CN103756764B - A kind of synthetic hydraulic fluid and preparation method thereof - Google Patents
A kind of synthetic hydraulic fluid and preparation method thereof Download PDFInfo
- Publication number
- CN103756764B CN103756764B CN201310727360.7A CN201310727360A CN103756764B CN 103756764 B CN103756764 B CN 103756764B CN 201310727360 A CN201310727360 A CN 201310727360A CN 103756764 B CN103756764 B CN 103756764B
- Authority
- CN
- China
- Prior art keywords
- hydraulic fluid
- synthetic
- oil
- miscella
- base oil
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 239000012530 fluid Substances 0.000 title claims abstract description 40
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- 239000002199 base oil Substances 0.000 claims abstract description 21
- 239000003921 oil Substances 0.000 claims abstract description 21
- 150000001875 compounds Chemical class 0.000 claims abstract description 19
- 239000000654 additive Substances 0.000 claims abstract description 18
- 230000000996 additive effect Effects 0.000 claims abstract description 18
- 150000002148 esters Chemical class 0.000 claims abstract description 13
- 229920001515 polyalkylene glycol Polymers 0.000 claims abstract description 13
- 239000003963 antioxidant agent Substances 0.000 claims description 8
- 230000003078 antioxidant effect Effects 0.000 claims description 8
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims description 6
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical group [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 6
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims description 6
- 239000007866 anti-wear additive Substances 0.000 claims description 6
- 239000003995 emulsifying agent Substances 0.000 claims description 6
- 239000011574 phosphorus Substances 0.000 claims description 6
- 229910052698 phosphorus Inorganic materials 0.000 claims description 6
- 239000011593 sulfur Substances 0.000 claims description 6
- 229910052717 sulfur Inorganic materials 0.000 claims description 6
- 229910052725 zinc Inorganic materials 0.000 claims description 6
- 239000011701 zinc Substances 0.000 claims description 6
- 239000013556 antirust agent Substances 0.000 claims description 5
- 229920000642 polymer Polymers 0.000 claims description 4
- 238000007334 copolymerization reaction Methods 0.000 claims description 3
- 150000002989 phenols Chemical class 0.000 claims description 3
- 229920005862 polyol Polymers 0.000 claims description 3
- -1 polyol ester Chemical class 0.000 claims description 3
- 229920005682 EO-PO block copolymer Polymers 0.000 claims description 2
- 239000003795 chemical substances by application Substances 0.000 claims description 2
- 238000006116 polymerization reaction Methods 0.000 claims description 2
- 238000003756 stirring Methods 0.000 claims description 2
- IKXFIBBKEARMLL-UHFFFAOYSA-N triphenoxy(sulfanylidene)-$l^{5}-phosphane Chemical group C=1C=CC=CC=1OP(OC=1C=CC=CC=1)(=S)OC1=CC=CC=C1 IKXFIBBKEARMLL-UHFFFAOYSA-N 0.000 claims 2
- 239000004593 Epoxy Substances 0.000 claims 1
- 238000012661 block copolymerization Methods 0.000 claims 1
- CASPZMCSNJZQMV-UHFFFAOYSA-N ethane;2-methyloxirane Chemical compound CC.CC1CO1 CASPZMCSNJZQMV-UHFFFAOYSA-N 0.000 claims 1
- 150000002460 imidazoles Chemical class 0.000 claims 1
- 229940079865 intestinal antiinfectives imidazole derivative Drugs 0.000 claims 1
- 229910052751 metal Inorganic materials 0.000 abstract description 8
- 239000002184 metal Substances 0.000 abstract description 8
- 230000003647 oxidation Effects 0.000 abstract description 7
- 238000007254 oxidation reaction Methods 0.000 abstract description 7
- 230000002378 acidificating effect Effects 0.000 abstract description 2
- 239000008393 encapsulating agent Substances 0.000 abstract description 2
- 239000007788 liquid Substances 0.000 abstract description 2
- 239000000463 material Substances 0.000 abstract description 2
- 230000009286 beneficial effect Effects 0.000 abstract 1
- 230000000452 restraining effect Effects 0.000 abstract 1
- 239000010720 hydraulic oil Substances 0.000 description 10
- 238000002474 experimental method Methods 0.000 description 8
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 6
- 239000000203 mixture Substances 0.000 description 6
- 238000013019 agitation Methods 0.000 description 5
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 4
- 238000010521 absorption reaction Methods 0.000 description 4
- 230000008901 benefit Effects 0.000 description 3
- 230000007062 hydrolysis Effects 0.000 description 3
- 238000006460 hydrolysis reaction Methods 0.000 description 3
