CN103704251A - Chlorfenapyr-containing missible oil and its application - Google Patents
Chlorfenapyr-containing missible oil and its application Download PDFInfo
- Publication number
- CN103704251A CN103704251A CN201310670227.2A CN201310670227A CN103704251A CN 103704251 A CN103704251 A CN 103704251A CN 201310670227 A CN201310670227 A CN 201310670227A CN 103704251 A CN103704251 A CN 103704251A
- Authority
- CN
- China
- Prior art keywords
- chlorfenapyr
- methidathion
- missible oil
- application
- isooctanol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- CWFOCCVIPCEQCK-UHFFFAOYSA-N chlorfenapyr Chemical compound BrC1=C(C(F)(F)F)N(COCC)C(C=2C=CC(Cl)=CC=2)=C1C#N CWFOCCVIPCEQCK-UHFFFAOYSA-N 0.000 title claims abstract description 61
- MEBQXILRKZHVCX-UHFFFAOYSA-N methidathion Chemical compound COC1=NN(CSP(=S)(OC)OC)C(=O)S1 MEBQXILRKZHVCX-UHFFFAOYSA-N 0.000 claims abstract description 41
- 241001414720 Cicadellidae Species 0.000 claims abstract description 10
- 241001122767 Theaceae Species 0.000 claims abstract description 10
- BWDBEAQIHAEVLV-UHFFFAOYSA-N 6-methylheptan-1-ol Chemical compound CC(C)CCCCCO BWDBEAQIHAEVLV-UHFFFAOYSA-N 0.000 claims description 9
- 210000000481 breast Anatomy 0.000 claims description 9
- 239000003350 kerosene Substances 0.000 claims description 9
- 239000004480 active ingredient Substances 0.000 claims description 5
- 241000594033 Liriomyza bryoniae Species 0.000 claims description 3
- 230000002195 synergetic effect Effects 0.000 abstract description 6
- 230000000694 effects Effects 0.000 abstract description 5
- 239000000575 pesticide Substances 0.000 abstract description 2
- 238000013329 compounding Methods 0.000 abstract 1
- 230000002265 prevention Effects 0.000 abstract 1
- 239000003814 drug Substances 0.000 description 12
- 239000000203 mixture Substances 0.000 description 8
- 239000012895 dilution Substances 0.000 description 6
- 238000010790 dilution Methods 0.000 description 6
- 239000002917 insecticide Substances 0.000 description 6
- 238000000034 method Methods 0.000 description 5
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 4
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 4
- 241000607479 Yersinia pestis Species 0.000 description 4
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 238000007796 conventional method Methods 0.000 description 3
- 238000002360 preparation method Methods 0.000 description 3
- 238000005507 spraying Methods 0.000 description 3
- 239000000375 suspending agent Substances 0.000 description 3
- 231100000419 toxicity Toxicity 0.000 description 3
- 230000001988 toxicity Effects 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 230000000895 acaricidal effect Effects 0.000 description 2
- 239000003905 agrochemical Substances 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 239000002131 composite material Substances 0.000 description 2
- JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 230000000749 insecticidal effect Effects 0.000 description 2
- 239000002574 poison Substances 0.000 description 2
- 231100000614 poison Toxicity 0.000 description 2
- 238000001228 spectrum Methods 0.000 description 2
- 210000002784 stomach Anatomy 0.000 description 2
- 230000009885 systemic effect Effects 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 241001124076 Aphididae Species 0.000 description 1
- XZMCDFZZKTWFGF-UHFFFAOYSA-N Cyanamide Chemical compound NC#N XZMCDFZZKTWFGF-UHFFFAOYSA-N 0.000 description 1
- IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 description 1
- 241000258937 Hemiptera Species 0.000 description 1
- 241000238631 Hexapoda Species 0.000 description 1
- 206010034133 Pathogen resistance Diseases 0.000 description 1
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000000642 acaricide Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000001055 chewing effect Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000006071 cream Substances 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 229960001760 dimethyl sulfoxide Drugs 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 125000000623 heterocyclic group Chemical group 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 231100000053 low toxicity Toxicity 0.000 description 1
- 230000010534 mechanism of action Effects 0.000 description 1
- 230000001069 nematicidal effect Effects 0.000 description 1
- 239000005645 nematicide Substances 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 230000003449 preventive effect Effects 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 231100000820 toxicity test Toxicity 0.000 description 1
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention belongs to the technical field of pesticide compounding, and concretely relates to a chlorfenapyr-containing missible oil and its application. The effective components of the chlorfenapyr-containing missible oil comprise chlorfenapyr and methidathion, wherein a weight ratio of methidathion to chlorfenapyr is 20:1-1:1. The chlorfenapyr-containing missible oil has a good prevention and control effect especially on tea lesser leafhopper under the synergistic effect of the above components.
