CN103750204A - Pomelo fragrance Chinese yam buccal tablet and preparation method thereof - Google Patents
Pomelo fragrance Chinese yam buccal tablet and preparation method thereof Download PDFInfo
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- CN103750204A CN103750204A CN201310647126.3A CN201310647126A CN103750204A CN 103750204 A CN103750204 A CN 103750204A CN 201310647126 A CN201310647126 A CN 201310647126A CN 103750204 A CN103750204 A CN 103750204A
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L19/00—Products from fruits or vegetables; Preparation or treatment thereof
- A23L19/03—Products from fruits or vegetables; Preparation or treatment thereof consisting of whole pieces or fragments without mashing the original pieces
- A23L19/07—Fruit waste products, e.g. from citrus peel or seeds
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L19/00—Products from fruits or vegetables; Preparation or treatment thereof
- A23L19/10—Products from fruits or vegetables; Preparation or treatment thereof of tuberous or like starch containing root crops
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/20—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents
- A23L29/206—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents of vegetable origin
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/30—Foods or foodstuffs containing additives; Preparation or treatment thereof containing carbohydrate syrups; containing sugars; containing sugar alcohols, e.g. xylitol; containing starch hydrolysates, e.g. dextrin
- A23L29/37—Sugar alcohols
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/15—Vitamins
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
- A23L5/20—Removal of unwanted matter, e.g. deodorisation or detoxification
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23P—SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
- A23P10/00—Shaping or working of foodstuffs characterised by the products
- A23P10/20—Agglomerating; Granulating; Tabletting
- A23P10/28—Tabletting; Making food bars by compression of a dry powdered mixture
Abstract
The invention discloses a pomelo fragrance Chinese yam buccal tablet and a preparation method thereof. The pomelo fragrance Chinese yam buccal tablet comprises Chinese yam powder, debittered honey pomelo peel powder, maltodextrin, xylitol, maltitol, citric acid monohydrate, licorice root, vitamin C and potassium sorbate. The preparation method of the buccal tablet comprises the following steps: preparing the debittered honey pomelo peel powder, blending according to the above formula, preparing a soft material, granulating and tabletting. The Chinese yam buccal tablet is prepared by using Chinese yam as a main raw material, fully utilizes the edible and medicinal values of Chinese yam, combines the edible values and mouthfeel flavor of honey pomelo, and has the characteristics of appropriate hardness, good disintegration property, low naringin content, and sweet but not oily mouthfeel.
Description
Technical field
The present invention discloses a kind of buccal tablet, particularly a kind of shaddock Fragrance Hill medicine buccal tablet.
Background technology
Buccal tablet refers to be contained in the compressed tablets of slowly dissolving in oral cavity.Buccal tablet because of its good mouthfeel and easily instructions of taking be subject to the welcome of extensive patients.On market, there are many kinds such as Chloranthus glaber, Dobell in federal Imacil, river to have original sales achievement at home.
Buccal tablet is not only for to oral cavity and the lasting drug effect of pharyngeal generation, if Caoshan Hu Hanpian is for local anti-inflammatory, sterilization; More be used in addition other purposes such as health food.For example, patent CN101791096A discloses a kind of oleaster sweet buccal tablets, take arrow-leaved oleaster as primary raw material, be aided with the raw materials such as Radix Glycyrrhizae, by the preparation of following step: the preparation of arrow-leaved oleaster powder or arrow-leaved oleaster water extract powder, the preparation of Radix Glycyrrhizae powder, batching, mixing, wet method material processed, dry, compressing tablet and packaging and other steps.This kind of oleaster sweet buccal tablets quality be good, be difficult for moisture regaining and metamorphism, and color is all good, and lozenge hardness is high, and taste arrow-leaved oleaster is unique and nutritive value is high, and be masses' acceptance.Patent CN102342515A discloses a kind of persimmon buccal tablets, by persimmon thickened pulp, traditional Chinese drug inspissation slurry, food starch, sweet mellow wine, sucrose and dolomol mixed pressuring plate, is made; Each constituent mass proportioning is: persimmon thickened pulp 31-35%, traditional Chinese drug inspissation slurry 12-16%, food starch 34-38%, sweet mellow wine 5-8%, sucrose 4-7% and dolomol 0.7-1.5%; It is high that this kind of persimmon buccal tablets has production efficiency, and utilization rate of equipment and installations is high, is convenient to the advantages such as mechanization production; Product special flavour is unique, mouthfeel is pure, color and luster is good, is easy to moulding, has antioxidation, and quality meets the requirement of national Related product quality standard.A kind of buccal tablet for reducing blood sugar of patent CN102488815A disclosure of the invention, component by following weight portion is made: blue or green money willow extract 16-20 part, cinnamomum cassia extract 15-19 part, Bitter Melon P.E 11-15 part, taurine 8-12 part, yam extract 10-14 part, kudzu root extract 10-14 part, Ac-Di-Sol 5-10 part, aspartame 2-5 part, dolomol 6-9 part, Mint Essence 0.2-0.5 part, this buccal tablet has taking convenience, easily store and portable advantage, and bioavilability is than the obvious improve of ordinary preparation, for the life taste that adapts to present allegro life requirement and constantly promote provides again a method of administration easily.
