CN103657588B - A kind of preparation method of zeolite powder adsorbent - Google Patents
A kind of preparation method of zeolite powder adsorbent Download PDFInfo
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- CN103657588B CN103657588B CN201310722118.0A CN201310722118A CN103657588B CN 103657588 B CN103657588 B CN 103657588B CN 201310722118 A CN201310722118 A CN 201310722118A CN 103657588 B CN103657588 B CN 103657588B
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- zeolite powder
- zeolite
- adsorbent
- pasty state
- powder adsorbent
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Abstract
The invention discloses a kind of preparation method of zeolite powder adsorbent, first zeolite superfine mill is crushed to more than fineness 325 order; The zeolite powder pulverized out is put into homemade agitating device according to the ratio of corresponding 200 ml waters of 100 grams of zeolite powders; Add the water of certain proportioning, special starch, copper sulphate, heat after sodium acid carbonate and calcite, reach between 80 to 100 degree, and continuous heating more than 45 minutes, zeolite powder is become pasty state; Proceeded to by the zeolite powder of pasty state to dry in booth and dry in geothermal tube mode, dried by a large amount of moisture content, described pasty state zeolite powder is dried into hard block; By the zeolite powder of this hard block after crushing pulverizer processing, obtain zeolite powder adsorbent.Made by zeolite powder adsorbent out processed by natural crystal, to human body without harm, and high adsorption capacity, effect is more lasting.
Description
Technical field
The present invention relates to technical field of absorbent, particularly relate to a kind of preparation method of zeolite powder adsorbent.
Background technology
At present, in adsorbent application aspect, the suction type of common adsorbents generally needs to carry out in sealing place, its effect can only act on about three months, and conventional adsorbent contains chemical synthesis material, has certain harmfulness to human body, and sterilizing function is unsatisfactory, effect also can disappearance slowly; Another kind of acticarbon then needs ventilating system, and needs in use procedure to change at any time, causes practicality not strong.
Lack a kind of strong, natural harmless in prior art, and the adsorbent product of lasts.
Summary of the invention
The object of this invention is to provide a kind of preparation method of zeolite powder adsorbent, made zeolite powder adsorbent is out processed by natural crystal, to human body without harm, and high adsorption capacity, effect is more lasting.
A preparation method for zeolite powder adsorbent, described method comprises:
Zeolite superfine mill is crushed to more than fineness 325 order;
The zeolite powder pulverized out is put into homemade agitating device according to the ratio of corresponding 200 ml waters of 100 grams of zeolite powders;
Add the water of certain proportioning, special starch, copper sulphate, heat after sodium acid carbonate and calcite, reach between 80 to 100 degree, and continuous heating more than 45 minutes, zeolite powder is become pasty state;
Proceeded to by the zeolite powder of pasty state to dry in booth and dry in geothermal tube mode, dried by a large amount of moisture content, described pasty state zeolite powder is dried into hard block;
By the zeolite powder of this hard block after crushing pulverizer processing, obtain zeolite powder adsorbent.
In described zeolite, the mass percentage content of each composition is:
The Al of 14.55%
2o
3; The SiO of 69.78%
2; The Fe of 0.98%
2o
3; The FeO of 0.20%; The CaO of 1.59%; The TiO of 0.03%
2.
Obtained zeolite powder adsorbent is fineness 500 order ~ 600 object white powders.
As seen from the above technical solution provided by the invention, made zeolite powder adsorbent is out processed by natural crystal, to human body without harm, and high adsorption capacity, effect is more lasting.
Accompanying drawing explanation
In order to be illustrated more clearly in the technical scheme of the embodiment of the present invention, below the accompanying drawing used required in describing embodiment is briefly described, apparently, accompanying drawing in the following describes is only some embodiments of the present invention, for those of ordinary skill in the art, under the prerequisite not paying creative work, other accompanying drawings can also be obtained according to these accompanying drawings.
Fig. 1 provides by the embodiment of the present invention preparation method schematic flow sheet of zeolite powder adsorbent.
Detailed description of the invention
Below in conjunction with the accompanying drawing in the embodiment of the present invention, be clearly and completely described the technical scheme in the embodiment of the present invention, obviously, described embodiment is only the present invention's part embodiment, instead of whole embodiments.Based on embodiments of the invention, those of ordinary skill in the art, not making the every other embodiment obtained under creative work prerequisite, belong to protection scope of the present invention.
