CN103720030B - A kind of tobacco juice for electronic smoke utilizing offal extract to prepare and preparation method thereof - Google Patents
A kind of tobacco juice for electronic smoke utilizing offal extract to prepare and preparation method thereof Download PDFInfo
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- CN103720030B CN103720030B CN201310677976.8A CN201310677976A CN103720030B CN 103720030 B CN103720030 B CN 103720030B CN 201310677976 A CN201310677976 A CN 201310677976A CN 103720030 B CN103720030 B CN 103720030B
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- offal
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Abstract
The present invention relates to a kind of tobacco juice for electronic smoke utilizing offal extract to prepare and preparation method thereof, this tobacco juice for electronic smoke is made by after following raw material blending: offal supercritical CO
2extract, tobacco maillard reaction product, natural nicotine, deionized water, glycerine and propane diols; Described offal supercritical CO
2the preparation method of extract is as follows: cigarette offal is placed in supercritical extraction unit and extracts, and extracting pressure is 20 ~ 30Mpa, and temperature is 35 DEG C ~ 45 DEG C, static extracting, and extraction time is that 3 ~ 4h obtains.The present invention is that the recycling of offal provides effective way, can reduce environmental pressure, improves utilization ratio of tobacco; Tobacco juice for electronic smoke of the present invention is with offal supercritical CO
2extract is main component, and containing essence spice for cigarette in extract, tobacco flavor composition etc., namely can save reinforced composition, also make electronic cigarette aesthetic quality and traditional cigarette more close.
Description
Technical field
The invention belongs to the technical field of electronic cigarette, specifically relate to a kind of tobacco juice for electronic smoke utilizing offal extract to prepare and preparation method thereof.
Background technology
In recent years, the sale of electronic cigarette has been in the gesture of significantly rising, in 2 years in the past, global electronic tobacco product sales volume has increased to 300,000,000 dollars, some analysts point out, between coming 10 years, the consumption of electronic cigarette likely can the consumption of beyond tradition tobacco product, and not good enough on the aesthetic quality of existing electronic cigarette after suction.Can produce a certain amount of offal discarded object at present in cigarette enterprise production process, the tobacco of these particle diameters tiny (being less than 0.3 millimeter) fails to be fully used, substantially discarded, both increases environmental pressure, also reduces utilization ratio of tobacco simultaneously.The relevant report utilizing offal supercritical CO_2 extraction thing to prepare tobacco juice for electronic smoke is there is not yet in prior art.
Summary of the invention
In order to solve above-mentioned technical problem, an object of the present invention is to provide a kind of tobacco juice for electronic smoke utilizing offal extract to prepare, the application of this tobacco juice can realize the recycling of offal discarded object, reduces the waste of resource.Another object of the present invention is to provide the preparation method of above-mentioned tobacco juice for electronic smoke.
In order to realize first above-mentioned object, present invention employs following technical scheme:
Utilize a tobacco juice for electronic smoke prepared by offal extract, this tobacco juice for electronic smoke is made by after the raw material blending of following mass percent:
Offal supercritical CO
2extract 20 ~ 25%
Tobacco maillard reaction product 5 ~ 10%
Natural nicotine 0.5 ~ 0.8%
Deionized water 3 ~ 5%
Glycerine 10 ~ 20%
All the other are propane diols;
Described offal supercritical CO
2the preparation method of extract is as follows: cigarette offal is placed in supercritical extraction unit and extracts, and extracting pressure is 20 ~ 30Mpa, and temperature is 35 DEG C ~ 45 DEG C, static extracting, and extraction time is that 3 ~ 4h obtains.
In order to realize second above-mentioned object, present invention employs following technical scheme:
Prepare a preparation method for above-mentioned tobacco juice for electronic smoke, the method comprises the following steps:
1) cigarette offal is placed in supercritical extraction unit to extract, extracting pressure is 20 ~ 30Mpa, and temperature is 35 DEG C ~ 45 DEG C, static extracting, and extraction time is that 3 ~ 4h obtains offal supercritical CO
2extract;
2) by offal supercritical CO
2extract 20 ~ 25%, tobacco maillard reaction product 5 ~ 10%, natural nicotine 0.5 ~ 0.8%, deionized water 3 ~ 5%, glycerine 10 ~ 20%, all the other are propane diols, make described tobacco juice for electronic smoke after mixing.