Buccal tablet is industrialization on a large scale, and application is more and more wider, and its processing technology is very ripe, and its flow process is common is: the allotment → softwood → granulation processed → oven dry of process → formula of raw material, whole grain → compressing tablet → packing.Wherein granulation is a key operation point in tablet technique: can prevent that powdered food from adding dust from flying in man-hour, also can improve charging efficiency, prevent tablet water suction.Generally, in order to make each material composition, effectively bonding is in blocks, must in film-making process, add adhesive; For buccal tablet is easily come off from template, can in mixed material, add lubricant.
Patent CN1339310A discloses a kind of shaddock-lozenge tablet and preparation method thereof, comprises the raw material of following weight proportion: shaddock powder 83-87%, licorice powder 3-7%, loguat leaf powder 3-7%, balloonflower powder 3-7%, stevioside 1-5%, menthol 0.5-1.5%.Its manufacture craft is: whole shaddock is crushed to pasty state, and pectin is broken separated with fruit; Dry pectin and fruit are broken respectively, and water content is controlled below 7%; Pectin and fruit broken sieve respectively after, mix; Respectively Radix Glycyrrhizae, loguat leaf, balloonflower root are pulverized, after sieving, dry; Jelly powder, fruit powder, licorice powder, loguat leaf powder and balloonflower powder are added to stevioside, menthol again, mix, with tablet press machine, be pressed into sheet.This buccal tablet be take shaddock powder as main body composition, but shaddock fruit pulp processes without debitterize, and buccal tablet astringent taste is obvious; Its sweetener mainly relies on a high proportion of Radix Glycyrrhizae, and its sugariness is excessively sweet, and nutritional labeling disappearance.
Market has no any shaddock Fragrance Hill medicine buccal tablet product temporarily at present.For meeting the consumer of the Chinese yam buccal tablet like sweet shaddock local flavor, be also badly in need of a take Chinese yam as raw material, add the buccal tablet of sweet shaddock local flavor.Both required this buccal tablet can add sweet shaddock local flavor, mouthfeel is agreeably sweet, need again the content of the contained aurantiin low shaddock Fragrance Hill medicine buccal tablet product of (being also that de-bittering effect is good).
Summary of the invention
The object of the present invention is to provide a kind of shaddock Fragrance Hill medicine buccal tablet, take Chinese yam as raw material, be aided with that sweet shaddock component is prepared from, can meet the consumer who likes sweet shaddock local flavor buccal tablet.This buccal tablet soft or hard appropriateness, disintegrative is good, has both added sweet shaddock local flavor, mouthfeel is agreeably sweet, and the de-bittering effect of sweet shaddock raw material content good, contained aurantiin is low.
Another object of the present invention is to provide a kind of method of preparing shaddock Fragrance Hill medicine buccal tablet, and the method technical process is simple, is applicable to industrialization and produces, and the aurantiin removal effect in sweet shaddock raw material is good.
The invention provides a kind of shaddock Fragrance Hill medicine buccal tablet, the component that comprises following weight portion: yam flour 40-50 part, debittering honey pomelo skin powder 7-9 part, maltodextrin 18-22 part, xylitol 14-18 part, maltitol 9-11 part, Citric Acid Mono 0.2-0.4 part, Radix Glycyrrhizae 0.1-0.3 part, vitamin C 0.06-0.1 part and potassium sorbate 0.02-0.04 part.
Wherein, described debittering honey pomelo skin powder is prepared by following step:
A1. sweet shaddock ped forming step: sweet shaddock fresh fruit is cut into lobe fresh fruit, and become the honey pomelo pericarp of lobe fresh fruit separated with sweet shaddock pulp, get honey pomelo pericarp and cut into the sweet shaddock fruit fourth of specification shape;
A2. sweet shaddock ped debitterize step: remove the bitter principle in sweet shaddock fruit fourth by debitterize liquid, sweet shaddock fruit fourth after debitterize is separated with debitterize liquid, and the composition components by weight percentage of wherein said debitterize liquid is: the water of sodium chloride 3.5-5.5%, cycloheptaamylose 0.3-0.4% and surplus;
A3. rinsing dehydration: after water cleans, then drying dehydration, obtain debittering honey pomelo skin;
A4. be ground into last step: debittering honey pomelo skin is pulverized in pulverizer, made debittering honey pomelo skin powder.
