CN103719267A - Preparation method of novel edible film-coated fruit and vegetable fresh-keeping agent - Google Patents
Preparation method of novel edible film-coated fruit and vegetable fresh-keeping agent Download PDFInfo
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- CN103719267A CN103719267A CN201310710861.4A CN201310710861A CN103719267A CN 103719267 A CN103719267 A CN 103719267A CN 201310710861 A CN201310710861 A CN 201310710861A CN 103719267 A CN103719267 A CN 103719267A
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- 235000012055 fruits and vegetables Nutrition 0.000 title claims abstract description 32
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 30
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 20
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 20
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 13
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims abstract description 10
- 239000008103 glucose Substances 0.000 claims abstract description 10
- NCXMLFZGDNKEPB-FFPOYIOWSA-N natamycin Chemical compound O[C@H]1[C@@H](N)[C@H](O)[C@@H](C)O[C@H]1O[C@H]1/C=C/C=C/C=C/C=C/C[C@@H](C)OC(=O)/C=C/[C@H]2O[C@@H]2C[C@H](O)C[C@](O)(C[C@H](O)[C@H]2C(O)=O)O[C@H]2C1 NCXMLFZGDNKEPB-FFPOYIOWSA-N 0.000 claims abstract description 10
- 229960003255 natamycin Drugs 0.000 claims abstract description 10
- 235000010298 natamycin Nutrition 0.000 claims abstract description 10
- 239000004311 natamycin Substances 0.000 claims abstract description 10
- 235000010987 pectin Nutrition 0.000 claims abstract description 10
- 229920001277 pectin Polymers 0.000 claims abstract description 10
- 239000001814 pectin Substances 0.000 claims abstract description 10
- 150000008442 polyphenolic compounds Chemical class 0.000 claims abstract description 10
- 235000013824 polyphenols Nutrition 0.000 claims abstract description 10
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 10
- 239000011734 sodium Substances 0.000 claims abstract description 10
- 239000003755 preservative agent Substances 0.000 claims description 10
- 230000002335 preservative effect Effects 0.000 claims description 10
- 229920002134 Carboxymethyl cellulose Polymers 0.000 claims description 9
- 235000010948 carboxy methyl cellulose Nutrition 0.000 claims description 9
- 229920006184 cellulose methylcellulose Polymers 0.000 claims description 9
- 238000012710 chemistry, manufacturing and control Methods 0.000 claims description 9
- 239000007888 film coating Substances 0.000 claims description 7
- 238000009501 film coating Methods 0.000 claims description 7
- 239000012153 distilled water Substances 0.000 claims description 5
- 239000011153 ceramic matrix composite Substances 0.000 claims description 2
- 231100000252 nontoxic Toxicity 0.000 abstract description 7
- 230000003000 nontoxic effect Effects 0.000 abstract description 7
- 230000001954 sterilising effect Effects 0.000 abstract description 4
- 238000004659 sterilization and disinfection Methods 0.000 abstract description 3
- 229920001661 Chitosan Polymers 0.000 abstract description 2
- 125000002057 carboxymethyl group Chemical group [H]OC(=O)C([H])([H])[*] 0.000 abstract description 2
- 239000010408 film Substances 0.000 abstract 2
- 241001122767 Theaceae Species 0.000 abstract 1
- 235000019441 ethanol Nutrition 0.000 abstract 1
- 230000003020 moisturizing effect Effects 0.000 abstract 1
- 230000003647 oxidation Effects 0.000 abstract 1
- 238000007254 oxidation reaction Methods 0.000 abstract 1
- 230000002265 prevention Effects 0.000 abstract 1
- 239000010409 thin film Substances 0.000 abstract 1
- 238000005303 weighing Methods 0.000 abstract 1
- 238000000034 method Methods 0.000 description 6
- 230000000844 anti-bacterial effect Effects 0.000 description 5
- 235000013399 edible fruits Nutrition 0.000 description 4
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000013043 chemical agent Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 238000004320 controlled atmosphere Methods 0.000 description 1
- 230000002079 cooperative effect Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 235000011187 glycerol Nutrition 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 description 1
- 229920000053 polysorbate 80 Polymers 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000000241 respiratory effect Effects 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 230000005068 transpiration Effects 0.000 description 1
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- Storage Of Fruits Or Vegetables (AREA)
Abstract
The invention discloses a preparation method of a novel edible film-coated fruit and vegetable fresh-keeping agent. The preparation method comprises the following steps: respectively weighing 10-18 parts of pectin, 8-15 parts of glucose, 3-8 parts of tea polyphenol, 5-15 parts of carboxymethyl chitosan, 3-8 parts of Vc-sodium, 0.5-2 parts of natamycin, 3-8 parts of citric acid and 10-20 parts of ethyl alcohol according to the formula, and dissolving the components in matching amount of water at 30-50 DEG C to prepare the edible film-coated fruit and vegetable fresh-keeping agent. The fresh-keeping system prepared by the preparation method disclosed by the invention is aqueous, easy to store, safe and nontoxic, forms a very thin film on the surfaces of fruits and vegetables, has the advantages of good broad-spectrum bacteriostasis and sterilization properties, oxidation resistance, browning prevention, long fresh-keeping period and good moisturizing agent and is edible and nontoxic.