- 239000001294 propane Substances 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 2
- 230000015556 catabolic process Effects 0.000 description 2
- 238000005260 corrosion Methods 0.000 description 2
- 230000007797 corrosion Effects 0.000 description 2
- 238000006731 degradation reaction Methods 0.000 description 2
- 230000008021 deposition Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 2
- 229920000570 polyether Polymers 0.000 description 2
- RBACIKXCRWGCBB-UHFFFAOYSA-N 1,2-Epoxybutane Chemical compound CCC1CO1 RBACIKXCRWGCBB-UHFFFAOYSA-N 0.000 description 1
- JECYNCQXXKQDJN-UHFFFAOYSA-N 2-(2-methylhexan-2-yloxymethyl)oxirane Chemical compound CCCCC(C)(C)OCC1CO1 JECYNCQXXKQDJN-UHFFFAOYSA-N 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical group C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 239000004721 Polyphenylene oxide Substances 0.000 description 1
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 1
- 238000005299 abrasion Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- 150000004982 aromatic amines Chemical class 0.000 description 1
- 229910052788 barium Inorganic materials 0.000 description 1
- DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 description 1
- 230000006399 behavior Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000013329 compounding Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 229920001971 elastomer Polymers 0.000 description 1
- 239000000806 elastomer Substances 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 239000010687 lubricating oil Substances 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 239000002480 mineral oil Substances 0.000 description 1
- 235000010446 mineral oil Nutrition 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 150000002898 organic sulfur compounds Chemical class 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 125000001273 sulfonato group Chemical group [O-]S(*)(=O)=O 0.000 description 1
- 230000001629 suppression Effects 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 230000002194 synthesizing effect Effects 0.000 description 1
Landscapes
- Lubricants (AREA)
Abstract
The present invention relates to artificial oil field, particularly disclose a kind of synthetic hydraulic fluid and preparation method thereof.This synthetic hydraulic fluid, the component including following percentage by weight makes: compound additive bag 1.45～6.0%, oil soluble polyalkylene glycol 60～90%, surplus is synthetic ester base oil.The invention has the beneficial effects as follows: component is reasonable, has suitable viscosity and viscosity-temperature characteristic, can active balance mechanical efficiency and volumetric efficiency, thermal oxidation stability is good, the acidic materials produced by oxidation during effectively restraining use and greasy filth；Strainability is good, can meet the rigors that precision is high, gap is little, control the complicated hydraulic system of element, moreover it is possible to meet hydraulic means when operating temperature with requirement for liquid viscosity during start-up temperature；And hydraulic system metal and encapsulant are had good compatibility, demulsification resistance, air release property, wear resistence etc. are functional.
Description
(1) technical field
The present invention relates to artificial oil field, particularly to a kind of synthetic hydraulic fluid and preparation method thereof.
(2) background technology
Hydraulic oil is the working media of hydraulic system, modern hydraulic systems have component size little, lightweight,
The features such as compact conformation, hydraulic operation is affected by hydraulic oil character, but existing hydraulic oil thermal oxide is stabilized
Property, strainability, compatibility and wear resistence etc. are the most poor, can not meet the demand of modern hydraulic systems.
(3) summary of the invention
The present invention is in order to make up the deficiencies in the prior art, it is provided that a kind of component is reasonable, thermal oxidation stability good,
Synthetic hydraulic fluid that strainability is good, compatibility good, wear resistence is good and preparation method thereof.
The present invention is achieved through the following technical solutions:
A kind of synthetic hydraulic fluid, the component including following percentage by weight makes: compound additive bag 1.45～
6.0%, oil soluble polyalkylene glycol 60～90%, surplus is synthetic ester base oil.
Described compound additive bag includes antioxidant 0.8～3.0%, antirust agent 0.05～0.5% and extreme-pressure anti-wear
Agent 0.5～1.5%.