Preferably, described sweet shaddock ped debitterize step is under vacuum condition, to carry out debitterize, and preferred vacuum is 0.02MPa-0.15MPa, and the debitterize time is 60-90 minute, and debitterize temperature is 50-80 ℃.
This shaddock Fragrance Hill medicine buccal tablet is prepared by following step:
A. prepare debittering honey pomelo skin powder;
B. the adaptation step of filling a prescription: the component raw material of following weight parts is mixed: yam flour 40-50 part, debittering honey pomelo skin powder 7-9 part, maltodextrin 18-22 part, xylitol 14-18 part, maltitol 9-11 part, Citric Acid Mono 0.2-0.4 part, potassium sorbate 0.02-0.04 part, Radix Glycyrrhizae 0.1-0.3 part, vitamin C 0.06-0.1 part;
C. softwood step processed: the formula material mixing is mixed with edible ethanol, make softwood;
D. granulation step: gained softwood is crossed to 16-24 mesh sieve and granulate, and dry at 45-65 ℃, make its moisture be less than 5%, carry out whole grain after 35-45 mesh sieve;
E. compressing tablet step: send into tablet press machine and carry out compressing tablet, make shaddock Fragrance Hill medicine buccal tablet.
Chinese yam, herbaceos perennial, stem is overgrow, and is often with purple, and piece root is cylindrical, and leaf is to life, avette or oval, flower milky, dioecism.In Chinese yam, contain much starch and protein, B family vitamin, vitamin C, vitamin E, glucose, crude protein amino acid, bile alkaline (holine), allantoin (allantoin) etc.Starch-containing and the protein of the piece root of Chinese yam, edible; The mucilaginous substance of the GL-PP composition containing in stem tuber, zymigen etc., can prevent cardiovascular fat deposition, contributes to digesting and assimilating of stomach and intestine.Chinese yam is also rich in various vitamin and useful trace element, cement polysaccharide etc.; Also contain the medicinal ingredients such as allantoin, batatasins, saponin, choline, Dopamine hydrochloride; The integration of drinking and medicinal herbs food that nutritive value is very high.The traditional Chinese medical science also thinks to have the multiple efficacies such as Chinese yam has invigorating the spleen, tonifying lung, reinforces the kidney, benefit essence and improve the health and medical care effect.By Chinese yam stem tuber, grind the yam flour forming and can prevent cardiovascular system adipopexis, keep the elasticity of blood vessel, atherosclerosis occurs too early, reduces subcutaneous fat deposition.Take Chinese yam as the buccal tablet that primary raw material makes, and is a kind of high nutrition, food low in calories, can add relievedly edible and do not have the trouble and worry of getting fat.
Because the sugariness of Radix Glycyrrhizae is hundred times of sucrose, add after micro-Radix Glycyrrhizae, can not affect in the sugar content situation of shaddock Fragrance Hill medicine buccal tablet, increase considerably shaddock Fragrance Hill medicine buccal tablet sweet taste, improve its sour-sweet degree; In Radix Glycyrrhizae, contain the tens of kinds of compounds such as glycyrrhizin, enoxolone, liquiritin, isoliquiritin, neoliquriitin, neoisoliquiritin, glycyrrhizin, isoliquiritigenin and licoricidin, glycyrol, isoglycyrol, 7-methylcoumarin essence, umbelliferone simultaneously, can play the effect of other components of mediation.
In the selection of sweetener, xylitol has hygroscopicity and preventing caries function; Maltitol has significant hygroscopicity, also can prevent the crystallization of sucrose, and maltitol is difficult to digested metabolism in human body simultaneously, is good low-yield sweetener.Adopt the cooperation of xylitol and maltitol, and proportioning is controlled at 3:2 left and right, adds again micro-Radix Glycyrrhizae, both can guarantee the agreeable to the taste sweet taste of buccal tablet, can significantly reduce again the total sugar content of finished product, relatively cost-saving again.The sugar content of the buccal tablet making is low, total amount of heat is low, is not easy to make people to get fat, and diabetic patients.The used in amounts of xylitol and maltitol will adapt to control, and it not only affects the sour-sweet degree of sweet shaddock buccal tablet finished product, if can cause occurring in compressing tablet process sliver problem by quantity not sufficient.