Description
technical field:
The present invention relates to a kind of fruit and vegetable fresh-keeping agent, particularly a kind of preparation method of novel feeding habits coated preservative for fruits and vegetables.
background technology:
Fruit and vegetable is the indispensable living materials of the mankind, but the production of fruits and vegetables has very strong seasonality and region, and physiologically active is high, water content is large, springy texture, perishablely mildews, freshness declines, and brings very large difficulty therefore to the fresh-keeping of fruits and vegetables and circulation.Postharvest technology of fruits and vegetables has at present: low temperature controlled atmosphere method, and this method is expensive; Inner wrapping is fresh-keeping, and it is slow that oxygen speed falls in this method, and fresh-keeping effect is poor; Chemical preservative method, due to have toxic and side effect chemical agent residual, not easy cleaning remove affect health, therefore, safety, nontoxic, the exploitation of natural fruit and vegetable fresh-keeping agent, application prospect is very extensive.CN02157908.3 discloses a kind of antibrown type fruits and vegetables and has been coated with by antistaling agent and preparation method thereof, and the antibacterial sterilizing ability of the made antistaling agent of this method is poor.CN2007100515.6 discloses a kind of browning preventing broad spectrum fruit preservative, the lock water poor-performing of the prepared antistaling agent of this method to fruit, and fruit dehydration is high.CN200710045893.1 discloses carboxymethyl chitosan fruit preserving coating agent and preparation method thereof, and the uses such as this antistaling agent needed raw material glycerine, Tween 80 have certain standard, can not exceed standard edible.
summary of the invention:
Goal of the invention: for the defect of prior art, provide a kind of safe, nontoxic, nuisanceless, built agent cooperative effect is good, broad-spectrum antibacterial sterilization, the anti-soft rotten performance of anti-brown stain is good, the preparation method of edible natural film composite antistaling agent for fruits and vegetables with low cost.
To achieve the object of the present invention, a kind of preparation method of novel feeding habits coated preservative for fruits and vegetables, takes following technical formula:
Title weight portion
10~18 parts of pectin
8~15 parts of glucose
3~8 parts of Tea Polyphenols
5~15 parts of CMCs
Vc-sodium 3~8
Natamycin 0.5~2
Citric acid 3~8
10~20 parts of ethanol
900~960 parts, water
The preparation method of described a kind of novel feeding habits coated preservative for fruits and vegetables, take respectively pectin, glucose, Tea Polyphenols, CMC, Vc-sodium, natamycin, citric acid, ethanol, at 30~50 ℃, be dissolved in the water of proportional quantity, make edible film-coating fruit and vegetable fresh-keeping agent.
The preparation method of described a kind of novel feeding habits coated preservative for fruits and vegetables, take respectively pectin 15g, glucose 12g, Tea Polyphenols 4g, CMC 12g, Vc-sodium 5g, natamycin 1g, citric acid 5g, ethanol 18g, at 30~40 ℃, be dissolved in 946g distilled water, make edible film-coating fruit and vegetable fresh-keeping agent.
Beneficial effect of the present invention: system is water-based, is easy to store, safety non-toxic, and it is good that the film that antistaling agent of the present invention forms at fruit and vegetable surfaces has broad-spectrum antibacterial bactericidal property, the anti-brown stain of antioxygen, long fresh-keeping period, moisture-keeping efficacy is good and edible nontoxic.
the specific embodiment:
Below in conjunction with embodiment, the present invention is done further and described in detail, but the scope of protection of present invention is not limited to the scope that embodiment represents.
Embodiment 1:
Take respectively pectin 15g, glucose 12g, Tea Polyphenols 4g, CMC 12g, Vc-sodium 5g, natamycin 1g, citric acid 5g, ethanol 18g, at 30~40 ℃, is dissolved in 946g distilled water, makes edible film-coating fruit and vegetable fresh-keeping agent.
