CN103693913B - A kind of modified vitrified micro ball thermal-insulating mortar - Google Patents
A kind of modified vitrified micro ball thermal-insulating mortar Download PDFInfo
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- CN103693913B CN103693913B CN201310671521.5A CN201310671521A CN103693913B CN 103693913 B CN103693913 B CN 103693913B CN 201310671521 A CN201310671521 A CN 201310671521A CN 103693913 B CN103693913 B CN 103693913B
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- 239000004570 mortar (masonry) Substances 0.000 title claims abstract description 15
- 239000011806 microball Substances 0.000 title claims abstract description 11
- 239000000843 powder Substances 0.000 claims abstract description 14
- 229910052624 sepiolite Inorganic materials 0.000 claims abstract description 10
- 235000019355 sepiolite Nutrition 0.000 claims abstract description 10
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000011324 bead Substances 0.000 claims abstract description 8
- 239000011521 glass Substances 0.000 claims abstract description 8
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000010881 fly ash Substances 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 7
- 229960004418 trolamine Drugs 0.000 claims abstract description 7
- 239000004568 cement Substances 0.000 claims abstract description 5
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims abstract description 4
- 239000004372 Polyvinyl alcohol Substances 0.000 claims abstract description 4
- 244000223014 Syzygium aromaticum Species 0.000 claims abstract description 4
- 235000016639 Syzygium aromaticum Nutrition 0.000 claims abstract description 4
- 150000001412 amines Chemical class 0.000 claims abstract description 4
- 229940077388 benzenesulfonate Drugs 0.000 claims abstract description 4
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 claims abstract description 4
- 239000000920 calcium hydroxide Substances 0.000 claims abstract description 4
- 229910001861 calcium hydroxide Inorganic materials 0.000 claims abstract description 4
- 235000011116 calcium hydroxide Nutrition 0.000 claims abstract description 4
- 125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 claims abstract description 4
- 229910052602 gypsum Inorganic materials 0.000 claims abstract description 4
- 239000010440 gypsum Substances 0.000 claims abstract description 4
- 229960003742 phenol Drugs 0.000 claims abstract description 4
- 229920002451 polyvinyl alcohol Polymers 0.000 claims abstract description 4
- 229920002545 silicone oil Polymers 0.000 claims abstract description 4
- 239000011734 sodium Substances 0.000 claims abstract description 4
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 4
- -1 sodium alkyl benzene Chemical class 0.000 claims abstract description 4
- 235000019154 vitamin C Nutrition 0.000 claims abstract description 4
- 239000011718 vitamin C Substances 0.000 claims abstract description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 9
- 238000003756 stirring Methods 0.000 claims description 7
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 6
- 239000000463 material Substances 0.000 claims description 6
- 239000011325 microbead Substances 0.000 claims description 6
- 238000002360 preparation method Methods 0.000 claims description 6
- 238000004017 vitrification Methods 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 3
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 3
- 239000004113 Sepiolite Substances 0.000 claims description 3
- 239000006087 Silane Coupling Agent Substances 0.000 claims description 3
- DPDMMXDBJGCCQC-UHFFFAOYSA-N [Na].[Cl] Chemical compound [Na].[Cl] DPDMMXDBJGCCQC-UHFFFAOYSA-N 0.000 claims description 3
- 238000000498 ball milling Methods 0.000 claims description 3
- CQEYYJKEWSMYFG-UHFFFAOYSA-N butyl acrylate Chemical compound CCCCOC(=O)C=C CQEYYJKEWSMYFG-UHFFFAOYSA-N 0.000 claims description 3
- 239000008367 deionised water Substances 0.000 claims description 3
- 229910021641 deionized water Inorganic materials 0.000 claims description 3
- 239000012467 final product Substances 0.000 claims description 3
- 238000013467 fragmentation Methods 0.000 claims description 3
- 238000006062 fragmentation reaction Methods 0.000 claims description 3