Below in conjunction with accompanying drawing, the embodiment of the present invention is described in further detail, be illustrated in figure 1 the embodiment of the present invention the preparation method schematic flow sheet of zeolite powder adsorbent is provided, described method comprises:
Step 11: zeolite superfine mill is crushed to more than fineness 325 order;
In this step, in described zeolite, the mass percentage content of each composition is:
The Al of 14.55%
2o
3; The SiO of 69.78%
2; The Fe of 0.98%
2o
3; The FeO of 0.20%; The CaO of 1.59%; The TiO of 0.03%
2.
Step 12: the zeolite powder pulverized out is put into homemade agitating device according to the ratio of corresponding 200 ml waters of 100 grams of zeolite powders;
Step 13: the water adding certain proportioning, special starch, copper sulphate, sodium acid carbonate and calcite (400 order) heat afterwards, and reach between 80 to 100 degree, continuous heating more than 45 minutes, becomes zeolite powder into pasty state;
In this step, the fineness of calcite is 400 orders.
By heating, zeolite cavity is increased, the moisture that starch enters into the inside in duct is extruded, thus absorption affinity is increased.
Step 14: proceeded to by the zeolite powder of pasty state to dry in booth and dry in geothermal tube mode, dried by a large amount of moisture content, described pasty state zeolite powder is dried into hard block;
In this step, the moisture in pasty state zeolite powder dissipates in air with the form of steam.
Step 15: by the zeolite powder of this hard block after crushing pulverizer processing, obtain zeolite powder adsorbent.
In this step, obtained zeolite powder adsorbent is fineness 500 order ~ 600 object white powders; In addition, increased by specific area after pulverizing, the large then absorption affinity of specific area increases.
The adsorption capacity of processing the zeolite powder adsorbent obtained through above-mentioned process can reach diameter 20m, owing to being by natural crystal thermal synthesis process, thus harmless, and suction-operated can be played under normal temperature state.
Below the zeolite powder adsorbent of above-mentioned preparation is tested:
Test through antibiotic property: at 25 DEG C, after 24 hours micro-cultures of bacteria, measurement result bacterium reduces 99.9%;
Test through absorption affinity: test coal gas is adsorbed as 98.4% in 5 minutes; The humidity ratio absorbing air is 6.8%.
After tested, to promote that the photosynthesis of plant grows faster for this zeolite powder adsorbent; Making soil become fertile after this zeolite powder adsorbent and soil combine, is also its strong point and feature.
Due to plant growth easily by Changes in weather affect temperature deviation more than 10 time (particularly in booth) bacterium will generate and make plant sick; and after using this zeolite powder adsorbent; then do not need to spray insecticide and just can remove bacterium; germ is stoped to grow up; not that this zeolite powder adsorbent has violent toxicity; but the rack construction attracts bacteria molecule of zeolite, it can be made to stop breeding and die, thus protective plant.Be sprayed onto on blade face by this zeolite powder adsorbent, the absorption affinity of zeolite works, and the nutrient absorption in bacterium ovum in zeolite pores, ovum will dry up and die.In addition, this zeolite powder adsorbent can not by absorption precipitation, and agricultural chemicals and growth agent can remain in soil and plant or be absorbed, by the Si contained in this zeolite powder adsorbent, Fe1, Fe2, Na, Ma, the elements such as K, Ti, P, Al decompose after the bacterial adsorption in environment.
In sum, according to the zeolite powder adsorbent that method described in the embodiment of the present invention is obtained, there is following features:
1, be placed in refrigerator, effectively decompose odor molecules, extend food preservation time, improve storing and fresh-keeping degree, excellent; Do not damage original smell of varieties of food items; Nontoxic, harmless, healthy, environmental protection.
2, be placed on indoor, the pernicious gases such as Absorbable rod formaldehyde in air have very strong adsorption capacity, and can according to the difference of ambient temperature and humidity, discharge the moisture content of self or the hydrone that absorbs in air, keep environment relatively dry.
3, add fish, chicken, in the feeds such as pig, poultry can be made to grow and accelerate, body strengthens that meat is fresh, and laying rate is high, can promote the performance of growth of animal, can not have a negative impact to the health of animal.Also can be used for raiseeing disease control, reduce and use antibiotic.Further, the ight soil of animal has no stink, and that also can reduce fish jar changes waterside number.