Use this antistaling agent to spray or to soak mode processing fruits and vegetables, form film layer as thin as a wafer, effectively reduce respiratory intensity and the transpiration of fruits and vegetables, prevent brown stain, broad-spectrum antibacterial sterilization, thereby the freshness of maintenance fruits and vegetables, extend the shelf-life of fruits and vegetables, this product is edible nontoxic.
Embodiment 2:
Take respectively pectin 12g, glucose 15g, Tea Polyphenols 6g, CMC 10g, Vc-sodium 4g, natamycin 1g, citric acid 4g, ethanol 15g, at 30~40 ℃, is dissolved in 930g distilled water, makes edible film-coating fruit and vegetable fresh-keeping agent.
Embodiment 3:
Take respectively pectin 10g, glucose 10g, Tea Polyphenols 8g, CMC 15g, Vc-sodium 8g, natamycin 1g, citric acid 4g, ethanol 15g, at 30~40 ℃, is dissolved in 930g distilled water, makes edible film-coating fruit and vegetable fresh-keeping agent.
Claims (3)
1. a preparation method for novel feeding habits coated preservative for fruits and vegetables, is characterized in that, takes following technical formula:
Title weight portion
10~18 parts of pectin
8~15 parts of glucose
3~8 parts of Tea Polyphenols
5~15 parts of CMCs
Vc-sodium 3~8
Natamycin 0.5~2
Citric acid 3~8
10~20 parts of ethanol
900~960 parts, water.
2. the preparation method of novel feeding habits coated preservative for fruits and vegetables according to claim 1, it is characterized in that, take respectively pectin, glucose, Tea Polyphenols, CMC, Vc-sodium, natamycin, citric acid, ethanol, at 30~50 ℃, be dissolved in the water of proportional quantity, make edible film-coating fruit and vegetable fresh-keeping agent.
3. the preparation method of novel feeding habits coated preservative for fruits and vegetables according to claim 1, is characterized in that, takes respectively pectin 15g, glucose 12g, Tea Polyphenols 4g, CMC 12g, Vc-sodium 5g, natamycin 1g, citric acid 5g, ethanol 18g, at 30~40 ℃, be dissolved in 946g distilled water, make edible film-coating fruit and vegetable fresh-keeping agent.
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CN201310710861.4A CN103719267A (en) | 2013-12-23 | 2013-12-23 | Preparation method of novel edible film-coated fruit and vegetable fresh-keeping agent |
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CN201310710861.4A CN103719267A (en) | 2013-12-23 | 2013-12-23 | Preparation method of novel edible film-coated fruit and vegetable fresh-keeping agent |
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CN201310710861.4A Pending CN103719267A (en) | 2013-12-23 | 2013-12-23 | Preparation method of novel edible film-coated fruit and vegetable fresh-keeping agent |
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Cited By (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104430836A (en) * | 2014-12-24 | 2015-03-25 | 镇江市官塘生态农业有限公司 | Strawberry preservative and preparation method thereof |
CN104642533A (en) * | 2014-06-24 | 2015-05-27 | 何松 | Fruit and vegetable coating preservative and preparation method thereof |
CN104642532A (en) * | 2014-06-24 | 2015-05-27 | 何松 | Preservation method of litchi |
ES2550219A1 (en) * | 2015-09-21 | 2015-11-05 | Tabuenca, S.A. | Composition of an edible coating for the preservation of fruits and vegetables, its preparation process and way of application on fruits and vegetables (Machine-translation by Google Translate, not legally binding) |
CN105794962A (en) * | 2016-04-14 | 2016-07-27 | 华中农业大学 | Fresh-cut fruit and vegetable color-protecting and freshness-retaining method |
CN104286156B (en) * | 2014-10-21 | 2017-07-04 | 华蒙通物流控股(集团)有限公司 | A kind of tomato film composite preservative and preparation method thereof |
CN107047749A (en) * | 2017-06-08 | 2017-08-18 | 合肥慧明瀚生态农业科技有限公司 | A kind of environmental protection fruit and vegetable fresh-keeping agent and preparation method thereof |
CN107279278A (en) * | 2017-08-25 | 2017-10-24 | 太仓优活生物技术有限公司 | A kind of natural fruit and vegetables preservative |
CN108497389A (en) * | 2018-04-11 | 2018-09-07 | 安徽省义门苔干有限公司 | A kind of processing method of puffing dried lactuca |
