12-16 parts of diphenol propane epoxy resin. Compared with the prior art, the technical solution disclosed by the invention has the technical effects that the production process is simple, the cost is low, the self-dry speed is high, the prepared solid metal rust-resisting material is convenient to use, has acid-base resistance, aging resistance and good corrosion resistance, and the rust-resisting duration can reach 8-12 years.

Description

A kind of solid metallic antirust material and preparation method thereof
Technical field
The invention belongs to rush-resisting material field, relate in particular to a kind of solid metallic antirust material and preparation method thereof.
Background technology
Machinery does not contact with airborne oxygen, moisture or other corrosive medium with being difficult in storage in operation, these materials get rusty generation galvanic corrosion in metallic surface, prevent that corrosion from must stop above material and metallic contact, need to use rust-preventive agent to form thin film in metallic surface, prevent the chemical of corrosion of metal, along with industrial expansion, the progress of mechanical skill, design a kind of production technique simple, cost is low and can quick self-drying, easy to use, the rust-preventive agent of antirust time length, to meet the need of market, is very important.
Summary of the invention
The technical problems such as the problems referred to above that the present invention need to solve are for complex manufacturing, and price is high, and the antirust time is short, and provide a kind of production technique simple, cost is low and can quick self-drying, easy to use, solid metallic antirust material that the antirust time is long and preparation method thereof.
Technical scheme of the present invention:
A kind of solid metallic antirust material, its composition is take mass fraction representation as methylcellulose gum 10-16 part, ethyl cellulose 10-12 part, Bisphthalate 8-12 part, methyl alcohol 9-10 part, sodium hydroxide 6-8 part of 25%, formaldehyde 6-8 part, Sodium Nitrite 1-2 part, rust transforming agent 0.1-0.2 part, double thioether 2.5-3 part, oil soluble static inhibitor 2.5-3 part, light color machinery oil 65-70 part, propane type epoxy resin of di phenolic group 12-16 part.
A kind of solid metallic antirust material, its composition is take mass fraction representation as 12 parts of methylcellulose gum, 11 parts of ethyl cellulose, 10 parts of Bisphthalates, 9.5 parts of methyl alcohol, 7 parts, 25% sodium hydroxide, 7 parts, formaldehyde, 1.5 parts of Sodium Nitrites, 0.15 part of rust transforming agent, 2.8 parts of double thioethers, 2.8 parts, oil soluble static inhibitor, 66 parts, light color machinery oil, 15 parts of propane type epoxy resin of di phenolic group.
The preparation method of described solid metallic antirust material, it is characterized in that: comprise the following steps: according to quality proportioning, (1) methylcellulose gum, ethyl cellulose, Bisphthalate, methyl alcohol are added in reactor, at the temperature of 100-120 ℃, add formaldehyde, under the katalysis of formaldehyde, generate the glutinous material of white, then be compounded to form transparent glue; (2) transparent glue with in 25% sodium hydroxide and after, add Sodium Nitrite, rust transforming agent, double thioether, oil soluble static inhibitor and stir; (3) mixing solutions is warmed up to 180-200 ℃, adds propane type epoxy resin of di phenolic group, light machinery oil mixes, and under 160-180 ℃ of high-temperature vacuum, dehydration, de-bubble, obtain finished product.
Beneficial effect: a kind of solid metallic antirust material of the present invention adopts above technical scheme compared with prior art, have following technique effect: production technique is simple, cost is low and can quick self-drying, easy to use, acid and alkali-resistance, ageing-resistant, good corrosion resistance, the antirust time can reach 8-12.
Embodiment
Embodiment 1:
A kind of solid metallic antirust material, its composition is take mass fraction representation as 10 parts of methylcellulose gum, 10 parts of ethyl cellulose, 8 parts of Bisphthalates, 9 parts of methyl alcohol, 6 parts, 25% sodium hydroxide, 6 parts, formaldehyde, 1 part of Sodium Nitrite, 0.1 part of rust transforming agent, 2.5 parts of double thioethers, 2.5 parts, oil soluble static inhibitor, 65 parts, light color machinery oil, 12 parts of propane type epoxy resin of di phenolic group.