Described antioxidant is ashless aromatic amine antioxidant or Hinered phenols antioxidant, and oxidation resistance is strong, energy
Suppression oil ageing, reduces precipitation, paint film and the generation of greasy filth, thus suppresses the increasing of lubricating oil viscosity
Long；Described antirust agent is sulfonate (slaine is sodium, calcium, magnesium, zinc, barium etc.), organic amine or jeterocyclic chemistry
Compound, it forms physics in metal surface due to dipole and the metal surface generation electrostatic attraction of polar molecule
Absorption, or the chemisorbed that the molecule of absorption chemically reacts with metal, can be formed in metal surface closely
Molecular shield, prevents corrosion；Described extreme pressure anti-wear additives is organic sulfur compound extreme pressure anti-wear additives or organic phosphatization
Thing extreme pressure anti-wear additives, under conditions of the ability to bear load of metal surface, plays the metal surface of anti-sliding stop
Abrasion, the effect that even sinters of scratch.
Described compound additive bag also includes anti emulsifier 0.1～1.0%.
Described anti emulsifier is cithrol or ethylene oxide-propylene oxide block copolymer, absorption
At oil-water interface, change oil-water boundary tension force, or absorption destroy hydrophilic-lipophilic balance (HLB) on emulsifying agent,
Make emulsion oil-water separation during phase inversion.
Traditional polyethers base oil, is to be with oxirane, expoxy propane, epoxy butane and oxolane etc.
Raw material, under catalyst action, the linear polymer that open loop homopolymerization or copolymerization prepare.Oil of the present invention
Dissolubility ployalkylene glycol is not traditional oxirane (EO) and expoxy propane (PO) homopolymerization copolymerized polymer,
But the oil-soluble polymers prepared by block polymerization, random copolymerization, reverse block, have the advantage that
Viscosity grade is extensive, and Viscosity Index is high, and high temperature performance is excellent, and film strength is high, has outstanding deposition
Control and equipment cleaning, do not hydrolyze, use safety, and have at the aspect such as elastomer compatibility, hygroscopicity
Outstanding behaviours, particularly by alkoxylate chemical technology, improves conventional polyether base oil and other base oils
A difficult problem for intermiscibility difference.Dissolubility ployalkylene glycol also has high biological degradation rate, is the environment-friendly type of a kind of high-quality
Base oil.
Described synthetic ester base oil is polyol ester base oil, use compounding with oil soluble polyalkylene glycol.
The preparation method of this synthetic hydraulic fluid, is characterized in that: comprise the steps:
(1) oil soluble polyalkylene glycol and synthetic ester base oil are mixed, heated and stirred, constant temperature 50～60 DEG C
Lower mix homogeneously obtains miscella A；
(2) in the miscella A that step (1) prepares, compound additive bag, constant temperature 50～60 DEG C of bars are added
Continue stirring 1～2h under part, prepare miscella B；
(3) the miscella B that step (2) prepares is filtered, i.e. under 0.1MPa～0.2MPa pressure
Obtain limpid transparent synthetic hydraulic fluid.
Synthetic hydraulic fluid of the present invention and preparation method thereof provides the benefit that: component is reasonable, has suitable sticking
Degree and viscosity-temperature characteristic, can active balance mechanical efficiency and volumetric efficiency, thermal oxidation stability is good, can effectively press down
The acidic materials produced by oxidation during only using and greasy filth；Strainability is good, can meet precision high,
Gap is little, control the rigors of the complicated hydraulic system of element, moreover it is possible to meet hydraulic means in operating temperature
Time with during start-up temperature for the requirement of liquid viscosity, viscosity-temperature characteristic meets the various need that different purposes are proposed
Want；And hydraulic system metal and encapsulant are had good compatibility, demulsification resistance, air release property,
Wear resistences etc. are functional；Owing to using the oil soluble polyalkylene glycol base oil of high biological degradation rate, make this
Invention synthetic hydraulic fluid also has good environmental friendliness characteristic.
(4) detailed description of the invention
Below in conjunction with embodiment, the invention will be further described, but the invention is not limited in this, embodiment
In preparation method be customary preparation methods, no longer describe in detail.
Embodiment 1:(is in terms of double centner, as follows)
This compound additive bag, wherein sulfur-bearing 6.74%, phosphorus 3.38%, zinc 3.88%.
The preparation method of this synthetic hydraulic fluid, employing following steps:
(1) oil soluble polyalkylene glycol and the polyol ester base oil gear pump of above-mentioned weight are pumped into mediation
In, heated and stirred, at constant temperature 60 DEG C, mix homogeneously obtains miscella A；
(2) in the miscella A that step (1) prepares, add the compound additive bag of above-mentioned weight, constant temperature
Continue mechanical agitation 2h under the conditions of 60 DEG C, prepare miscella B；
(3) the miscella B that step (2) prepares is filtered, under 0.2MPa pressure, through having
The filter of Filter bag device filters, and obtains limpid transparent synthetic hydraulic fluid.
