CN103653125A - Production method of natural active chrysanthemum nankingense drink - Google Patents

Production method of natural active chrysanthemum nankingense drink Download PDF

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Publication number
CN103653125A
CN103653125A CN201310616129.0A CN201310616129A CN103653125A CN 103653125 A CN103653125 A CN 103653125A CN 201310616129 A CN201310616129 A CN 201310616129A CN 103653125 A CN103653125 A CN 103653125A
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China
Prior art keywords
chrysanthemum brain
chrysanthemum
drink
temperature
brain
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CN201310616129.0A
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CN103653125B (en
Inventor
李春阳
田野
荣德昌
杨明
王艳秋
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NANJING FEIMA FOOD Co Ltd
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NANJING FEIMA FOOD Co Ltd
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/38Other non-alcoholic beverages
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/70Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
    • A23L2/84Clarifying or fining of non-alcoholic beverages; Removing unwanted matter using microorganisms or biological material, e.g. enzymes
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Polymers & Plastics (AREA)
  • Nutrition Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Molecular Biology (AREA)
  • Zoology (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)

Abstract

The invention provides a production method of a natural active chrysanthemum nankingense drink. The production method is characterized in that through blanching, zinc acetate and ascorbic acid combined color protection, enzymatic oxidation and the formation of phaeophytin are inhibited, and the natural green of fresh chrysanthemum nankingense is maintained; through wall breakage with a biological enzyme method, the release of active materials is promoted, and the nutrition and active functions of the drink are improved; and a high-voltage pulse electric field is adopted for sterilization, so that bioactive components of the chrysanthemum nankingense are reserved effectively, and phenolic substance oxidation and activity loss are reduced. According to the production method, a bipolar positive/negative pulse OSU-4L laboratory-scale pulse processor (produced by Ohio State University) is adopted, and Escherichia coli and pathogenic bacteria in the chrysanthemum nankingense drink can be effectively killed, so that the commercial sterilization can be realized, the drink does not contain any preservative and has a special fresh scent of chrysanthemum nankingense, and the shelf life is more than 6 months.