Description
Technical field
The invention belongs to the composite technical field of agricultural chemical insecticide, be specially a kind of missible oil that contains chlorfenapyr and application.
Background technology
Methidathion
One of English name is Methidathion, CAS 950-37-8, molecular formula C
6h
11n
2o
4pS
3, molecular weight 302.3313.
Sterling is colourless crystallization.Relative density 1.495 (20 ℃), in the time of 20 ℃, solvability is: cyclohexanone 850g/kg, acetone 690g/kg, dimethylbenzene 600g/kg, ethanol 260g/kg, water 250mg/kg.
Have and tag and stomach poison function; There is osmosis, but without systemic action; Wide spectrum, high malicious Insecticidal and acaricidal agent, be a kind of comparatively ideal scale insect medicament that kills, and can doublely control mite class, aleyrodid, aphid.
But its action effect is also very single, after large-scale application, resistance risk is also very high.
Chlorfenapyr
English name Chlorfenapyr, a kind of new type heterocycle class desinsection that Shi You American Cyanamid Company succeeds in developing, kills mite, nematocide.Along with the appearance of national replace of hypertoxic insecticides policy and the raising of people's environmental consciousness, as non-polluted farm product diseases and pests controlling recommend the representative of pesticide species, the application of the efficient chlorfenapyr of low toxicity is more and more extensive.
No. CAS: 122453-73-0
Molecular formula: C
15h
11brClF
3n
2o
Molecular weight: 437.2
Physical behavior: white crystals
Molecular weight: 407.62
Proterties: sterling is white or off-white color oiliness powder
Fusing point: 100～101 ℃
Dissolubility: be dissolved in acetone, ether, methyl-sulfoxide, oxolane, acetonitrile, the organic solvents such as alcohol, toluene, dimethylbenzene, water insoluble.
Acidity of Aikalinity: neutrality, pH6～8
Content: 98.00-99.50%
The pyroles Insecticidal and acaricidal agent of structure novel, has good preventive effect to boring moth, thorn suction and chewing type insect and mite class.This medicament has following characteristics: broad spectrum insecticide, miticide; Have stomach toxicity and action of contace poison concurrently; With other insecticides without cross resistance; On crop, there is medium residual activity; In nutrient solution through the selective systemic activity of Root Absorption; It is high that this class has selectivity, and the mechanism of action is unique, and toxicity is low waits good characteristic, but its action effect is also very single, and after large-scale application, resistance risk is also very high.
Summary of the invention
The object of the present invention is to provide a kind of missible oil that contains chlorfenapyr and application, active ingredient is chlorfenapyr and methidathion, wherein the weight ratio of chlorfenapyr and methidathion is, methidathion: chlorfenapyr=10:1-1:10, especially good to control tea lesser leafhopper, be mainly by the result of the synergistic function between each component.
Technical scheme of the present invention is:
A missible oil that contains chlorfenapyr, active ingredient is chlorfenapyr and methidathion, wherein the weight ratio of chlorfenapyr and methidathion is, methidathion: chlorfenapyr=10:1-1:10.