Relative to prior art, the present invention has following advantage:
1. the present invention is that the recycling of offal provides effective way, can reduce environmental pressure, improve utilization ratio of tobacco;
2. tobacco juice for electronic smoke of the present invention is with offal supercritical CO
2extract is main component, and containing essence spice for cigarette in extract, tobacco flavor composition etc., namely can save reinforced composition, also make electronic cigarette aesthetic quality and traditional cigarette more close;
3. tobacco juice for electronic smoke of the present invention, harmful components are few, can not produce the harm of second-hand-cigarette.
Detailed description of the invention
embodiment 1
A kind of offal supercritical CO_2 extraction thing preparation method: by 3.5kg cigarette offal, be placed in HA221-50-02 supercritical extraction unit and extract, extracting pressure is 25Mpa, temperature is 40 DEG C, static extracting extraction time is 3.5h, and gained offal extract is black paste, and yield is 3.5%.
One utilizes this extract to prepare tobacco juice for electronic smoke, and concrete mass ratio is: offal supercritical CO_2 extraction thing 25%, tobacco maillard reaction product 5%, natural nicotine 0.5%, deionized water 3%, glycerine 10%, and all the other are propane diols.Each raw material is mixed in proportion, mixes by vortex oscillator.
embodiment 2
A kind of offal supercritical CO_2 extraction thing preparation method: by 3.0kg cigarette offal, be placed in HA221-50-02 supercritical extraction unit and extract, extracting pressure is 20Mpa, temperature is 35 DEG C, static extracting extraction time is 4h, and gained offal extract is black paste, and yield is 4%.
One utilizes this extract to prepare tobacco juice for electronic smoke, and concrete mass ratio is: offal supercritical CO_2 extraction thing 20%, tobacco maillard reaction product 5%, natural nicotine 0.5%, deionized water 3%, glycerine 10%, and all the other are propane diols.Each raw material is mixed in proportion, mixes by vortex oscillator.
embodiment 3
A kind of offal supercritical CO_2 extraction thing preparation method: by 4.0kg cigarette offal, be placed in HA221-50-02 supercritical extraction unit and extract, extracting pressure is 30Mpa, temperature is 40 DEG C, static extracting extraction time is 3h, and gained offal extract is black paste, and yield is 5.5%.
One utilizes this extract to prepare tobacco juice for electronic smoke, and concrete mass ratio is: offal supercritical CO_2 extraction thing 20%, tobacco maillard reaction product 10%, natural nicotine 0.8%, deionized water 3%, glycerine 20%, and all the other are propane diols.Each raw material is mixed in proportion, mixes by vortex oscillator.
embodiment 4
A kind of offal supercritical CO_2 extraction thing preparation method: by 3.8kg cigarette offal, be placed in HA221-50-02 supercritical extraction unit and extract, extracting pressure is 27Mpa, temperature is 42 DEG C, static extracting extraction time is 3h, and gained offal extract is black paste, and yield is 4.5%.
One utilizes this extract to prepare tobacco juice for electronic smoke, and concrete mass ratio is: offal supercritical CO_2 extraction thing 22%, tobacco maillard reaction product 8%, natural nicotine 0.8%, deionized water 4%, glycerine 15%, and all the other are propane diols.Each raw material is mixed in proportion, mixes by vortex oscillator.
Electronic cigarette sensory quality assessment method:
According to GB5606.4-2005 Sensory Quality of Cigarette judgment criteria, in conjunction with electronic cigarette organoleptic features, 6 evaluation indexes and score value are set by different weight.Concrete meaning is in table 1.
Smoking result is added up: according to each expert's smoking result, try to achieve arithmetic mean of instantaneous value, result retains a position effective digital, and statistics is in table 2.