Description

A kind of production method of natural activity chrysanthemum brain drink
One, technical field
The production method that the invention provides a kind of natural activity chrysanthemum brain drink, belongs to deep-processing technical field of agricultural products.
Two, background technology
Chrysanthemum brain, claim again florists chrysanthemum leaf, LUBIANHUANG, in composite family Chrysanthemum, to take young stem and leaf as main cultivar, belong to annual or herbaceos perennial, contain the nutriments such as rich in protein, fat, vitamin, cellulose, mineral matter, salt, wherein vitamin A and content of mineral substances are the most outstanding.Refrigerant, improving eyesight that chrysanthemum brain has, whets the appetite in tune, also has removing toxic substances, hypotensive effect, to preventing and treating influenza, epidemic meningitis, hepatitis, dysentery, suppresses pathogenic microorganism, bacterium and virus and dermatophyte growth all plays an important role.The contained volatile oil of chrysanthemum brain is a kind of important bioactivator, can maintain the normal function of capillary, removes free radical, suppresses tumour.
Chrysanthemum brain is In Nanjing special product edible wild herbs, belongs to one of Nanjing Triratna, is deeply subject to Nanjing consumers in general's favor.At present, domestic scholars focuses mostly at aspects such as artificial cultivation, Analysis of Nutritive Composition, product are fresh-keeping to chrysanthemum brain research, and chrysanthemum brain intensive processing product is rarely found.The natural chrysanthemum brain drink of this patent research and development, can fully retain whole nutritional labelings of chrysanthemum brain, and shelf life of products is long, and product delicate fragrance, long times of aftertaste meet consumers in general's back to nature, pursue green fashion, have very large market development space.
Three, summary of the invention
Technical problem the present invention mainly develops the production technology of the active drink of natural chrysanthemum brain, take fresh chrysanthemum brain as raw material, blanching is protected after look, through biological enzymolysis broken wall, greatly discharge bioactive ingredients, by high-pressure pulse electric sterilization and sterile filling, finally obtain having the active chrysanthemum brain clear liquid of Nutrition and health function.
Technical scheme the invention provides a kind of natural activity chrysanthemum brain drink processing technique, specific as follows:
1, the blanching of chrysanthemum brain with protect look: fresh chrysanthemum brain is put into 50-100 ℃ of sodium bicarbonate solution (concentration is 0.01-0.50%), and blanching 30-300s, is cooled to room temperature with circulating water rapidly; With 0.01-0.3% ascorbic acid and 0.01-0.3% acetic acid zinc solution, soak 1.5-4.5h, pull out, with clear water, clean the raffinate on chrysanthemum brain surface, standby.
2, the preparation of chrysanthemum brain Normal juice: by the chrysanthemum brain protecting after look, by 1:4, add water making beating, and add the cellulase of 0.02-0.20%, enzymolysis 1-4h under 40-60 ℃ and pH3.5-7.0 condition, cooling, centrifugal in the instrument centrifuge of H1650-W Hunan, temperature is controlled at 10-30 ℃, rotating speed 2000-5000r/min, centrifugal 10-30min, obtains the green chrysanthemum brain clear liquid of clear.
3, sterilization, filling and refrigeration: adopt bipolar positive negative pulse stuffing, pulse width 2 μ s, the OSU-4L laboratory scale pulse processor of pulse frequency 200Hz (Ohio State Univ-Columbus USA's making), in electric-field intensity, be under 20-35kV/cm condition, the chrysanthemum brain clear liquid that is 1500-2500 μ s by electrical conductivity carries out sterilization processing 100-300 μ s (guaranteeing that feeding temperature and drop temperature are 2-10 ℃), finally carry out sterile filling, under 0-18 ℃ of condition, preserve.
The present invention compared with prior art, has the following advantages:
1, selecting fresh chrysanthemum brain is raw material, through blanching and color retention, has kept the emerald green of chrysanthemum brain stoste, has avoided the appearance of assorted blue or green taste.
2, adopt biological enzyme broken wall treatment, promoted the release of nutrition and active material in chrysanthemum brain, the bioactive functions of raising product.
3, adopt high-pressure pulse electric sterilization, efficiently solve the oxidation of phenols active material and biological function loss that thermal sterilization causes, improved its Nutrition and health function.
Four, the specific embodiment
Embodiment 1
Get fresh chrysanthemum brain, cleaning, clean, blanching 60s in the sodium bicarbonate solutions of 65 ℃ (concentration is 0.3%), is cooled to room temperature with circulating water rapidly; Ascorbic acid with 0.2% and 0.2% acetic acid zinc solution soak 3h, and chrysanthemum brain is pulled out, with clear water, clean surperficial raffinate, in the ratio of 1:4, add water making beating; Add 0.06% cellulase, under 50 ℃ and pH4.6 condition, enzymolysis 3h, cooling; Centrifugal in the instrument centrifuge of H1650-W Hunan, temperature is controlled at 20 ℃, rotating speed 3000r/min, and centrifugal 15min, obtains chrysanthemum brain clear liquid; Control chrysanthemum brain clear liquid electrical conductivity in 2000 μ s left and right, adopt 6 continuous process chambers, bipolar positive negative pulse stuffing, pulse width 2 μ s, pulse frequency 200Hz, the OSU-4L laboratory scale pulse processor (Ohio State Univ-Columbus USA) that electric-field intensity is 30kV/cm, sterilization 240 μ s, sterile filling is preserved under 4 ℃ of conditions.
Embodiment 2
Get fresh chrysanthemum brain, arrange, clean, in the sodium bicarbonate solutions of 75 ℃ (concentration is 0.4%) blanching 50s, with circulating water, be cooled to room temperature rapidly; Ascorbic acid with 0.2% and 0.2% acetic acid zinc solution soak after 4h, and chrysanthemum brain is pulled out, with clear water, clean surperficial raffinate, in the ratio of 1:4, add water making beating; Add 0.06% cellulase, under 60 ℃ and pH4.0 condition, enzymolysis 3h, cooling; Centrifugal in the instrument centrifuge of H1650-W Hunan, temperature is controlled at 15 ℃, rotating speed 2500r/min, and centrifugal 10min, obtains chrysanthemum brain clear liquid; Control chrysanthemum brain clear liquid electrical conductivity in 2000 μ s left and right, adopt 6 continuous process chambers, bipolar positive negative pulse stuffing, pulse width 2 μ s, pulse frequency 200Hz, the OSU-4L laboratory scale pulse processor (Ohio State Univ-Columbus USA) that electric-field intensity is 25kV/cm, sterilization 280 μ s, sterile filling is preserved under 10 ℃ of conditions.

Claims (5)