CN108813668A (en) * | 2018-06-27 | 2018-11-16 | 广东天运乐享大健康生物科技有限公司 | A kind of residual device of lichee fresh fruit drop agriculture and operating method |
CN111264611A (en) * | 2020-02-26 | 2020-06-12 | 贵州省亚热带作物研究所 | Dual fresh-keeping method for sterilization before picking and antisepsis after picking of oil pears |
CN111742980A (en) * | 2020-07-23 | 2020-10-09 | 武汉轻工大学 | A kind of biofilm inhibitor and its preparation method and application |
CN113261585A (en) * | 2021-06-08 | 2021-08-17 | 浙江海洋大学 | Method for prolonging shelf life of chilled fresh water product |
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CN101189981A (en) * | 2006-11-28 | 2008-06-04 | 国家农产品保鲜工程技术研究中心(天津) | Composite antistaling agent for fruits and vegetables |
CN102388957A (en) * | 2011-11-21 | 2012-03-28 | 广西壮族自治区农业科学院农产品加工研究所 | Lichee natural coating antistaling agent and its preparation method |
CN103300142A (en) * | 2013-05-08 | 2013-09-18 | 南京年吉冷冻食品有限公司 | Method for preparing tender and fresh keeping agent of green corn |
CN103444862A (en) * | 2013-05-08 | 2013-12-18 | 南京年吉冷冻食品有限公司 | Preparation method of preservative for water rice |
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2013
- 2013-12-23 CN CN201310710861.4A patent/CN103719267A/en active Pending
Patent Citations (4)
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CN101189981A (en) * | 2006-11-28 | 2008-06-04 | 国家农产品保鲜工程技术研究中心(天津) | Composite antistaling agent for fruits and vegetables |
CN102388957A (en) * | 2011-11-21 | 2012-03-28 | 广西壮族自治区农业科学院农产品加工研究所 | Lichee natural coating antistaling agent and its preparation method |
CN103300142A (en) * | 2013-05-08 | 2013-09-18 | 南京年吉冷冻食品有限公司 | Method for preparing tender and fresh keeping agent of green corn |
CN103444862A (en) * | 2013-05-08 | 2013-12-18 | 南京年吉冷冻食品有限公司 | Preparation method of preservative for water rice |
Cited By (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104642533A (en) * | 2014-06-24 | 2015-05-27 | 何松 | Fruit and vegetable coating preservative and preparation method thereof |
CN104642532A (en) * | 2014-06-24 | 2015-05-27 | 何松 | Preservation method of litchi |
CN104286156B (en) * | 2014-10-21 | 2017-07-04 | 华蒙通物流控股(集团)有限公司 | A kind of tomato film composite preservative and preparation method thereof |
CN104430836A (en) * | 2014-12-24 | 2015-03-25 | 镇江市官塘生态农业有限公司 | Strawberry preservative and preparation method thereof |
ES2550219A1 (en) * | 2015-09-21 | 2015-11-05 | Tabuenca, S.A. | Composition of an edible coating for the preservation of fruits and vegetables, its preparation process and way of application on fruits and vegetables (Machine-translation by Google Translate, not legally binding) |
CN105794962A (en) * | 2016-04-14 | 2016-07-27 | 华中农业大学 | Fresh-cut fruit and vegetable color-protecting and freshness-retaining method |
CN107047749A (en) * | 2017-06-08 | 2017-08-18 | 合肥慧明瀚生态农业科技有限公司 | A kind of environmental protection fruit and vegetable fresh-keeping agent and preparation method thereof |
CN107279278A (en) * | 2017-08-25 | 2017-10-24 | 太仓优活生物技术有限公司 | A kind of natural fruit and vegetables preservative |
CN108497389A (en) * | 2018-04-11 | 2018-09-07 | 安徽省义门苔干有限公司 | A kind of processing method of puffing dried lactuca |
CN108813668A (en) * | 2018-06-27 | 2018-11-16 | 广东天运乐享大健康生物科技有限公司 | A kind of residual device of lichee fresh fruit drop agriculture and operating method |
CN111264611A (en) * | 2020-02-26 | 2020-06-12 | 贵州省亚热带作物研究所 | Dual fresh-keeping method for sterilization before picking and antisepsis after picking of oil pears |
CN111742980A (en) * | 2020-07-23 | 2020-10-09 | 武汉轻工大学 | A kind of biofilm inhibitor and its preparation method and application |
CN113261585A (en) * | 2021-06-08 | 2021-08-17 | 浙江海洋大学 | Method for prolonging shelf life of chilled fresh water product |
WO2022257244A1 (en) * | 2021-06-08 | 2022-12-15 | 浙江海洋大学 | Method for prolonging shelf life of chilled aquatic products |
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Application publication date: 20140416 |