Claims (1)
1. the preparation method of a tobacco juice for electronic smoke, it is characterized in that the method comprises the following steps: 1) cigarette offal is placed in supercritical extraction unit extracts, extracting pressure is 27Mpa, and temperature is 42 DEG C, static extracting, extraction time is that 3h obtains offal supercritical CO
2extract, gained offal extract is black paste, and yield is 4.5%; 2) offal supercritical CO
2extract 22%, tobacco maillard reaction product 8%, natural nicotine 0.8%, deionized water 4%, glycerine 15%, all the other are propane diols, to be mixed in proportion by each raw material make electronic cigarette liquid by vortex oscillator.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310677976.8A CN103720030B (en) | 2013-12-13 | 2013-12-13 | A kind of tobacco juice for electronic smoke utilizing offal extract to prepare and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310677976.8A CN103720030B (en) | 2013-12-13 | 2013-12-13 | A kind of tobacco juice for electronic smoke utilizing offal extract to prepare and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103720030A CN103720030A (en) | 2014-04-16 |
| CN103720030B true CN103720030B (en) | 2015-08-05 |
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| CN201310677976.8A Active CN103720030B (en) | 2013-12-13 | 2013-12-13 | A kind of tobacco juice for electronic smoke utilizing offal extract to prepare and preparation method thereof |
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Families Citing this family (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103989244B (en) * | 2014-06-06 | 2016-10-05 | 山东中烟工业有限责任公司 | A kind of Chinese style tobacco juice for electronic smoke and preparation method thereof |
| CN104000302B (en) * | 2014-06-17 | 2017-09-22 | 云南中烟工业有限责任公司 | A kind of tobacco juice for electronic smoke and its quality determining method |
| CN104450186B (en) * | 2014-10-29 | 2017-04-19 | 山东中烟工业有限责任公司 | Method for preparing tobacco herbal fragrant substance for cigarette solution of electronic cigarette |
| CN104585865B (en) * | 2015-01-20 | 2016-02-03 | 川渝中烟工业有限责任公司 | A kind of tobacco juice for electronic smoke containing tobacco extract and preparation method thereof |
| CN104818117B (en) * | 2015-03-31 | 2019-01-15 | 四川中烟工业有限责任公司 | Utilize the cigarette wooden fork essential oil of tobacco waste preparation and its application and preparation method |
| CN105011354A (en) * | 2015-05-06 | 2015-11-04 | 济南九州富得香料有限责任公司 | Method for supercritical CO2 extraction of upper-tobacco leaves of tobaccos, extract and application |
| CN106418660B (en) * | 2015-08-13 | 2020-03-24 | 上海烟草集团有限责任公司 | Preparation method and application of electronic cigarette liquid |
| CN105199850B (en) * | 2015-10-16 | 2019-07-09 | 华宝香精股份有限公司 | A kind of preparation method and applications of tobacco aromaticss |
| CN105310103B (en) * | 2015-11-04 | 2017-10-24 | 深圳瀚星翔科技有限公司 | A kind of electronic cigarette tobacco tar and preparation method thereof |
| CN106551420A (en) * | 2017-01-23 | 2017-04-05 | 江苏中烟工业有限责任公司 | A kind of method that application cabo prepares tobacco juice for electronic smoke |
| GB201707758D0 (en) | 2017-05-15 | 2017-06-28 | British American Tobacco Investments Ltd | Ground tobacco composition |
| CN110122919B (en) * | 2018-02-02 | 2023-04-21 | 10150703加拿大有限公司 | Nicotine ion pair formulations neutralized with carbon dioxide and methods thereof |
| CN110338451B (en) * | 2018-04-04 | 2022-12-02 | 中国农业科学院烟草研究所 | Preparation method of electronic cigarette liquid |
| US11690396B2 (en) | 2018-10-24 | 2023-07-04 | Zanoprima Lifesciences Limited | Electronic cigarette compositions, devices, and related methods |
| AU2019365396B2 (en) * | 2018-10-24 | 2022-02-03 | Zanoprima Lifesciences Limited | Composition |
-
2013
- 2013-12-13 CN CN201310677976.8A patent/CN103720030B/en active Active
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| CN103720030A (en) | 2014-04-16 |
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