Maltodextrin is to take starch as raw material, through enzyme method technique controlled hydrolysis, is transformed, be a kind of cheap, mouthfeel is satiny, without any the trophism polysaccharide of taste.Its solubility property is good, has appropriate viscosity; Hygroscopicity is low, is difficult for conglomeration.Having good carrier function, is the excellent carrier of various sweeteners, flavouring agent, filler etc.; Also have good emulsification and thickening effect, be convenient to promote tablet formed product; Filming performance is good, can prevent that tablet deformation of products from can improve product appearance again; Also very easily be absorbed by the body simultaneously, suitable especially patient and the infant food done.This Chinese yam buccal tablet selects maltodextrin as filler, it not only avoided traditional Icing Sugar class filler easily draw wet, easily cause the shortcomings such as carious tooth, and can also with the primary raw material good knitting such as yam flour.
In buccal tablet of the present invention, xylitol and maltitol had both been made diluent, played again flavoring and adhesive effect, simultaneously also as sweetener.The proportioning of main body composition, sweet taste pulvis and soluble starch is controlled: (yam flour+debittering honey pomelo skin powder): (xylitol+maltitol): maltodextrin=(10-12): (5-6): 5 left and right, both added sweet shaddock natural flavour mountaineous, guarantee again the performance indications such as hardness, melting time of tablet finished product, also overcome the problems such as the loose sheet that is prone in process, sliver, flower sheet.
Citric Acid Mono, as acidic flavouring agent, for coordinating the sour-sweet degree of yam flour and debittering honey pomelo skin powder, also can improve the sensory properties of buccal tablet simultaneously, whets the appetite and promotes digesting and assimilating of the interior calcium of body, phosphorus substance.
The present invention also provides a kind of method of preparing shaddock Fragrance Hill medicine buccal tablet, following step:
A. prepare debittering honey pomelo skin powder;
B. the adaptation step of filling a prescription: the component raw material of following weight parts is mixed: yam flour 40-50 part, debittering honey pomelo skin powder 7-9 part, maltodextrin 18-22 part, xylitol 14-18 part, maltitol 9-11 part, Citric Acid Mono 0.2-0.4 part, potassium sorbate 0.02-0.04 part, Radix Glycyrrhizae 0.1-0.3 part, vitamin C 0.06-0.1 part;
C. softwood step processed: the formula material mixing is mixed with edible ethanol, make softwood;
D. granulation step: gained softwood is crossed to 16-24 mesh sieve and granulate, and dry at 45-65 ℃, make its moisture be less than 5%, carry out whole grain after 35-45 mesh sieve;
E. compressing tablet step: send into tablet press machine and carry out compressing tablet, make shaddock Fragrance Hill medicine buccal tablet.
Particle too tide can produce sticking problem in compressing tablet process; Pellet moisture content is too low can cause occurring in compressing tablet process loose sheet problem.Simultaneously, the terminal of the drying and processing in granulation step is controlled has larger impact to the disintegrative of buccal tablet finished product, need suitable control: make the softwood moisture of dry terminal be less than 5% and be advisable, now the soft durometer of softwood with hand pinch agglomerating (and feel is clear-cut, tack-free), light press loose.Preferably, dry terminal control should be 2-4% in the moisture of softwood.
The interpolation of lubricant not only needs to consider its release, stripping result, also will consider the residue problem after its introducing, and the impact on the disintegrative of the surface flower point problem of buccal tablet and buccal tablet.Preferably, in described compressing tablet step, in the particle after granulation step, add the dolomol of percentage by weight 1-2%.Dolomol is water insoluble, ethanol or ether, can be used as lubricant, is convenient to buccal tablet and easily from template, comes off; Simultaneously less on the disintegrative impact of the surface flower point problem of this honey shaddock fruit powder buccal tablet and buccal tablet.
Wherein, the step of preparing debittering honey pomelo skin powder comprises:
A1. sweet shaddock ped forming step: sweet shaddock fresh fruit is cut into lobe fresh fruit, and become the honey pomelo pericarp of lobe fresh fruit separated with sweet shaddock pulp, get honey pomelo pericarp and cut into the sweet shaddock fruit fourth of specification shape;
A2. sweet shaddock ped debitterize step: remove the bitter principle in sweet shaddock fruit fourth by debitterize liquid, sweet shaddock fruit fourth after debitterize is separated with debitterize liquid, and the composition components by weight percentage of wherein said debitterize liquid is: the water of sodium chloride 3.5-5.5%, cycloheptaamylose 0.3-0.4% and surplus;
A3. rinsing dehydration: after water cleans, then drying dehydration, obtain debittering honey pomelo skin;
A4. be ground into last step: debittering honey pomelo skin is pulverized in pulverizer, made debittering honey pomelo skin powder.
Preferably, described sweet shaddock ped debitterize step is under vacuum condition, to carry out debitterize, and preferred vacuum is 0.02MPa-0.15MPa, and the debitterize time is 60-90 minute, and debitterize temperature is 50-80 ℃.