- 238000005984 hydrogenation reaction Methods 0.000 claims description 3
- 238000000034 method Methods 0.000 claims description 3
- 238000004806 packaging method and process Methods 0.000 claims description 3
- RUOJZAUFBMNUDX-UHFFFAOYSA-N propylene carbonate Chemical compound CC1COC(=O)O1 RUOJZAUFBMNUDX-UHFFFAOYSA-N 0.000 claims description 3
- 239000002002 slurry Substances 0.000 claims description 3
- KKCBUQHMOMHUOY-UHFFFAOYSA-N sodium oxide Chemical compound [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 claims description 3
- 229910001948 sodium oxide Inorganic materials 0.000 claims description 3
- 238000005507 spraying Methods 0.000 claims description 3
- 239000000725 suspension Substances 0.000 claims description 3
- 238000000227 grinding Methods 0.000 claims description 2
- 238000009413 insulation Methods 0.000 description 4
- 239000000654 additive Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
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- Curing Cements, Concrete, And Artificial Stone (AREA)
Abstract
The invention discloses a kind of modified vitrified micro ball thermal-insulating mortar; it is obtained by the raw material of following weight parts: glass bead 50-70, amine hydroxybenzene 1-2, dimethyl silicone oil 0.3-0.5, vitamins C 0.5-1, cement 40-60, gypsum 2-4, flyash 10-15, polyvinyl alcohol 1-2, Syzygium aromaticum stem oil 0.3-0.5, trolamine 1-2, sodium alkyl benzene sulfonate 0.2-0.4, slaked lime 1-2; magnesium powder 0.05-0.1, pull open powder 0.005-0.008, modified meerschaum powder 10-20.
Description
Technical field
The present invention relates to thermal insulation mortar field, is exactly a kind of modified vitrified micro ball thermal-insulating mortar.
Background technology
Thermal insulation mortar is with various light material for aggregate, is gelating material, admixes some property-modifying additives with cement, is uniformly mixed and a kind of premixing dry-mix made through manufacturing enterprise.For constructing a kind of material of construction of building surface thermal insulation layer.
Summary of the invention
The object of the present invention is to provide a kind of modified vitrified micro ball thermal-insulating mortar
Above-mentioned purpose is realized by following scheme:
A kind of modified vitrified micro ball thermal-insulating mortar, it is obtained by the raw material of following weight parts:
Glass bead 50-70, amine hydroxybenzene 1-2, dimethyl silicone oil 0.3-0.5, vitamins C 0.5-1, cement 40-60, gypsum 2-4, flyash 10-15, polyvinyl alcohol 1-2, Syzygium aromaticum stem oil 0.3-0.5, trolamine 1-2, sodium alkyl benzene sulfonate 0.2-0.4, slaked lime 1-2, magnesium powder 0.05-0.1, pull open powder 0.005-0.008, modified meerschaum powder 10-20;
The preparation method of described modified meerschaum powder is:
After getting sepiolite fragmentation, be equivalent to the tetrahydroglyoxaline of its weight 1-2%, the sodium-chlor of 1.5-2%, the butyl acrylate of 1-2% mix, add alcohol and carry out Ball milling process 4-6 hour, take out, dry in the shade, at 600-700 DEG C, sinter 2-4 hour, add suitable quantity of water again, stir, become suspension, then add concentration be 10-15% hydrochloric acid soln adjust PH be 5-6, after ground slurry to 400-500 order, repeated hydrogenation sodium oxide is adjusted to neutrality, and spraying dry obtains powder.
Described a kind of modified vitrified micro ball thermal-insulating mortar, is characterized in that:
Preparation method is:
(1) getting glass bead is soak 6-8 hour in the hydrogen peroxide solution of 10-15% in concentration, take out, deionized water wash, dry, add again and be equivalent to the propylene carbonate of its weight 1-1.5%, the Silane coupling agent KH550 of 1.2-1.7%, and appropriate water, stir 10-15 minute under 100-200 rev/min after, dry, obtain modified vitrification micro-bead;
(2) modified vitrification micro-bead, flyash, trolamine are mixed by weight; 5-10 minute is stirred under 1100-1200 rev/min; take out; again with residue whole raw material blending after; 600-800 rev/min is at the uniform velocity stirred 20-30 minute; the material three-roll grinder grinding 1-2 hour that will be stirred again, after packaging and get final product.