Embodiment 2:
This compound additive bag, wherein sulfur-bearing 6.5%, phosphorus 0.7%, nitrogen 3.2%.
The preparation method of this synthetic hydraulic fluid, employing following steps:
(1) oil soluble polyalkylene glycol and the synthetic ester base oil gear pump of above-mentioned weight are pumped into mediation
In, heated and stirred, at constant temperature 55 DEG C, mix homogeneously obtains miscella A；
(2) in the miscella A that step (1) prepares, add the compound additive bag of above-mentioned weight, constant temperature
Continue mechanical agitation 1.5h under the conditions of 55 DEG C, prepare miscella B；
(3) the miscella B that step (2) prepares is filtered, under 0.15MPa pressure, Jing Guoyou
The filter of filter bag device filters, and obtains limpid transparent synthetic hydraulic fluid.
Embodiment 3:
This compound additive bag, wherein sulfur-bearing 7.5%, phosphorus 3.7%, zinc 7.8%.
The preparation method of this synthetic hydraulic fluid, employing following steps:
(1) oil soluble polyalkylene glycol and the synthetic ester base oil gear pump of above-mentioned weight are pumped into mediation
In, heated and stirred, at constant temperature 50 DEG C, mix homogeneously obtains miscella A；
(2) in the miscella A that step (1) prepares, add the compound additive bag of above-mentioned weight, constant temperature
Continue mechanical agitation 1h under the conditions of 50 DEG C, prepare miscella B；
(3) the miscella B that step (2) prepares is filtered, under 0.1MPa pressure, through having
The filter of Filter bag device filters, and obtains limpid transparent synthetic hydraulic fluid.
Embodiment 4:
This compound additive bag, wherein sulfur-bearing 6.5%, phosphorus 3.0%, zinc 2.7%.
The preparation method of this synthetic hydraulic fluid, employing following steps:
(1) oil soluble polyalkylene glycol and the synthetic ester base oil gear pump of above-mentioned weight are pumped into mediation
In, heated and stirred, at constant temperature 55 DEG C, mix homogeneously obtains miscella A；
(2) in the miscella A that step (1) prepares, add the compound additive bag of above-mentioned weight, constant temperature
Continue mechanical agitation 2h under the conditions of 55 DEG C, prepare miscella B；
(3) the miscella B that step (2) prepares is filtered, under 0.15MPa pressure, Jing Guoyou
The filter of filter bag device filters, and obtains limpid transparent synthetic hydraulic fluid.
Embodiment 5:
This compound additive bag, wherein sulfur-bearing 9.2%, phosphorus 2.4%, zinc 5.2%.
The preparation method of this synthetic hydraulic fluid, employing following steps:
(1) oil soluble polyalkylene glycol and the synthetic ester base oil gear pump of above-mentioned weight are pumped into mediation
In, heated and stirred, at constant temperature 60 DEG C, mix homogeneously obtains miscella A；
(2) in the miscella A that step (1) prepares, add the compound additive bag of above-mentioned weight, constant temperature
Continue mechanical agitation 1.5h under the conditions of 60 DEG C, prepare miscella B；
(3) the miscella B that step (2) prepares is filtered, under 0.2MPa pressure, through having
The filter of Filter bag device filters, and obtains limpid transparent synthetic hydraulic fluid.