While producing for ease of industrialization, better control the stability of quality and the uniformity of mouthfeel of shaddock Fragrance Hill medicine buccal tablet, can be before preparing the sweet shaddock ped forming step of debittering honey pomelo skin powder, increase the step of cleaning and sterilizing: adopt the aqueous solution of chlorine dioxide that concentration is 10-500mg/L to carry out cleaning and sterilizing to sweet shaddock fresh fruit, thereby better cleaning milk shaddock fresh fruit grow, gather and transportation in the dust, silt, insect, microorganism etc. of surface attachment.The agricultural chemicals that the fresh epidermis of sweet shaddock is remaining if remove or heavy oil etc., can first use 0.5%-1.5%(weight) aqueous hydrochloric acid solution cleans, then uses 1%(weight) aqueous sodium carbonate cleans; Or, first use 0.03%-0.1%(weight) liquor potassic permanganate or the Eusol of 0.04%-0.06% soak 10-15 minute, then use clear water rinsing.
Beneficial effect of the present invention has: shaddock Fragrance Hill medicine buccal tablet be take yam flour as raw material, be aided with debittering honey pomelo skin powder, by formula allocate, softwood processed, granulation, compressing tablet step make, kept suitable sour-sweet degree, guaranteed ascorbic content, the content of contained aurantiin is controlled reduced levels, and total sugar content is low and heat is low.The food and medicament dual-purpose that this buccal tablet had both made full use of Chinese yam is worth, and merges again edibility and the taste flavor of sweet shaddock; Its soft or hard appropriateness, disintegrative is good, and the content of contained aurantiin is low, and mouthfeel is agreeably sweet.
The specific embodiment
By specific embodiments of the invention given below and comparing embodiment, can further be well understood to the present invention, but they not limitation of the invention.The part not describing in detail in specific embodiment and comparing embodiment is to adopt prior art, known technology means and industry standard to obtain.
Except as otherwise noted, the percentage adopting in the present invention is percetage by weight.
embodiment 1
By following step method, prepare shaddock Fragrance Hill medicine buccal tablet:
(1) prepare debittering honey pomelo skin powder:
Honey shaddock ped forming step: sweet shaddock fresh fruit is cut into lobe fresh fruit, and become the honey pomelo pericarp of lobe fresh fruit separated with sweet shaddock pulp, by honey pomelo pericarp and cut into the sweet shaddock fruit fourth of specification shape, honey pomelo pericarp enters machine and dices, be cut into the sweet shaddock fruit fourth that specification is (3.2-3.8cm) * (3.2-3.8cm) * (3.2-3.8cm), send into again sweet shaddock fruit fourth stepping device stepping, obtain qualified sweet shaddock fruit fourth.
Honey shaddock ped debitterize step: in vacuum, be under 0.05MPa, adopt debitterize liquid to remove the bitter principle in sweet shaddock fruit fourth, the sweet shaddock fruit fourth after debitterize is separated with debitterize liquid.Debitterize liquid components by weight percentage is: the water of sodium chloride 3.5-5.5%, cycloheptaamylose 0.3-0.4% and surplus.The debitterize liquid of above-mentioned formula and sweet shaddock fruit fourth are inserted to vacuum debitterize tank, and the weight ratio of sweet shaddock fruit fourth and debitterize liquid is 1:3, and under 60 ℃ of temperature and 0.05MPa vacuum degree condition, debitterize is 80 minutes.
Rinsing dehydration: after water cleans, then with centrifuge drying dehydration to not having the globule residual, make debittering honey pomelo skin.
Be ground into last step: with pulverizer, debittering honey pomelo skin is pulverized evenly, and crossed 100 mesh sieves, guarantee that grain diameter is less than 0.15mm, make debittering honey pomelo skin powder.
(2) formula adaptation step: by the component raw material of following weight parts: 46 parts of yam flours, 8 parts, debittering honey pomelo skin powder, 20 parts of maltodextrins, 16 parts of xylitols, 10 parts of maltitols, 0.2 part of Citric Acid Mono, 0.03 part of potassium sorbate, 0.2 part, Radix Glycyrrhizae, 0.08 part of vitamin C, after pulverizing, pulverizer after 100 mesh sieves, guarantees that granularity is less than 0.15mm;
(3) softwood step processed: slowly add the ethanol as wetting agent, mix, adjust raw material humidity, make softwood; Wherein, the mass concentration of ethanol is understood the mixing uniformity of remote-effects Icing Sugar, and then affects a surface flower point problem for tablet finished product, and preferably, concentration of alcohol is controlled at 30-50% and is advisable; In the present embodiment, the mass percentage concentration of ethanol is 40%.