The preparation method of the present embodiment, comprise the following steps: according to quality proportioning, (1) methylcellulose gum, ethyl cellulose, Bisphthalate, methyl alcohol are added in reactor, at the temperature of 100-120 ℃, add formaldehyde, under the katalysis of formaldehyde, generate the glutinous material of white, then be compounded to form transparent glue; (2) transparent glue with in 25% sodium hydroxide and after, add Sodium Nitrite, rust transforming agent, double thioether, oil soluble static inhibitor and stir; (3) mixing solutions is warmed up to 180-200 ℃, adds propane type epoxy resin of di phenolic group, light machinery oil mixes, and under 160-180 ℃ of high-temperature vacuum, dehydration, de-bubble, obtain finished product.
Beneficial effect: production technique is simple, cost is low and can quick self-drying, easy to use, acid and alkali-resistance, ageing-resistant, good corrosion resistance, the antirust time can reach 8 years.
Embodiment 2:
A kind of solid metallic antirust material, its composition is take mass fraction representation as 16 parts of methylcellulose gum, 12 parts of ethyl cellulose, 12 parts of Bisphthalates, 10 parts of methyl alcohol, 8 parts, 25% sodium hydroxide, 8 parts, formaldehyde, 2 parts of Sodium Nitrites, 0.2 part of rust transforming agent, 3 parts of double thioethers, 3 parts, oil soluble static inhibitor, 70 parts, light color machinery oil, 16 parts of propane type epoxy resin of di phenolic group.
The preparation method of the present embodiment, comprise the following steps: according to quality proportioning, (1) methylcellulose gum, ethyl cellulose, Bisphthalate, methyl alcohol are added in reactor, at the temperature of 100-120 ℃, add formaldehyde, under the katalysis of formaldehyde, generate the glutinous material of white, then be compounded to form transparent glue; (2) transparent glue with in 25% sodium hydroxide and after, add Sodium Nitrite, rust transforming agent, double thioether, oil soluble static inhibitor and stir; (3) mixing solutions is warmed up to 180-200 ℃, adds propane type epoxy resin of di phenolic group, light machinery oil mixes, and under 160-180 ℃ of high-temperature vacuum, dehydration, de-bubble, obtain finished product.
Beneficial effect: production technique is simple, cost is low and can quick self-drying, easy to use, acid and alkali-resistance, ageing-resistant, good corrosion resistance, the antirust time can reach 10 years.
Embodiment 3:
A kind of solid metallic antirust material, its composition is take mass fraction representation as 12 parts of methylcellulose gum, 11 parts of ethyl cellulose, 10 parts of Bisphthalates, 9.5 parts of methyl alcohol, 7 parts, 25% sodium hydroxide, 7 parts, formaldehyde, 1.5 parts of Sodium Nitrites, 0.15 part of rust transforming agent, 2.8 parts of double thioethers, 2.8 parts, oil soluble static inhibitor, 66 parts, light color machinery oil, 15 parts of propane type epoxy resin of di phenolic group.
The preparation method of the present embodiment, comprise the following steps: according to quality proportioning, (1) methylcellulose gum, ethyl cellulose, Bisphthalate, methyl alcohol are added in reactor, at the temperature of 100-120 ℃, add formaldehyde, under the katalysis of formaldehyde, generate the glutinous material of white, then be compounded to form transparent glue; (2) transparent glue with in 25% sodium hydroxide and after, add Sodium Nitrite, rust transforming agent, double thioether, oil soluble static inhibitor and stir; (3) mixing solutions is warmed up to 180-200 ℃, adds propane type epoxy resin of di phenolic group, light machinery oil mixes, and under 160-180 ℃ of high-temperature vacuum, dehydration, de-bubble, obtain finished product.
Beneficial effect: production technique is simple, cost is low and can quick self-drying, easy to use, acid and alkali-resistance, ageing-resistant, good corrosion resistance, the antirust time can reach 12 years.
All components in above embodiment all can business be bought.
Above-described embodiment is just for content of the present invention is set forth, rather than restriction, and therefore any change in implication and the scope suitable with claims of the present invention, all should think to be included in the scope of claims.