As preferably, the weight ratio of chlorfenapyr and methidathion is, methidathion: chlorfenapyr=5:1-1:1.
The missible oil that contains chlorfenapyr of the present invention, it consists of following component by weight percentage:
Methidathion 1-50%,
Chlorfenapyr 1-50%,
Agriculture breast 500#15-40%,
Isooctanol 10-25%,
Kerosene 5-25%.
As preferably, the missible oil that contains chlorfenapyr of the present invention, it consists of following component by weight percentage:
Methidathion 10-50%,
Chlorfenapyr 5-10%,
Agriculture breast 500#15-40%,
Isooctanol 10-25%,
Kerosene 5-25%.
Wherein, the total weight percentage of described active ingredient is 30～60%.
As further preferred, the missible oil that contains chlorfenapyr of the present invention, it consists of following component by weight percentage:
Methidathion 50%,
Chlorfenapyr 10%,
Agriculture breast 500#20%
Isooctanol 10%
Kerosene 10%.
The missible oil that contains chlorfenapyr of the present invention, for preventing and treating liriomyza bryoniae, large trypetid, tea lesser leafhopper, is particularly useful for preventing and treating tea lesser leafhopper.
Beneficial effect of the present invention is:
Said composition is compounded cream composition, compare with single product, the feature with binary composition, strengthened significantly effect, delay the generation of pest resistance to insecticide, and expanded effective active control spectrum, and thering is speed fast, the lasting period is long, consumption is low, eco-friendly feature, the more important thing is, this compounded combination has effectively resisted the problem that pest resistance produces, farthest alleviated the problem of current pest resistance to insecticide, thereby reduced the consumption of agricultural chemicals, also alleviated the impact for environment, met the trend of future society environmental protection.The control efficiency of composition of the present invention is especially good to control tea lesser leafhopper, is mainly by the result of the synergistic function between each component.
To the compound synergic research of composition of the present invention, test adopts tea lesser leafhopper for test.
Concrete grammar is: according to the abundant method of Sun Yun, calculate the toxicity index of medicament and mixed co-toxicity coefficient (CTC value).
The toxicity test result of the different proportion relations of table 1 to tea lesser leafhopper
| Process | Co-toxicity coefficient |
| Methidathion 10: chlorfenapyr 1 | 135.7 |
| Methidathion 5: chlorfenapyr 1 | 207.5 |
| Methidathion 1: chlorfenapyr 1 | 210.3 |
| Methidathion 1: chlorfenapyr 5 | 134.2 |
| Methidathion 1: chlorfenapyr 10 | 121.9 |
| Chlorfenapyr | ? |
| Methidathion | ? |
As can be seen from Table 1, chlorfenapyr and methidathion composite, has very high synergistic effect, especially methidathion: during chlorfenapyr=5:1-1:1, synergistic effect is more obvious.
Embodiment
Below by specific embodiment, technical scheme of the present invention is described in detail.
Embodiment 1
The composition of 60% chlorfenapyr and methidathion
Methidathion 50%,
Chlorfenapyr 10%,
Agriculture breast 500#20%
Isooctanol 10%
Kerosene 10%.
Preparation method is the conventional method of this area.
This embodiment medicament is applied to prevent and treat tea lesser leafhopper:
Co-toxicity coefficient is: 208.5;
By the spraying of 6000 times of thin ups, after medicine, 7 days control efficiency are 5000 times of 99.2%, 10% 600 times of chlorfenapyr suspending agent dilutions and the dilutions of 50% methidathion missible oil, and respectively with same method use, after medicine 7 days, control efficiency was respectively 67.5% and 73.9%, significant difference.
Embodiment 2
The composition of 30% chlorfenapyr and methidathion
Chlorfenapyr 5%,
Methidathion 25%,
Agriculture breast 500#30%
Isooctanol 20%
Kerosene 20%.