(4) granulation step: gained softwood is crossed to 20 mesh sieves, dry 1-3 hour under 55 ℃ of conditions, dry terminal is: the soft durometer of softwood is pinched loose being advisable of energy agglomerating (feel is clear-cut, tack-free), light pressure with hand, and making its water content is 2-4%, after the whole grain of 40 mesh sieves;
(5) compressing tablet step: add the dolomol of percentage by weight 1% in particle, send into tablet press machine and carry out compressing tablet, make shaddock Fragrance Hill medicine buccal tablet.
embodiment 2
The process of this embodiment is substantially the same manner as Example 1, and its difference is:
1. prepare in debittering honey pomelo skin powder step, before sweet shaddock ped forming step, increase the step of cleaning and sterilizing: sweet shaddock fresh fruit automatically cleans 2 minutes in 45 ℃ of hot water, entering the cooling rinsing of clean water, is that in 100mg/L ClO 2 solution, normal temperature is sterilized and dries up in concentration.
2. the adjustment of formula allotment and technological parameter specifically refers to table 1, table 2.
embodiment 3
The process of this embodiment is substantially the same manner as Example 1, and the adjustment of formula allotment and technological parameter refers to table 1, table 2.
comparative example 1
By following step method, prepare persimmon buccal tablets.
(1) prepare persimmon thickened pulp: the persimmon of fresh maturation is really rinsed, drains rear rapid making beating, press persimmon slurry amount 1-3mL/kg and add pectase, 50-55 ℃ enzymolysis 90-150min, standing clarification 30-40min, filtration, 60-80 ℃ of evaporation and concentration to soluble solid content reaches 75% one-tenth persimmon thickened pulp;
(2) prepare traditional Chinese drug inspissation slurry: by weight 3:1:1:1:1 extracting honeysuckle, peppermint, the leaf of bamboo, Fermented Soybean and great burdock achene, cold water soak 40min, fried 50min, 80 ℃ of evaporations, by volume 6:1 is condensed into traditional Chinese drug inspissation slurry;
(3) in mass ratio by persimmon thickened pulp 35%, traditional Chinese drug inspissation slurry 16%, food starch 38%, sweet mellow wine 8%, sucrose 7% batching mixing, softwood processed, mix in sufficient softwood input granulator and carry out granulation, cross 20 mesh sieves, wet granular is put into drying box is dry, temperature is controlled at 40-50 ℃, pellet moisture is controlled at 3～5%;
(4) 1.5% dolomol added in above-mentioned dried particle, mix, particle is put into tablet press machine compressing tablet, moulding, makes persimmon buccal tablets.
comparative example 2
The process of this embodiment is substantially the same manner as Example 1, and the adjustment of formula allotment and technological parameter refers to table 1, table 2.
comparative example 3
The process of this embodiment is substantially the same manner as Example 1, and the adjustment of formula allotment and technological parameter refers to table 1, table 2.
comparative example 4
The process of this embodiment is substantially the same manner as Example 1, and the concrete adjustment of formula allotment and technological parameter refers to table 1, table 2.
The allotment of table 1 formula
| ? | Embodiment 1 | Embodiment 2 | Embodiment 3 | Comparative example 2 | Comparative example 3 | Comparative example 4 |
| Yam flour | 46 | 40 | 50 | 30 | 20 | 46 |
| Debittering honey pomelo skin powder | 8 | 7 | 9 | 10 | 8 | 8 |
| Maltodextrin | 20 | 22 | 18 | 20 | 40 | 30 |
| Xylitol | 16 | 18 | 14 | 5 | 10 | 25 |
| Maltitol | 10 | 9 | 11 | 20 | 15 | 10 |
| Citric Acid Mono | 0.2 | 0.3 | 0.4 | 2.2 | 0.2 | 0.2 |
| Radix Glycyrrhizae | 0.2 | 0.1 | 0.3 | 0.3 | 1 | 0.2 |
| Vitamin C | 0.08 | 0.06 | 0.1 | 0.08 | 0.08 | 0.08 |
| Potassium sorbate | 0.03 | 0.02 | 0.04 | 0.03 | 0.03 | 0.03 |
Table 2 technological parameter
Table 3 has provided the results of sensory evaluation of the Shi Ren group of the buccal tablet that embodiment 1 to 3 and comparative example 1 to 4 make; Table 4 has provided the performance indications of the buccal tablet that embodiment 1 to 3 and comparative example 1 to 4 make, wherein, naringin content adopts the assay method of the naringin content of the Fructus Aurantii in 2005 editions > > of < < Chinese pharmacopoeia, and hardness adopts tablet four-function analyzer to measure.