Beneficial effect of the present invention is: the present invention is by the modification to glass bead, and improve the heat-insulating property of mortar, bonding strength, make thermal insulation mortar excellent property of the present invention, effect is good.
Embodiment
A kind of modified vitrified micro ball thermal-insulating mortar, it is obtained by the raw material of following weight kg:
Glass bead 70, amine hydroxybenzene 2, dimethyl silicone oil 0.5, vitamins C 1, cement 60, gypsum 4, flyash 15, polyvinyl alcohol 2, Syzygium aromaticum stem oil 0.5, trolamine 2, sodium alkyl benzene sulfonate 0.4, slaked lime 1.2, magnesium powder 0.04, pull open powder 0.006, modified meerschaum powder 18;
The preparation method of described modified meerschaum powder is:
After getting sepiolite fragmentation, be equivalent to the tetrahydroglyoxaline of its weight 1.5%, the sodium-chlor of 1.8%, the butyl acrylate of 1% mix, add alcohol and carry out Ball milling process 5 hours, take out, dry in the shade, at 700 DEG C, sinter 2 hours, add suitable quantity of water again, stir, become suspension, then add concentration be 14% hydrochloric acid soln adjust PH be 5.5, after ground slurry to 500 order, repeated hydrogenation sodium oxide is adjusted to neutrality, and spraying dry obtains powder.
Described a kind of modified vitrified micro ball thermal-insulating mortar, preparation method is:
(1) getting glass bead is soak 8 hours in the hydrogen peroxide solution of 14% in concentration, take out, deionized water wash, dry, add again and be equivalent to the propylene carbonate of its weight 1.5%, the Silane coupling agent KH550 of 1.2%, and appropriate water, stir under 200 revs/min after 15 minutes, dry, obtain modified vitrification micro-bead;
(2) by modified vitrification micro-bead, flyash, trolamine mixing, stir 5 minutes under 1200 revs/min, take out; again with residue whole raw material blending after; 800 revs/min are at the uniform velocity stirred 30 minutes, then the material three-roll grinder be stirred are ground 2 hours, after packaging and get final product.
Products obtained therefrom test result is as follows:
Claims (1)
1. a modified vitrified micro ball thermal-insulating mortar, it is characterized in that: it is obtained by the raw material of following weight parts: glass bead 50-70, amine hydroxybenzene 1-2, dimethyl silicone oil 0.3-0.5, vitamins C 0.5-1, cement 40-60, gypsum 2-4, flyash 10-15, polyvinyl alcohol 1-2, Syzygium aromaticum stem oil 0.3-0.5, trolamine 1-2, sodium alkyl benzene sulfonate 0.2-0.4, slaked lime 1-2, magnesium powder 0.05-0.1, pull open powder 0.005-0.008, modified meerschaum powder 10-20;
The preparation method of described modified meerschaum powder is: after getting sepiolite fragmentation, with be equivalent to the tetrahydroglyoxaline of its weight 1-2%, the sodium-chlor of 1.5-2%, the butyl acrylate of 1-2% mix, add alcohol and carry out Ball milling process 4-6 hour, take out, dry in the shade, 2-4 hour is sintered at 600-700 DEG C, add suitable quantity of water again, stir, become suspension, then add concentration be 10-15% hydrochloric acid soln adjust pH be 5-6, after ground slurry to 400-500 order, repeated hydrogenation sodium oxide is adjusted to neutrality, and spraying dry obtains powder;
Described modified vitrified micro ball thermal-insulating mortar preparation method is:
(1) getting glass bead is soak 6-8 hour in the hydrogen peroxide solution of 10-15% in concentration, take out, deionized water wash, dry, add again and be equivalent to the propylene carbonate of its weight 1-1.5%, the Silane coupling agent KH550 of 1.2-1.7%, and appropriate water, stir 10-15 minute under 100-200 rev/min after, dry, obtain modified vitrification micro-bead;