1. a production method for natural activity chrysanthemum brain drink, is characterized in that taking following technique and method
The blanching of A, chrysanthemum brain with protect look: fresh chrysanthemum brain is put into 50-100 ℃ of sodium bicarbonate solution (concentration is 0.01-0.50%), and blanching 30-300s, is cooled to room temperature with circulating water rapidly; With 0.01-0.3% ascorbic acid and 0.01-0.3% acetic acid zinc solution, soak 1.5-4.5h, pull out, with clear water, clean the raffinate on chrysanthemum brain surface, standby.
The preparation of B, chrysanthemum brain liquid: by the chrysanthemum brain protecting after look, add water making beating by 1:4, and add the cellulase of 0.02-0.20%, enzymolysis 1-4h under 35-65 ℃ and pH3.5-7.0; Enzymolysis liquid is cooling, and centrifugal in the instrument centrifuge of H1650-W Hunan, temperature is controlled at 10-30 ℃, rotating speed 2000-5000r/min, and centrifugal 10-30min, obtains the green chrysanthemum brain clear liquid of clear.
C, sterilization, filling and refrigeration: adopt bipolar positive negative pulse stuffing, pulse width 2 μ s, the OSU-4L laboratory scale pulse processor of pulse frequency 200Hz (Ohio State Univ-Columbus USA's making), in electric-field intensity, be under 20-35kV/cm condition, the chrysanthemum brain clear liquid that is 1500-2500 μ s by electrical conductivity carries out sterilization processing 100-300 μ s (guaranteeing that feeding temperature and drop temperature are 2-10 ℃), finally carry out sterile filling, under 0-18 ℃ of condition, preserve.
2. according to claim 1, it is characterized in that: fresh chrysanthemum brain is at 50-100 ℃ of sodium bicarbonate solution (concentration is 0.01-0.50%), blanching 30-300s.Adopt zinc acetate and ascorbic acid combination to protect look, in 0.01-0.3% ascorbic acid and 0.01-0.3% acetic acid zinc solution, soak 1.5-4.5h.
3. according to claim 1, it is characterized in that: adopt cellulose hydrolyzation chrysanthemum brain, hydrolysis temperature 35-65 ℃, enzymolysis pH3.5-7.0, the addition of enzyme is 0.02-0.2% (mass fraction), and enzymolysis time 1-4h has promoted the release of bioactivator in chrysanthemum brain.
4. according to claim 1, it is characterized in that: centrifugal with H1650-W Hunan instrument centrifuge, temperature is controlled at 10-30 ℃, rotating speed 2000-5000r/min, centrifugal 10-30min, obtains green chrysanthemum brain clear liquid.
5. according to claim 1, it is characterized in that: adopt bipolar positive negative pulse stuffing, pulse width 2 μ s, pulse frequency 200Hz, by OSU-4L laboratory scale pulse processor (Ohio State Univ-Columbus USA's making), in electric-field intensity, be under 20-35kV/cm condition, the chrysanthemum brain clear liquid that is 1500-2500 μ s by electrical conductivity carries out sterilization processing 100-300 μ s (guaranteeing that feeding temperature and drop temperature are 2-10 ℃), finally carry out sterile filling, product is preserved under 0-18 ℃ of condition.
CN201310616129.0A 2013-11-25 2013-11-25 A kind of production method of natural active chrysanthemum nankingense drink Expired - Fee Related CN103653125B (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104178386A (en) * 2014-09-08 2014-12-03 南京飞马食品有限公司 Chrysanthemum nankingense beer and processing method thereof
CN105748549A (en) * 2016-04-15 2016-07-13 时维静 Method for preventing chrysanthemum brewing and extraction discoloration
CN105876554A (en) * 2016-05-27 2016-08-24 朱广双 Production method of chrysanthemum nankingense health beverage
CN103919843B (en) * 2014-05-04 2017-03-15 镇江市药品检验所 A kind of liver protection Chinese medicine composition and preparation method thereof
CN107582595A (en) * 2017-09-22 2018-01-16 安徽菊泰滁菊草本科技有限公司 A kind of concocting method of chrysanthemum indicum

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1106238A (en) * 1994-08-15 1995-08-09 中外合资南京圣晖实业有限公司 Beverage using chrysanthemum nankingense as main material and its prodn. technique
CN1718031A (en) * 2005-07-12 2006-01-11 江南大学 Method for producing sugar-free tea beverage by using high voltage pulsation electric-field sterilizing tech.

Patent Citations (2)

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Publication number Priority date Publication date Assignee Title
CN1106238A (en) * 1994-08-15 1995-08-09 中外合资南京圣晖实业有限公司 Beverage using chrysanthemum nankingense as main material and its prodn. technique
CN1718031A (en) * 2005-07-12 2006-01-11 江南大学 Method for producing sugar-free tea beverage by using high voltage pulsation electric-field sterilizing tech.

Non-Patent Citations (3)

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肖玫 等: "菊花叶的矿物元素及其饮料配方的研究", 《农业工程学报》 *
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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103919843B (en) * 2014-05-04 2017-03-15 镇江市药品检验所 A kind of liver protection Chinese medicine composition and preparation method thereof
CN104178386A (en) * 2014-09-08 2014-12-03 南京飞马食品有限公司 Chrysanthemum nankingense beer and processing method thereof
CN105748549A (en) * 2016-04-15 2016-07-13 时维静 Method for preventing chrysanthemum brewing and extraction discoloration
CN105876554A (en) * 2016-05-27 2016-08-24 朱广双 Production method of chrysanthemum nankingense health beverage
CN107582595A (en) * 2017-09-22 2018-01-16 安徽菊泰滁菊草本科技有限公司 A kind of concocting method of chrysanthemum indicum

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