Table 3 Shi Ren group results of sensory evaluation
| ? | Embodiment 1 embodiment 2 | Embodiment 3 | Comparative example 1 | Comparative example 2 | Comparative example 3 | Comparative example 4 |
| Local flavor | The fragrant shaddock of shaddock is fragrant | Shaddock is fragrant | Persimmon local flavor | Shaddock is fragrant | Shaddock is fragrant | Shaddock is fragrant |
| Sour-sweet degree | Sour and sweet palatability sour and sweet palatability | Sour and sweet palatability | Partially sweet | Peracid | Cross sweet | Partially sweet |
| Mouthfeel | Delicate mouthfeel delicate mouthfeel | Delicate mouthfeel | Coarse mouthfeel | Coarse mouthfeel | Coarse mouthfeel | Delicate mouthfeel |
| Quality | Homogeneous | Homogeneous | Quality is uneven | Homogeneous | Quality is uneven | Quality is uneven |
| Surface flower point | Few, evenly few, evenly | Few, evenly | Many, inequality | Few, evenly | Many, irregular | Many, irregular |
| Disintegrative | Carefully | Good | Good | Poor | Better | Better |
Table 4 performance indications
| ? | Embodiment 1 | Embodiment 2 | Embodiment 3 | Comparative example 1 | Comparative example 2 | Comparative example 3 | Comparative example 4 |
| Naringin content | 0.19% | 0.21% | 0.20% | — | 0.18% | 0.19% | 0.46% |
| Hardness kg/20 sheet | 8.5 | 8.4 | 8.2 | 6.4 | 6.7 | 6.3 | 6.1 |
| Melting time/min | 19 | 18 | 19 | 10 | 14 | 11 | 11 |
Above disclosed is only the preferred embodiments of the present invention, certainly can not limit with this interest field of the present invention, and the equivalent variations of therefore doing according to the present patent application the scope of the claims, still belongs to the scope that the present invention is contained.
Claims (9)
1. a shaddock Fragrance Hill medicine buccal tablet, it is characterized in that: the component that comprises following weight portion: yam flour 40-50 part, debittering honey pomelo skin powder 7-9 part, maltodextrin 18-22 part, xylitol 14-18 part, maltitol 9-11 part, Citric Acid Mono 0.2-0.4 part, Radix Glycyrrhizae 0.1-0.3 part, vitamin C 0.06-0.1 part and potassium sorbate 0.02-0.04 part.
2. shaddock according to claim 1 Fragrance Hill medicine buccal tablet, is characterized in that: by following step, prepared:
A. prepare debittering honey pomelo skin powder;
B. the adaptation step of filling a prescription: the component raw material of following weight parts is mixed: yam flour 40-50 part, debittering honey pomelo skin powder 7-9 part, maltodextrin 18-22 part, xylitol 14-18 part, maltitol 9-11 part, Citric Acid Mono 0.2-0.4 part, potassium sorbate 0.02-0.04 part, Radix Glycyrrhizae 0.1-0.3 part, vitamin C 0.06-0.1 part;
C. softwood step processed: the formula material mixing is mixed with edible ethanol, make softwood;
D. granulation step: gained softwood is crossed to 16-24 mesh sieve and granulate, and dry at 45-65 ℃, make its moisture be less than 5%, carry out whole grain after 35-45 mesh sieve;
E. compressing tablet step: send into tablet press machine and carry out compressing tablet, make shaddock Fragrance Hill medicine buccal tablet.
3. shaddock according to claim 1 and 2 Fragrance Hill medicine buccal tablet, is characterized in that: described debittering honey pomelo skin powder is prepared by following step:
A1. sweet shaddock ped forming step: sweet shaddock fresh fruit is cut into lobe fresh fruit, and become the honey pomelo pericarp of lobe fresh fruit separated with sweet shaddock pulp, get honey pomelo pericarp and cut into the sweet shaddock fruit fourth of specification shape;
A2. sweet shaddock ped debitterize step: remove the bitter principle in sweet shaddock fruit fourth by debitterize liquid, sweet shaddock fruit fourth after debitterize is separated with debitterize liquid, and the composition components by weight percentage of wherein said debitterize liquid is: the water of sodium chloride 3.5-5.5%, cycloheptaamylose 0.3-0.4% and surplus;
A3. rinsing dehydration: after water cleans, then drying dehydration, obtain debittering honey pomelo skin;
A4. be ground into last step: debittering honey pomelo skin is pulverized in pulverizer, made debittering honey pomelo skin powder.
4. shaddock according to claim 3 Fragrance Hill medicine buccal tablet, is characterized in that: described sweet shaddock ped debitterize step is under the vacuum condition of 0.02MPa-0.15MPa, to carry out debitterize, and the debitterize time is 60-90 minute, and debitterize temperature is 50-80 ℃.