(2) modified vitrification micro-bead, flyash, trolamine are mixed by weight; 5-10 minute is stirred under 1100-1200 rev/min; take out; again with residue whole raw material blending after; 600-800 rev/min is at the uniform velocity stirred 20-30 minute; the material three-roll grinder grinding 1-2 hour that will be stirred again, after packaging and get final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310671521.5A CN103693913B (en) | 2013-12-07 | 2013-12-07 | A kind of modified vitrified micro ball thermal-insulating mortar |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310671521.5A CN103693913B (en) | 2013-12-07 | 2013-12-07 | A kind of modified vitrified micro ball thermal-insulating mortar |
Publications (2)
| Publication Number | Publication Date |
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| CN103693913A CN103693913A (en) | 2014-04-02 |
| CN103693913B true CN103693913B (en) | 2015-12-02 |
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| CN201310671521.5A Expired - Fee Related CN103693913B (en) | 2013-12-07 | 2013-12-07 | A kind of modified vitrified micro ball thermal-insulating mortar |
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Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104261751A (en) * | 2014-08-29 | 2015-01-07 | 明光市第二建筑安装有限责任公司 | Composite wall thermal-insulation material and preparation method thereof |
| CN104926259B (en) * | 2015-06-29 | 2018-01-12 | 石河子大学 | A kind of water-fast low density polyethylene (LDPE) enhancing gypsum of lightweight and preparation method thereof |
| CN105541235B (en) * | 2016-01-28 | 2018-04-20 | 青岛天地彩涂料工程应用有限公司 | A kind of heat preservation mortar for outer wall and preparation method |
| CN105967569A (en) * | 2016-05-11 | 2016-09-28 | 王星烨 | Anti-cracking mortar and preparation method thereof |
| CN108863237A (en) * | 2018-07-27 | 2018-11-23 | 芜湖市棠华建材科技有限公司 | A kind of building heat-insulating mortar and preparation method |
| CN115626801A (en) * | 2022-11-01 | 2023-01-20 | 冯建鹏 | Anti-crack mortar for external wall heat insulation |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101525226A (en) * | 2009-04-13 | 2009-09-09 | 吕运征 | Insulating dry powder mortar |
| CN101811846A (en) * | 2009-12-08 | 2010-08-25 | 河南省绿韵建材有限公司 | Polymer vitrified microsphere building heat-insulating mortar |
| CN102206071A (en) * | 2011-03-22 | 2011-10-05 | 上海奇葩环境科技有限公司 | Formula design for novel fly-ash-based insulating dry powder |
| CN102863197A (en) * | 2012-09-13 | 2013-01-09 | 上海宇培特种建材有限公司 | Desulfurization gypsum-based thermal insulation mortar and preparation method thereof |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101286259B1 (en) * | 2010-11-17 | 2013-07-18 | 주철완 | Manufacture method of inorganic foam using geopolymer silica sol·gel method |
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2013
- 2013-12-07 CN CN201310671521.5A patent/CN103693913B/en not_active Expired - Fee Related
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101525226A (en) * | 2009-04-13 | 2009-09-09 | 吕运征 | Insulating dry powder mortar |
| CN101811846A (en) * | 2009-12-08 | 2010-08-25 | 河南省绿韵建材有限公司 | Polymer vitrified microsphere building heat-insulating mortar |
| CN102206071A (en) * | 2011-03-22 | 2011-10-05 | 上海奇葩环境科技有限公司 | Formula design for novel fly-ash-based insulating dry powder |
| CN102863197A (en) * | 2012-09-13 | 2013-01-09 | 上海宇培特种建材有限公司 | Desulfurization gypsum-based thermal insulation mortar and preparation method thereof |
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| CN103693913A (en) | 2014-04-02 |
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