With conventional hydraulic oil phase ratio, synthetic hydraulic fluid of the present invention has the advantage that
A) pour point (experimental technique ASTM D97), the pour point of synthetic hydraulic fluid of the present invention is lower than conventional hydraulic oil
15～30 DEG C, more adapt to extreme low temperature applied environment；
B) Viscosity Index (experimental technique ASTM D2270), synthetic hydraulic fluid of the present invention improves 15～30, sticks
Warm nature can more preferably, and high-temperature viscosity rate of descent reduces by 15～30%, and high temperature oil-film retention property is more preferable；
C) abrasion-resistance, uses micro-pull strength analyzer to test, and synthetic hydraulic fluid abrasion-resistance of the present invention compares V
Class base oil improves 20%, improves 65～85% than IV class base oil, is more far superior to mineral oil；
D) depositional control and cleansing performance (experimental technique ASTM D2893B), synthetic hydraulic fluid of the present invention is few
Producing deposition, acid number change and viscosity change are little, have obvious cleansing performance；
E) hydrolysis stability (experimental technique ASTM D2619), synthetic hydraulic fluid of the present invention is retaining other IV
While class and V class synthetic hydraulic fluid performance, improve hydrolysis stability, especially with synthesizing ester hydraulic oil
Comparing, hydrolysis stability improves 30～70%；
F) air release property (experimental technique ASTM D3427), the air release value of synthetic hydraulic fluid of the present invention
Ratio conventional hydraulic oil low 70～80%, can be substantially reduced the oil product cavitation corrosion to gear apparatus, slow down oil product old
Change, extend the service life of oil product；
G) abrasion-resistance (experimental technique ASTM D6973), synthetic hydraulic fluid of the present invention rubs than conventional hydraulic oil
Loss rate reduces about 86%, has significant abrasion-resistance；
H) bearing capacity (experimental technique DIN51354), the inefficacy rank of synthetic hydraulic fluid of the present invention is than tradition
Hydraulic oil improves 2～5 grades, and bearing capacity is higher, can provide equipment preferably under high temperature high sliding speed
Oil film is protected；
I) biological degradability of synthetic hydraulic fluid of the present invention is up to more than 70%, belongs to environmentally friendly product；
J) oxidation stability (experimental technique ASTM D2272), synthetic hydraulic fluid of the present invention is than synthesis hydrocarbon, conjunction
The synthetic hydraulic fluid becoming ester improves 70～80%, effectively extends service life；
K) overlength uses the cycle, and the drain period of synthetic hydraulic fluid of the present invention is 1～5 times of conventional hydraulic oil.
Claims (3)
1. a synthetic hydraulic fluid, is characterized in that: be made up of the component of following percentage by weight: antioxygen
Agent 2.5%, antirust agent 0.4%, extreme pressure anti-wear additives 1.2%, anti emulsifier 0.76%, oil soluble polyalkylene glycol
75%, surplus is synthetic ester base oil；
Wherein, described antioxidant is Hinered phenols antioxidant；Described antirust agent is imdazole derivatives；Described pole
Pressure antiwear additive is triphenylphosphorothionate；Described anti emulsifier is epoxy ethane-epoxy propane block copolymerization
Thing；
Described antioxidant, antirust agent, extreme pressure anti-wear additives and anti emulsifier are mixed and made into compound additive bag, institute
State sulfur-bearing 6.5% in compound additive bag, phosphorus 3.0%, zinc 2.7%.
The preparation method of this synthetic hydraulic fluid, comprises the steps:
(1) oil soluble polyalkylene glycol and synthetic ester base oil are mixed, heated and stirred, mixed at constant temperature 55 DEG C
Close uniform miscella A；
(2) in the miscella A that step (1) prepares, above-mentioned Hinered phenols antioxidant, imidazole derivatives are added
The compound additive that thing, triphenylphosphorothionate and ethylene oxide-propylene oxide block copolymer are mixed
Bag, continues stirring 2h, prepares miscella B under the conditions of constant temperature 55 DEG C；
(3) the miscella B that step (2) prepares is filtered under 0.15MPa pressure, obtain limpid
Transparent synthetic hydraulic fluid.
A kind of synthetic hydraulic fluid the most according to claim 1, is characterized in that: oil soluble polyalkylene glycol
For the oil-soluble polymers prepared by block polymerization or random copolymerization.