Preparation method is the conventional method of this area.
This embodiment medicament is applied to prevent and treat liriomyza bryoniae:
Co-toxicity coefficient is: 205.4;
By the spraying of 3000 times of thin ups, after medicine, 7 days control efficiency are 2000 times of 98.2%, 5% 300 times of chlorfenapyr suspending agent dilutions and the dilutions of 25% methidathion missible oil, and respectively with same method use, after medicine 7 days, control efficiency was respectively 66.2% and 68.7%, significant difference.
Embodiment 3
The composition of 32% chlorfenapyr and methidathion
Chlorfenapyr 8%,
Methidathion 24%,
Agriculture breast 500#35%
Isooctanol 15%
Kerosene 18%.
Preparation method is the conventional method of this area.
This embodiment medicament is applied to prevent and treat large trypetid:
Co-toxicity coefficient is: 209.4;
By the spraying of 3000 times of thin ups, after medicine, 7 days control efficiency are 2000 times of 99.3%, 8% 300 times of chlorfenapyr suspending agent dilutions and the dilutions of 24% methidathion missible oil, and respectively with same method use, after medicine 7 days, control efficiency was respectively 72.4% and 64.3%, significant difference.
Claims (7)
1. a missible oil that contains chlorfenapyr, active ingredient is chlorfenapyr and methidathion, wherein the weight ratio of chlorfenapyr and methidathion is, methidathion: chlorfenapyr=10:1-1:10.
2. the missible oil that contains chlorfenapyr according to claim 1, is characterized in that, the weight ratio of chlorfenapyr and methidathion is, methidathion: chlorfenapyr=5:1-1:1.
3. the missible oil that contains chlorfenapyr according to claim 1 and 2, is characterized in that, it consists of following component by weight percentage:
Methidathion 1-50%,
Chlorfenapyr 1-50%,
Agriculture breast 500# 15-40%,
Isooctanol 10-25%,
Kerosene 5-25%.
4. the missible oil that contains chlorfenapyr according to claim 3, is characterized in that, it consists of following component by weight percentage:
Methidathion 10-50%,
Chlorfenapyr 5-10%,
Agriculture breast 500# 15-40%,
Isooctanol 10-25%,
Kerosene 5-25%.
5. according to the missible oil that contains chlorfenapyr described in the arbitrary claim of claim 1-4, it is characterized in that, the total weight percentage of described active ingredient is 30～60%.
6. the missible oil that contains chlorfenapyr according to claim 5, is characterized in that, it consists of following component by weight percentage:
Methidathion 50%,
Chlorfenapyr 10%,
Agriculture breast 500#20%
Isooctanol 10%
Kerosene 10%.
7. according to the missible oil that contains chlorfenapyr described in the arbitrary claim of claim 1-6, for preventing and treating liriomyza bryoniae, large trypetid, tea lesser leafhopper, be particularly useful for preventing and treating tea lesser leafhopper.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310670227.2A CN103704251B (en) | 2013-12-10 | 2013-12-10 | Missible oil containing chlorfenapyr and application |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310670227.2A CN103704251B (en) | 2013-12-10 | 2013-12-10 | Missible oil containing chlorfenapyr and application |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103704251A true CN103704251A (en) | 2014-04-09 |
| CN103704251B CN103704251B (en) | 2015-12-02 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310670227.2A Expired - Fee Related CN103704251B (en) | 2013-12-10 | 2013-12-10 | Missible oil containing chlorfenapyr and application |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103704251B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105165810A (en) * | 2015-07-02 | 2015-12-23 | 河北岗恩生物科技有限公司 | Benzene series solvent substitute sulfonated kerosene and application thereof in abamectin emulsifiable concentrate |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4929634A (en) * | 1987-10-23 | 1990-05-29 | American Cyanamid Company | Method of and bait compositions for controlling mollusks |