4, in vegetable disease control, the prevention effect of more than 95% can omnidistance be reached.
5, solve and often there will be residual problem when clean tableware; some chemicals remaining in bowls and chopsticks can cause significant damage to the health of people; especially the residual of some wooden bowls and chopsticks cannot be eradicated; just can remove totally with zeolite powder; car appearance surface shell can also be removed simultaneously, after wiping, be not easy ash.
The above; be only the present invention's preferably detailed description of the invention, but protection scope of the present invention is not limited thereto, is anyly familiar with those skilled in the art in the technical scope that the present invention discloses; the change that can expect easily or replacement, all should be encompassed within protection scope of the present invention.Therefore, protection scope of the present invention should be as the criterion with the protection domain of claims.
Claims (2)
1. a preparation method for zeolite powder adsorbent, is characterized in that, described method comprises:
Zeolite superfine mill is crushed to more than fineness 325 order;
The zeolite powder pulverized out is put into homemade agitating device according to the ratio of corresponding 200 ml waters of 100 grams of zeolite powders;
Add the water of certain proportioning, special starch, copper sulphate, heat after sodium acid carbonate and calcite, reach between 80 to 100 degree, and continuous heating more than 45 minutes, zeolite powder is become pasty state; Described special starch is used for, after being made by heating zeolite cavity increase, entering in this zeolite cavity and being extruded by the moisture of the inside;
Proceeded to by the zeolite powder of pasty state to dry in booth and dry in geothermal tube mode, dried by a large amount of moisture content, described pasty state zeolite powder is dried into hard block;
By the zeolite powder of this hard block after crushing pulverizer processing, obtain zeolite powder adsorbent.
2. the preparation method of zeolite powder adsorbent according to claim 1, it is characterized in that, obtained zeolite powder adsorbent is fineness 500 order ~ 600 object white powders.
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| CN201310722118.0A CN103657588B (en) | 2013-12-24 | 2013-12-24 | A kind of preparation method of zeolite powder adsorbent |
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|---|---|---|---|
| CN201310722118.0A CN103657588B (en) | 2013-12-24 | 2013-12-24 | A kind of preparation method of zeolite powder adsorbent |
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| CN103657588A CN103657588A (en) | 2014-03-26 |
| CN103657588B true CN103657588B (en) | 2016-02-10 |
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Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104971701A (en) * | 2014-04-01 | 2015-10-14 | 上海工程技术大学 | Polysaccharide modified natural zeolite suspension solution as well as preparation method and application thereof |
| CN108975836B (en) * | 2018-08-29 | 2020-11-10 | 广州大学 | Electromagnetic wave transmission composite material and preparation method and application thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1034314A (en) * | 1988-06-22 | 1989-08-02 | 福建省上杭县侨兴饲料加工厂 | A kind of mineral additive for feed |
| CN101574647A (en) * | 2009-04-23 | 2009-11-11 | 中国海洋石油总公司 | Preparation method of ultra-deep absorption desulfurization and denitrogenation agent for hydrocracking tail oil |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0653036B2 (en) * | 1985-08-20 | 1994-07-20 | 益三 村上 | Cleaning method for aquaculture pond using molded zeolite |
| JP2013006174A (en) * | 2011-05-24 | 2013-01-10 | Hakki Sangyo Kk | Flocculant composition and flocculation method for purifying dye wastewater |
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2013
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1034314A (en) * | 1988-06-22 | 1989-08-02 | 福建省上杭县侨兴饲料加工厂 | A kind of mineral additive for feed |
| CN101574647A (en) * | 2009-04-23 | 2009-11-11 | 中国海洋石油总公司 | Preparation method of ultra-deep absorption desulfurization and denitrogenation agent for hydrocracking tail oil |
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Effective date of registration: 20180814 Address after: 530028 Nanning 1020, National Road 115-1, Qingxiu District, the Guangxi Zhuang Autonomous Region Patentee after: Lan Fengyun Address before: 132013 1-31-113, building 2, Shui Yun City, Jilin street, Fengman District, Jilin, Jilin. Patentee before: Zheng Yongjun |
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Granted publication date: 20160210 Termination date: 20181224 |