A kind of synthetic hydraulic fluid the most according to claim 1, is characterized in that: described synthetic ester base oil
For polyol ester base oil.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310727360.7A CN103756764B (en) | 2013-12-25 | 2013-12-25 | A kind of synthetic hydraulic fluid and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310727360.7A CN103756764B (en) | 2013-12-25 | 2013-12-25 | A kind of synthetic hydraulic fluid and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103756764A CN103756764A (en) | 2014-04-30 |
| CN103756764B true CN103756764B (en) | 2016-08-17 |
Family
ID=50524094
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310727360.7A Active CN103756764B (en) | 2013-12-25 | 2013-12-25 | A kind of synthetic hydraulic fluid and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103756764B (en) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104232274A (en) * | 2014-10-16 | 2014-12-24 | 中国石油化工股份有限公司 | Hydrodynamic drive oil |
| CN104804818A (en) * | 2015-04-21 | 2015-07-29 | 苏州劲元油压机械有限公司 | Biodegradable environment-friendly hydraulic oil |
| CN105038936A (en) * | 2015-08-27 | 2015-11-11 | 黄进堂 | Antiwear hydraulic oil |
| CN105567377A (en) * | 2015-12-28 | 2016-05-11 | 芜湖市创源新材料有限公司 | Excellent-anti-corrosion-performance synthetic hydraulic oil |
| US10995178B2 (en) | 2016-08-10 | 2021-05-04 | Nof Corporation | Alkyloxirane derivative, cosmetic material for hair, hydraulic oil composition, resin composition curable by actinic rays, and oil cleansing agent |
| CN106479648A (en) * | 2016-10-17 | 2017-03-08 | 中国石油化工股份有限公司 | A kind of high viscosity synthetic hydraulic fluid compositionss and its application |
| DE102020111403A1 (en) * | 2020-04-27 | 2021-10-28 | Klüber Lubrication München Se & Co. Kg | Lubricant composition and its use |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101113383A (en) * | 2007-07-03 | 2008-01-30 | 杭州新港石油化工有限公司 | Ester flame-proof hydraulic-oil containing nano abrasion-resistant additive and production method thereof |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP5122114B2 (en) * | 2006-11-17 | 2013-01-16 | Ｊｘ日鉱日石エネルギー株式会社 | Hydraulic fluid and hydraulic system using the same |
-
2013
- 2013-12-25 CN CN201310727360.7A patent/CN103756764B/en active Active
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101113383A (en) * | 2007-07-03 | 2008-01-30 | 杭州新港石油化工有限公司 | Ester flame-proof hydraulic-oil containing nano abrasion-resistant additive and production method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 油溶性PAG的性能特点及应用;韩耀坤;《石油商技》;20120229(第1期);33-38 * |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103756764A (en) | 2014-04-30 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103756764B (en) | A kind of synthetic hydraulic fluid and preparation method thereof | |
| US6972275B2 (en) | Oil-in-oil emulsion lubricants for enhanced lubrication | |
| JP6549576B2 (en) | Organosiloxane composition | |
| JP4667761B2 (en) | Refrigerator oil composition | |
| CN104364357A (en) | Engine lubricant composition | |
| CN103695133B (en) | A kind of synthesis gas compressor cooling fluid and preparation method thereof | |
| CN103773575B (en) | Biodegradable screw air compressor oil | |
| CN104130842A (en) | Oil-soluble polyether oil for screw-type air compressor | |
| CN108291170B (en) | Method for improving air release of lubricating oil | |
| WO2014189711A1 (en) | Polyalkylene glycols useful as lubricant additives for hydrocarbon base oils | |
| CN107847820A (en) | Defoamer and lubricant oil composite | |
| WO2008089130A1 (en) | Lubricant compositions and methods of making same | |
| CN103695134B (en) | A kind of engine and wheel box synthesis wash oil and preparation method thereof | |
| CN103710113B (en) | A kind of lubricating oil reinforcing agent and preparation method thereof | |
| JP6602366B2 (en) | Alkyl-capped oil-soluble polymer viscosity index improver for automotive base oils | |
| JP2008127426A (en) | Hydraulic oil and hydraulic system using the same | |
| CN106947570A (en) | A kind of antiwear hydraulic oil and preparation method thereof | |
| CN103773574B (en) | A kind of compound probability gear oil and preparation method thereof | |
| CN103695131B (en) | A kind of synthesis automatic transmission fluid and preparation method thereof | |
| CN103710114B (en) | Gear oil for hybrid vehicle and preparation method of gear oil | |
| CN103695132B (en) | A kind of synthetic gasoline engine oil and preparation method thereof | |
| JP6190287B2 (en) | Water based lubricant | |
| CN111944584B (en) | Polyaziridine polymers as lubricating oil additives | |
| CN105121610A (en) | Modified hydrogen-based lubricants |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CP03 | Change of name, title or address | ||
| CP03 | Change of name, title or address |
Address after: 264006 No. 1, Yichang Road, development zone, Yantai City, Shandong Province Patentee after: Yantai Degao Petroleum Co.,Ltd. Address before: 264006 Kexin Industrial Park, No. 38 Tianshan Road, Yantai Development Zone, Shandong Province Patentee before: TEXAS PETROCHEM (YANTAI) Ltd. |
|
| PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A synthetic hydraulic oil and its preparation method Effective date of registration: 20231031 Granted publication date: 20160817 Pledgee: Yantai financing guarantee Group Co.,Ltd. Pledgor: Yantai Degao Petroleum Co.,Ltd. Registration number: Y2023980063455 |