5. a method of preparing shaddock Fragrance Hill medicine buccal tablet, is characterized in that: comprise the following steps:
A. prepare debittering honey pomelo skin powder;
B. the adaptation step of filling a prescription: the component raw material of following weight parts is mixed: yam flour 40-50 part, debittering honey pomelo skin powder 7-9 part, maltodextrin 18-22 part, xylitol 14-18 part, maltitol 9-11 part, Citric Acid Mono 0.2-0.4 part, potassium sorbate 0.02-0.04 part, Radix Glycyrrhizae 0.1-0.3 part, vitamin C 0.06-0.1 part;
C. softwood step processed: the formula material mixing is mixed with edible ethanol, make softwood;
D. granulation step: gained softwood is crossed to 16-24 mesh sieve and granulate, and dry at 45-65 ℃, make its moisture be less than 5%, carry out whole grain after 35-45 mesh sieve;
E. compressing tablet step: send into tablet press machine and carry out compressing tablet, make shaddock Fragrance Hill medicine buccal tablet.
6. method according to claim 5, is characterized in that: the step of preparing debittering honey pomelo skin powder comprises:
A1. sweet shaddock ped forming step: sweet shaddock fresh fruit is cut into lobe fresh fruit, and become the honey pomelo pericarp of lobe fresh fruit separated with sweet shaddock pulp, get honey pomelo pericarp and cut into the sweet shaddock fruit fourth of specification shape;
A2. sweet shaddock ped debitterize step: remove the bitter principle in sweet shaddock fruit fourth by debitterize liquid, sweet shaddock fruit fourth after debitterize is separated with debitterize liquid, and the composition components by weight percentage of wherein said debitterize liquid is: the water of sodium chloride 3.5-5.5%, cycloheptaamylose 0.3-0.4% and surplus;
A3. rinsing dehydration: after water cleans, then drying dehydration, obtain debittering honey pomelo skin;
A4. be ground into last step: debittering honey pomelo skin is pulverized in pulverizer, made debittering honey pomelo skin powder.
7. according to the method described in claim 5 or 6, it is characterized in that: before described sweet shaddock ped forming step, increase cleaning and sterilizing step: adopt the aqueous solution of chlorine dioxide that concentration is 10-500mg/L to carry out cleaning and sterilizing to sweet shaddock fresh fruit.
8. method according to claim 6, is characterized in that: under the vacuum condition that described sweet shaddock ped debitterize step is is 0.02MPa-0.15MPa in vacuum, carry out debitterize, the debitterize time is 60-90 minute, and debitterize temperature is 50-80 ℃.
9. according to the method described in any one in claim 5 to 8, it is characterized in that: in described compressing tablet step, in the particle after granulation step, add the dolomol of percentage by weight 1-2%.
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| CN201310647126.3A CN103750204A (en) | 2013-12-05 | 2013-12-05 | Pomelo fragrance Chinese yam buccal tablet and preparation method thereof |
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| CN201310647126.3A CN103750204A (en) | 2013-12-05 | 2013-12-05 | Pomelo fragrance Chinese yam buccal tablet and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105341900A (en) * | 2015-06-29 | 2016-02-24 | 开平市水口镇卡摩商行 | Making method of Chinese yam and radish eight-treasure porridge |
| CN105495477A (en) * | 2015-12-09 | 2016-04-20 | 西南大学柑桔研究所 | Manufacturing method of spicy shaddock peel pickles |
| CN106418337A (en) * | 2016-12-12 | 2017-02-22 | 保龄宝生物股份有限公司 | Fruit and vegetable meal replacement tablets with cool and refresh mouthfeel |
| CN107412572A (en) * | 2017-09-28 | 2017-12-01 | 苟稳 | One kind, which is relaxed, swallows buccal tablet |
-
2013
- 2013-12-05 CN CN201310647126.3A patent/CN103750204A/en active Pending
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105341900A (en) * | 2015-06-29 | 2016-02-24 | 开平市水口镇卡摩商行 | Making method of Chinese yam and radish eight-treasure porridge |
| CN105495477A (en) * | 2015-12-09 | 2016-04-20 | 西南大学柑桔研究所 | Manufacturing method of spicy shaddock peel pickles |
| CN106418337A (en) * | 2016-12-12 | 2017-02-22 | 保龄宝生物股份有限公司 | Fruit and vegetable meal replacement tablets with cool and refresh mouthfeel |
| CN107412572A (en) * | 2017-09-28 | 2017-12-01 | 苟稳 | One kind, which is relaxed, swallows buccal tablet |
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