Claims (3)

1. a solid metallic antirust material, is characterized in that: its composition is take mass fraction representation as methylcellulose gum 10-16 part, ethyl cellulose 10-12 part, Bisphthalate 8-12 part, methyl alcohol 9-10 part, sodium hydroxide 6-8 part of 25%, formaldehyde 6-8 part, Sodium Nitrite 1-2 part, rust transforming agent 0.1-0.2 part, double thioether 2.5-3 part, oil soluble static inhibitor 2.5-3 part, light color machinery oil 65-70 part, propane type epoxy resin of di phenolic group 12-16 part.
2. solid metallic antirust material according to claim 1, is characterized in that: its composition is take mass fraction representation as 12 parts of methylcellulose gum, 11 parts of ethyl cellulose, 10 parts of Bisphthalates, 9.5 parts of methyl alcohol, 7 parts, 25% sodium hydroxide, 7 parts, formaldehyde, 1.5 parts of Sodium Nitrites, 0.15 part of rust transforming agent, 2.8 parts of double thioethers, 2.8 parts, oil soluble static inhibitor, 66 parts, light color machinery oil, 15 parts of propane type epoxy resin of di phenolic group.
3. the preparation method of solid metallic antirust material according to claim 1 and 2, it is characterized in that: comprise the following steps: according to quality proportioning, (1) methylcellulose gum, ethyl cellulose, Bisphthalate, methyl alcohol are added in reactor, at the temperature of 100-120 ℃, add formaldehyde, under the katalysis of formaldehyde, generate the glutinous material of white, then be compounded to form transparent glue; (2) transparent glue with in 25% sodium hydroxide and after, add Sodium Nitrite, rust transforming agent, double thioether, oil soluble static inhibitor and stir; (3) mixing solutions is warmed up to 180-200 ℃, adds propane type epoxy resin of di phenolic group, light machinery oil mixes, and under 160-180 ℃ of high-temperature vacuum, dehydration, de-bubble, obtain finished product.
CN201310703510.0A 2013-12-20 2013-12-20 Solid metal rust-resisting material and preparation method thereof Pending CN103757638A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107217265A (en) * 2017-05-26 2017-09-29 山东大业股份有限公司 It is a kind of applied to rush-resisting material of steel bead wire and preparation method thereof
CN107326365A (en) * 2017-07-13 2017-11-07 山东大业股份有限公司 It is a kind of available for volatile rust preventive material of various metals and preparation method thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1793427A (en) * 2005-12-30 2006-06-28 徐鹏 Multifunctional solid metallic antirust material and production process thereof
CN102321428A (en) * 2011-08-15 2012-01-18 淮南市荣达化工技术研究所 Multifunctional steel anticorrosive paint and preparation method thereof
CN103254765A (en) * 2013-04-17 2013-08-21 马鞍山拓锐金属表面技术有限公司 Anti-rust oil employing methyl phenyl silicone oil as base oil and preparation method thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1793427A (en) * 2005-12-30 2006-06-28 徐鹏 Multifunctional solid metallic antirust material and production process thereof
CN102321428A (en) * 2011-08-15 2012-01-18 淮南市荣达化工技术研究所 Multifunctional steel anticorrosive paint and preparation method thereof
CN103254765A (en) * 2013-04-17 2013-08-21 马鞍山拓锐金属表面技术有限公司 Anti-rust oil employing methyl phenyl silicone oil as base oil and preparation method thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107217265A (en) * 2017-05-26 2017-09-29 山东大业股份有限公司 It is a kind of applied to rush-resisting material of steel bead wire and preparation method thereof
CN107326365A (en) * 2017-07-13 2017-11-07 山东大业股份有限公司 It is a kind of available for volatile rust preventive material of various metals and preparation method thereof

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Application publication date: 20140430