| CN1108884A (en) * | 1994-12-26 | 1995-09-27 | 徐建军 | Organophosphorus insecticide |
| CN101606517A (en) * | 2009-07-27 | 2009-12-23 | 深圳诺普信农化股份有限公司 | A kind of farm chemical emulsion preparation |
| CN102057897A (en) * | 2009-11-17 | 2011-05-18 | 联合国南通农药剂型开发中心 | Chlorpyrifos microcapsule suspension and preparation method thereof |
| EP2481284A2 (en) * | 2011-01-27 | 2012-08-01 | Basf Se | Pesticidal mixtures |
-
2013
- 2013-12-10 CN CN201310670227.2A patent/CN103704251B/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4929634A (en) * | 1987-10-23 | 1990-05-29 | American Cyanamid Company | Method of and bait compositions for controlling mollusks |
| CN1108884A (en) * | 1994-12-26 | 1995-09-27 | 徐建军 | Organophosphorus insecticide |
| CN101606517A (en) * | 2009-07-27 | 2009-12-23 | 深圳诺普信农化股份有限公司 | A kind of farm chemical emulsion preparation |
| CN102057897A (en) * | 2009-11-17 | 2011-05-18 | 联合国南通农药剂型开发中心 | Chlorpyrifos microcapsule suspension and preparation method thereof |
| EP2481284A2 (en) * | 2011-01-27 | 2012-08-01 | Basf Se | Pesticidal mixtures |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105165810A (en) * | 2015-07-02 | 2015-12-23 | 河北岗恩生物科技有限公司 | Benzene series solvent substitute sulfonated kerosene and application thereof in abamectin emulsifiable concentrate |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103704251B (en) | 2015-12-02 |
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Effective date of registration: 20151023 Address after: 510640 Guangdong city of Guangzhou province Tianhe District gold Yinglu No. 1 was 1106 room two Applicant after: GUANGDONG HUABO ENTERPRISE MANAGEMENT CONSULTING Co.,Ltd. Address before: 250199, building 389, Huaxin Road, Licheng District, Shandong, Ji'nan 401 Applicant before: JINAN CAVIN BIOTECHNOLOGY Co.,Ltd. |
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Effective date of registration: 20151109 Address after: 311812 Zhuji, Zhejiang, Cao Cao Town, Tianyuan Road, No. 86, No. Applicant after: Chu Juanying Address before: 510640 Guangdong city of Guangzhou province Tianhe District gold Yinglu No. 1 was 1106 room two Applicant before: GUANGDONG HUABO ENTERPRISE MANAGEMENT CONSULTING Co.,Ltd. |
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Address after: Seven 225453 Wei Jiangsu province Taixing City Economic Development Zone, Hongqiao Industrial Park Patentee after: Chu Juanying Address before: 311812 Zhuji, Zhejiang, Cao Cao Town, Tianyuan Road, No. 86, No. Patentee before: Chu Juanying |
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Effective date of registration: 20161207 Address after: 510665 Tianhe District, Guangzhou, No. five, No. Road, building, building, No. 702, No. 371 Patentee after: GUANGDONG GAOHANG INTELLECTUAL PROPERTY OPERATION Co.,Ltd. Address before: Seven 225453 Wei Jiangsu province Taixing City Economic Development Zone, Hongqiao Industrial Park Patentee before: Chu Juanying Effective date of registration: 20161207 Address after: 542800 the Guangxi Zhuang Autonomous Region Hezhou Zijin Mountain County Huilong Zhen Quan Ling Cun Wei Shang Quan Cun Patentee after: GUANGXI ZHONGSHAN FUQIANG YAYAO HUAXIANG AGRICULTURE CO.,LTD. Address before: 510665 Tianhe District, Guangzhou, No. five, No. Road, building, building, No. 702, No. 371 Patentee before: GUANGDONG GAOHANG INTELLECTUAL PROPERTY OPERATION Co.,Ltd. |
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Granted publication date: 20151202 Termination date: 20181210 |